Analytical Data Report for Sediment Samples Collected From 100-NR-2 Operable Unit
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1 PNNL Analytical Data Report for Sediment Samples Collected From 100-NR-2 Operable Unit Michael Lindberg October 2011
2 DISCLAIMER This report was prepared as an account of work sponsored by an agency of the United States Government. Neither the United States Government nor any agency thereof, nor Battelle Memorial Institute, nor any of their employees, makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness, or usefulness of any information, apparatus, product, or process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific commercial product, process, or service by trade name, trademark, manufacturer, or otherwise does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United States Government or any agency thereof, or Battelle Memorial Institute. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Government or any agency thereof. PACIFIC NORTHWEST NATIONAL LABORATORY operated by BATTELLE for the UNITED STATES DEPARTMENT OF ENERGY under Contract DE-AC05-76RL01830 Printed in the United States of America Available to DOE and DOE contractors from the Office of Scientific and Technical Information, P.O. Box 62, Oak Ridge, TN ; ph: (865) fax: (865) Available to the public from the National Technical Information Service, U.S. Department of Commerce, 5285 Port Royal Rd., Springfield, VA ph: (800) fax: (703) online ordering: This document was printed on recycled paper. (9/2003)
3 PNNL Analytical Data Report for Sediment Samples Collected From 100-NR-2 Operable Unit MJ Lindberg October 2011 Prepared for the U.S. Department of Energy under Contract DE-AC05-76RL01830 Pacific Northwest National Laboratory Richland, Washington 99352
4 09/30/11 09:44 To: Anna Radloff From: M ichael J. Lindberg Environmental Sciences Laboratory Energy and Environment Directorate, Pacific Northwest National Laboratory Subject: Analytical Data Report for Sediment Samples Collected From 100-NR-2 Operable Unit, Sample Delivery Group ESL090023, SAF Number F This letter contains the following information for sample delivery group ESL Cover Sheet Narrative Analytical s Quality Control Chain of Custodies Page 1 of 52
5 Introduction Between April 7, 2011 and September 20, 2011 sediment samples were received from the 100-NR-2 Operable Unit for geochemical studies. Analytical s/methodology The analyses for this project were performed at the 331 building located in the 300 Area of the Hanford Site. The analyses were performed according to Pacific Northwest National Laboratory (PNNL) approved procedures and/or nationally recognized test procedures. The data sets include the sample identification numbers, analytical results, estimated quantification limits (EQL), and quality control data. Quality Control The preparatory and analytical quality control requirements, calibration requirements, acceptance criteria, and failure actions are defined in the on-line QA plan Conducting Analytical Work in Support of Regulatory Programs (CAW). This QA plan implements the Hanford Analytical Services Quality Assurance Requirements Documents (HASQARD) for PNNL. Definitions Dup NR ND Duplicate Relative Percent Difference No Recovery (percent recovery less than zero) Non-Detectable Percent Recovery Sample Receipt Samples were received with a chain of custody (COC) and were analyzed according to the sample identification numbers supplied by the client. All Samples were refrigerated upon receipt until prepared for analysis. All samples were received with custody seals intact unless noted in the Case Narrative. Holding Times Holding time is defined as the time from sample preparation to the time of analyses. The prescribed holding times were met for all analytes unless noted in the Case Narrative. Analytical s All reported analytical results meet the requirements of the CAW or client specified SOW unless noted in the case narrative. Page 2 of 52
6 Case Narrative Report Hold Time: Due to the requirements of the statement of work and sampling events in the field, the 28 day and the 48 hr requirements cannot be met. The statement of work requires samples to be selected at the completion of the borehole. It is not always possible to complete a borehole and have the samples shipped to the laboratory within the hold time requirements. Preparation Blank (PB): No discrepancies noted. Duplicate (DUP): Duplicate for (37.8%) was above the acceptance limit (35) in 1I26009-DUP1 for ICPMS-RCRA-AE All other duplicates and QC associated with the batch were in limits. Duplicate failure may be due to sample heterogeneity. There should be no impact to sample data as reported. Laboratory Control Samples (LCS): No discrepancies noted. Post Spike (PS): Post-Spike Recovery for (140%) was outside acceptance limits (75-125) in 1I26009-PS1 for ICPMS-RCRA-AE The native sample concentration of the sample was greater than 5 times the spike concentration. There should be not impact to data as reported. Matrix Spike (MS): Matrix Spike Recovery for (41.6%) was outside acceptance limits (75-125) in 1H18007-MS1 for Hexavalent /Soil Potential Matrix interference. Sample results associated with this batch are below the EQL. There should be no impact to the data as reported. Other QC Criteria: No discrepancies noted. Page 3 of 52
