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16 TABLE 2A. NEWARK BAY/STATEN ISLAND KILLS COMPLEX - NATURAL CLAYS RESULTS OF CHEMICAL ANALYSIS OF SITE WATER AND ELUTRIATE SITE WATER ELUTRIATE CONSTITUENTS DETECTION LIMITS CONCENTRATION DETECTION LIMITS CONCENTRATION Metals ppb (ug/l) ppb (ug/l) ppb (ug/l) ppb (ug/l) Cadmium Chromium Copper Lead Mercury Nickel Silver Zinc Pesticides pptr (ng/l) pptr (ng/l) pptr (ng/l) pptr (ng/l) Aldrin 0.8 ND 0.8 ND alpha-chlordane trans-nonachlor Dieldrin 0.3 ND 3.1 4,4'-DDT ,4'-DDT 0.7 ND 0.7 ND 4,4'-DDD ,4'-DDD ,4'-DDE ,4'-DDE 1.4 ND 1.4 ND Total DDT Endosulfan I Endosulfan II 0.5 ND 1.8 Endosulfan sulfate 2.4 ND 2.7 Heptachlor Heptachlor epoxide Industrial Chemicals pptr (ng/l) pptr (ng/l) pptr (ng/l) pptr (ng/l) PCB BZ ND PCB BZ ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND PCB BZ ND 0.1 ND PCB BZ ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.1 ND PCB BZ ND 0.2 ND PCB BZ ND 0.5 PCB BZ ND 0.1 ND Total PCB ND = Not detected Total PCB = sum of all congeners * 2. Total DDT = sum of 2,4' and 4,4' DDD, DDE, and DDT.
17 NEWARK BAY/STATEN ILAND KILLS COMPLEX - NATURAL CLAYS TABLE 2B. TOXICITY TEST RESULTS Suspended Particulate Phase - Raw Clay Test Species Test Duration LC50/EC50 LPC (a) Menidia beryllina 96 hours >100% (b) > 1 Mysidposis bahia 96 hours >100% (b) > 1 Mytilus sp. 48 hours >100% (b) > 1 (larval survival) Mytilus sp. 48 hours >100% (c) > 1 (larval normal development) (a) Limiting Permissible Concentration (LPC) is the LC50 or EC50 times (b) Median Lethal Concentration (LC50) resulting in 50% mortatlity at test termination. (c) Median Effective Concentration (EC50) based on normal development to the D-cell, prodissoconch 1 stage. Whole Sediment (10 days) - Raw Clay Test Species % Survival % Survival % Difference Is Difference statistically in Reference in Test Reference -Test significant? (a=0.05) Ampelisca abdita 89% 86% 3% No Mysidopsis bahia 93% 95% 0% (a) No (a) Survival in the test material was greater than in the Reference.
