Certifications: New York (EPA: NY00906, ELAP: 11078), New Jersey (NY026), Connecticut (PH-0337), Massachusetts (M-NY906), Virginia (1884)
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- Giles Elwin Bradford
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1 Pace Analytical e-report *Issuance of this report is prior to full data package. Report prepared for: ARCADIS 6723 TOWPATH RD SYRACUSE, NY 324 CONTACT: DON SAUDA Project ID: DEWEY LOEFFEL LANDFILL SUPERFUND SITE Sampling Date(s): July 02, 203 Lab Report ID: Client Service Contact: Kelly Miller (58) ext Analysis Included: VOCs by GCMS (CLP 4.3 List Soil) SVOCs by GCMS (CLP 4.3 List) PCB Analysis Pesticide Analysis (Solid) Metals by ICP (TAL) Test results meet all National Environmental Laboratory Accreditation Conference (NELAC) requirements unless noted in the case narrative. The results contained within the document relate only to the samples included in this report. Pace Analytical is responsible only for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. This report shall not be reproduced, except in full, without the written consent of Dan Pfalzer Laboratory Director Certifications: New York (EPA: NY00906, ELAP: 078), New Jersey (NY026), Connecticut (PH-0337), Massachusetts (M-NY906), Virginia (884) internet: Page of 64
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3 Table of Contents Section : QUALIFIERS... 4 Section 2: SAMPLE CHAIN OF CUSTODY... 6 Section 3: GC/MS Volatiles... 8 Section 4: GC/MS Semivolatiles...29 Section 5: GC - PCB...34 Section 6: GC - Pesticides...37 Section 7: Metals - ICP...40 Section 8: Quality Control Samples (Lab) Page 3 of 64
4 QUALIFIERS Page 4 of 64
5 Organic Laboratory Qualifiers Defined B - Denotes analyte observed in associated method blank or extraction blank. Analyte concentration should be considered as estimated. D - Surrogate was diluted. The analysis of the sample required a dilution such that the surrogate concentration was diluted below the laboratory acceptance criteria. E - Denotes analyte concentration exceeded calibration range of instrument. Sample could not be reanalyzed at secondary dilution due to insufficient sample amount, quick turn-around request, sample matrix interference or hold time excursion. Concentration result should be considered as estimated. J - Denotes an estimated concentration. The concentration result is greater than or equal to the Method Detection Limit (MDL) but less than the Reporting Limit (RL). P - Indicates relative percent difference (RPD) between primary and secondary gas chromatograph (GC) column analysis exceeds 40 % or indicates percent difference (PD) between primary and secondary gas chromatograph (GC) column analysis exceeds 25 %. U - Denotes analyte not detected at concentration greater than or equal to the Reporting Limit (RL). Reporting Limit s (RL) are adjusted for sample weight/volume and dilution factors. Z - Chromatographic interference due to polychlorinated biphenyl (PCB) co-elution. * - Value not within control limits. Inorganic Laboratory Qualifiers Defined B - Denotes analyte observed in associated method blank or digestion blank. Analyte concentration should be considered as estimated. E - Denotes analyte concentration exceeded calibration range of instrument. Sample could not be reanalyzed at secondary dilution due to insufficient sample amount, quick turn-around request, sample matrix interference or hold time excursion. Concentration result should be considered as estimated. J - Denotes an estimated concentration. The concentration result is greater than or equal to the Method Detection Limit (MDL) but less than the Reporting Limit (RL). U - Denotes analyte not detected at concentration greater than or equal to the Reporting Limit (RL). Reporting Limit s (RL) are adjusted for sample weight/volume and dilution factors. * - Value not within control limits Page 5 of 64
6 2 SAMPLE CHAIN OF CUSTODY Page 6 of 64
7 Page 7 of 64 2
8 GC/MS Volatiles Page 8 of 64
9 Analytical Sample Results Client Sample ID: B8 (0-2) Lab Sample ID: (AQ5350) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 6:46 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :40 BH 4.89 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone MS Hexanone Methyl-2-pentanone Acetone MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 9 of 64
