|
|
|
- Teresa Perkins
- 7 years ago
- Views:
Transcription
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47 ANALYTICAL SUMMARY REPORT July 06, Irene St Helena, MT Workorder No.: H Project Name: Beal Mtn Quote ID: H634 - Beal 2011 Site Wide Monitoring Energy Laboratories Inc Helena MT received the following 3 samples for on 6/17/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test H SBB /16/11 12:15 06/17/11 Aqueous Metals by ICP/ICPMS, Tot. Rec. Cyanide, Free Cyanide, Total Manual Distillation Total Cyanide Digestion Cyanide, Weak Acid Dissociable WAD Cyanide Distillation Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite Metals Digestion by EPA Preparation for TDS Solids, Total Dissolved H SBB /16/11 16:35 06/17/11 Aqueous Metals by ICP/ICPMS, Dissolved Alkalinity Conductivity Hardness as CaCO3 Anions by Ion Chromatography ph H WRMW-1 06/16/11 13:50 06/17/11 Aqueous Same As Above This report was prepared by Energy Laboratories, Inc., 3161 E. Lyndale Ave., Helena, MT Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: Page 1 of 27
48 CLIENT: Project: Beal Mtn Report Date: 07/06/11 Sample Delivery Group: H CASE NARRATIVE Tests associated with analyst identified as ELI-B were subcontracted to Energy Laboratories, 1120 S. 27th St., Billings, MT, EPA Number MT Page 2 of 27
49 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SBB Report Date: 07/06/11 Collection Date: 06/16/11 12:15 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Dissolved 180 C A2540 C 06/20/11 15:05 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable D Kelada mod A4500-CN-F D2036C 06/28/11 14:30 / eli-b 06/29/11 17:02 / eli-b 06/28/11 12:33 / eli-b NUTRIENTS Nitrogen, Ammonia as N 0.1 E350.1 Nitrogen, Nitrate+Nitrite as N E353.2 METALS, TOTAL RECOVERABLE Copper Selenium /22/11 12:44 / reh 06/20/11 11:24 / reh 06/23/11 19:01 / dck 06/23/11 19:01 / dck Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. Page 3 of 27
50 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SBB Report Date: 07/06/11 Collection Date: 06/16/11 16:35 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES ph Conductivity s.u. umhos/cm A4500-H B A2510 B 06/17/11 23:25 / zeg 06/17/11 16:06 / cmm INORGANICS Alkalinity, Total as CaCO A2320 B Sulfate 840 D 5 E300.0 Hardness as CaCO A2340 B METALS, DISSOLVED Arsenic Barium 0.1 Cadmium Calcium Chromium 0.01 Lead 0.01 Magnesium 22 1 Mercury Selenium Silver 06/17/11 23:25 / zeg 06/30/11 15:31 / zeg 06/29/11 15:39 / abb 06/23/11 19:05 / dck 06/23/11 19:05 / dck 06/23/11 19:05 / dck 06/23/11 19:05 / dck 06/23/11 19:05 / dck 06/23/11 19:05 / dck 06/23/11 19:05 / dck 06/23/11 19:05 / dck 06/23/11 19:05 / dck 06/23/11 19:05 / dck Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. Page 4 of 27
51 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID WRMW-1 Report Date: 07/06/11 Collection Date: 06/16/11 13:50 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES ph Conductivity s.u. umhos/cm A4500-H B A2510 B 06/17/11 23:32 / zeg 06/17/11 16:07 / cmm INORGANICS Alkalinity, Total as CaCO A2320 B Sulfate 950 D 5 E300.0 Hardness as CaCO A2340 B METALS, DISSOLVED Arsenic Barium 0.1 Cadmium Calcium Chromium 0.01 Lead 0.01 Magnesium 25 1 Mercury Selenium Silver 06/17/11 23:32 / zeg 06/30/11 15:42 / zeg 06/29/11 15:39 / abb 06/23/11 19:28 / dck 06/23/11 19:28 / dck 06/23/11 19:28 / dck 06/29/11 18:44 / dck 06/23/11 19:28 / dck 06/23/11 19:28 / dck 06/23/11 19:28 / dck 06/23/11 19:28 / dck 06/23/11 19:28 / dck 06/23/11 19:28 / dck Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. Page 5 of 27
52 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: A2320 B Batch: R71942 Sample ID: MBLK Method Blank Run: MAN-TECH_110617D 06/17/11 16:38 Alkalinity, Total as CaCO Sample ID: LCS Laboratory Control Sample Run: MAN-TECH_110617D 06/17/11 16:46 Alkalinity, Total as CaCO Sample ID: H AMS Sample Matrix Spike Run: MAN-TECH_110617D 06/17/11 23:04 Alkalinity, Total as CaCO S Sample ID: H ADUP Sample Duplicate Run: MAN-TECH_110617D 06/17/11 23:18 Alkalinity, Total as CaCO Qualifiers: S - Spike recovery outside of advisory limits. Page 6 of 27
53 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: A2510 B Analytical Run: CO_110617A Sample ID: ICV1_110617A Initial Calibration Verification Standard 06/17/11 10:00 Conductivity 1000 umhos/cm Sample ID: CCV7_110617A Continuing Calibration Verification Standard 06/17/11 15:09 Conductivity 1410 umhos/cm Method: A2510 B Batch: A-CO-PROBE-W Sample ID: MBLK1_110617A Method Blank Run: CO_110617A 06/17/11 10:00 Conductivity 2 umhos/cm Sample ID: H ADUP Sample Duplicate Run: CO_110617A 06/17/11 10:20 Conductivity 284 umhos/cm Sample ID: H ADUP Sample Duplicate Run: CO_110617A 06/17/11 10:27 Conductivity 1.21 umhos/cm Qualifiers: Page 7 of 27
54 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: A2540 C Batch: Sample ID: MB Method Blank Run: ACCU-124 ( )_ /20/11 15:05 Solids, Total Dissolved 180 C Sample ID: LCS Laboratory Control Sample Run: ACCU-124 ( )_ /20/11 15:05 Solids, Total Dissolved 180 C Sample ID: H ADUP Sample Duplicate Run: ACCU-124 ( )_ /20/11 15:06 Solids, Total Dissolved 180 C Sample ID: H BMS Sample Matrix Spike Run: ACCU-124 ( )_ /20/11 15:06 Solids, Total Dissolved 180 C Sample ID: H BDUP Sample Duplicate Run: ACCU-124 ( )_ /20/11 15:12 Solids, Total Dissolved 180 C Qualifiers: Page 8 of 27
55 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: A4500-H B Analytical Run: MAN-TECH_110617D Sample ID: CCV Continuing Calibration Verification Standard 06/17/11 16:19 ph 3.92 s.u Sample ID: CCV Continuing Calibration Verification Standard 06/17/11 16:25 ph 9.98 s.u Sample ID: ICV-1942 Initial Calibration Verification Standard 06/17/11 16:28 ph 6.96 s.u Sample ID: CCV-1943 Continuing Calibration Verification Standard 06/17/11 22:33 ph 6.98 s.u Method: A4500-H B Batch: R71942 Sample ID: H ADUP Sample Duplicate Run: MAN-TECH_110617D 06/17/11 19:25 ph 5.43 s.u R Sample ID: H ADUP Sample Duplicate Run: MAN-TECH_110617D 06/17/11 20:57 ph 8.05 s.u Sample ID: H ADUP Sample Duplicate Run: MAN-TECH_110617D 06/17/11 22:00 ph 8.25 s.u Qualifiers: R - RPD exceeds advisory limit. Page 9 of 27
56 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: D2036C Batch: B_54987 Sample ID: B EMSD Sample Matrix Spike Duplicate Run: SUB-B /28/11 12:00 Cyanide, Weak Acid Dissociable Sample ID: B EMS Sample Matrix Spike Run: SUB-B /28/11 11:58 Cyanide, Weak Acid Dissociable Sample ID: MB Method Blank Run: SUB-B /28/11 11:51 Cyanide, Weak Acid Dissociable Sample ID: LCS Laboratory Control Sample Run: SUB-B /28/11 11:47 Cyanide, Weak Acid Dissociable Qualifiers: Page 10 of 27
57 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Analytical Run: ICPMS204-B_110622A Sample ID: ICV STD 11 Initial Calibration Verification Standard 06/22/11 23:20 Arsenic Barium Cadmium Calcium Chromium Copper Lead Magnesium Mercury Selenium Silver Sample ID: ICSA 11 Interference Check Sample A 06/22/11 23:25 Arsenic Barium Cadmium Calcium Chromium Copper Lead Magnesium Mercury 4.90E Selenium Silver Sample ID: ICSAB 11 Interference Check Sample AB 06/22/11 23:29 Arsenic Barium Cadmium Calcium Chromium Copper Lead 8.00E Magnesium Mercury 3.10E Selenium Silver Sample ID: ICV STD 11 Initial Calibration Verification Standard 06/23/11 05:52 Arsenic Barium Cadmium Calcium Chromium Copper Qualifiers: Page 11 of 27
58 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Analytical Run: ICPMS204-B_110622A Sample ID: ICV STD 11 Initial Calibration Verification Standard 06/23/11 05:52 Lead Magnesium Mercury Selenium Silver Sample ID: ICSA 11 Interference Check Sample A 06/23/11 05:57 Arsenic Barium Cadmium Calcium Chromium Copper Lead Magnesium Mercury 5.40E Selenium Silver Sample ID: ICSAB 11 Interference Check Sample AB 06/23/11 06:01 Arsenic Barium Cadmium Calcium Chromium Copper Lead 6.90E Magnesium Mercury 2.70E Selenium Silver Sample ID: ICV STD 11 Initial Calibration Verification Standard 06/23/11 15:57 Arsenic Barium Cadmium Calcium Chromium Copper Lead Magnesium Mercury Selenium Silver Qualifiers: Page 12 of 27