18 TABLE 2C. NEWARK BAY / STATEN ISLAND KILLS COMPLEX - NATURAL CLAYS 28-DAY BIOACCUMULATION TEST RESULTS: CHEMICAL ANALYSIS OF TISSUE (in wet weight concentration) Macoma nasuta Nereis virens REFERENCE TEST REFERENCE TEST Detection Mean Detection Mean Detection Mean Detection Mean Constituents Limits Concentration Limits Concentration Limits Concentration Limits Concentration Metals ug/g ug/g ug/g ug/g ug/g ug/g ug/g ug/g Arsenic Cadmium Chromium Copper Lead Mercury Nickel Silver ND Zinc Pesticides ng/g ng/g ng/g ng/g ng/g ng/g ng/g ng/g Aldrin ND alpha-chlordane trans-nonachlor ND ND Dieldrin ,4'-DDT ,4'-DDT ND * ,4'-DDD ,4'-DDD ,4'-DDE ,4'-DDE 0.14 ND ND Total DDT Endosulfan I Endosulfan II ND Endosulfan sulfate * ND 1.16 ND 1.16 * ND Heptachlor ND ND * Heptachlor epoxide Industrial Chemicals ng/g ng/g ng/g ng/g ng/g ng/g ng/g ng/g PCB BZ PCB BZ PCB BZ ND * ND 0.22 * PCB BZ PCB BZ ND ND PCB BZ * ND ND * PCB BZ ND 1.06 ND * ND PCB BZ PCB BZ ND 0.37 ND PCB BZ ND * ND PCB BZ * ND ND 0.46 * ND PCB BZ ND * ND ND * ND PCB BZ ND * ND PCB BZ ND 0.36 ND PCB BZ ND ND ND ND PCB BZ ND ND PCB BZ ND * ND ND ND PCB BZ ND * ND PCB BZ ND ND ND PCB BZ ND ND PCB BZ ND ND ND ND PCB BZ ND ND 0.2 ND ND Total PCB
19 1,4-Dichlorobenzene 0.2 ND 0.2 ND 0.2 ND 0.2 ND Dioxins and Furans pg/g pg/g pg/g pg/g pg/g pg/g pg/g pg/g 2378-TCDD ND ND PeCDD ND ND HxCDD ND HxCDD HxCDD HpCDD OCDD TCDF ND ND PeCDF PeCDF ND HxCDF ND HxCDF HxCDF ND ND ND * ND HxCDF HpCDF HpCDF ND ND ND OCDF PAHs ng/g ng/g ng/g ng/g ng/g ng/g ng/g ng/g Acenaphthene ND 3.78 ND Acenaphthylene 56.4 ND 56.2 * ND 56.5 ND 56.4 * ND Anthracene 1.98 ND 2.0 ND 2.0 ND 2.0 ND Fluorene 3.56 ND 3.6 ND 3.55 ND 3.58 ND Naphthalene 1.7 ND 1.7 ND 1.7 ND 1.7 ND Phenanthrene ND 1.3 ND 1.3 ND Benzo[a]anthracene 1.6 ND 1.6 ND 1.6 ND 1.6 ND Benzo[a]pyrene ND 1.3 ND 1.3 ND Benzo[g,h,i]perylene 1.4 ND 1.4 ND 1.4 ND 1.4 ND Benzo[b]fluoranthene 1.4 ND 1.4 ND 1.4 ND 1.4 ND Benzo[k]fluoranthene 1.2 ND 1.2 ND 1.2 ND 1.2 ND Chrysene ND 2 ND 2 ND Dibenz[a,h]anthracene 1.6 ND 1.6 ND 1.6 ND 1.6 ND Fluoranthene 3.16 ND 3.2 ND 3.15 ND 3.18 ND Indeno[1,2,3-cd]pyrene ND ND ND ND Pyrene Total PAHs * * Concentrations shown are the mean of 5 replicate analyses in wet weight with the following exceptions: PAH concentrations for Nereis virens Reference tissue are the mean of 4 replicate analyses; 1,4 dichlorobenzene concentration for Nereis virens Test tissue is the mean of 4 replicate analyses due to limited tissue volume; 1,4 dichlorobenzene concentration for Nereis virens Reference tissue is the result of one set of analyses due to limited tissue volume. * Significantly higher than reference at 95% confidence. ND = Not Detected Total PAHs = sum of all PAHs Total PCB = sum of congeners reported * 2 Total DDT = sum of 2.4'- and 4,4'-DDD, DDE, and DDT Means and statistical comparisons were determined using conservative estimates of concentrations of constituents that were at concentrations below the detection limit.