10 Analytical Sample Results Client Sample ID: B8 (0-2) Lab Sample ID: (AQ5350) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 6:46 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :40 BH 4.89 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene MS Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 0 of 64
11 Analytical Sample Results Client Sample ID: B8 (2-5) Lab Sample ID: (AQ535) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 7:2 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :4 BH 7.53 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page of 64
12 Analytical Sample Results Client Sample ID: B8 (2-5) Lab Sample ID: (AQ535) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 7:2 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :4 BH 7.53 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 2 of 64
13 Analytical Sample Results Client Sample ID: B9 (0-2) Lab Sample ID: (AQ5352) Collection Date: 07/02/203 3:20 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 7:37 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :4 BH 5.66 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 3 of 64
14 Analytical Sample Results Client Sample ID: B9 (0-2) Lab Sample ID: (AQ5352) Collection Date: 07/02/203 3:20 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 7:37 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :4 BH 5.66 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene MS Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 4 of 64
15 Analytical Sample Results Client Sample ID: B9 (2-5) Lab Sample ID: (AQ5353) Collection Date: 07/02/203 3:20 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 8:03 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :42 BH 5.9 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 5 of 64
16 Analytical Sample Results Client Sample ID: B9 (2-5) Lab Sample ID: (AQ5353) Collection Date: 07/02/203 3:20 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 8:03 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :42 BH 5.9 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene MS Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 6 of 64
17 Analytical Sample Results Client Sample ID: B0 (0-2) Lab Sample ID: (AQ5354) Collection Date: 07/02/203 :40 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 8:29 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :43 BH 7.25 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 7 of 64
18 Analytical Sample Results Client Sample ID: B0 (0-2) Lab Sample ID: (AQ5354) Collection Date: 07/02/203 :40 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 8:29 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 :43 BH 7.25 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 8 of 64
19 Analytical Sample Results Client Sample ID: B0 (2-5) Lab Sample ID: (AQ5355) Collection Date: 07/02/203 :40 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 8:54 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 4:05 BH 5.24 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene MS Butanone MS Hexanone Methyl-2-pentanone Acetone MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 9 of 64
20 Analytical Sample Results Client Sample ID: B0 (2-5) Lab Sample ID: (AQ5355) Collection Date: 07/02/203 :40 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/08/203 8:54 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 4:05 BH 5.24 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 20 of 64
21 Analytical Sample Results Client Sample ID: B (0-2) Lab Sample ID: (AQ5356) Collection Date: 07/02/203 2:25 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/2/203 00:27 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 4: BH 4.9 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane MS ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone ND U MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 2 of 64
22 Analytical Sample Results Client Sample ID: B (0-2) Lab Sample ID: (AQ5356) Collection Date: 07/02/203 2:25 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/2/203 00:27 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 4: BH 4.9 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 22 of 64