59 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Analytical Run: ICPMS204-B_110622A Sample ID: ICSA 11 Interference Check Sample A 06/23/11 16:01 Arsenic Barium Cadmium Calcium Chromium Copper Lead 9.20E Magnesium Mercury 5.70E Selenium Silver Sample ID: ICSAB 11 Interference Check Sample AB 06/23/11 16:06 Arsenic Barium Cadmium Calcium Chromium Copper Lead 6.90E Magnesium Mercury 1.80E Selenium Silver Sample ID: ICV STD 11 Initial Calibration Verification Standard 06/24/11 06:10 Arsenic Barium Cadmium Calcium Chromium Copper Lead Magnesium Mercury Selenium Silver Sample ID: ICSA 11 Interference Check Sample A 06/24/11 06:14 Arsenic Barium Cadmium Calcium Chromium Copper Qualifiers: Page 13 of 27
60 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Analytical Run: ICPMS204-B_110622A Sample ID: ICSA 11 Interference Check Sample A 06/24/11 06:14 Lead 9.40E Magnesium Mercury 3.90E Selenium Silver Sample ID: ICSAB 11 Interference Check Sample AB 06/24/11 06:19 Arsenic Barium Cadmium Calcium Chromium Copper Lead 6.40E Magnesium Mercury 2.60E Selenium Silver Sample ID: ICV STD 11 Initial Calibration Verification Standard 06/24/11 12:34 Arsenic Barium Cadmium Calcium Chromium Copper Lead Magnesium Mercury Selenium Silver Sample ID: ICSA 11 Interference Check Sample A 06/24/11 12:41 Arsenic Barium Cadmium Calcium Chromium Copper Lead 8.20E Magnesium Mercury 4.60E Selenium Silver Qualifiers: Page 14 of 27
61 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Analytical Run: ICPMS204-B_110622A Sample ID: ICSAB 11 Interference Check Sample AB 06/24/11 12:46 Arsenic Barium Cadmium Calcium Chromium Copper Lead 6.30E Magnesium Mercury 2.60E Selenium Silver Sample ID: ICV STD 11 Initial Calibration Verification Standard 06/25/11 01:24 Arsenic Barium Cadmium Calcium Chromium Copper Lead Magnesium Mercury Selenium Silver Sample ID: ICSA 11 Interference Check Sample A 06/25/11 01:29 Arsenic Barium 9.10E Cadmium Calcium Chromium Copper Lead 8.40E Magnesium Mercury 4.80E Selenium Silver Sample ID: ICSAB 11 Interference Check Sample AB 06/25/11 01:34 Arsenic Barium 9.00E Cadmium Calcium Chromium Copper Qualifiers: Page 15 of 27
62 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Analytical Run: ICPMS204-B_110622A Sample ID: ICSAB 11 Interference Check Sample AB 06/25/11 01:34 Lead 6.50E Magnesium Mercury 2.10E Selenium Silver Method: Batch: R72108 Sample ID: ICB 11 Method Blank Run: ICPMS204-B_110622A 06/23/11 06:28 Arsenic 3E-05 Barium 3E-05 Cadmium 1E-05 Calcium Chromium 6E-05 Copper 3E-05 Lead 1.0E-05 Magnesium Mercury 9E-06 Selenium 4E-05 Silver 9E-05 3E-05 Sample ID: LFB 11 Laboratory Fortified Blank Run: ICPMS204-B_110622A 06/23/11 06:33 Arsenic Barium Cadmium Calcium Chromium Copper Lead Magnesium Mercury Selenium Silver Sample ID: H BMS 11 Sample Matrix Spike Run: ICPMS204-B_110622A 06/23/11 18:43 Arsenic Barium Cadmium Calcium S Chromium Copper Lead Magnesium A Mercury Selenium Silver Qualifiers: A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. S - Spike recovery outside of advisory limits. Page 16 of 27
63 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Batch: R72108 Sample ID: H BMS 11 Sample Matrix Spike Run: ICPMS204-B_110622A 06/23/11 18:43 Sample ID: H BMSD 11 Sample Matrix Spike Duplicate Run: ICPMS204-B_110622A 06/23/11 18:47 Arsenic Barium Cadmium Calcium S Chromium Copper Lead Magnesium A Mercury Selenium Silver Qualifiers: A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. S - Spike recovery outside of advisory limits. Page 17 of 27
64 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Analytical Run: ICPMS204-B_110628A Sample ID: ICV STD Initial Calibration Verification Standard 06/28/11 11:13 Calcium Sample ID: ICSA Interference Check Sample A 06/28/11 11:17 Calcium Sample ID: ICSAB Interference Check Sample AB 06/28/11 11:22 Calcium Sample ID: ICV STD Initial Calibration Verification Standard 06/29/11 00:24 Calcium Sample ID: ICSA Interference Check Sample A 06/29/11 00:28 Calcium Sample ID: ICSAB Interference Check Sample AB 06/29/11 00:33 Calcium Sample ID: ICSA Interference Check Sample A 06/29/11 11:39 Calcium Sample ID: ICSAB Interference Check Sample AB 06/29/11 11:44 Calcium Sample ID: ICV STD Initial Calibration Verification Standard 06/29/11 20:39 Calcium Sample ID: ICSA Interference Check Sample A 06/29/11 20:44 Calcium Sample ID: ICSAB Interference Check Sample AB 06/29/11 20:48 Calcium Method: Batch: R72226 Sample ID: ICB Method Blank Run: ICPMS204-B_110628A 06/28/11 12:07 Calcium Sample ID: LFB Laboratory Fortified Blank Run: ICPMS204-B_110628A 06/28/11 12:12 Calcium Sample ID: LFB Laboratory Fortified Blank Run: ICPMS204-B_110628A 06/28/11 14:28 Calcium mg/kg Sample ID: LFB Laboratory Fortified Blank Run: ICPMS204-B_110628A 06/28/11 20:10 Calcium mg/kg Sample ID: H CMS Sample Matrix Spike Run: ICPMS204-B_110628A 06/29/11 17:19 Calcium Sample ID: H CMSD Sample Matrix Spike Duplicate Run: ICPMS204-B_110628A 06/29/11 17:26 Calcium Qualifiers: Page 18 of 27
65 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Batch: R72226 Sample ID: H CMSD Sample Matrix Spike Duplicate Run: ICPMS204-B_110628A 06/29/11 17:26 Qualifiers: Page 19 of 27
66 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E300.0 Analytical Run: IC102-H_110630A Sample ID: ICV Initial Calibration Verification Standard 06/30/11 13:35 Sulfate Sample ID: CCV Continuing Calibration Verification Standard 06/30/11 14:10 Sulfate Method: E300.0 Batch: R72324 Sample ID: ICB Method Blank Run: IC102-H_110630A 06/30/11 13:46 Sulfate 0.02 Sample ID: LFB Laboratory Fortified Blank Run: IC102-H_110630A 06/30/11 13:58 Sulfate Sample ID: H AMS Sample Matrix Spike Run: IC102-H_110630A 06/30/11 16:17 Sulfate S Sample ID: H AMSD Sample Matrix Spike Duplicate Run: IC102-H_110630A 06/30/11 16:29 Sulfate S Qualifiers: S - Spike recovery outside of advisory limits. Page 20 of 27
67 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E350.1 Analytical Run: FIA203-HE_110622A Sample ID: ICV Initial Calibration Verification Standard 06/22/11 11:31 Nitrogen, Ammonia as N Sample ID: ICB Initial Calibration Blank, Instrument Blank 06/22/11 11:36 Nitrogen, Ammonia as N Method: E350.1 Batch: R72064 Sample ID: LCS Laboratory Control Sample Run: FIA203-HE_110622A 06/22/11 11:32 Nitrogen, Ammonia as N Sample ID: LFB Laboratory Fortified Blank Run: FIA203-HE_110622A 06/22/11 11:33 Nitrogen, Ammonia as N Sample ID: MBLK Method Blank Run: FIA203-HE_110622A 06/22/11 11:54 Nitrogen, Ammonia as N Sample ID: H CMS Sample Matrix Spike Run: FIA203-HE_110622A 06/22/11 12:49 Nitrogen, Ammonia as N Sample ID: H CMSD Sample Matrix Spike Duplicate Run: FIA203-HE_110622A 06/22/11 12:50 Nitrogen, Ammonia as N Qualifiers: Page 21 of 27
68 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E353.2 Analytical Run: NUTRIENTS_110620A Sample ID: ICV-1 Initial Calibration Verification Standard 06/20/11 10:08 Nitrogen, Nitrate+Nitrite as N Sample ID: ICB Initial Calibration Blank, Instrument Blank 06/20/11 10:15 Nitrogen, Nitrate+Nitrite as N Sample ID: CCV-33 Continuing Calibration Verification Standard 06/20/11 11:12 Nitrogen, Nitrate+Nitrite as N Method: E353.2 Batch: A _5_NO3_01 Sample ID: LCS-2 Laboratory Control Sample Run: NUTRIENTS_110620A 06/20/11 10:10 Nitrogen, Nitrate+Nitrite as N Sample ID: LFB-3 Laboratory Fortified Blank Run: NUTRIENTS_110620A 06/20/11 10:12 Nitrogen, Nitrate+Nitrite as N Sample ID: MBLK-7 Method Blank Run: NUTRIENTS_110620A 06/20/11 10:19 Nitrogen, Nitrate+Nitrite as N Sample ID: H DMS Sample Matrix Spike Run: NUTRIENTS_110620A 06/20/11 11:18 Nitrogen, Nitrate+Nitrite as N Sample ID: H DMSD Sample Matrix Spike Duplicate Run: NUTRIENTS_110620A 06/20/11 11:20 Nitrogen, Nitrate+Nitrite as N Qualifiers: Page 22 of 27
