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1 TEST REPOR Page 1 of 19 REPORT NUMBER : APPLICANT NAME ADDRESS SAMPLE DESCRIPTION : BUYER : TURA TETAŞ Đç Ve Dış Ticaret A.Ş. Çakmaklı Mah. Hadımköy Yolu 50. Sokak No: 2 Kıraç Büyükçekmece - Đstanbul FAX NO : Attention : Şenay Demirtaş One sample of Lineplus mm & mm Permanent Marker (Red-Blue-Black) TUKID/TETAŞ ĐÇ ve DIŞ TĐC. A.Ş. DATE IN : 03 November, 2011 (09:58) DATE OUT : 15 November, 2011 PHOTO OF PRODUCT TESTED : Part No Tested Part 1 MULTICOLOR OUTER PART 2 BLUE PLASTIC COVER 3 BLACK PLASTIC COVER 4 RED PLASTIC COVER 5 BLUE TIP 6 BLACK TIP 7 RED TIP Zeynep Akın Assistant Chemical Laboratory Manager Neslihan Sözer Chemical Laboratory Manager Merkez Mahallesi Sanayi Cad. No: 23 Altındağ Plaza Yenibosna ISTANBUL / TURKEY * * tugcekomurcu

2 R E S U L T S Page 2 of 19 RESULTS : Analysis Parameter Reference Analysis Method PASS FAIL Norm Limit Standard for Norm Limit Tested Part Azo Dyes 64 LFBG B P - 30 ppm 2004/21/EC Part 1-7 DBP/DEHP/BBP : (27893) Notification On Market Supervision And Phthalate EN by GC 1000 ppm Controls Regarding P - MS DINP/DNOP/ DIDP Hazardous Chemical Part 1-7 :1000 ppm Contents Of Some End- User Products Toxic Element Analysis BS EN 71-3:1995 P - Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Cd: 75 ppm Cr: 60 ppm EN 71-3 Part 1-7 Pb: 90 ppm Hg: 60 ppm Se: 500 ppm PAH ZEK Method P - Total PAH <10 ppm BaP <1 ppm 2005/69/EC Part 1-7 P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.

3 R E S U L T S Page 3 of 19 Azo Dyestuff 64 LFGB :2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis Part 1&2&3&4&5&6&7 1) Composite sample of Blue, Black, red plastic cover PASS 30 ppm 2) Composite sample of Blue, red, Black tip PASS 30 ppm 3) Multicolor outer part PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO 64 LFGB , LEATHER ACCORDĐNG TO 64 LFGB , PES ACCORDING TO 64 LFGB , EXTRACTED BY CITRATE BUFFERED SOLUTION ph 6 AT 70 C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS. FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL BENZIDINE CHLORO-O-4-CHLOR-O-TOLUIDINE NAPHTHYLAMINE *O-AMINOAZOTOLUENE *2-AMINO-4-NITROTOLUENE P-CHLOROANILINE ,4-DIAMINOANISOLE ,4 -DIAMINOBIPHENYLMETHANE ,3 -DICHLOROBENZIDINE ,3 -DIMETHOXYBENZIDINE ,3 -DIMETHYLBENZIDINE ,3 -DĐMETHYL-4,4 DIAMINOBIPHENYLMETHANE P-CRESIDINE ,4 -METHYLENE-BIS-(2 CHLOROANILINE) ,4 -OXYDIANILINE ,4 -THIODIANILINE O-TOLUIDINE ,4-TOLUYLENDIAMINE ,4,5-TRIMETHYLANILINE O-ANISIDINE **P-AMINOAZOBENZENE NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%

4 R E S U L T S Page 4 of 19 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 1 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

5 R E S U L T S Page 5 of 19 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 2 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

6 R E S U L T S Page 6 of 19 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 3 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

7 R E S U L T S Page 7 of 19 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 4 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

8 R E S U L T S Page 8 of 19 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 5 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

9 R E S U L T S Page 9 of 19 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 6 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

10 R E S U L T S Page 10 of 19 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 7 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

11 R E S U L T S Page 11 of 19 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 1 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 2 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 3 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 4 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

12 R E S U L T S Page 12 of 19 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 5 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 6 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 7 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

13 R E S U L T S Page 13 of 19 Polycyclic Aromatic Hydrocarbons (PAHs) Analysis IHTM AL ZEK : Harmonisierte Methode zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Kunststoffproben ZEK AS SOLVENT EXTRACTION AND FOLLOWED BY GAS CHROMATOGRAPHY MASS SPECTROMETRIC (GC/MS) ANALYSIS Part 1 RESULT (ppm) REQUIREMENT NAPHTHALENE Category 2 ACENAPHTHYLENE Total 16 PAH : 10 mg/kg ACENAPHTHEN Benzo(a)pyrene : 1 mg/kg FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO (a) ANTHRACENE CHRYSENE BENZO (b) FLUORANTHENE BENZO (k) FLUORANTHENE BENZO (a) PYRENE INDENO (1,2,3-cd) PYRENE DIBENZO (a,h) ANTHRACENE BENZO (ghi) PERYLENE ---- SUM (16 PAH): Detection Limit = 0.1 ppm n.d. = (Total Uncertainty= ± 3 %)

14 R E S U L T S Page 14 of 19 Polycyclic Aromatic Hydrocarbons (PAHs) Analysis IHTM AL ZEK : Harmonisierte Methode zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Kunststoffproben ZEK AS SOLVENT EXTRACTION AND FOLLOWED BY GAS CHROMATOGRAPHY MASS SPECTROMETRIC (GC/MS) ANALYSIS Part 2 RESULT (ppm) REQUIREMENT NAPHTHALENE Category 2 ACENAPHTHYLENE Total 16 PAH : 10 mg/kg ACENAPHTHEN Benzo(a)pyrene : 1 mg/kg FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO (a) ANTHRACENE CHRYSENE BENZO (b) FLUORANTHENE BENZO (k) FLUORANTHENE BENZO (a) PYRENE INDENO (1,2,3-cd) PYRENE DIBENZO (a,h) ANTHRACENE BENZO (ghi) PERYLENE ---- SUM (16 PAH): Detection Limit = 0.1 ppm n.d. = (Total Uncertainty= ± 3 %)