7 I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Analytical Manager as verified by this signature. Michael Lindberg DISCLAIMER This report was prepared as an account of work sponsored by an agency of the United States Government. Neither the United States Government nor any agency thereof, nor Battelle Memorial Institute, nor any of their employees, makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness, or usefulness of any information, apparatus, product, or process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific commercial product, process, or service by trade name, trademark, manufacturer, or otherwise does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United States Government or any agency thereof, or Battelle Memorial Institute. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Government or any agency thereof. PACIFIC NORTHWEST NATIONAL LABORATORY operated by BATTELLE for the UNITED STATES DEPARTMENT OF ENERGY under Contract DE-AC05-76RLOJ830 Page 4 of 52
8 The following analyses were performed on the following samples included in this report: Metals 1:1 DI Water Extract by ICPMS Metals 1:2.5 DI Water Extract by ICPMS Metals 1:5 DI Water Extract by ICPMS Metals Acid Extract by ICPMS Hexavalent by Colorimetric Determination Moisture Content Strontium 90 1:2.5 DI Water Extract by LSC Strontium 90 1:5 DI Water Extract by LSC Strontium 90 Acid Extract by LSC Strontium 90 Water Extract by LSC SAMPLES ANALYZED IN THIS REPORT HEIS No. B2C4B3 Laboratory ID Matrix SOIL Date Collected 3/31/11 11:25 Date Received 4/7/11 13:00 B2C4B SOIL 4/4/11 09:20 4/7/11 13:00 B2C4B SOIL 4/6/11 13:30 4/7/11 13:00 B2D4K SOIL 4/26/11 13:55 5/4/11 10:00 B2D1X SOIL 7/7/11 10:15 7/11/11 13:00 B2D1X SOIL 7/12/11 13:40 7/13/11 13:00 B2C4W SOIL 7/18/11 10:30 7/18/11 13:00 B2C4W SOIL 7/14/11 14:00 7/18/11 13:00 B2C SOIL 9/16/11 10:35 9/20/11 13:30 B2C SOIL 9/19/11 10:10 9/20/11 13:30 Page 5 of 52
9 Moisture Content (% by Weight) by AGG-WC-001 Wet Chemistry Lab ID HEIS No. s EQL Analyzed Batch B2C4B3 2.86E1 8/10/11 1H B2C4B4 2.73E1 8/10/11 1H B2C4B5 3.56E1 8/10/11 1H B2D4K4 1.02E1 8/10/11 1H B2D1X0 1.80E1 8/10/11 1H B2D1X1 2.42E1 8/10/11 1H B2C4W2 3.82E1 8/10/11 1H B2C4W3 2.23E1 8/10/11 1H B2C E1 9/22/11 1I B2C E1 9/22/11 1I20006 Page 6 of 52
10 Hexavalent /Soil (ug/g dry) by Colorimetric Determination Lab ID HEIS No. s EQL Analyzed Batch B2C4B3 <6.39E E-1 8/18/11 1H B2C4B4 <6.37E E-1 8/18/11 1H B2C4B5 <6.78E E-1 8/18/11 1H B2D4K4 <5.50E E-1 8/18/11 1H B2D1X0 <5.92E E-1 8/18/11 1H B2D1X1 <6.16E E-1 8/18/11 1H B2C4W2 <6.95E E-1 8/18/11 1H B2C4W3 <6.09E E-1 8/18/11 1H B2C414 <5.60E E-1 9/27/11 1I B2C415 <6.22E E-1 9/27/11 1I26012 Page 7 of 52
11 Hexavalent /1:1 Water Extract (ug/g dry) by Colorimetric Determination Lab ID HEIS No. s EQL Analyzed Batch B2C4B3 <4.99E E-2 8/16/11 1H B2C4B4 <5.00E E-2 8/16/11 1H B2C4B5 <5.21E E-2 8/16/11 1H B2D4K4 <5.15E E-2 8/16/11 1H B2D1X0 <5.00E E-2 8/16/11 1H B2D1X1 <5.00E E-2 8/16/11 1H B2C4W2 <5.08E E-2 8/16/11 1H B2C4W3 <5.08E E-2 8/16/11 1H B2C414 <5.08E E-2 9/26/11 1I B2C415 <5.00E E-2 9/26/11 1I26001 Page 8 of 52
12 Hexavalent /1:2.5 Water Extract (ug/g dry) by Colorimetric Determination Lab ID HEIS No. s EQL Analyzed Batch B2C4B3 <1.24E E-1 8/16/11 1H B2C4B4 <1.25E E-1 8/16/11 1H B2C4B5 <1.25E E-1 8/16/11 1H B2D4K4 <1.25E E-1 8/16/11 1H B2D1X0 <1.29E E-1 8/16/11 1H B2D1X1 <1.25E E-1 8/16/11 1H B2C4W2 <1.27E E-1 8/16/11 1H B2C4W3 <1.24E E-1 8/16/11 1H B2C414 <1.25E E-1 9/26/11 1I B2C415 <1.25E E-1 9/26/11 1I26002 Page 9 of 52
13 Hexavalent /1:5 Water Extract (ug/g dry) by Colorimetric Determination Lab ID HEIS No. s EQL Analyzed Batch B2C4B3 <2.50E E-1 8/16/11 1H B2C4B4 <2.50E E-1 8/16/11 1H B2C4B5 <2.50E E-1 8/16/11 1H B2D4K4 <2.50E E-1 8/16/11 1H B2D1X0 <2.51E E-1 8/16/11 1H B2D1X1 <2.49E E-1 8/16/11 1H B2C4W2 <2.49E E-1 8/16/11 1H B2C4W3 <2.48E E-1 8/16/11 1H B2C414 <2.42E E-1 9/26/11 1I B2C415 <2.50E E-1 9/26/11 1I26003 Page 10 of 52