23 Analytical Sample Results Client Sample ID: B (2-5) Lab Sample ID: (AQ5357) Collection Date: 07/02/203 2:25 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/0/203 3:48 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 3:30 BH 2.95 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone ND U MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 23 of 64
24 Analytical Sample Results Client Sample ID: B (2-5) Lab Sample ID: (AQ5357) Collection Date: 07/02/203 2:25 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/0/203 3:48 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 3:30 BH 2.95 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene MS Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 24 of 64
25 Analytical Sample Results Client Sample ID: B2 (0-2) Lab Sample ID: (AQ5358) Collection Date: 07/02/203 5:5 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/0/203 4:4 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 4: BH 5.4 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone ND U MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 25 of 64
26 Analytical Sample Results Client Sample ID: B2 (0-2) Lab Sample ID: (AQ5358) Collection Date: 07/02/203 5:5 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/0/203 4:4 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 4: BH 5.4 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene MS Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 26 of 64
27 Analytical Sample Results Client Sample ID: B2 (2-5) Lab Sample ID: (AQ5359) Collection Date: 07/02/203 5:5 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/0/203 4:39 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 3:3 BH 5.47 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID,,-Trichloroethane ,,2,2-Tetrachloroethane ,,2-Trichloro-,2,2-trifluoroethane 76-3-,,2-Trichloroethane ,-Dichloroethane ,-Dichloroethene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone MS Hexanone Methyl-2-pentanone Acetone B MS Benzene Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-,2-dichloroethene cis-,3-dichloropropene Cyclohexane Dibromochloromethane Dichlorodifluoromethane Ethylbenzene Isopropylbenzene m&p-xylene Methyl acetate Methyl tert-butyl ether Methylcyclohexane Methylene chloride ND U MS o-xylene Styrene Tetrachloroethene Phone Fax Page 27 of 64
28 Analytical Sample Results Client Sample ID: B2 (2-5) Lab Sample ID: (AQ5359) Collection Date: 07/02/203 5:5 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8260B CLP OLM 4.3 List 07/0/203 4:39 BH Restek, Rtx-VMS, 30 m, 0.25 mm ID,.40 µm Prep : 2042 EPA 5035A 07/08/203 3:3 BH 5.47 g 5.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Toluene trans-,2-dichloroethene trans-,3-dichloropropene Trichloroethene MS Trichlorofluoromethane Vinyl chloride Limits Surrogate CAS No. % Recovery (%) Q File ID Bromofluorobenzene MS Dibromofluoromethane MS toluene-d MS ,2-Dichloroethane-d * MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. B - Denotes analyte observed in associated method blank at a concentration exceeding the PQL. Phone Fax Page 28 of 64
29 GC/MS Semivolatiles Page 29 of 64
30 Analytical Sample Results Client Sample ID: B8 (0-2) Lab Sample ID: (AQ5360) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8270C CLP OLM 4.3 List 07/09/203 5:25 RMS Varian, VF-5MS,30 m, 0.25 mm ID, 0.25 µm Prep : 2288 EPA /07/203 8:06 MH 30.5 g.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID 2,4,5-Trichlorophenol ,4,6-Trichlorophenol ,4-Dichlorophenol ,4-Dimethylphenol ,4-Dinitrophenol ,4-Dinitrotoluene ,6-Dinitrotoluene Chloronaphthalene ND 96 2-Chlorophenol Methylnaphthalene ND 96 2-Methylphenol Nitroaniline Nitrophenol ,3'-Dichlorobenzidine Nitroaniline ,6-Dinitro-2-methylphenol Bromophenyl-phenylether Chloro-3-methylphenol Chloroaniline Chlorophenyl-phenylether Nitroaniline Nitrophenol Acenaphthene ND 96 Acenaphthylene ND 96 Anthracene ND 96 Benzo(a)anthracene ND 96 Benzo(a)pyrene ND 96 Benzo(b)fluoranthene ND 96 Benzo(g,h,i)perylene ND 96 Benzo(k)fluoranthene ND 96 bis(2-chloroethoxy)methane -9- bis(2-chloroethyl)ether bis(2-chloroisopropyl)ether bis(2-ethylhexyl)phthalate Butylbenzylphthalate Carbazole ND 96 Chrysene ND 96 Dibenz(a,h)anthracene ND 96 Dibenzofuran ND 96 Diethylphthalate Dimethylphthalate 3--3 Di-n-butylphthalate Di-n-octylphthalate Fluoranthene ND 96 4 Phone Fax Page 30 of 64