69 QA/QC Summary Report Project: Beal Mtn Report Date: 07/06/11 Work Order: H Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Kelada mod Analytical Run: SUB-B Sample ID: ICV-1 Initial Calibration Verification Standard 06/28/11 11:35 Cyanide, Total Method: Kelada mod Batch: B_55001 Sample ID: H D Sample Matrix Spike Duplicate Run: SUB-B /28/11 14:26 Cyanide, Total Sample ID: LCS Laboratory Control Sample Run: SUB-B /28/11 11:49 Cyanide, Total Sample ID: MB Method Blank Run: SUB-B /28/11 11:53 Cyanide, Total Sample ID: H D Sample Matrix Spike Run: SUB-B /28/11 14:24 Cyanide, Total Qualifiers: Page 23 of 27
70 Workorder Receipt Checklist H Login completed by: Reviewed by: Reviewed Date: Tracy L. Lorash BL2000\ablackburn 6/21/2011 Date Received: 6/17/2011 Received by: TLL Carrier name: Hand Del Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature: 4.8 C Water - VOA vials have zero headspace? Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No Not Applicable Contact and Corrective Action Comments: None Page 24 of 27
71 Page 25 of 27
72 Page 26 of 27
73 Page 27 of 27
74 ANALYTICAL SUMMARY REPORT July 07, Irene St Helena, MT Workorder No.: H Project Name: Beal Mtn Quote ID: H634 - Beal 2011 Site Wide Monitoring Energy Laboratories Inc Helena MT received the following 20 samples for on 6/17/2011 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test H SPR-Roadfill 06/15/11 8:15 06/17/11 Aqueous Metals by ICP/ICPMS, Tot. Rec. Cyanide, Free Cyanide, Total Manual Distillation Total Cyanide Digestion Cyanide, Weak Acid Dissociable WAD Cyanide Distillation Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite Metals Digestion by EPA Preparation for TSS Solids, Total Suspended H SPR-3 06/15/11 9:00 06/17/11 Aqueous Same As Above H SPR-D4 06/15/11 10:55 06/17/11 Aqueous Same As Above H SPR-18 06/15/11 11:30 06/17/11 Aqueous Same As Above H SPR-D2 06/15/11 12:15 06/17/11 Aqueous Same As Above H SPR-2 06/15/11 13:10 06/17/11 Aqueous Same As Above H SPR-19 06/15/11 13:45 06/17/11 Aqueous Same As Above H SPR-5 06/15/11 14:45 06/17/11 Aqueous Metals by ICP/ICPMS, Tot. Rec. Alkalinity Cyanide, Free Cyanide, Total Manual Distillation Total Cyanide Digestion Cyanide, Weak Acid Dissociable WAD Cyanide Distillation Conductivity Anions by Ion Chromatography Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite Metals Digestion by EPA Preparation for TSS Solids, Total Suspended H STA-4 06/15/11 15:00 06/17/11 Aqueous Metals by ICP/ICPMS, Tot. Rec. Cyanide, Free Cyanide, Total Manual Distillation Total Cyanide Digestion Cyanide, Weak Acid Dissociable WAD Cyanide Distillation Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite Metals Digestion by EPA Preparation for TSS Solids, Total Suspended Page 1 of 38
75 ANALYTICAL SUMMARY REPORT H SPR-10A 06/15/11 15:45 06/17/11 Aqueous Metals by ICP/ICPMS, Tot. Rec. Alkalinity Cyanide, Free Cyanide, Total Manual Distillation Total Cyanide Digestion Cyanide, Weak Acid Dissociable WAD Cyanide Distillation Conductivity Anions by Ion Chromatography Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite Metals Digestion by EPA Preparation for TSS Solids, Total Suspended H MB-Drain 06/15/11 16:10 06/17/11 Aqueous Same As Above H SPR-T 06/15/11 17:15 06/17/11 Aqueous Metals by ICP/ICPMS, Tot. Rec. Cyanide, Free Cyanide, Total Manual Distillation Total Cyanide Digestion Cyanide, Weak Acid Dissociable WAD Cyanide Distillation Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite Metals Digestion by EPA Preparation for TSS Solids, Total Suspended H STA-3A 06/15/11 17:40 06/17/11 Aqueous Same As Above H MINN-DN 06/16/11 10:25 06/17/11 Aqueous Same As Above H STA-2 06/16/11 14:30 06/17/11 Aqueous Same As Above H Toe Drain 06/16/11 16:50 06/17/11 Aqueous Metals by ICP/ICPMS, Tot. Rec. Alkalinity Cyanide, Free Cyanide, Total Manual Distillation Total Cyanide Digestion Cyanide, Weak Acid Dissociable WAD Cyanide Distillation Conductivity Anions by Ion Chromatography Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite Metals Digestion by EPA Preparation for TSS Solids, Total Suspended H BCD-A 06/16/11 18:05 06/17/11 Aqueous Metals by ICP/ICPMS, Tot. Rec. Cyanide, Free Cyanide, Total Manual Distillation Total Cyanide Digestion Cyanide, Weak Acid Dissociable WAD Cyanide Distillation Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite Metals Digestion by EPA Preparation for TSS Solids, Total Suspended H STA-1 06/16/11 19:00 06/17/11 Aqueous Same As Above H BS-D 06/16/11 19:45 06/17/11 Aqueous Same As Above H DUP-1 06/16/11 6:00 06/17/11 Aqueous Same As Above Page 2 of 38
76 ANALYTICAL SUMMARY REPORT This report was prepared by Energy Laboratories, Inc., 3161 E. Lyndale Ave., Helena, MT Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: Page 3 of 38
77 CLIENT: Project: Beal Mtn Report Date: 07/07/11 Sample Delivery Group: H CASE NARRATIVE Tests associated with analyst identified as ELI-B were subcontracted to Energy Laboratories, 1120 S. 27th St., Billings, MT, EPA Number MT Page 4 of 38
78 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-Roadfill Report Date: 07/07/11 Collection Date: 06/15/11 08:15 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 8 5 A2540 D 06/20/11 11:54 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 14:03 / eli-b1 Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:26 / reh 06/22/11 12:47 / reh 06/23/11 19:33 / dck 06/23/11 19:33 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 5 of 38
79 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-3 Report Date: 07/07/11 Collection Date: 06/15/11 09:00 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:54 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable Kelada mod A4500-CN-F D2036C 06/28/11 13:39 / eli-b 06/29/11 17:02 / eli-b 06/29/11 15:51 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 12:30 / reh 06/22/11 12:51 / reh 06/23/11 19:38 / dck 06/23/11 19:38 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 6 of 38
80 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-D4 Report Date: 07/07/11 Collection Date: 06/15/11 10:55 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:55 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable Kelada mod A4500-CN-F D2036C 06/28/11 13:48 / eli-b 06/29/11 17:02 / eli-b 06/29/11 15:53 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:29 / reh 06/22/11 12:52 / reh 06/23/11 19:42 / dck 06/23/11 19:42 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 7 of 38
81 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-18 Report Date: 07/07/11 Collection Date: 06/15/11 11:30 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:55 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable Kelada mod A4500-CN-F D2036C 06/28/11 13:49 / eli-b 06/29/11 17:02 / eli-b 06/29/11 16:02 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:32 / reh 06/22/11 12:53 / reh 06/23/11 19:47 / dck 06/23/11 19:47 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 8 of 38
82 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-D2 Report Date: 07/07/11 Collection Date: 06/15/11 12:15 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:55 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable Kelada mod A4500-CN-F D2036C 06/28/11 13:51 / eli-b 06/29/11 17:02 / eli-b 06/29/11 16:04 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:34 / reh 06/22/11 12:54 / reh 06/23/11 19:51 / dck 06/23/11 19:51 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 9 of 38
83 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-2 Report Date: 07/07/11 Collection Date: 06/15/11 13:10 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:56 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable 0.20 Kelada mod A4500-CN-F D2036C 06/28/11 14:13 / eli-b 06/29/11 17:02 / eli-b 06/29/11 17:00 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:40 / reh 06/22/11 12:56 / reh 06/23/11 19:56 / dck 06/23/11 19:56 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 10 of 38
