GLass LINING TECHNOLOGIES. A compendium of good characteristics

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GLass LINING TECHNOLOGIES A compendium of good characteristics 1

Significant all around the world A complete program Technical enamel from Düker caters for all requirements A hardness based on fire, water, air and earth is all that is needed for achieving safe production processes in sensitive industries. email800 is made in a number of stages from quartz, feldspar, borax, soda, saltpeter and metal oxides and by melting at 1.400 C (2552 F). The special mix ratio of the basic substances determines the final resistance to aggressive media. email800 is therefore a very special surface protection and its uses include the chemical, pharmaceutical and food industries. Why? This can be explained with quality and economical reasons: It meets quality and economic requirements in that components made of email800 reduce the usual amount of care and maintenance required. Pipelines, fittings, valves, bottom outlet valves and columns from Düker can be combined to form durable complex units. The many options for users include the standard range, the design of special parts or a customized combination of both. email800 from Düker is a convincing product in competition with different technologies and makes a great deal of current surface protection seem old-fashioned. This is the opinion not only of users but also of independent research bodies and independent test establishments. Customers technicians are primarily interested in hygiene, economic effectiveness, holding times and the particular corrosion protection appropriate for specific purposes. Opting for email800 not only provides them with high quality, long-lasting and permanently maintenance-free installations but also enables them to call upon the know-how of experienced specialists at every stage from planning and customised design to commissioning and after-care. Product range of our pipe parts, finished goods and special productions Modular constructed bottom outlet valves Highly acid resistant fittings, oblique seated valves and diaphragm valves, sight glasses, flat sight glasses Distillation coloumns, absorption, extraction, as gas washer or reaction tube 2 3

Resistance in full operation! Characteristics of email800 New products and new process techniques are creating larger areas of use and more exacting requirements for surface protection in plant engineering in the chemical, pharmaceutical and food industries. We catered for these requirements when developing our particularly durable email800. email800 is highly resistant against attack, wear and corrosion and to diffusion during long holding times. These characteristics have been confirmed by independent tests and major chemical laboratories in Germany and Switzerland. Acid Resistance according to DIN ISO 2743 (HCL 20%; 108 C / 227 F) according to DIN 51174 (HCL 20%; 140 C), abrasion 0.18 mm / year Alkali Resistance according to DIN ISO 2745 (NaOH 4%; 80 C / 176 F), abrasion 0.4 mm/ year according to DIN ISO 2745 as amended, abrasion 0.3 mm/year Email350 enamel quality in white Our email350 quality is the economical solution against plastic materials. Pipes and fittings as well as special parts can be delivered in this quality. They can be used, in respect of operating conditions, in high temperature areas (till 150 C / 320 F). The small production costs are a result of less coating layers. email850p special made for the pharmaceutical industry email850p colour is light blue. The application of email850p can be found in pharmaceutical areas, drinking water supply and sewage technology. It combines better surface properties, optimizes corrosion properties and neutral biological behavior to the advantage of plant safety and to avoid product contamination in pharmaceutical processes. 4 5

Pipeline components Best surface protection for use in the chemical and pharmaceutical industries. In situations involving aggressive media, the particular surface protection provided by email800 is highly resistant to attack, corrosion, diffusion, temperature and wear during long holding times. Our basic range comprises nominal diameters of 25 to 600 mm and standard lengths of up to 4metres depending on nominal diameter. Versions can be supplied both to DIN or ANSI. The usual external finish is zinc powder based primer, but galvanising and painting are available if desired to suit the particular application. Special fabrications and special technical versions or lengths are also feasible. The range of supply also includes jacket-heated pipeline components. Pipes, tees and bends with heating or cooling jackets afford a wide variety of ways of maintaining temperature stability without affecting quality characteristics and very high safety standards. R old R new The reduction by half of the flange radii minimises entrapment of residues and ensures better cleanability. From simple pipe section to Good connections are provided by our new push-in loose flange, developed from our DIN loose flange. The two halves are easy to assemble and secure without using any tools. It can be used in combination with any conventional flange to produce a reliable connection. double-wall pipeline components for heating or cooling and special fabrications to meet customer wishes all this is part of the range! Even in extreme temperature conditions and with vacuum (10-5 and 10-6 mbar l/s ) with this flange connection leakage rates are minimized. The high residual torques ensure permanent tightness regardless of fluctuating temperature influences. (source: Test Infraserv) 6 7 Exhaust air Columns Valves Bottom outlet valves Pipeline components