14 RCRA Metals By PNNL-AGG-415/1:1 Water Extract CAS # Analyte s Units EQL Analyzed Batch Method HEIS No. B2C4B3 Lab ID: <6.87E-3 ug/g dry 6.87E E-2 ug/g dry 5.66E-3 <1.58E-2 ug/g dry 1.58E-2 <6.24E-3 ug/g dry 6.24E-3 <1.14E-3 ug/g dry 1.14E-3 <2.32E-3 ug/g dry 2.32E E-2 ug/g dry 6.22E-4 8/24/11 1H22004 PNNL-AGG-415 HEIS No. B2C4B4 Lab ID: <6.89E-3 ug/g dry 6.89E E-2 ug/g dry 5.67E-3 <1.58E-2 ug/g dry 1.58E-2 <6.25E-3 ug/g dry 6.25E-3 <1.15E-3 ug/g dry 1.15E-3 <2.32E-3 ug/g dry 2.32E E-2 ug/g dry 6.24E-4 8/24/11 1H22004 PNNL-AGG-415 HEIS No. B2C4B5 Lab ID: <7.18E-3 ug/g dry 7.18E E-3 ug/g dry 5.91E-3 <1.65E-2 ug/g dry 1.65E-2 <6.52E-3 ug/g dry 6.52E-3 <1.19E-3 ug/g dry 1.19E-3 <2.42E-3 ug/g dry 2.42E E-2 ug/g dry 6.51E-4 8/24/11 1H22004 PNNL-AGG-415 HEIS No. B2D4K4 Lab ID: <7.10E-3 ug/g dry 7.10E-3 <5.85E-3 ug/g dry 5.85E-3 <1.63E-2 ug/g dry 1.63E-2 <6.45E-3 ug/g dry 6.45E-3 <1.18E-3 ug/g dry 1.18E-3 <2.40E-3 ug/g dry 2.40E E-2 ug/g dry 6.44E-4 8/24/11 1H22004 PNNL-AGG-415 HEIS No. B2D1X0 Lab ID: <6.89E-3 ug/g dry 6.89E E-2 ug/g dry 5.67E-3 <1.58E-2 ug/g dry 1.58E-2 <6.25E-3 ug/g dry 6.25E-3 <1.15E-3 ug/g dry 1.15E-3 <2.32E-3 ug/g dry 2.32E E-3 ug/g dry 6.24E-4 8/24/11 1H22004 PNNL-AGG-415 HEIS No. B2D1X1 Lab ID: <6.89E-3 ug/g dry 6.89E E-3 ug/g dry 5.67E-3 <1.58E-2 ug/g dry 1.58E-2 <6.26E-3 ug/g dry 6.26E-3 <1.15E-3 ug/g dry 1.15E-3 <2.32E-3 ug/g dry 2.32E E-3 ug/g dry 6.24E-4 8/24/11 1H22004 PNNL-AGG-415 Page 11 of 52
15 RCRA Metals By PNNL-AGG-415/1:1 Water Extract CAS # Analyte s Units EQL Analyzed Batch Method HEIS No. B2C4W2 Lab ID: <7.00E-3 ug/g dry 7.00E E-2 ug/g dry 5.76E-3 <1.61E-2 ug/g dry 1.61E-2 <6.35E-3 ug/g dry 6.35E-3 <1.16E-3 ug/g dry 1.16E-3 <2.36E-3 ug/g dry 2.36E E-2 ug/g dry 6.34E-4 8/24/11 1H22004 PNNL-AGG-415 HEIS No. B2C4W3 Lab ID: <7.00E-3 ug/g dry 7.00E E-2 ug/g dry 5.76E-3 <1.61E-2 ug/g dry 1.61E-2 <6.35E-3 ug/g dry 6.35E-3 <1.16E-3 ug/g dry 1.16E-3 <2.36E-3 ug/g dry 2.36E E-2 ug/g dry 6.34E-4 8/24/11 1H22004 PNNL-AGG-415 HEIS No. B2C414 Lab ID: <7.00E-3 ug/g dry 7.00E-3 9/26/11 1I26008 PNNL-AGG-415 <5.76E-3 ug/g dry 5.76E-3 9/26/11 1I26008 PNNL-AGG-415 <1.61E-2 ug/g dry 1.61E-2 9/26/11 1I26008 PNNL-AGG-415 <6.36E-3 ug/g dry 6.36E-3 9/26/11 1I26008 PNNL-AGG-415 <1.16E-3 ug/g dry 1.16E-3 9/26/11 1I26008 PNNL-AGG-415 <2.36E-3 ug/g dry 2.36E-3 9/26/11 1I26008 PNNL-AGG E-2 ug/g dry 6.34E-4 9/27/11 1I26008 PNNL-AGG-415 HEIS No. B2C415 Lab ID: <6.88E-3 ug/g dry 6.88E-3 9/26/11 1I26008 PNNL-AGG-415 <5.67E-3 ug/g dry 5.67E-3 9/26/11 1I26008 PNNL-AGG-415 <1.58E-2 ug/g dry 1.58E-2 9/26/11 1I26008 PNNL-AGG-415 <6.25E-3 ug/g dry 6.25E-3 9/26/11 1I26008 PNNL-AGG-415 <1.15E-3 ug/g dry 1.15E-3 9/26/11 1I26008 PNNL-AGG-415 <2.32E-3 ug/g dry 2.32E-3 9/26/11 1I26008 PNNL-AGG E-2 ug/g dry 6.24E-4 9/27/11 1I26008 PNNL-AGG-415 Page 12 of 52
16 RCRA Metals By PNNL-AGG-415/1:2.5 Water Extract CAS # Analyte s Units EQL Analyzed Batch Method HEIS No. B2C4B3 Lab ID: <1.71E-2 ug/g dry 1.71E E-2 ug/g dry 1.41E-2 <3.93E-2 ug/g dry 3.93E-2 <1.55E-2 ug/g dry 1.55E-2 <2.84E-3 ug/g dry 2.84E-3 <5.77E-3 ug/g dry 5.77E E-2 ug/g dry 1.55E-3 8/24/11 1H22003 PNNL-AGG-415 HEIS No. B2C4B4 Lab ID: <1.72E-2 ug/g dry 1.72E E-2 ug/g dry 1.42E-2 <3.95E-2 ug/g dry 3.95E-2 <1.56E-2 ug/g dry 1.56E-2 <2.86E-3 ug/g dry 2.86E-3 <5.80E-3 ug/g dry 5.80E E-2 ug/g dry 1.56E-3 8/24/11 1H22003 PNNL-AGG-415 HEIS No. B2C4B5 Lab ID: <1.72E-2 ug/g dry 1.72E-2 <1.42E-2 ug/g dry 1.42E-2 <3.96E-2 ug/g dry 3.96E-2 <1.56E-2 ug/g dry 1.56E-2 <2.86E-3 ug/g dry 2.86E-3 <5.81E-3 ug/g dry 5.81E E-2 ug/g dry 1.56E-3 8/24/11 1H22003 PNNL-AGG-415 HEIS No. B2D4K4 Lab ID: <1.72E-2 ug/g dry 1.72E-2 <1.42E-2 ug/g dry 1.42E-2 <3.96E-2 ug/g dry 3.96E-2 <1.57E-2 ug/g dry 1.57E-2 <2.87E-3 ug/g dry 2.87E-3 <5.82E-3 ug/g dry 5.82E E-2 ug/g dry 1.56E-3 8/24/11 1H22003 PNNL-AGG-415 HEIS No. B2D1X0 Lab ID: <1.78E-2 ug/g dry 1.78E E-2 ug/g dry 1.47E-2 <4.09E-2 ug/g dry 4.09E-2 <1.62E-2 ug/g dry 1.62E-2 <2.96E-3 ug/g dry 2.96E-3 <6.00E-3 ug/g dry 6.00E E-3 ug/g dry 1.61E-3 8/24/11 1H22003 PNNL-AGG-415 HEIS No. B2D1X1 Lab ID: <1.72E-2 ug/g dry 1.72E-2 <1.42E-2 ug/g dry 1.42E-2 <3.96E-2 ug/g dry 3.96E-2 <1.56E-2 ug/g dry 1.56E-2 <2.87E-3 ug/g dry 2.87E-3 <5.81E-3 ug/g dry 5.81E E-2 ug/g dry 1.56E-3 8/24/11 1H22003 PNNL-AGG-415 Page 13 of 52
17 RCRA Metals By PNNL-AGG-415/1:2.5 Water Extract CAS # Analyte s Units EQL Analyzed Batch Method HEIS No. B2C4W2 Lab ID: <1.74E-2 ug/g dry 1.74E E-2 ug/g dry 1.44E-2 <4.01E-2 ug/g dry 4.01E-2 <1.58E-2 ug/g dry 1.58E-2 <2.90E-3 ug/g dry 2.90E-3 <5.88E-3 ug/g dry 5.88E E-2 ug/g dry 1.58E-3 8/24/11 1H22003 PNNL-AGG-415 HEIS No. B2C4W3 Lab ID: <1.71E-2 ug/g dry 1.71E E-2 ug/g dry 1.41E-2 <3.94E-2 ug/g dry 3.94E-2 <1.56E-2 ug/g dry 1.56E-2 <2.85E-3 ug/g dry 2.85E-3 <5.78E-3 ug/g dry 5.78E-3 <1.55E-3 ug/g dry 1.55E-3 HEIS No. B2C414 Lab ID: <1.72E-2 ug/g dry 1.72E-2 9/26/11 1I26007 PNNL-AGG-415 <1.42E-2 ug/g dry 1.42E-2 9/26/11 1I26007 PNNL-AGG-415 <3.95E-2 ug/g dry 3.95E-2 9/26/11 1I26007 PNNL-AGG-415 <1.56E-2 ug/g dry 1.56E-2 9/26/11 1I26007 PNNL-AGG-415 <2.86E-3 ug/g dry 2.86E-3 9/26/11 1I26007 PNNL-AGG-415 <5.80E-3 ug/g dry 5.80E-3 9/26/11 1I26007 PNNL-AGG E-2 ug/g dry 1.56E-3 9/27/11 1I26007 PNNL-AGG-415 HEIS No. B2C415 Lab ID: <1.72E-2 ug/g dry 1.72E-2 9/26/11 1I26007 PNNL-AGG E-2 ug/g dry 1.42E-2 9/26/11 1I26007 PNNL-AGG-415 <3.96E-2 ug/g dry 3.96E-2 9/26/11 1I26007 PNNL-AGG-415 <1.56E-2 ug/g dry 1.56E-2 9/26/11 1I26007 PNNL-AGG-415 <2.86E-3 ug/g dry 2.86E-3 9/26/11 1I26007 PNNL-AGG-415 <5.81E-3 ug/g dry 5.81E-3 9/26/11 1I26007 PNNL-AGG E-1 ug/g dry 1.56E-3 9/27/11 1I26007 PNNL-AGG-415 Page 14 of 52