84 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-19 Report Date: 07/07/11 Collection Date: 06/15/11 13:45 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:56 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable Kelada mod A4500-CN-F D2036C 06/28/11 14:15 / eli-b 06/29/11 17:02 / eli-b 06/29/11 16:05 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:42 / reh 06/22/11 12:57 / reh 06/23/11 20:00 / dck 06/23/11 20:00 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 11 of 38
85 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-5 Report Date: 07/07/11 Collection Date: 06/15/11 14:45 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:56 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 14:37 / eli-b1 Alkalinity, Total as CaCO A2320 B 06/20/11 20:04 / zeg Sulfate 1200 D 5 E /20/11 23:55 / zeg Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:44 / reh 06/22/11 12:58 / reh 06/23/11 20:05 / dck 06/23/11 20:05 / dck Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. Page 12 of 38
86 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID STA-4 Report Date: 07/07/11 Collection Date: 06/15/11 15:00 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:56 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 14:40 / eli-b1 Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N 0.05 E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:45 / reh 06/22/11 12:59 / reh 06/23/11 20:41 / dck 06/23/11 20:41 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 13 of 38
87 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-10A Report Date: 07/07/11 Collection Date: 06/15/11 15:45 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:56 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 14:43 / eli-b1 Alkalinity, Total as CaCO A2320 B 06/20/11 20:18 / zeg Sulfate E /21/11 00:11 / zeg Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:52 / reh 06/22/11 13:00 / reh 06/23/11 20:45 / dck 06/23/11 20:45 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 14 of 38
88 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID MB-Drain Report Date: 07/07/11 Collection Date: 06/15/11 16:10 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 11:57 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 14:46 / eli-b1 Alkalinity, Total as CaCO A2320 B 06/20/11 20:34 / zeg Sulfate 990 D 5 E /21/11 00:26 / zeg Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:54 / reh 06/22/11 13:06 / reh 06/23/11 20:50 / dck 06/23/11 20:50 / dck Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. Page 15 of 38
89 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID SPR-T Report Date: 07/07/11 Collection Date: 06/15/11 17:15 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 12:01 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable Kelada mod A4500-CN-F D2036C 06/28/11 14:17 / eli-b 06/29/11 17:02 / eli-b 06/29/11 16:07 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:56 / reh 06/22/11 13:10 / reh 06/23/11 20:54 / dck 06/23/11 20:54 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 16 of 38
90 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID STA-3A Report Date: 07/07/11 Collection Date: 06/15/11 17:40 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 12:01 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 14:52 / eli-b1 Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 11:58 / reh 06/22/11 13:11 / reh 06/23/11 20:59 / dck 06/23/11 20:59 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 17 of 38
91 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID MINN-DN Report Date: 07/07/11 Collection Date: 06/16/11 10:25 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 8 5 A2540 D 06/20/11 12:01 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable 0.20 Kelada mod A4500-CN-F D2036C 06/28/11 14:19 / eli-b 06/29/11 17:02 / eli-b 06/29/11 17:00 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N 0.05 E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 12:00 / reh 06/22/11 13:12 / reh 06/23/11 21:44 / dck 06/23/11 21:44 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 18 of 38
92 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID STA-2 Report Date: 07/07/11 Collection Date: 06/16/11 14:30 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 12:01 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 14:58 / eli-b1 Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 12:06 / reh 06/22/11 13:14 / reh 06/23/11 22:24 / dck 06/23/11 22:24 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 19 of 38
93 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID Toe Drain Report Date: 07/07/11 Collection Date: 06/16/11 16:50 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 12:01 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 15:11 / eli-b1 Alkalinity, Total as CaCO A2320 B 06/20/11 20:41 / zeg Sulfate 1200 D 5 E /21/11 00:41 / zeg Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 12:12 / reh 06/22/11 13:15 / reh 06/23/11 22:28 / dck 06/23/11 22:28 / dck Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. Page 20 of 38
94 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID BCD-A Report Date: 07/07/11 Collection Date: 06/16/11 18:05 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 12:07 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable Kelada mod A4500-CN-F D2036C 06/28/11 14:20 / eli-b 06/29/11 17:02 / eli-b 06/29/11 16:09 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 12:32 / reh 06/22/11 13:16 / reh 06/23/11 22:33 / dck 06/23/11 22:33 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 21 of 38
95 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID STA-1 Report Date: 07/07/11 Collection Date: 06/16/11 19:00 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 8 5 A2540 D 06/20/11 12:07 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 15:22 / eli-b1 Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N 0.05 E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 12:16 / reh 06/22/11 13:17 / reh 06/23/11 22:37 / dck 06/23/11 22:37 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 22 of 38
96 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID BS-D Report Date: 07/07/11 Collection Date: 06/16/11 19:45 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 12:07 / cmm INORGANICS Cyanide, Total Cyanide, Free Cyanide, Weak Acid Dissociable 0.20 Kelada mod A4500-CN-F D2036C 06/28/11 14:22 / eli-b 06/29/11 17:02 / eli-b 06/29/11 17:00 / eli-b NUTRIENTS Nitrogen, Nitrate+Nitrite as N E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 12:18 / reh 06/22/11 13:18 / reh 06/23/11 22:42 / dck 06/23/11 22:42 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 23 of 38
97 LABORATORY ANALYTICAL REPORT Project: Beal Mtn Lab ID: H Client Sample ID DUP-1 Report Date: 07/07/11 Collection Date: 06/16/11 06:00 DateReceived: 06/17/11 Matrix: Aqueous MCL/ Analyses Result Units Qualifiers RL QCL Method Analysis Date / By PHYSICAL PROPERTIES Solids, Total Suspended 105 C 5 A2540 D 06/20/11 12:07 / cmm INORGANICS Cyanide, Total Kelada mod 06/22/11 15:27 / eli-b1 Cyanide, Free 0.20 A4500-CN-F 06/27/11 08:04 / eli-b Cyanide, Weak Acid Dissociable NA D2036C 06/27/11 07:57 / eli-b - The Total Cyanide was analyzed, and was less than the reporting limit for Weak Acid Dissociable (WAD) Cyanide. WAD Cyanide was not analyzed. NUTRIENTS Nitrogen, Nitrate+Nitrite as N 0.05 E353.2 Nitrogen, Ammonia as N 0.1 E350.1 METALS, TOTAL RECOVERABLE Copper Selenium /20/11 12:19 / reh 06/22/11 13:20 / reh 06/23/11 22:46 / dck 06/23/11 22:46 / dck Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 24 of 38
ANALYTICAL SUMMARY REPORT
ANALYTICAL SUMMARY REPORT OST-003 August 06, 2015 PO Box 2003 Rapid City, SD 57709 Work Order: Project Name: G15070702 Energy Laboratories Inc. Gillette WY received the following 2 samples for on 7/31/2015
Texas Commission on Environmental Quality
Matrix: Drinking Water Method EPA 1603 (modified mtec) AB ID Method ID Escherichia coli (enumeration) TX 2525 10236201 Method EPA 200.5 AB ID Method ID Arsenic TX 1010 10213975 Beryllium TX 1020 10213975
Introduction. The following definitions may help you better understand the components of the data report.