The New Generation Glass lined bottom outlet valves with gap free design Düker innovations are characterized by low maintenance and good cleanability. For the new generation the number of convolutions in the bellows has been reduced to 6 which reduces the risk of product entry or crystallizatio and improves the cleanability. Bottom outlet valves according to DGRL 97/23/EG (PED) Category II, Module A1 with CE mark und declaration of conformity. Designed in accordance to TA-Luft with bellow, safety packing and connection thread for bellow monitoring. seal with valve seat and sealing cap towards the glass lined vessel nozzle (no product entry or crystallization behind the valve seat) valve seat (PFA) with stainless steel core and integrated gaskets (better stability with high temperatures) new bellows of TFM1600 (6 convolution bellows and seal with PTFE-encapsulated O-ring) replaceable PT100 (without dismantling the valve) Actuator made of electro-polished stainless steel with emergency opening Headpiece with stainless steel cladding against dirt Flushing nozzle provided as standard Easy assembly with lifting device Limit switch by NAMUR Tight and clean The new sealing cap can be used for all Düker bottom outlet valves to avoid a gap between the glass lined vessel nozzle and the valve seat. In addition large tolerances can be eliminated. Columns Valves Bottom outlet valves Versions: Lateral actuator for vessels with small space Check gauge to find out the right O-Ring. 8 9 Exhaust air

Highly acid resistant valves with smooth surfaces, scratch resistant, easy to clean are authorised, depending on version, for temperatures up to 180 C / 356 F and operating pressures ranging from - 1 to +16 bar. All versions can be supplied to DIN or ANSI. Our forged-steel valve bodies and precision cast steel or class GGG 40.3 spheroidalgraphite iron components meet the high safety standards required in chemical plants. Particularly in the pharmaceutical industry, smooth and scratch resistant surfaces and easy cleaning are further important criteria for optimum production results. The QHD guidelines set all this out in black and white. Glass lined flat sight glass Ball valves DN 25 and 50 (1 and 2 ) Diaphragm valves DN 25 to 100 (1 to 4 ) Oblique-seates valve DN 25 to 50 (1 to 4 In-line sightglass DN 25 to 150 (1 to 6 ) Flat sightglass DN 40 to 200 (1 1/2 to 8 ) Glass lined sight glass Exhaust air Columns Valves GMP Diaphragm valves: Head piece optional made of plastics or stainless steel. Sealing through PTFE-Protection shield with rubber back-up diaphragm Glass lined ball valve 10 11

Glass lined columns for distillation, absorption, extraction, in gas scrubber or reaction tube Construction and equipment are each designed for the desired application and specific process, up to and including DN 600 (24 ) and in section lengths of up to 4 meters. The various column sections up to DN 400 (16 ) are usually connected by loose flanges. Nominal diameters of 500 (20 ) and 600 mm (24 ) require the use of profile rings and pipe clamps. If the customer so desires, the supply includes internals such as supporting rings, perforated plates, inlet pipes, flow distributors and the like. Comprehensive internal testing to DIN, ISO, ASME and factory standards, company-specific regulations and TÜV acceptances afford optimum certified safety. The development and setting up of complex process equipment call for a great deal of planning and advice. You can rely on Düker as a competent partner when it comes to operationally safe and economic incorporation of reliable units and columns into a production system. Our expertise is available not only for the process of making plant items but right through the tender and design stages, project work, installation and after-care. Beside the production of pipes, fittings and columns we are also reglassing. Reglassing is not only cost saving but also time saving than a new production. A spark test with 20 KV will be made of course after glass lining. We offer our columns in three different enamel qualities, which vary in specification, coat application or other special operating conditions. These are: Columns email350 white enamel, applicable till 150 C / 302 F email800 dark blue enamel, all-purpose in chemical and pharmaceutical industry email850p light blue enamel, special made for pharmaceutical industry Exhaust air 12 13