18 RCRA Metals By PNNL-AGG-415/1:5 Water Extract CAS # Analyte s Units EQL Analyzed Batch Method HEIS No. B2C4B3 Lab ID: <3.44E-2 ug/g dry 3.44E E-2 ug/g dry 2.83E-2 <7.90E-2 ug/g dry 7.90E-2 <3.12E-2 ug/g dry 3.12E-2 <5.72E-3 ug/g dry 5.72E E-2 ug/g dry 1.16E E-2 ug/g dry 3.12E-3 8/24/11 1H22002 PNNL-AGG-415 HEIS No. B2C4B4 Lab ID: <3.44E-2 ug/g dry 3.44E-2 <2.83E-2 ug/g dry 2.83E-2 <7.91E-2 ug/g dry 7.91E-2 <3.12E-2 ug/g dry 3.12E-2 <5.72E-3 ug/g dry 5.72E-3 <1.16E-2 ug/g dry 1.16E E-2 ug/g dry 3.12E-3 8/24/11 1H22002 PNNL-AGG-415 HEIS No. B2C4B5 Lab ID: <3.45E-2 ug/g dry 3.45E-2 <2.84E-2 ug/g dry 2.84E-2 <7.93E-2 ug/g dry 7.93E-2 <3.13E-2 ug/g dry 3.13E-2 <5.74E-3 ug/g dry 5.74E-3 <1.16E-2 ug/g dry 1.16E E-2 ug/g dry 3.13E-3 8/24/11 1H22002 PNNL-AGG-415 HEIS No. B2D4K4 Lab ID: <3.44E-2 ug/g dry 3.44E-2 <2.83E-2 ug/g dry 2.83E-2 <7.90E-2 ug/g dry 7.90E-2 <3.12E-2 ug/g dry 3.12E-2 <5.72E-3 ug/g dry 5.72E-3 <1.16E-2 ug/g dry 1.16E E-2 ug/g dry 3.12E-3 8/24/11 1H22002 PNNL-AGG-415 HEIS No. B2D1X0 Lab ID: <3.45E-2 ug/g dry 3.45E E-2 ug/g dry 2.84E-2 <7.93E-2 ug/g dry 7.93E-2 <3.13E-2 ug/g dry 3.13E-2 <5.74E-3 ug/g dry 5.74E-3 <1.16E-2 ug/g dry 1.16E-2 <3.13E-3 ug/g dry 3.13E-3 8/24/11 1H22002 PNNL-AGG-415 HEIS No. B2D1X1 Lab ID: <3.43E-2 ug/g dry 3.43E-2 <2.83E-2 ug/g dry 2.83E-2 <7.89E-2 ug/g dry 7.89E-2 <3.12E-2 ug/g dry 3.12E-2 <5.71E-3 ug/g dry 5.71E-3 <1.16E-2 ug/g dry 1.16E E-2 ug/g dry 3.11E-3 8/24/11 1H22002 PNNL-AGG-415 Page 15 of 52
19 RCRA Metals By PNNL-AGG-415/1:5 Water Extract CAS # Analyte s Units EQL Analyzed Batch Method HEIS No. B2C4W2 Lab ID: <3.43E-2 ug/g dry 3.43E E-2 ug/g dry 2.82E-2 <7.88E-2 ug/g dry 7.88E-2 <3.11E-2 ug/g dry 3.11E-2 <5.70E-3 ug/g dry 5.70E-3 <1.16E-2 ug/g dry 1.16E E-2 ug/g dry 3.11E-3 8/24/11 1H22002 PNNL-AGG-415 HEIS No. B2C4W3 Lab ID: <3.41E-2 ug/g dry 3.41E E-2 ug/g dry 2.81E-2 <7.85E-2 ug/g dry 7.85E-2 <3.10E-2 ug/g dry 3.10E-2 <5.68E-3 ug/g dry 5.68E-3 <1.15E-2 ug/g dry 1.15E E-2 ug/g dry 3.09E-3 8/24/11 1H22002 PNNL-AGG-415 HEIS No. B2C414 Lab ID: <3.33E-2 ug/g dry 3.33E-2 9/26/11 1I26006 PNNL-AGG-415 <2.74E-2 ug/g dry 2.74E-2 9/26/11 1I26006 PNNL-AGG-415 <7.65E-2 ug/g dry 7.65E-2 9/26/11 1I26006 PNNL-AGG-415 <3.02E-2 ug/g dry 3.02E-2 9/26/11 1I26006 PNNL-AGG-415 <5.54E-3 ug/g dry 5.54E-3 9/26/11 1I26006 PNNL-AGG-415 <1.12E-2 ug/g dry 1.12E-2 9/26/11 1I26006 PNNL-AGG E-2 ug/g dry 3.02E-3 9/27/11 1I26006 PNNL-AGG-415 HEIS No. B2C415 Lab ID: <3.45E-2 ug/g dry 3.45E-2 9/26/11 1I26006 PNNL-AGG E-2 ug/g dry 2.84E-2 9/26/11 1I26006 PNNL-AGG-415 <7.92E-2 ug/g dry 7.92E-2 9/26/11 1I26006 PNNL-AGG-415 <3.13E-2 ug/g dry 3.13E-2 9/26/11 1I26006 PNNL-AGG-415 <5.73E-3 ug/g dry 5.73E-3 9/26/11 1I26006 PNNL-AGG-415 <1.16E-2 ug/g dry 1.16E-2 9/26/11 1I26006 PNNL-AGG E-1 ug/g dry 3.12E-3 9/27/11 1I26006 PNNL-AGG-415 Page 16 of 52
20 RCRA Metals By PNNL-AGG-415/Acid Extract CAS # Analyte s Units EQL Analyzed Batch Method HEIS No. B2C4B3 Lab ID: E1 ug/g dry 8.46E E0 ug/g dry 3.68E-1 9/07/11 1H22005 PNNL-AGG-415 <7.12E-1 ug/g dry 7.12E E-1 ug/g dry 2.30E E-1 ug/g dry 6.08E E0 ug/g dry 2.31E E1 ug/g dry 2.80E-2 8/24/11 1H22005 PNNL-AGG-415 HEIS No. B2C4B4 Lab ID: E0 ug/g dry 8.33E E0 ug/g dry 3.63E-1 9/07/11 1H22005 PNNL-AGG-415 <7.01E-1 ug/g dry 7.01E E-2 ug/g dry 2.27E E-2 ug/g dry 5.99E E0 ug/g dry 2.27E E1 ug/g dry 1.38E-1 9/02/11 1H22005 PNNL-AGG-415 HEIS No. B2C4B5 Lab ID: E0 ug/g dry 8.75E E0 ug/g dry 3.81E-1 9/07/11 1H22005 PNNL-AGG-415 <7.37E-1 ug/g dry 7.37E E-2 ug/g dry 2.38E-2 <6.29E-2 ug/g dry 6.29E E0 ug/g dry 2.39E E1 ug/g dry 2.90E-2 8/24/11 1H22005 PNNL-AGG-415 HEIS No. B2D4K4 Lab ID: E0 ug/g dry 7.17E E0 ug/g dry 3.12E-1 9/07/11 1H22005 PNNL-AGG-415 <6.04E-1 ug/g dry 6.04E E-2 ug/g dry 1.95E-2 <5.16E-2 ug/g dry 5.16E E0 ug/g dry 1.95E E1 ug/g dry 2.38E-2 8/24/11 1H22005 PNNL-AGG-415 HEIS No. B2D1X0 Lab ID: E0 ug/g dry 7.73E E0 ug/g dry 3.36E-1 9/07/11 1H22005 PNNL-AGG-415 <6.50E-1 ug/g dry 6.50E E-2 ug/g dry 2.10E-2 <5.55E-2 ug/g dry 5.55E E0 ug/g dry 2.11E E1 ug/g dry 2.56E-2 8/24/11 1H22005 PNNL-AGG-415 HEIS No. B2D1X1 Lab ID: E1 ug/g dry 7.93E E0 ug/g dry 3.45E-1 9/07/11 1H22005 PNNL-AGG-415 <6.67E-1 ug/g dry 6.67E E-2 ug/g dry 2.16E E-1 ug/g dry 5.70E E0 ug/g dry 2.16E E1 ug/g dry 1.31E-1 9/02/11 1H22005 PNNL-AGG-415 Page 17 of 52