Introduction This document is designed to help our clients understand the quality control requirements and limitations of data reporting. There are three sections to this document. The first section will
Pace Analytical e-report
Date Issued: July 28, 2014 Pace Analytical e-report Report prepared for: ATLANTIC TESTING LABORATORIES, LTD 22 CORPORATE DR CLIFTON PARK, NY 12065 CONTACT: Derek Converse ----------------------------------------------
1 Quality Assurance and Quality Control Project Plan
1 Quality Assurance and Quality Control Project Plan The purpose of this section is to describe the quality assurance/quality control program that will be used during the system specific field testing
ANALYTICAL RESULTS. Project: NLNA - Cistern Water Testing. Submittal Date: 04/26/2010 Group Number: 1191887 State of Sample Origin: PA
ANALYTICAL RESULTS Prepared by: Lancaster Laboratories 2425 New Holland Pike Lancaster, PA 7605-2425 Prepared for: Philadelphia PA 923 May 0, 200 Project: - Cistern Water Testing Submittal Date: 04/26/200
Innovative Removal of Agricultural Related Water Pollutants in the Chesapeake Bay Watershed
Innovative Removal of Agricultural Related Water Pollutants in the Chesapeake Bay Watershed William E. Roper, Kelly P. Rock, and Howard E. Sorber III Micronic Technologies, Wise, VA National Capital Regional
Standard methods in water analysis
Branch General analytical laboratories; water analysis Keywords Water analysis; standard methods; ASTM; DIN; ISO; USP; EPA; SLMB; EN; SCA; titration; ion chromatography; voltammetry; branch 1; branch 2
Ecology Quality Assurance Glossary
Ecology Quality Assurance Glossary Edited by William Kammin, Ecology Quality Assurance Officer Accreditation - A certification process for laboratories, designed to evaluate and document a lab s ability
APPENDIX II TIER I CHECKLIST
APPENDIX II TIER I CHECKLIST Data Validation PRF - Tier I Page 1 Data Validation Plan Review Form Tier I This Plan Review Form is # 1 of 1 forms completed in the review of this closure plan. Facility Name
Appendix D lists the Field Services Standard Operating Procedures. Appendix E lists the Biological Monitoring Standard Operating Procedures.
Page 16 of 87 3.3 Sample Collection, Storage and Preservation Figure 3 details required containers, sample volumes, preservation techniques, and holding times for proper sample collection. A discussion
APPENDIX L DATA VALIDATION REPORT
APPENDIX L DATA VALIDATION REPORT FIELD AND DATA REPORT DOWNTOWN PORTLAND SEDIMENT CHARACTERIZATION PHASE II WILLAMETTE RIVER PORTLAND, OREGON JUNE 2010 Data Validation Report Downtown Portland Sediment
DMR-QA Planning Guide 2015 DMR-QA 35: Plan for Success
DMR-QA Planning Guide 2015 DMR-QA 35: Plan for Success [ THE INDUSTRY STANDARD ] Your Partner In Defensible Data We understand that the art of our superior service is just as important as the science of
TERRA TEK LIMITED GUIDE TO SAMPLE HANDLING. Version 1.06
TERRA TEK LIMITED GUIDE TO SAMPLE HANDLING Version 1.06 September 2009 Guidance on Sample Containers & Storage Conditions - SOIL SAMPLES 500ml Plastic Tub Suitable for: Inorganic Parameters, usually sufficient
On-Site Waste Water Fees
On-Site Waste Water Fees Description Gallons Per Day Number of Bedrooms FY 11 Fee Addition to System (Per Bedroom) IP/AC/RV 0-120 $250 Improvement Permit (IP) Only 240-360 2-3 $500 Authorization to Construct
This example of a completed sampling plan worksheet has been included to illustrate the information
APPENDIX B EXAMPLE OF A COMPLETED SAMPLING PLAN WORKSHEET This example of a completed sampling plan worksheet has been included to illustrate the information necessary to document a sampling program for
APPENDIX B. Magna Reservoir Leak Detection & Water Quality Sampling Plan (Revised June 2011)
APPENDIX B Magna Reservoir Leak Detection & Water Quality Sampling Plan (Revised June 2011) 1.0 Introduction The Magna Reservoir System, located in the North Concentrator facilities area, acts as a central
Third Party Data Validation: What you need to know and do!
Third Party Data Validation: What you need to know and do! Anand Mudambi & Pamela Wehrmann 2012 DoD EMDQ Workshop San Diego, CA Course Objectives/Outline The course will provide an overview of third party
CALIFORNIA DEPARTMENT OF PUBLIC HEALTH ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM Accredited Fields of Testing
CALIFORNIA DEPARTMENT OF PUBLIC HEALTH ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM Accredited Fields of Testing Babcock Laboratories, Inc. 6100 Quail Valley Court Riverside, CA 92507 Phone: (951) 653-3351
Quality Manual for SJCUEL
St. Johns County Board of County Commissioners St. Johns County Utility Environmental Laboratory P.O. Drawer 3006 St. Augustine, FL 32085 3006 Technical Director, & QA Officer: Stacy Kowlsen 860 West 16
South Dakota s Statewide Ground Water Quality Monitoring Network
South Dakota s Statewide Ground Water Quality Monitoring Network Derric L. Iles State Geologist Geological Survey Program Department of Environment and Natural Resources 2014 Eastern South Dakota Water
Sample Management SOP 2v8 Page 1 STANDARD OPERATING PROCEDURE NO. 2 SAMPLE MANAGEMENT REVISION LOG. Revision Number Description Date
Sample Management SOP 2v8 Page 1 STANDARD OPERATING PROCEDURE NO. 2 SAMPLE MANAGEMENT REVISION LOG Revision Number Description Date 2.0 Original SOP 2.1 Revisions by McLemore after field testing 1/3/04
ANALYTICAL REPORT LABORATORY DETAILS. Telephone Facsimile Email. SGS Reference Report Number Date Reported Date Received
ANALYTICAL REPORT CLIENT DETAILS Contact Client Address Matthew Behre SGS Metallurgical Services 431 Victoria Street Malaga MALAGA WA 6090 LABORATORY DETAILS Manager Laboratory Address Said Hirad SGS Newburn
CLIENT NAME: MISC AGAT CLIENT ON, ON (403) ATTENTION TO: Chantell Cambal
CLIENT NAME: MISC AGAT CLIENT ON, ON (403) WATER ANALYSIS REVIEWED BY: Anthony Dapaah, PhD (Chem), Inorganic Lab Manager DATE REPORTED: May 19, 2015 PAGES (INCLUDING COVER): 5 VERSION*: 1 Should you require
CERTIFICATE OF ANALYSIS
Attention: Angela Mazza / Kathleen Wilson Catholic Education Centre 80 Sheppard Ave E North York, ON M2N 6E8 Your Project #: ANNUNCIATION Your C.O.C. #: na Report #: R3046860 Version: 1 MAXXAM JOB #: B488250
Nitrogen, Phosphorus, and Suspended Solids Concentrations in Tributaries to the Great Bay Estuary Watershed in 2011
Nitrogen, Phosphorus, and Suspended Solids Concentrations in Tributaries to the Great Bay Estuary Watershed in 2011 A Final Report to The Piscataqua Region Estuaries Partnership Submitted by Matthew A.