20 TABLE 3A. RESULTS OF CHEMICAL ANALYSIS OF SITE WATER AND ELUTRIATE ARTHUR KILL - CONTRACT AREA 1A SITE WATER ELUTRIATE CONSTITUENTS DETECTION LIMITS CONCENTRATION DETECTION LIMITS CONCENTRATION Metals ppb ppb ppb ppb Ag Cd Cr Cu Hg Ni Pb Zn Pesticides pptr (ng/l) pptr (ng/l) pptr (ng/l) pptr (ng/l) Aldrin 2.83 ND 2.83 ND a-chlordane 1.08 ND 1.08 ND trans Nonachlor 1.01 ND 1.01 ND Dieldrin 0.98 ND 0.98 ND 4,4'-DDT 0.56 ND 0.56 ND 2,4'-DDT 1.98 ND 1.98 ND 4,4'-DDD 0.59 ND 0.59 ND 2,4'-DDD 0.75 ND 0.75 ND 4,4'-DDE 0.84 ND 0.84 ND 2,4'-DDE 1.71 ND 1.71 ND Total DDT Endosulfan I 1.11 ND 1.11 ND Endosulfan II 0.51 ND 0.51 ND Endosulfan sulfate 0.56 ND 0.56 ND Heptachlor 1.17 ND 1.17 ND Heptachlor epoxide 0.95 ND 0.95 ND Industrial Chemicals pptr (ng/l) pptr (ng/l) pptr (ng/l) pptr (ng/l) PCB ND ND PCB ND 1.38 ND PCB ND 1.73 ND PCB ND 1.45 ND PCB ND 1.49 ND PCB ND 1.43 ND PCB ND 1.49 ND PCB ND 1.13 ND PCB ND 1.14 ND PCB ND 0.57 ND PCB ND 0.87 ND PCB ND 1.40 ND PCB ND 1.32 ND PCB ND 1.06 ND PCB ND 1.01 ND PCB ND 0.96 ND PCB ND 0.93 ND PCB ND 0.92 ND PCB ND 0.86 ND PCB ND 1.08 ND PCB ND 1.22 ND PCB ND 1.26 ND Total PCB ND = Not detected Total DDT = sum of 2,4'- and 4,4'-DDD, DDE, and DDT Total PCB = sum of congeners reported x 2 Concentrations shown are the mean of three replicate analyses. Means were determined using conservative estimates of concentrations of constituents that were at concentrations below the detection limit.
21 TABLE 3B. ARTHUR KILL - CONTRACT AREA 1A TOXICITY TEST RESULTS Suspended Particulate Phase Test Species Test Duration LC 50 /EC 50 LPC (a) Menidia beryllina 96 hours >100% (b) 1.00 Mysidposis bahia 96 hours >100% (b) 1.00 Mytilus edulis (larval survival) 48 hours >100% (b) 1.00 Mytilus edulis (larval normal development) 48 hours >100% (c) 1.00 (a) Limiting Permissible Concentration (LPC) is the LC 50 or EC 50 times (b) Median Lethal Concentration (LC50) resulting in 50% mortatlity at test termination. (c) Median Effective Concentration (EC50) based on normal development to the D-cell, prodissoconch 1 stage. Whole Sediment (10 days) Test Species % Survival % Survival % Difference Is difference statistically in Reference in Test Reference -Test significant? (a=0.05) Ampelisca abdita 80% 95% 15% No Mysidopsis bahia 99% 97% 2% No