21 RCRA Metals By PNNL-AGG-415/Acid Extract CAS # Analyte s Units EQL Analyzed Batch Method HEIS No. B2C4W2 Lab ID: E0 ug/g dry 8.91E E0 ug/g dry 3.88E-1 9/07/11 1H22005 PNNL-AGG-415 <7.50E-1 ug/g dry 7.50E E-2 ug/g dry 2.43E E-1 ug/g dry 6.40E E0 ug/g dry 2.43E E1 ug/g dry 2.95E-2 8/24/11 1H22005 PNNL-AGG-415 HEIS No. B2C4W3 Lab ID: E1 ug/g dry 7.88E-1 8/23/11 1H22005 PNNL-AGG E0 ug/g dry 3.43E-1 9/07/11 1H22005 PNNL-AGG-415 <6.63E-1 ug/g dry 6.63E-1 8/23/11 1H22005 PNNL-AGG E-2 ug/g dry 2.15E-2 8/23/11 1H22005 PNNL-AGG E-1 ug/g dry 5.66E-2 8/23/11 1H22005 PNNL-AGG E0 ug/g dry 2.15E-1 8/31/11 1H22005 PNNL-AGG E1 ug/g dry 1.31E-1 9/02/11 1H22005 PNNL-AGG-415 HEIS No. B2C414 Lab ID: E0 ug/g dry 7.42E-1 9/27/11 1I26009 PNNL-AGG E-1 ug/g dry 3.23E-1 9/28/11 1I26009 PNNL-AGG-415 <6.25E-1 ug/g dry 6.25E-1 9/26/11 1I26009 PNNL-AGG E-2 ug/g dry 2.02E-2 9/26/11 1I26009 PNNL-AGG-415 <5.34E-2 ug/g dry 5.34E-2 9/26/11 1I26009 PNNL-AGG E0 ug/g dry 2.02E-1 9/26/11 1I26009 PNNL-AGG E1 ug/g dry 1.23E-1 9/27/11 1I26009 PNNL-AGG-415 HEIS No. B2C415 Lab ID: E1 ug/g dry 8.31E-1 9/27/11 1I26009 PNNL-AGG E0 ug/g dry 3.62E-1 9/28/11 1I26009 PNNL-AGG-415 <7.00E-1 ug/g dry 7.00E-1 9/26/11 1I26009 PNNL-AGG E-2 ug/g dry 2.26E-2 9/26/11 1I26009 PNNL-AGG E-1 ug/g dry 5.98E-2 9/26/11 1I26009 PNNL-AGG E0 ug/g dry 2.27E-1 9/26/11 1I26009 PNNL-AGG E2 ug/g dry 1.38E-1 9/27/11 1I26009 PNNL-AGG-415 Page 18 of 52
22 (pci/g dry) by AGG-RRL-002 Strontium 90/Acid Extract Lab ID HEIS No. s MDA UNC Analyzed Batch B2C4B3 <5.89E E-1 9/06/11 1H B2C4B4 <5.86E E-1 9/06/11 1H B2C4B5 <5.78E E-1 9/06/11 1H B2D4K4 <5.83E E-1 9/06/11 1H B2D1X0 <5.86E E-1 9/06/11 1H B2D1X1 <5.72E E-1 9/06/11 1H B2C4W2 <5.77E E-1 9/06/11 1H B2C4W3 <5.77E E-1 9/06/11 1H B2C414 <6.81E E-1 9/28/11 1I B2C415 <6.87E E-1 9/28/11 1I23004 Page 19 of 52
23 (pci/g dry) by AGG-RRL-002 Strontium 90/1:1 Water Extract Lab ID HEIS No. s MDA UNC Analyzed Batch B2C4B3 <5.89E E-1 9/06/11 1H B2C4B4 <5.90E E-1 9/06/11 1H B2C4B5 <6.15E E-1 9/06/11 1H B2D4K4 <6.09E E-1 9/06/11 1H B2D1X0 <5.90E E-1 9/06/11 1H B2D1X1 <5.91E E-1 9/06/11 1H B2C4W2 <6.00E E-1 9/06/11 1H B2C4W3 <6.00E E-1 9/06/11 1H B2C414 <6.87E E-1 9/28/11 1I B2C415 <6.76E E-1 9/28/11 1I23001 Page 20 of 52
24 (pci/g dry) by AGG-RRL-002 Strontium 90/1:2.5 Water Extract Lab ID HEIS No. s MDA UNC Analyzed Batch B2C4B3 <1.47E0 1.47E0 9/06/11 1H B2C4B4 <1.47E0 1.47E0 9/06/11 1H B2C4B5 <1.48E0 1.48E0 9/06/11 1H B2D4K4 <1.48E0 1.48E0 9/06/11 1H B2D1X0 <1.53E0 1.53E0 9/06/11 1H B2D1X1 <1.48E0 1.48E0 9/06/11 1H B2C4W2 <1.49E0 1.49E0 9/06/11 1H B2C4W3 <1.47E0 1.47E0 9/06/11 1H B2C414 <1.69E0 1.69E0 9/28/11 1I B2C415 <1.69E0 1.69E0 9/28/11 1I23002 Page 21 of 52
25 (pci/g dry) by AGG-RRL-002 Strontium 90/1:5 Water Extract Lab ID HEIS No. s MDA UNC Analyzed Batch B2C4B3 <2.95E0 2.95E0 9/06/11 1H B2C4B4 <2.95E0 2.95E0 9/06/11 1H B2C4B5 <2.96E0 2.96E0 9/06/11 1H B2D4K4 <2.95E0 2.95E0 9/06/11 1H B2D1X0 <2.96E0 2.96E0 9/06/11 1H B2D1X1 <2.94E0 2.94E0 9/06/11 1H B2C4W2 <2.94E0 2.94E0 9/06/11 1H B2C4W3 <2.93E0 2.93E0 9/06/11 1H B2C414 <3.27E0 3.27E0 9/28/11 1I B2C415 <3.38E0 3.38E0 9/28/11 1I23003 Page 22 of 52
26 Equilibrium Kd 1:1 Calculations B2C4B B2C4B B2C4B5 Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) 6.06E E E E E E+00 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND B2D4K B2D1X B2D1X1 Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) ND ND ND 3.05E E E+00 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND B2C4W B2C4W Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) 1.11E E-01 ND 4.02E E E+00 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Analyte (Total) Kd (L/g) ND 4.65E+00 ND ND ND ND ND ND ND Page 23 of 52
27 Equilibrium Kd 1:2.5 Calculations B2C4B B2C4B B2C4B5 Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) 3.07E E-02 ND 1.80E E E+00 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND B2D4K B2D1X B2D1X1 Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) ND ND ND 2.03E E E+00 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND B2C4W B2C4W Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) 4.65E E-02 ND 3.21E+00 ND 1.05E+00 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Analyte (Total) Kd (L/g) 1.92E E+00 ND ND ND ND ND ND ND Page 24 of 52
28 Equilibrium Kd 1:5 Calculations B2C4B B2C4B B2C4B5 Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) 1.90E-02 ND ND 7.67E E E+00 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND 1.85E-01 ND ND ND ND ND ND ND ND ND ND ND B2D4K B2D1X B2D1X1 Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) ND ND ND 1.45E+00 ND 3.97E+00 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND B2C4W B2C4W Analyte Kd (L/g) Analyte Kd (L/g) Analyte Kd (L/g) 2.97E E-02 ND 1.93E E E-01 ND ND ND (Total) ND (Total) ND (Total) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Analyte (Total) Kd (L/g) 6.88E E-01 ND ND ND ND ND ND ND Page 25 of 52
29 Hexavalent /Soil - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H Hexavalent Digest Blank (1H18007-BLK1) Prepared & Analyzed: 08/18/11 <5.00E E-2 ug/g wet LCS (1H18007-BS1) Prepared & Analyzed: 08/18/ E E-2 ug/g wet 5.01E Duplicate (1H18007-DUP1) Source: Prepared & Analyzed: 08/18/11 <5.84E E-1 ug/g dry ND 20 Matrix Spike (1H18007-MS1) Source: Prepared & Analyzed: 08/18/ E-1 Batch 1I Hexavalent Digest 5.46E-1 ug/g dry 5.00E E Blank (1I26012-BLK1) Prepared: 09/26/11 Analyzed: 09/27/11 <5.00E E-2 ug/g wet LCS (1I26012-BS1) Prepared: 09/26/11 Analyzed: 09/27/ E E-2 ug/g wet 5.01E Duplicate (1I26012-DUP1) Source: Prepared: 09/26/11 Analyzed: 09/27/11 <6.22E E-1 ug/g dry ND 20 Matrix Spike (1I26012-MS1) Source: Prepared: 09/26/11 Analyzed: 09/27/ E E-1 ug/g dry 5.00E E Page 26 of 52