ST. CLOUD TECHNICAL AND COMMUNITY COLLEGE HAZARDOUS WASTE PROCEDURE
APPLICABILITY This procedure is applicable to all St. Cloud Technical & Community College faculty, staff and students. GENERAL Federal, state and local governments impose strict regulations concerning
Bryte Chemical Laboratory Quality Assurance Manual
Quality Assurance Technical Document 8 Bryte Chemical Laboratory Quality Assurance Manual May 2006 State of California The Resources Agency Department of Water Resources Bryte Chemical Laboratory Quality
ATTACHMENT 2. BMP Monitoring Plan Template
ATTACHMENT 2 BMP Monitoring Plan Template Project SPR - 335 Water Quality Facility Investigation Response to Modified Task 4: Development of BMP Monitoring Plan Template December 2002 i Table of Contents
Total Suspended Solids Total Dissolved Solids Hardness
Total Suspended Solids (TSS) are solids in water that can be trapped by a filter. TSS can include a wide variety of material, such as silt, decaying plant and animal matter, industrial wastes, and sewage.
GUIDELINES FOR USE BY CLASS A LICENSEES IN MEETING SNP REQUIREMENTS JULY 1996
QUALITY ASSURANCE (QA) AND QUALITY CONTROL (QC) GUIDELINES FOR USE BY CLASS A LICENSEES IN MEETING SNP REQUIREMENTS AND FOR SUBMISSION OF A QA/QC PLAN JULY 1996 DEPARTMENT OF INDIAN AND NORTHERN AFFAIRS
The purpose of this bid is to procure a contract with a laboratory to provide analytical testing services on an as-needed basis.
Page 1 of 11 1. GENERAL The purpose of this bid is to procure a contract with a laboratory to provide analytical testing services on an as-needed basis. Special consideration may be given to laboratories
Draft. Quality Assurance Project Plan. Haul Road Fugitive Dust Study. Red Dog Mine, Alaska. Prepared for. Teck Cominco Alaska Inc.
Draft Quality Assurance Project Plan Haul Road Fugitive Dust Study Red Dog Mine, Alaska Prepared for Teck Cominco Alaska Inc. Anchorage, Alaska Draft Quality Assurance Project Plan Haul Road Fugitive Dust
Water Analysis Report Report Date: March 31, 2012 Testing Period: 1st - 4th Quarter 2011
Volatile Organic Compounds Benzene 0.0005 0.005 ND Carbon tetrachloride 0.0005 0.005 ND Chlorobenzene (Monochlorobenzene) 0.0005 0.100 ND 1,2-Dichlorobenzene (o-dcb) 0.0005 0.600 ND 1,4-Dichlorobenzene
Quality Assurance Manual
Clinical Laboratory of San Bernardino, Inc. Quality Assurance Manual Clinical Laboratory of San Bernardino, Inc. 21881 Barton Road, Grand Terrace, CA 92313 Telephone (909) 825-7693 Facsimile (909) 825-7696
Analytical Data Package Reports
Analytical Data Package Reports TriMatrix offers a variety of analytical data packages formatted to meet the reporting needs and varying data quality objectives of its clients. The data packages offered
Environmental Water Testing: Surface Water, Groundwater, Hard Water, Wastewater, & Seawater
Document: AND Sol Env 08 2013 Environmental Water Testing: Surface Water, Groundwater, Hard Water, Wastewater, & Seawater Matrix specific sample preparation and testing methods for environmental waters
Data Quality. Tips for getting it, keeping it, proving it! Central Coast Ambient Monitoring Program
Data Quality Tips for getting it, keeping it, proving it! Central Coast Ambient Monitoring Program Why do we care? Program goals are key what do you want to do with the data? Data utility increases directly
BOTTLED WATER QUALITY REPORT INTRODUCTION VOSS SOURCE SPECIFIC MINERAL ANALYSIS. VOSS Still. VOSS Sparkling. General Mineral Analysis
BOTTLED WATER QUALITY REPORT Voss ion AS, N-4730 Vatnestrøm, Norway 1-877-525-VOSS INTRODUCTION At VOSS, we are proud of the quality of our products. VOSS Artesian Water from Norway meets all bottled water
Purity of water is defined in part by the mineral level found in specific bottled waters and is referred to as
BOTTLED WATER QUALITY REPORT Voss ion AS, N-4730 Vatnestrøm, Norway 1-877-525-VOSS INTRODUCTION At VOSS, we are proud of the quality of our products. VOSS Artesian Water from Norway meets all bottled water
Work Assignment 5-03. Prepared for: Office of Air Quality Planning and Standards U.S. Environmental Protection Agency Research Triangle Park, NC
ERG No.: 0143.04.005 EPA Contract No.: 68-D-00-264 Standard Operating Procedure for the Determination of Metals In Ambient Particulate Matter Analyzed By Inductively Coupled Plasma/Mass Spectrometry (ICP/MS)
Removing Thallium from Industrial FGD Scrubber Water with Sorbster Adsorbent Media
Case History MAR Systems Inc. Removing Thallium from Industrial FGD Scrubber Water with Sorbster Adsorbent Media Trace thallium levels in process and wastewater streams pose a human toxicity threat. Tidwell
Characterizing Beauty Salon Wastewater for the Purpose of Regulating Onsite Disposal Systems
Characterizing Beauty Salon Wastewater for the Purpose of Regulating Onsite Disposal Systems Fred Bowers 1,2, Ph.D. New Jersey Department of Environmental Protection Division of Water Quality August 14,
Data Management Tool -
Data Management Tool - Continuous Logger Data Uploading, Multisite Uploading, and Reporting Tools Created June 2013 Updated May 2015 Developed by: & Funded by: Research Office of Information Technology
QUALITY ASSURANCE / QUALITY CONTROL POLICY BREG SOIL AND WATER QUALITY LABORATORY UNIVERSITY OF DELAWARE
QUALITY ASSURANCE / QUALITY CONTROL POLICY BREG SOIL AND WATER QUALITY LABORATORY UNIVERSITY OF DELAWARE Department of Bioresources Engineering Rm 111 Worrilow Hall 531 S. College Ave. Newark, DE 19716-2140
Commonwealth of Kentucky. Wastewater Laboratory Certification Manual
Commonwealth of Kentucky Wastewater Laboratory Certification Manual March 2013 This page intentionally left blank ii TABLE OF CONTENTS I. INTRODUCTION I-1 II. GENERAL LABORATORY REQUIREMENTS II-1 1.0 Personnel
Determination of Total Suspended Solids (TSS) and Total Volatile Solids (TVS) in Waters of Fresh/Estuarine/Coastal Waters
Determination of Total Suspended Solids (TSS) and Total Volatile Solids (TVS) in Waters of Fresh/Estuarine/Coastal Waters 1. SCOPE and APPLICATION 1.1 Gravimetric analysis is used to determine total suspended
General Chemistry and Metals
The drop on water General Chemistry and Metals Water for drinking, cooking, and other domestic uses should be of good quality. It should be free from organisms that may cause disease and free from chemical
To meet our acceptance criteria, we may require you to partially treat your wastewater before it discharges to sewer.