email250light glass lined pipe system for aggressive exhaust air and waste water Under the trade name email250light Düker produce glass lined piping for aggressive exhaust air and waste water. email250light is easy to mount, stable and a longlife product. Because of the inner glass lining this pipe system is proper for aggressive fluids. In general email250light has a coating thickness of 0.4 mm. In case of higher aggressive substances in connection with higher temperature we are using email250-hsf. Here we have a thickness of 0.5 mm. Both types are pore free glass lined of course. Components between diameter DN50 and DN300 are produced with a wall thickness of 3 mm respectively 4 mm. As a general rule the sealing is a graphite gasket alternative with a PTFE envelope. The advantages of email250light at a glance: high thermal loading up to 200 C / 392 F high long-term resistance no material embrittlement typical of plastic high safety factor in the case of fire easy-to-clean and anti-adhesive fracture-proof smooth surfaces to counteract abrasion low weight Exhaust air Our email250light pipe components are connected with easy-to-mount loose flanges. The shown graphite gasket with a PTFE envelope is favored built in besides of the pure graphite gasket. 14 15

with system to solutions Vendor with competent experts The trend for operator of chemical plants is the reduction of contact points. Chemical and Pharmaceutical industries decide to count on less suppliers instead of many. Düker concentrates and structures the expertise of particular areas in one hand. The close teamwork of our experts brings safety in technical matters and a big economical advantage. Extensive technical advise, exact planning and calculation will show already in the planning phase the best efficiency of your plant concept. Complete supplier of chemical + pharmaceutical pipeline technology s services include: Planning Glas lined steel Glass Special materials Installation engineering and planning supply of glass lined pipeline components supply of PTFE-lined pipeline components procurement of glass lined vessels installation and validation 16 17

email800 in use worldwide Certified to meet highest quality requirements The particular nature of the chemical and pharmaceu- The first stage is the careful selection of suitable tical industries calls for high standards of safety in materials, authorised by TÜV regulations, for high- Since May 2002, Düker has also been making fittings, Pipe systems with email800 are durable and processing and production and in maintenance and quality linings, and initial material checks with our columns, vessels and complete piping systems accor- resistant to aggressive media and their long ser- care. suppliers. Before being glass lined, each part is che- ding to the European Pressure Equipment Direc- vice life is convincing. In addition, the materials used cked for exact dimensional accuracy. We use parts tives ( PED ) 97/23/EC (German abbreviation DGRL). are recyclable to become 100% available for reuse! Düker s products, particularly email800, cater for with overdimensioned wall thicknesses for glass li- these requirements in theory and practice at all levels. ned components. The frequent changes in production campaigns make We thus supply a product that corresponds to As early as 1994 Düker set up quality management to hygiene and clean ability important factors, including the state of the art and properly certified at ISO 9001 and successfully audited all installations The regular tests included in the comprehensive from the economic point of view. The QHD (Qualified that to TÜV CERT. technical monitoring for all products include high- Hygienic Design ) test method enables us to comply voltage tests after lining, measurement of lining with relevant standards concerning choice of mate- thicknesses and monitoring of angularity and plane rials, design, manufacture, installation and surfaces. parallelism. Its second stage produces practical evidence of clean ability. CERTIFICATE Making pressure vessels to the ASME Code involves specifically defined materials, welding processes and documentation. Plant constructors and clients throughout the world have the benefit of Düker s quality management and uniformly conducted certifications. This supports and eases procedures and promotes objectivity in the placing of orders. The Certification Body of TÜV SÜD Management Service GmbH certifies that Düker GmbH & Co. KGaA Würzburger Straße 10 D-97753 Karlstadt Hauptstraße 39-41 D-63846 Laufach has established and applies a Quality Management System for Development, manufacture, supply and service of valves used in water- and gas industries, high pressure ductile iron fittings, drain pipes and fittings, highly acid resistant glass lined components, castings made to specification centrifugal casting plants for production of castings as well as cookless cupola furnaces An audit was performed, Report No. 70008454 Proof has been furnished that the requirements according to ISO 9001: 2008 are fulfilled. The certificate is valid until 2012-03-23 Certificate Registration No. 12 100 21864 TMS Munich, 2009-04-08 QMS-TGA-ZM-07-92 18 19

GLASS LINING TECHNOLOGies JOBBING FOUNDRY Fittings And Valves DRAINAGE TECHNOLOGY Engineering 04.09 Specifications subject to change without notice. Düker GmbH & Co. KGaA Hauptstraße 39-41 D-63846 Laufach Germany Tel +49 6093 87-0 Fax +49 6093 87-303 Internet: www.dueker.de E-Mail: info@dueker.de 20