15 R E S U L T S Page 15 of 19 Polycyclic Aromatic Hydrocarbons (PAHs) Analysis IHTM AL ZEK : Harmonisierte Methode zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Kunststoffproben ZEK AS SOLVENT EXTRACTION AND FOLLOWED BY GAS CHROMATOGRAPHY MASS SPECTROMETRIC (GC/MS) ANALYSIS Part 3 RESULT (ppm) REQUIREMENT NAPHTHALENE Category 2 ACENAPHTHYLENE Total 16 PAH : 10 mg/kg ACENAPHTHEN Benzo(a)pyrene : 1 mg/kg FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO (a) ANTHRACENE CHRYSENE BENZO (b) FLUORANTHENE BENZO (k) FLUORANTHENE BENZO (a) PYRENE INDENO (1,2,3-cd) PYRENE DIBENZO (a,h) ANTHRACENE BENZO (ghi) PERYLENE ---- SUM (16 PAH): Detection Limit = 0.1 ppm n.d. = (Total Uncertainty= ± 3 %)

16 R E S U L T S Page 16 of 19 Polycyclic Aromatic Hydrocarbons (PAHs) Analysis IHTM AL ZEK : Harmonisierte Methode zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Kunststoffproben ZEK AS SOLVENT EXTRACTION AND FOLLOWED BY GAS CHROMATOGRAPHY MASS SPECTROMETRIC (GC/MS) ANALYSIS Part 4 RESULT (ppm) REQUIREMENT NAPHTHALENE Category 2 ACENAPHTHYLENE Total 16 PAH : 10 mg/kg ACENAPHTHEN Benzo(a)pyrene : 1 mg/kg FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO (a) ANTHRACENE CHRYSENE BENZO (b) FLUORANTHENE BENZO (k) FLUORANTHENE BENZO (a) PYRENE INDENO (1,2,3-cd) PYRENE DIBENZO (a,h) ANTHRACENE BENZO (ghi) PERYLENE ---- SUM (16 PAH): Detection Limit = 0.1 ppm n.d. = (Total Uncertainty= ± 3 %)

17 R E S U L T S Page 17 of 19 Polycyclic Aromatic Hydrocarbons (PAHs) Analysis IHTM AL ZEK : Harmonisierte Methode zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Kunststoffproben ZEK AS SOLVENT EXTRACTION AND FOLLOWED BY GAS CHROMATOGRAPHY MASS SPECTROMETRIC (GC/MS) ANALYSIS Part 5 RESULT (ppm) REQUIREMENT NAPHTHALENE Category 2 ACENAPHTHYLENE Total 16 PAH : 10 mg/kg ACENAPHTHEN Benzo(a)pyrene : 1 mg/kg FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO (a) ANTHRACENE CHRYSENE BENZO (b) FLUORANTHENE BENZO (k) FLUORANTHENE BENZO (a) PYRENE INDENO (1,2,3-cd) PYRENE DIBENZO (a,h) ANTHRACENE BENZO (ghi) PERYLENE ---- SUM (16 PAH): Detection Limit = 0.1 ppm n.d. = (Total Uncertainty= ± 3 %)

18 R E S U L T S Page 18 of 19 Polycyclic Aromatic Hydrocarbons (PAHs) Analysis IHTM AL ZEK : Harmonisierte Methode zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Kunststoffproben ZEK AS SOLVENT EXTRACTION AND FOLLOWED BY GAS CHROMATOGRAPHY MASS SPECTROMETRIC (GC/MS) ANALYSIS Part 6 RESULT (ppm) REQUIREMENT NAPHTHALENE Category 2 ACENAPHTHYLENE Total 16 PAH : 10 mg/kg ACENAPHTHEN Benzo(a)pyrene : 1 mg/kg FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO (a) ANTHRACENE CHRYSENE BENZO (b) FLUORANTHENE BENZO (k) FLUORANTHENE BENZO (a) PYRENE INDENO (1,2,3-cd) PYRENE DIBENZO (a,h) ANTHRACENE BENZO (ghi) PERYLENE ---- SUM (16 PAH): Detection Limit = 0.1 ppm n.d. = (Total Uncertainty= ± 3 %)

19 R E S U L T S Page 19 of 19 Polycyclic Aromatic Hydrocarbons (PAHs) Analysis IHTM AL ZEK : Harmonisierte Methode zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Kunststoffproben ZEK AS SOLVENT EXTRACTION AND FOLLOWED BY GAS CHROMATOGRAPHY MASS SPECTROMETRIC (GC/MS) ANALYSIS Part 7 RESULT (ppm) REQUIREMENT NAPHTHALENE Category 2 ACENAPHTHYLENE Total 16 PAH : 10 mg/kg ACENAPHTHEN Benzo(a)pyrene : 1 mg/kg FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO (a) ANTHRACENE CHRYSENE BENZO (b) FLUORANTHENE BENZO (k) FLUORANTHENE BENZO (a) PYRENE INDENO (1,2,3-cd) PYRENE DIBENZO (a,h) ANTHRACENE BENZO (ghi) PERYLENE ---- SUM (16 PAH): Detection Limit = 0.1 ppm n.d. = (Total Uncertainty= ± 3 %) ## END OF TEST REPORT ##

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