Trade Waste Acceptance criteria for trade waste Information sheet 6 Acceptance criteria for industrial waste Water Corporation s wastewater system is designed primarily to service households with normal
The ground water region in the area of the proposed Project site is made-up of sedimentary rocks (Figure 5.6-1)
EIS Section 5.6 Groundwater Quantity and Quality 5.6 GROUNDWATER QUANTITY AND QUALITY For the purpose of this EIS, the inventory and description of groundwater resources (hydrogeology) within the footprint
ITS REWORK DATA VERIFICATION REPORT for samples collected from CAMP STANLEY STORAGE ACTIVITY BOERNE, TEXAS
INTRODUCTION ITS REWORK DATA VERIFICATION REPORT for samples collected from CAMP STANLEY STORAGE ACTIVITY BOERNE, TEXAS Data Verifiers: Michelle Wolfe & Tammy Chang Parsons The following data validation
Evaluating Laboratory Data. Tom Frick Environmental Assessment Section Bureau of Laboratories
Evaluating Laboratory Data Tom Frick Environmental Assessment Section Bureau of Laboratories Overview of Presentation Lab operations review QA requirements MDLs/ PQLs Why do we sample? Protect physical,
After review of the limits proposed, DEQ submits the public comment draft 401 water quality ce1tification containing an antidegradation review.
STATE OF IDAHO DEPARTMENT OF ENVIRONMENTAL QUALITY 900 North Skyline, Suite B Idaho Falls, ID 83402 (208) 528-2650 C. L. "Butch" Otter, Governor Curt A. Fransen, Director February 9, 2015 Mr. Michael Lidgard
Approvals [Signature On File]
![Approvals [Signature On File]](/thumbs/24/4276680.jpg "Approvals [Signature On File]")
Page 1 of 7 Minimum Reporting Requirements for Analytical Data (Chemistry) for the Water Quality Planning Bureau Approvals SOP WQPBDMS-010 Prepared by: Chris Shirley, QA Officer, WQPB Michael Pipp, Environmental
QUALITY ASSURANCE PLAN
QUALITY ASSURANCE PLAN Revision 16.0 June 2013 (Initial Version Release: January 2001) Prepared By: J. Nathan Hawley and Josh Kirkpatrick Basic Laboratory, Inc. Basic Laboratory, Inc. 2218 Railroad Avenue
Measurement by Ion Selective Electrodes
Measurement by Ion Selective Electrodes Adrian Vazquez May 8, 2012 Why Use Ion Selective Electrodes? Responsive over a wide concentration range Not affected by color or turbidity of sample Rugged and durable
METHOD 353.2 DETERMINATION OF NITRATE-NITRITE NITROGEN BY AUTOMATED COLORIMETRY
METHOD 353.2 DETERMINATION OF NITRATE-NITRITE NITROGEN BY AUTOMATED COLORIMETRY Edited by James W. O'Dell Inorganic Chemistry Branch Chemistry Research Division Revision 2.0 August 1993 ENVIRONMENTAL MONITORING
A White Paper Describing a Watershed-based Monitoring Network Design for the Purgatoire River Basin
A White Paper Describing a Watershed-based Monitoring Network Design for the Purgatoire River Basin This white paper summarizes a watershed-based monitoring network design for the Purgatoire River Basin,
ALS TRIBOLOGY Engine Coolant Reference Guide
ALS TRIBOLOGY Engine Coolant Reference Guide Engine coolants are a mixture of, inhibitors, and water. Each formula is designed for specific protection and engine requirements. Mixing different coolants
SOFIA UNIVERSITY ST. KLIMENT OHRIDSKI Faculty:...Chemistry and Pharmacy... Subject area: (code and name) C H L 3 8 2 4 1 3
Approved by:.. Dean Date... SOFIA UNIVERSITY ST. KLIMENT OHRIDSKI Faculty:...Chemistry and Pharmacy... Subject area: (code and name) C H L 3 8 3...Pharmacy... M.Sc. Program: (code and name) C H L 3 8 3...Pharmacy...
ASSURING THE QUALITY OF TEST RESULTS
Page 1 of 12 Sections Included in this Document and Change History 1. Purpose 2. Scope 3. Responsibilities 4. Background 5. References 6. Procedure/(6. B changed Division of Field Science and DFS to Office
METHOD 200.8 DETERMINATION OF TRACE ELEMENTS IN WATERS AND WASTES BY INDUCTIVELY COUPLED PLASMA - MASS SPECTROMETRY. Revision 5.
METHOD 200.8 DETERMINATION OF TRACE ELEMENTS IN WATERS AND WASTES BY INDUCTIVELY COUPLED PLASMA - MASS SPECTROMETRY Revision 5.4 EMMC Version S.E. Long (Technology Applications Inc.), T.D. Martin, and
City of Bloomington. and
Lead Paint Soil Assessment Long Meadow Lake Bridge Old Cedar Avenue over the Minnesota River Bloomington, Minnesota Prepared for City of Bloomington and SRF Consulting Group, Inc. Project B14-01875 July
AGL UPSTREAM INVESTMENTS PTY LTD
AGL UPSTREAM INVESTMENTS PTY LTD GLOUCESTER GAS PROJECT October 2014 Water Monitoring Report Waukivory Pilot Project: Fracture Stimulation and Flow Test EPL 20358 Reporting Period: September - October
DEPARTMENT OF NATURAL RESOURCES and ENVIRONMENTAL CONTROL SITE INVESTIGATION & RESTORATION BRANCH
Page 1 DEPARTMENT OF NATURAL RESOURCES and ENVIRONMENTAL CONTROL SITE INVESTIGATION & RESTORATION BRANCH STANDARD OPERATING PROCEDURES FOR CHEMICAL ANALYTICAL PROGRAMS UNDER THE HAZARDOUS SUBSTANCE CLEANUP
Section A LABORATORY QUALITY ASSURANCE/QUALITY CONTROL. Her Majesty the Queen in Right of the Province of British Columbia 2013 All Rights Reserved.
Section A LABORATORY QUALITY ASSURANCE/QUALITY CONTROL Her Majesty the Queen in Right of the Province of British Columbia 2013 All Rights Reserved. TABLE OF CONTENTS SECTION A Laboratory Quality Assurance/Quality
DATA VALIDATION STANDARD OPERATING PROCEDURES FOR CONTRACT LABORATORY PROGRAM ROUTINE ANALYTICAL SERVICES
DATA VALIDATION STANDARD OPERATING PROCEDURES FOR CONTRACT LABORATORY PROGRAM ROUTINE ANALYTICAL SERVICES UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION IV SCIENCE AND ECOSYSTEM SUPPORT DIVISION
How To Remove Selenium From Water
Information Technology Solutions ABSTRACT The discharge of selenium to natural water systems is regulated by law. Those with permitted outfalls must treat the waste stream to below the US EPA regulatory
Proficiency Testing In A Global Analytical Environment Benefits & Challenges. AOAC September 2007
Proficiency Testing In A Global Analytical Environment Benefits & Challenges AOAC September 2007 1 The Coca-Cola Company The Coca-Cola Company is the largest manufacturer, distributor and marketer of nonalcoholic
STORMWATER MONITORING: POLLUTANTS, SOURCES, AND SOLUTIONS
RICHLAND COUNTY STORMWATER MANAGEMENT DIVISION STORMWATER MONITORING: POLLUTANTS, SOURCES, AND SOLUTIONS As part of the federal government s National Pollutant Discharge Elimination System Permit (NPDES)
Where does it come from?
What is Phosphorus? Phosphorus (P) is a nutrient that is vital to human, animal, and plant growth. It s one of the most common substances found in nature. It s found in our water, our food, and our bodies.