30 Hexavalent /1:1 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :1 Water Extract (Cr6) Blank (1H16001-BLK1) Prepared & Analyzed: 08/16/11 <5.00E E-2 ug/g wet LCS (1H16001-BS1) Prepared & Analyzed: 08/16/ E E-2 ug/g wet 5.01E Duplicate (1H16001-DUP1) Source: Prepared & Analyzed: 08/16/11 <4.99E E-2 ug/g dry ND 20 Post Spike (1H16001-PS1) Source: Prepared & Analyzed: 08/16/11 Batch 1I :1 Water Extract (Cr6) 5.11E-1 ug/ml 4.96E-1 ND Blank (1I26001-BLK1) Prepared & Analyzed: 09/26/11 <5.00E E-2 ug/g wet LCS (1I26001-BS1) Prepared & Analyzed: 09/26/ E E-2 ug/g wet 5.01E Duplicate (1I26001-DUP1) Source: Prepared & Analyzed: 09/26/11 <5.00E E-2 ug/g dry ND 20 Post Spike (1I26001-PS1) Source: Prepared & Analyzed: 09/26/ E-1 ug/ml 4.96E E Page 27 of 52
31 Hexavalent /1:2.5 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :2.5 Water Extract (Cr6) Blank (1H16002-BLK1) Prepared & Analyzed: 08/16/11 <5.00E E-2 ug/g wet LCS (1H16002-BS1) Prepared & Analyzed: 08/16/ E E-2 ug/g wet 5.01E Duplicate (1H16002-DUP1) Source: Prepared & Analyzed: 08/16/11 <1.29E E-1 ug/g dry ND 20 Post Spike (1H16002-PS1) Source: Prepared & Analyzed: 08/16/11 Batch 1I :2.5 Water Extract (Cr6) 5.03E-1 ug/ml 4.96E-1 ND Blank (1I26002-BLK1) Prepared & Analyzed: 09/26/11 <5.00E E-2 ug/g wet LCS (1I26002-BS1) Prepared & Analyzed: 09/26/ E E-2 ug/g wet 5.01E Duplicate (1I26002-DUP1) Source: Prepared & Analyzed: 09/26/11 <1.25E E-1 ug/g dry ND 20 Post Spike (1I26002-PS1) Source: Prepared & Analyzed: 09/26/ E-1 ug/ml 4.96E E Page 28 of 52
32 Hexavalent /1:5 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :5 Water Extract (Cr6) Blank (1H16003-BLK1) Prepared & Analyzed: 08/16/11 <5.00E E-2 ug/g wet LCS (1H16003-BS1) Prepared & Analyzed: 08/16/ E E-2 ug/g wet 5.01E Duplicate (1H16003-DUP1) Source: Prepared & Analyzed: 08/16/11 <2.02E E-1 ug/g dry ND 20 Post Spike (1H16003-PS1) Source: Prepared & Analyzed: 08/16/11 Batch 1I :5 Water Extract (Cr6) 5.08E-1 ug/ml 4.96E-1 ND Blank (1I26003-BLK1) Prepared & Analyzed: 09/26/11 <5.00E E-2 ug/g wet LCS (1I26003-BS1) Prepared & Analyzed: 09/26/ E E-2 ug/g wet 5.01E Duplicate (1I26003-DUP1) Source: Prepared & Analyzed: 09/26/11 <2.50E E-1 ug/g dry ND 20 Post Spike (1I26003-PS1) Source: Prepared & Analyzed: 09/26/ E-1 ug/ml 4.96E E Page 29 of 52
33 RCRA Metals By PNNL-AGG-415/1:1 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :1 Water Extract (ICP/ICPMS) Blank (1H22004-BLK1) Prepared & Analyzed: 08/22/11 <6.89E-3 <5.67E-3 <1.58E-2 <6.26E-3 <1.15E-3 <2.32E-3 <6.24E E E E E E E E-4 ug/g wet LCS (1H22004-BS1) Prepared & Analyzed: 08/22/ E0 5.10E0 4.94E0 4.84E0 4.87E0 4.98E0 5.11E0 3.44E E E E E E E-2 ug/g wet 4.99E E E E E E E Duplicate (1H22004-DUP1) Source: Prepared & Analyzed: 08/22/11 <6.88E E-2 <1.58E-2 <6.25E-3 <1.14E-3 <2.32E E E E E E E E E-4 ug/g dry ND E ND 35 ND 35 ND 35 ND E Post Spike (1H22004-PS1) Source: Prepared & Analyzed: 08/22/ E0 6.22E0 5.24E0 4.84E0 4.93E0 5.01E0 6.13E0 ug/l 5.00E0 1.15E E0 1.18E E0 ND E0 2.28E E0 4.77E E0 2.98E E0 1.06E Page 30 of 52
34 RCRA Metals By PNNL-AGG-415/1:1 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1I :1 Water Extract (ICP/ICPMS) Blank (1I26008-BLK1) Prepared & Analyzed: 09/26/11 <6.89E-3 <5.67E-3 <1.58E-2 <6.26E-3 <1.15E-3 <2.32E-3 <6.24E E E E E E E E-4 ug/g wet LCS (1I26008-BS1) Prepared & Analyzed: 09/26/ E0 4.66E0 5.01E0 4.88E0 4.75E0 4.92E0 5.01E0 3.44E E E E E E E-2 ug/g wet 4.99E E E E E E E Duplicate (1I26008-DUP1) Source: Prepared & Analyzed: 09/26/11 <6.89E-3 <5.67E-3 <1.58E-2 <6.25E-3 <1.15E-3 <2.32E E E E E E E E E-4 ug/g dry ND 35 ND 35 ND 35 ND 35 ND 35 ND E Post Spike (1I26008-PS1) Source: Prepared & Analyzed: 09/26/ E0 5.51E0 5.07E0 4.80E0 4.92E0 5.11E0 1.05E1 ug/l 5.00E0 2.55E E0 5.28E E0 ND E0 3.93E E0 1.68E E0 1.56E E0 5.42E Page 31 of 52
35 RCRA Metals By PNNL-AGG-415/1:2.5 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :2.5 Water Extract (ICP/ICPMS) Blank (1H22003-BLK1) Prepared & Analyzed: 08/22/11 <6.89E-3 <5.67E-3 <1.58E-2 <6.26E-3 <1.15E-3 <2.32E-3 <6.24E E E E E E E E-4 ug/g wet LCS (1H22003-BS1) Prepared & Analyzed: 08/22/ E0 4.80E0 5.02E0 4.75E0 4.69E0 4.95E0 5.15E0 3.44E E E E E E E-2 ug/g wet 4.99E E E E E E E Duplicate (1H22003-DUP1) Source: Prepared & Analyzed: 08/22/11 <1.78E E-2 <4.09E-2 <1.61E-2 <2.96E-3 <6.00E E E E E E E E E-3 ug/g dry ND E ND 35 ND 35 ND 35 ND E Post Spike (1H22003-PS1) Source: Prepared & Analyzed: 08/22/ E0 6.07E0 5.40E0 4.83E0 4.89E0 4.97E0 5.69E0 ug/l 5.00E0 4.97E E0 1.07E E0 8.66E E0 8.39E E0 4.09E E0 7.55E E0 6.38E Page 32 of 52