31 Analytical Sample Results Client Sample ID: B8 (0-2) Lab Sample ID: (AQ5360) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8270C CLP OLM 4.3 List 07/09/203 5:25 RMS Varian, VF-5MS,30 m, 0.25 mm ID, 0.25 µm Prep : 2288 EPA /07/203 8:06 MH 30.5 g.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Fluorene ND 96 Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(,2,3-cd)pyrene ND 96 Isophorone m & p-methylphenol* / Naphthalene ND 96 Nitrobenzene N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene ND 96 Phenol Pyrene ND 96 4 Limits Surrogate CAS No. % Recovery (%) Q File ID 2,4,6-Tribromophenol MS Fluorobiphenyl MS Fluorophenol MS Terphenyl-d MS Nitrobenzene-d MS Phenol-d MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. *3&4-Methylphenol is reported as a co-elution of 3-Methylphenol and 4-Methylphenol. 3-Methylphenol was not a calibration component in the initial calibration curve. Phone Fax Page 3 of 64
32 Analytical Sample Results Client Sample ID: B8 (2-5) Lab Sample ID: (AQ536) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8270C CLP OLM 4.3 List 07/09/203 5:47 RMS Varian, VF-5MS,30 m, 0.25 mm ID, 0.25 µm Prep : 2288 EPA /07/203 8:07 MH 30.5 g.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID 2,4,5-Trichlorophenol ,4,6-Trichlorophenol ,4-Dichlorophenol ,4-Dimethylphenol ,4-Dinitrophenol ,4-Dinitrotoluene ,6-Dinitrotoluene Chloronaphthalene ND 82 2-Chlorophenol Methylnaphthalene ND 82 2-Methylphenol Nitroaniline Nitrophenol ,3'-Dichlorobenzidine Nitroaniline ,6-Dinitro-2-methylphenol Bromophenyl-phenylether Chloro-3-methylphenol Chloroaniline Chlorophenyl-phenylether Nitroaniline Nitrophenol Acenaphthene ND 82 Acenaphthylene ND 82 Anthracene ND 82 Benzo(a)anthracene ND 82 Benzo(a)pyrene ND 82 Benzo(b)fluoranthene ND 82 Benzo(g,h,i)perylene ND 82 Benzo(k)fluoranthene ND 82 bis(2-chloroethoxy)methane -9- bis(2-chloroethyl)ether bis(2-chloroisopropyl)ether bis(2-ethylhexyl)phthalate Butylbenzylphthalate Carbazole ND 82 Chrysene ND 82 Dibenz(a,h)anthracene ND 82 Dibenzofuran ND 82 Diethylphthalate Dimethylphthalate 3--3 Di-n-butylphthalate Di-n-octylphthalate Fluoranthene ND 82 4 Phone Fax Page 32 of 64
33 Analytical Sample Results Client Sample ID: B8 (2-5) Lab Sample ID: (AQ536) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : MS EPA Method 8270C CLP OLM 4.3 List 07/09/203 5:47 RMS Varian, VF-5MS,30 m, 0.25 mm ID, 0.25 µm Prep : 2288 EPA /07/203 8:07 MH 30.5 g.00 ml Analyte CAS No. Result (ug/kg) PQL Dilution Factor Flags File ID Fluorene ND 82 Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(,2,3-cd)pyrene ND 82 Isophorone m & p-methylphenol* / Naphthalene ND 82 Nitrobenzene N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene ND 82 Phenol Pyrene ND 82 4 Limits Surrogate CAS No. % Recovery (%) Q File ID 2,4,6-Tribromophenol MS Fluorobiphenyl MS Fluorophenol MS Terphenyl-d MS Nitrobenzene-d MS Phenol-d MS Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. *3&4-Methylphenol is reported as a co-elution of 3-Methylphenol and 4-Methylphenol. 3-Methylphenol was not a calibration component in the initial calibration curve. Phone Fax Page 33 of 64
34 GC - PCB Page 34 of 64
35 Analytical Sample Results Client Sample ID: B8 (0-2) Lab Sample ID: (AQ5360) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : GC20F SW (PCB) 07/09/203 20:3 TEH Phenomenex, Zebron ZB-MS, 20 m, 0.8 mm ID, 0.8 µm Prep : EPA /08/203 0:06 CAP 0. g 25.0 ml Analyte CAS No. Result (ug/g) PQL Dilution Factor Flags File ID Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Total PCB Amount > RL ND.00 U GC20F Limits Surrogate CAS No. % Recovery (%) Q File ID Tetrachloro-meta-xylene GC20F Decachlorobiphenyl GC20F Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 35 of 64