APPLICATION OF ICP-MS TECHNOLOGY FOR TRACE METALS ANALYSIS
MR. TELLIARD: Our next speaker is Paula Hogg. Paula is currently a lab manager at Hampton Roads Sanitation District s Central Environmental Laboratory. We would like to also thank Hampton Roads for sending
Additional Lecture: TITRATION BASICS
Additional Lecture: TITRATION BASICS 1 Definition and Applications Titration is the incremental addition of a reagent solution (called titrant) to the analyte until the reaction is complete Common applications:
ANALYTICAL REPORT LABORATORY DETAILS. Telephone Facsimile Email. SGS Reference Report Number Date Reported
ANALYTICAL REPORT CLIENT DETAILS Contact Client Address Luke Zambelli W2R PTY LTD 26 RIVERGUM DRIVE EATONS HILL QLD 4037 LABORATORY DETAILS Manager Laboratory Address Andrew Tomlins SGS Brisbane Environmental
Electronic Reporting to BTS
Electronic Reporting to BTS EPA s Electronic Reporting Tool (ERT) Software to Standardize Source Test Planning, Reporting and Assessment. http://www.epa.gov/ttnchie1/ert/ Enhancements made to improve and
Hazardous Waste Management & Waste Minimization Training
Hazardous Waste Management & Waste Minimization Training Environmental Health and Safety Safety Training Building Inspections Accident Investigations Fire Safety Hazardous Materials Management Laboratory
Quality Assurance Plan
Page 1 of 115 Department of Environmental Conservation Laboratory UVM Hills Building D.E.C. Laboratory 105 Carrigan Drive Burlington VT 05405 Quality Assurance Plan 2015 Dan Needham March 2015 Interim
Evaluation of Chemical Quality in 17 Brands of Iranian Bottled Drinking Waters
Original Article J Res Health Sci, Vol. 9, No., 9, pp. J Res 5 Health Sci, Vol. 9, No., 9, pp. 5 Evaluation of Chemical Quality in Brands of Iranian Bottled Drinking Waters *Samadi MT. PhD, *Rahmani AR.
DATA QUALITY OBJECTIVES
The Wastewater Treatment Plant Operators Guide to Biosolids Sampling Plans CHAPTER 5 DATA QUALITY OBJECTIVES Goals of the Sampling Plan ESSENTIAL ELEMENTS OF A SAMPLING PLAN Description of the Facility
Removing Heavy Metals from Wastewater
Removing Heavy Metals from Wastewater Engineering Research Center Report David M. Ayres Allen P. Davis Paul M. Gietka August 1994 1 2 Removing Heavy Metals From Wastewater Introduction This manual provides
Division of Environmental Response and Revitalization
Division of Environmental Response and Revitalization Guidelines and Specifications for Preparing Quality Assurance Project Plans (QAPPs) September 1, 1998 - Final Purpose This document (1) presents guidelines
www.epa.gov Method OIA 1677-09: Available Cyanide by Ligand Exchange and Flow Injection Analysis (FIA)
www.epa.gov 2010 Method OIA 1677-09: Available Cyanide by Ligand Exchange and Flow Injection Analysis (FIA) Methodology Method OIA-1677: Available Cyanide by Ligand Exchange and Flow Injection Analysis
How to read your Oil Analysis Report
How to read your Oil Analysis Report A better understanding Petroleum Technologies Group, LLC. 4665 Broadmoor S.E. Ste#15 Grand Rapids, MI 49512 Phone # 616/698 9399 Fax # 616/698 9395 www.oil lab.com
Calculating Molar Mass of a Compound
Instructions for Conversion Problems For every conversion problem Write the number in the problem down with unit and a multiplication sign Decide which conversion factor you should use, Avagadro s or molar
Appendix B. Eugene/Springfield Environmental Services Laboratory Quality Assurance Plan
Appendix B Eugene/Springfield Environmental Services Laboratory Quality Assurance Plan City of Eugene NPDES Stormwater Monitoring Plan May 2011 Users of this document are responsible to ensure it is the
Chlorine, Total. DPD Method 1 Method 10101 0.09 to 5.00 mg/l Cl 2 Test 'N Tube Vials. Test preparation. Instrument-specific information
Chlorine, Total DOC316.53.01028 DPD Method 1 Method 10101 0.09 to 5.00 mg/l Cl 2 Test 'N Tube Vials Scope and application: For testing higher levels of total (free plus combined) chlorine in drinking water,
The mining industry, regulators and most service laboratories generally use the following guidelines for cyanide species.
INTERNATIONAL CYANIDE MANAGEMENT INSTITUTE www.cyanidecode.org \ Cyanide Facts: Cyanide Sampling and Analytical Methods for Gold Mining May 2002 SAMPLING AND ANALYTICAL METHODS This document provides general
Developing Quality Assurance Project Plans using Data Quality Objectives and other planning tools. Developing QAPPs 5/10/2012 1
Developing Quality Assurance Project Plans using Data Quality Objectives and other planning tools 1 Introductions 2 Agenda I. Developing a QAPP II. Systematic Planning using Data Quality Objectives III.
Vieques Island Biota Sampling Project. Data Validation Report; October 14, 2005 Revision 1 January 26, 2006 Page 1
Page 1 1.0 INTRODUCTION This report summarizes the validation of analytical results generated from field sampling in 2005, in support of the. Sampling and analyses were performed according to the Laboratory
TERMS OF REFERENCE FOR THE RAPID EIA STUDY FOR SHIVKAR LIGNITE BLOCK, DIST. BARMER, RAJASTHAN
1. GENERAL TERMS OF REFERENCE FOR THE RAPID EIA STUDY FOR SHIVKAR LIGNITE BLOCK, DIST. BARMER, RAJASTHAN The main objective of the EIA study is to assess the positive and negative impacts likely to accrue
Analytical Data Report for Sediment Samples Collected From 100-NR-2 Operable Unit
PNNL- 20826 Analytical Data Report for Sediment Samples Collected From 100-NR-2 Operable Unit Michael Lindberg October 2011 DISCLAIMER This report was prepared as an account of work sponsored by an agency
LED Life-Cycle Assessment & Environmental Testing
LED Life-Cycle Assessment & Environmental Testing DOE Solid State Lighting Booth Presentation LightFair 2013 Jason Tuenge Pacific Northwest National Laboratory Program Name or Ancillary Text eere.energy.gov
Dissolved and precipitated oxalate
Accepted 2005 Process liquors from bleach plants Dissolved and precipitated oxalate Using Ion Chromatography 0 Introduction In bleach plants of pulp mills with a high degree of system closure, there is
Samples RMN070714. Analytical Report (0714-63) GC/FID Analysis (RM01) Nicotine Purity
For the benefit of VaporFi, Inc. Samples RMN070714 Analytical Report (0714-63) GC/FID Analysis (RM01) Nicotine Purity GC/MS Analysis (QG02) Anabasine, Anatabine, Myosmine, Nornicotine Enthalpy Analytical,
Laboratory Information Management System (LIMS) in EMRL
Laboratory Information Management System (LIMS) in EMRL History of LIMS at EMRL November of 2003, EMRL purchased a commercial LIMS system to replace an LLNL built system Use for multiple groups Keep current
DRAFT Changes to 25 Pa. Code Chapter 252 For Discussion Purposes Only January 21, 2015 CHAPTER 252. ENVIRONMENTAL LABORATORY ACCREDITATION
CHAPTER 252. ENVIRONMENTAL LABORATORY ACCREDITATION Subchapter A. GENERAL PROVISIONS B. APPLICATION, FEES AND SUPPORTING DOCUMENTS C. GENERAL STANDARDS FOR ACCREDITATION D. QUALITY ASSURANCE AND QUALITY
Ontario Drinking Water Parameter Limits and Descriptions
Ontario Drinking Water Parameter Limits and Descriptions Notes on tables: Limits, where listed, taken from Ontario Drinking Water Quality Standards. MAC = Maximum Allowable Concentration OG = Operational
MUNICIPAL NPDES PERMIT. issued to. Facility ID: 095-001 Permit ID: CT0100382 Permit Expires: September 20, 2011
MUNICIPAL NPDES PERMIT issued to Permittee: Location Address City of New London Water Pollution Control Facility 181 State Street 100 Trumbull Street New London, Connecticut 06320 New London, Connecticut
WRITING CHEMICAL FORMULA
WRITING CHEMICAL FORMULA For ionic compounds, the chemical formula must be worked out. You will no longer have the list of ions in the exam (like at GCSE). Instead you must learn some and work out others.
NUTC R304. Use of Absorption Mechanisms to Decrease Heavy Metal Mobility
Use of Absorption Mechanisms to Decrease Heavy Metal Mobility by Jianmin Wang Honglan Shi Joe G. Burken NUTC R304 A National University Transportation Center at Missouri University of Science and Technology