36 RCRA Metals By PNNL-AGG-415/1:2.5 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1I :2.5 Water Extract (ICP/ICPMS) Blank (1I26007-BLK1) Prepared & Analyzed: 09/26/11 <6.89E-3 <5.67E-3 <1.58E-2 <6.26E-3 <1.15E-3 <2.32E-3 <6.24E E E E E E E E-4 ug/g wet LCS (1I26007-BS1) Prepared & Analyzed: 09/26/ E0 4.63E0 4.95E0 4.74E0 4.69E0 4.90E0 5.07E0 3.44E E E E E E E-2 ug/g wet 4.99E E E E E E E Duplicate (1I26007-DUP1) Source: Prepared & Analyzed: 09/26/11 <1.72E E-2 <3.96E-2 <1.56E-2 <2.86E-3 <5.81E E E E E E E E E-3 ug/g dry ND E ND 35 ND 35 ND 35 ND E Post Spike (1I26007-PS1) Source: Prepared & Analyzed: 09/26/ E0 6.10E0 5.56E0 4.83E0 5.00E0 5.10E0 1.25E1 ug/l 5.00E0 1.39E E0 7.80E E0 ND E0 3.01E E0 1.03E E0 2.68E E0 7.48E Page 33 of 52
37 RCRA Metals By PNNL-AGG-415/1:5 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :5 Water Extract (ICP/ICPMS) Blank (1H22002-BLK1) Prepared: 08/22/11 Analyzed: 08/31/11 <6.89E-3 <5.67E-3 <1.58E-2 <6.26E-3 <1.15E-3 <2.32E-3 <6.24E E E E E E E E-4 ug/g wet LCS (1H22002-BS1) Prepared: 08/22/11 Analyzed: 08/31/ E0 4.69E0 4.92E0 4.67E0 4.81E0 4.85E0 5.08E0 3.44E E E E E E E-2 ug/g wet 4.99E E E E E E E Duplicate (1H22002-DUP1) Source: Prepared & Analyzed: 08/22/11 <2.79E E-2 <6.41E-2 <2.53E-2 <4.64E-3 <9.41E-3 <2.53E E E E E E E E-3 ug/g dry ND E ND 35 ND 35 ND 35 ND 35 ND 35 Post Spike (1H22002-PS1) Source: Prepared & Analyzed: 08/22/ E0 5.69E0 5.11E0 4.82E0 4.89E0 5.04E0 5.62E0 ug/l 5.00E0 3.20E E0 7.50E E0 ND E0 1.54E E0 6.32E E0 3.07E E0 4.65E Page 34 of 52
38 RCRA Metals By PNNL-AGG-415/1:5 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1I :5 Water Extract (ICP/ICPMS) Blank (1I26006-BLK1) Prepared & Analyzed: 09/26/11 <6.89E-3 <5.67E-3 <1.58E-2 <6.26E-3 <1.15E-3 <2.32E-3 <6.24E E E E E E E E-4 ug/g wet LCS (1I26006-BS1) Prepared & Analyzed: 09/26/ E0 4.62E0 4.74E0 4.89E0 4.78E0 4.95E0 5.28E0 3.44E E E E E E E-2 ug/g wet 5.00E E E E E E E Duplicate (1I26006-DUP1) Source: Prepared & Analyzed: 09/26/11 <3.44E E-2 <7.92E-2 <3.13E-2 <5.73E-3 <1.16E E E E E E E E E-3 ug/g dry ND E ND 35 ND 35 ND 35 ND E Post Spike (1I26006-PS1) Source: Prepared & Analyzed: 09/26/ E0 6.04E0 4.96E0 4.95E0 4.99E0 5.07E0 1.15E1 ug/l 5.00E0 1.16E E0 1.08E E0 3.04E E0 4.05E E0 6.83E E0 4.82E E0 6.49E Page 35 of 52
39 RCRA Metals By PNNL-AGG-415/Acid Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H ASTM D 5198 (ICP/ICPMS) Blank (1H22005-BLK1) Prepared & Analyzed: 08/22/11 <1.88E-1 <8.20E-2 <1.59E-1 <5.13E-3 <1.35E-2 <5.13E-2 <6.24E E E E E E E E-3 ug/g wet LCS (1H22005-BS1) Prepared & Analyzed: 08/22/ E0 5.79E0 6.10E0 5.65E0 5.84E0 6.05E0 6.13E0 9.42E E E E E E E-2 ug/g wet 5.90E E E E E E E Duplicate (1H22005-DUP1) Source: Prepared & Analyzed: 08/22/ E1 2.43E0 <6.44E E-2 <5.50E E0 2.84E1 7.65E E E E E E E-2 ug/g dry 9.05E E ND E ND E E Post Spike (1H22005-PS1) Source: Prepared: 08/22/11 Analyzed: 08/23/ E1 1.00E1 5.04E0 4.32E0 5.01E0 2.09E1 4.25E1 ug/l 5.00E0 2.86E E0 4.97E E0 2.53E E0 7.49E E0 5.55E E0 1.70E E0 3.83E Page 36 of 52
40 RCRA Metals By PNNL-AGG-415/Acid Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1I ASTM D 5198 (ICP/ICPMS) Blank (1I26009-BLK1) Prepared: 09/26/11 Analyzed: 09/27/11 <1.88E-1 <8.20E-2 <1.59E-1 <5.13E-3 <1.35E-2 <5.13E-2 <3.12E E E E E E E E-2 ug/g wet LCS (1I26009-BS1) Prepared: 09/26/11 Analyzed: 09/27/ E0 5.67E0 5.99E0 5.68E0 5.74E0 5.98E0 6.21E0 9.42E E E E E E E-2 ug/g wet 5.73E E E E E E E Duplicate (1I26009-DUP1) Source: Prepared: 09/26/11 Analyzed: 09/27/ E1 4.68E0 <6.82E E E E0 1.72E2 8.10E E E E E E E-1 ug/g dry 1.35E E ND E E E E Post Spike (1I26009-PS1) Source: Prepared: 09/26/11 Analyzed: 09/27/ E1 1.30E1 5.15E0 4.95E0 5.39E0 1.87E1 1.21E2 ug/l 5.00E0 3.05E E0 8.51E E0 6.14E E0 1.51E E0 5.07E E0 1.46E E0 1.14E Page 37 of 52
41 Strontium 90/Acid Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H ASTM D 5198 (RadChem) Blank (1H26006-BLK1) Prepared: 08/26/11 Analyzed: 09/06/11 <1.69E E-1 pci/g wet LCS (1H26006-BS1) Prepared: 08/26/11 Analyzed: 09/06/ E1 1.69E-1 pci/g wet 6.02E Duplicate (1H26006-DUP1) Source: Prepared: 08/26/11 Analyzed: 09/06/11 <5.80E E-1 pci/g dry ND 35 Matrix Spike (1H26006-MS1) Source: Prepared: 08/26/11 Analyzed: 09/06/11 Batch 1I ASTM D 5198 (RadChem) 6.16E1 1.69E-1 pci/g dry 6.50E1 ND Blank (1I23004-BLK1) Prepared: 09/23/11 Analyzed: 09/28/11 <1.93E E-1 pci/g wet LCS (1I23004-BS1) Prepared: 09/23/11 Analyzed: 09/28/ E1 1.93E-1 pci/g wet 8.04E Duplicate (1I23004-DUP1) Source: Prepared: 09/23/11 Analyzed: 09/28/11 <6.69E E-1 pci/g dry ND 35 Matrix Spike (1I23004-MS1) Source: Prepared: 09/23/11 Analyzed: 09/28/ E1 1.93E-1 pci/g dry 8.04E1 ND Page 38 of 52
42 Strontium 90/1:1 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :1 Water Extract (RadChem) Blank (1H26003-BLK1) Prepared: 08/26/11 Analyzed: 09/06/11 <5.90E E-1 pci/g wet LCS (1H26003-BS1) Prepared: 08/26/11 Analyzed: 09/06/ E1 5.90E-1 pci/g wet 6.02E Duplicate (1H26003-DUP1) Source: Prepared: 08/26/11 Analyzed: 09/06/11 <5.90E E-1 pci/g dry ND 35 Matrix Spike (1H26003-MS1) Source: Prepared: 08/26/11 Analyzed: 09/06/ E1 Batch 1I :1 Water Extract (RadChem) 8.03E-1 pci/g dry 6.50E1 ND Blank (1I23001-BLK1) Prepared: 09/23/11 Analyzed: 09/28/11 <6.76E E-1 pci/g wet LCS (1I23001-BS1) Prepared: 09/23/11 Analyzed: 09/28/ E1 6.76E-1 pci/g wet 8.04E Duplicate (1I23001-DUP1) Source: Prepared: 09/23/11 Analyzed: 09/28/11 <6.76E E-1 pci/g dry ND 35 Matrix Spike (1I23001-MS1) Source: Prepared: 09/23/11 Analyzed: 09/28/ E1 1.00E0 pci/g dry 8.04E1 ND Page 39 of 52