22 TABLE 3C. ARTHUR KILL - CONTRACT AREA 1A 28-DAY BIOACCUMULATION TEST RESULTS: CHEMICAL ANALYSIS OF TISSUE Wet weight concentrations Tapes japonica Nereis virens REFERENCE TEST REFERENCE TEST CONSTITUENTS DETECTION CONCEN- DETECTION CONCEN- DETECTION CONCEN- DETECTION CONCEN- LIMITS TRATION LIMITS TRATION LIMITS TRATION LIMITS TRATION Metals ppm (mg/kg) ppm (mg/kg) ppm (mg/kg) ppm (mg/kg) ppm (mg/kg) ppm (mg/kg) ppm (mg/kg) ppm (mg/kg) Ag ND As Cd Cr 0.04 * Cu Hg Ni * 0.37 Pb Zn Pesticides ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) Aldrin ND 0.01 ND 0.02 ND 0.08 ND a-chlordane trans Nonachlor Dieldrin 0.01 ND ,4'-DDT 0.01 ND 0.01 ND ND 2,4'-DDT 0.02 ND 0.02 ND ND 4,4'-DDD ,4'-DDD 0.01 ND 0.01 ND ,4'-DDE ND 0.13 * ND 2,4'-DDE 0.05 ND 0.05 ND 0.06 ND 0.33 * ND Total DDT Endosulfan I 0.02 ND 0.02 ND 0.02 ND 0.12 * ND Endosulfan II 0.03 ND 0.03 ND ND Endosulfan sulfate 0.03 ND 0.03 ND Heptachlor 0.01 ND 0.01 ND 0.02 ND 0.10 ND Heptachlor epoxide 0.01 ND 0.01 ND Industrial Chemicals ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) PCB ND 0.17 ND 0.22 ND * 0.80 PCB ND 0.02 ND 0.02 ND 0.13 * ND PCB ND 0.03 ND 0.16 * ND PCB ND 0.11 * ND PCB ND 0.01 ND 0.02 ND 0.09 ND PCB ND 0.01 ND 0.02 ND 0.08 ND PCB ND 0.02 ND 0.02 ND 0.10 ND PCB PCB PCB ND 0.02 ND ND PCB ND 0.02 ND ND PCB ND 0.05 ND PCB PCB PCB ND PCB ND 0.02 ND PCB ND 0.02 ND PCB ND 0.03 ND 0.03 ND 0.18 * ND PCB ND 0.02 ND PCB ND 0.02 ND PCB ND ND PCB ND 0.02 ND 0.22 * 0.38 Total PCB ,4-Dichlorobenzene
23 TABLE 3C. (Continued) ARTHUR KILL - CONTRACT AREA 1A Tapes japonica Nereis virens REFERENCE TEST REFERENCE TEST CONSTITUENTS DETECTION CONCEN DETECTION CONCEN DETECTION CONCEN DETECTION CONCEN LIMITS TRATION LIMITS TRATION LIMITS TRATION LIMITS TRATION PAH's ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) ppb (ug/kg) Naphthalene Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)anthracene Chrysene Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1,2,3-cd)pyrene 0.01 ND ND 0.06 * ND Dibenzo(a,h)antracene 0.03 ND ND 0.07 Benzo(g,h,i)perylene 0.02 ND ND * 0.19 Total PAH's Dioxins pptr (ng/kg) pptr (ng/kg) pptr (ng/kg) pptr (ng/kg) pptr (ng/kg) pptr (ng/kg) pptr (ng/kg) pptr (ng/kg) 2,3,7,8 TCDD 0.10 ND 0.08 ND ,2,3,7,8 PeCDD 0.12 ND 0.10 ND ND 1,2,3,4,7,8 HxCDD 0.06 ND * ,2,3,6,7,8 HxCDD * ,2,3,7,8,9 HxCDD 0.07 ND ,2,3,4,6,7,8 HpCDD ,2,3,4,7,8,9 OCDD ,3,7,8 TCDF ,2,3,7,8 PeCDF ND 2,3,4,7,8 PeCDF ,2,3,4,7,8 HxCDF ,2,3,6,7,8 HxCDF ,3,4,6,7,8 HxCDF ,2,3,7,8,9 HxCDF ND 0.06 ND 0.11 * ND 1,2,3,4,6,7,8 HpCDF ,2,3,4,7,8,9 HpCDF 0.08 ND ND * ,2,3,4,6,7,8,9 OCDF ND = Not detected Total PAH = Sum of all PAH's. Total DDT = sum of 2,4'- and 4,4'-DDD, DDE, and DDT Total PCB = 2(x), where x = sum of PCB congeners Concentrations shown are the mean of 5 replicate analyses in wet weight. Means were determined using conservative estimates of concentrations of constituents that were at concentrations below the detection limit. * = Statistically significant at the 95% confidence level
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