36 Analytical Sample Results Client Sample ID: B8 (2-5) Lab Sample ID: (AQ536) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : GC20F SW (PCB) 07/09/203 20:44 JES Phenomenex, Zebron ZB-MS, 20 m, 0.8 mm ID, 0.8 µm Prep : EPA /08/203 0:07 CAP 0.3 g 25.0 ml Analyte CAS No. Result (ug/g) PQL Dilution Factor Flags File ID Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Aroclor ND U GC20F Total PCB Amount > RL ND.00 U GC20F Limits Surrogate CAS No. % Recovery (%) Q File ID Tetrachloro-meta-xylene GC20F Decachlorobiphenyl GC20F Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 36 of 64
37 GC - Pesticides Page 37 of 64
38 Analytical Sample Results Client Sample ID: B8 (0-2) Lab Sample ID: (AQ5360) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : GC8B SW-846 Method 808A, Pesticides 07/09/203 9:05 JKA Phenomenex, Zebron MR-2, 20 m, 0.8 mm ID, 0.8 µm Prep : EPA /08/203 2:06 CAP 0.2 g 25.0 ml Analyte CAS No. Result (ug/g) PQL Dilution Factor Flags File ID Aldrin ND U GC8B alpha Chlordane ND U GC8B alpha-bhc ND U GC8B beta-bhc ND U GC8B Chlordane ND U GC8B delta-bhc ND U GC8B Dieldrin ND U GC8B Endosulfan I ND U GC8B Endosulfan II ND U GC8B Endosulfan sulfate ND U GC8B Endrin ND U GC8B Endrin aldehyde ND U GC8B Endrin ketone ND U GC8B gamma Chlordane ND U GC8B gamma-bhc ND U GC8B Heptachlor ND U GC8B Heptachlor epoxide ND U GC8B Hexachlorobenzene ND U GC8B Methoxychlor ND U GC8B p,p'-ddd ND U GC8B p,p'-dde ND U GC8B p,p'-ddt ND U GC8B Toxaphene ND U GC8B Limits Surrogate CAS No. % Recovery (%) Q File ID Tetrachloro-meta-xylene GC8B Decachlorobiphenyl GC8B Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 38 of 64
39 Analytical Sample Results Client Sample ID: B8 (2-5) Lab Sample ID: (AQ536) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : GC8B SW-846 Method 808A, Pesticides 07/09/203 9:5 JKA Phenomenex, Zebron MR-2, 20 m, 0.8 mm ID, 0.8 µm Prep : EPA /08/203 6:06 CAP 0.4 g 25.0 ml Analyte CAS No. Result (ug/g) PQL Dilution Factor Flags File ID Aldrin ND U GC8B alpha Chlordane ND U GC8B alpha-bhc ND U GC8B beta-bhc ND U GC8B Chlordane ND U GC8B delta-bhc ND U GC8B Dieldrin ND U GC8B Endosulfan I ND U GC8B Endosulfan II ND U GC8B Endosulfan sulfate ND U GC8B Endrin ND U GC8B Endrin aldehyde ND U GC8B Endrin ketone ND U GC8B gamma Chlordane ND U GC8B gamma-bhc ND U GC8B Heptachlor ND U GC8B Heptachlor epoxide ND U GC8B Hexachlorobenzene ND U GC8B Methoxychlor ND U GC8B p,p'-ddd ND U GC8B p,p'-dde ND U GC8B p,p'-ddt ND U GC8B Toxaphene ND U GC8B Limits Surrogate CAS No. % Recovery (%) Q File ID Tetrachloro-meta-xylene GC8B Decachlorobiphenyl GC8B Qualifier column where '*' denotes value outside the control limits or 'D' denotes value was diluted out. ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 39 of 64
40 Metals - ICP Page 40 of 64
41 Analytical Sample Results Client Sample ID: B8 (0-2) Lab Sample ID: (AQ5360) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : ICP SW B 07/09/203 7:2 CJH Prep : 379 EPA 3050B 07/09/203 09:0 CYC g 50.0 ml Analyte CAS No. Result (mg/kg) PQL Dilution Factor Flags File ID Aluminum ICP Antimony ND U ICP Arsenic ICP Barium ICP Beryllium ICP Cadmium ND U ICP Calcium ICP Chromium ICP Cobalt ICP Copper ICP Iron ICP Lead ICP Magnesium ICP Manganese ICP Nickel ICP Potassium ICP Selenium ND.8.00 U ICP Silver ND U ICP Sodium ICP Thallium ND.8.00 U ICP Vanadium ICP Zinc ICP ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 4 of 64
42 Analytical Sample Results Client Sample ID: B8 (2-5) Lab Sample ID: (AQ536) Collection Date: 07/02/203 :05 Received Date: 07/02/203 8:07 Percent Solid: Results are based on dry weight unless otherwise noted. Analysis : ICP SW B 07/0/203 5:30 CJH Prep : 379 EPA 3050B 07/09/203 09:02 CYC g 50.0 ml Analyte CAS No. Result (mg/kg) PQL Dilution Factor Flags File ID Aluminum ICP Antimony ND U ICP Arsenic ICP Barium ICP Beryllium ND U ICP Cadmium ND U ICP Calcium ICP Chromium ICP Cobalt ICP Copper ICP Iron ICP Lead ICP Magnesium ICP Manganese ICP Nickel ICP Potassium ICP Selenium ND U ICP Silver ND U ICP Sodium ND U ICP Thallium ND U ICP Vanadium ICP Zinc ICP ND: Denotes analyte not detected at a concentration greater than the PQL. PQL (Practical Quantitation Limit). Denotes lowest analyte concentration reportable for the sample. Phone Fax Page 42 of 64
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