43 Strontium 90/1:2.5 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :2.5 Water Extract (RadChem) Blank (1H26004-BLK1) Prepared: 08/26/11 Analyzed: 09/06/11 <5.90E E-1 pci/g wet LCS (1H26004-BS1) Prepared: 08/26/11 Analyzed: 09/06/ E1 5.90E-1 pci/g wet 6.02E Duplicate (1H26004-DUP1) Source: Prepared: 08/26/11 Analyzed: 09/06/11 <1.52E0 1.52E0 pci/g dry ND 35 Matrix Spike (1H26004-MS1) Source: Prepared: 08/26/11 Analyzed: 09/06/ E1 Batch 1I :2.5 Water Extract (RadChem) 8.03E-1 pci/g dry 6.50E1 ND Blank (1I23002-BLK1) Prepared: 09/23/11 Analyzed: 09/28/11 <6.76E E-1 pci/g wet LCS (1I23002-BS1) Prepared: 09/23/11 Analyzed: 09/28/ E1 6.76E-1 pci/g wet 8.04E Duplicate (1I23002-DUP1) Source: Prepared: 09/23/11 Analyzed: 09/28/11 <1.69E0 1.69E0 pci/g dry ND 35 Matrix Spike (1I23002-MS1) Source: Prepared: 09/23/11 Analyzed: 09/28/ E1 1.00E0 pci/g dry 8.04E1 ND Page 40 of 52
44 Strontium 90/1:5 Water Extract - Quality Control Environmental Science Laboratory Analyte Reporting Units Spike Level Source s Notes Batch 1H :5 Water Extract (RadChem) Blank (1H26005-BLK1) Prepared: 08/26/11 Analyzed: 09/06/11 <5.90E E-1 pci/g wet LCS (1H26005-BS1) Prepared: 08/26/11 Analyzed: 09/06/ E1 5.90E-1 pci/g wet 6.02E Duplicate (1H26005-DUP1) Source: Prepared: 08/26/11 Analyzed: 09/06/11 <2.39E0 2.39E0 pci/g dry ND 35 Matrix Spike (1H26005-MS1) Source: Prepared: 08/26/11 Analyzed: 09/06/ E1 Batch 1I :5 Water Extract (RadChem) 8.03E-1 pci/g dry 6.50E1 ND Blank (1I23003-BLK1) Prepared: 09/23/11 Analyzed: 09/28/11 <6.76E E-1 pci/g wet LCS (1I23003-BS1) Prepared: 09/23/11 Analyzed: 09/28/ E1 6.76E-1 pci/g wet 8.04E Duplicate (1I23003-DUP1) Source: Prepared: 09/23/11 Analyzed: 09/28/11 <3.38E0 3.38E0 pci/g dry ND 35 Matrix Spike (1I23003-MS1) Source: Prepared: 09/23/11 Analyzed: 09/28/ E1 1.00E0 pci/g dry 8.04E1 ND Page 41 of 52
45 Strontium 90 - Quality Control ASTM D 5198 (RadChem) Sample ID HEIS ID Tracer Recovery B2C4B3 94.1% B2C4B4 92.3% B2C4B5 93.7% B2D4K4 92.2% B2D1X0 92.7% B2D1X1 94.6% B2C4W2 95.1% B2C4W3 94.3% B2C % B2C % Strontium 90 - Quality Control 1:1 Water Extract (RadChem) Sample ID HEIS ID Tracer Recovery B2C4B3 91.2% B2C4B4 91.2% B2C4B5 89.7% B2D4K4 90.6% B2D1X0 92.0% B2D1X1 91.9% B2C4W2 90.7% B2C4W3 92.6% B2C % B2C % Strontium 90 - Quality Control 1:2.5 Water Extract (RadChem) Sample ID HEIS ID Tracer Recovery B2C4B3 93.4% B2C4B4 93.2% B2C4B5 95.6% B2D4K4 91.6% B2D1X0 93.8% B2D1X1 92.2% B2C4W2 93.5% B2C4W3 92.4% B2C % B2C % Strontium 90 - Quality Control 1:5 Water Extract (RadChem) Sample ID HEIS ID Tracer Recovery B2C4B3 90.6% B2C4B4 93.8% B2C4B5 92.1% B2D4K4 90.5% B2D1X0 92.1% B2D1X1 91.0% B2C4W2 93.0% B2C4W3 89.8% B2C % B2C % Page 42 of 52
46 ~~--~ ~--~---~ CH2MHill Plateau Remediation Company COMPANY CONTACT RADLOFF,AW ----~---~ CHAIN OF CUSTODY /SAMPLE ANALYSIS REQUEST ,-TELEPHONE NO.--- ~OJECT COORDINATOR - ~~~~ - ~ ~- l --- RADLOFF, AW ~-- ~ PROJECT DESIGNATION Area Remedial Investigation/Feasibility Analysis NR-2 - Sediment SAF NO. ---~---- F F1~ S-- ~ II PAGE 1 OF 1 ~-- --~~~-~ -- ~ j AIR QUALITY ' ICE CHEST NO. I FIELD LOGBOOK NO. ~CTUAL SAMPLE DEPTH -. COA I M. ETHOD OF SHIPMENT SH D DATA TURNAROUND 30 Days /30 Days ORIGINAL I ;J {It_ }-1}1~-N-Ljf{,-) PlsJ?lbj '-1'1-7~ 5J.-3 Pf ES10 _l~overn~.ntvehicle ' SHIPPED TO OFFSITE PROPERTY NO. BILL OF LADING/ AIR BILL NO. J Environmental Sciences Laboratory MATRIX* A=Air DL=Drum Liquids DS=Drum Solids L=Liquid O=Oil S=Soil SE=Sediment T=Tissue V=Vegetation W=Water Wl=Wipe X=Other POSSIBLE SAMPLE HAZARDS/ REMARKS Contains Radioactive Material at concentrations that may or may not be regulated for transportation per 49 CFR 1 lata Dangerous Goods Regulations but are not releasable per DOE Order (1990/1993) SPECIAL HANDLING AND/OR STORAGE PRESERVATION HOLDING TIME TYPE OF CONTAINER NO. OF CONTAINER(S) VOLUME G/P ll SAMPLE NO. MATRIX* B2C4B3 SOIL!J-.31- J CHAIN OF POSSESSION I-~-~...!.: _!_?... ~- ~ ~~!. 't DAn/TIME J).lfO SIGN/ PRINT NAMES RECEIVED BY /STORED IN () '1 /3.5!?' f. 3-3)-1/ RECEIVED BY/STORED in ~. ~ ,.,, c:rv v lma I,J\.\ -hhv\a.1. ~ 1./~7: 11. t:l-q;j~-.,. D,..,.,- 1 SPECIAL INSTRUCTIONS ** The 100 Area S&GRP Characterization and Monitoring Sampling and Analysis GKI applies to this SAF.D (2 () l1 -~~- 1 3 s-6 cr RELINQUISHED BY /REII!OVED FROM DAn/TIME RECEIVED BY /STORED IN RELINQUISHED BY/REMOVED FROM DAn/TIME RECEIVED BY /STORED IN RELINQUISHED BY/REMOVED FROM DAn/TIME RECEIVED BY /STORED IN LABORATORY SECTION FINAL SAMPLE DISPOSMON PRINTED ON 3/10/2011 RECEIVED BY DISPOSAL METHOD Page 43 of 52 SDG-# tslcjgou!3 TITLE DAn/TIME DISPOSED BY DAn/TIME - I A (REV 2)
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