The international database for certified reference materials
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1 The international database for certified reference materials Thomas Steiger Rita Pradel Federal Institute for Materials Research and Testing (BAM) Germany 1
2 Use of CRMs Certified reference materials: are measurement benchmarks ensure reliability and comparability provide traceability in chemical analysis are required in quality assurance (ISO 17025) One main problem for users: How to find the proper CRM needed? Ways out: catalogues of producers websites of producers COMAR database 2
3 Main topics What is COMAR? - a short overview and history Information about CRM in COMAR How to get access to COMAR? Examples for searching by - CRM name or description - country or producer - physical property - conventional property - field of application - composition of elements or molecules Statistics 3
4 What is COMAR? COMAR has been developed to assist users in finding the reference materials they need Software and performance Oracle 8.1 database, internet interface PHP 4.0 Browser independent (Microsoft, Netscape, Opera) CRM information language is English Navigation language can be multilingual Update rights are given to the national or international coding centres CRM classification by harmonised catalogues 4
5 History French Laboratoire National d' Essais (LNE) proposed an index Code of Reference Materials in the late 1970s COde MAteriaux Reference --> COMAR COMAR was improved and established in the mid 80s by LNE (France), LGC (United Kingdom) and BAM (Germany) - not free of charge - floppy disks were updated and distributed once a year Today COMAR is supported by 16 national or international coding centres - free of charge for users since March available via internet and can be directly updated 5
6 COMAR coding centres AGAL/NARL Australia NCM Bulgaria BAM Germany NIST USA BIS India NITE Japan CANMET Canada NMi The Netherlands GUM Poland NRC-CRM China IRMM European Union SMU Slovakia LGC United Kingdom SP Sweden LNE France UNIIM Russian Federation 6
7 Statistics September CRMs from 248 producers in 25 countries Australia Germany South Africa Austria India Spain Brazil Japan Sweden Bulgaria Mexico Switzerland Canada Mongolia The Netherlands China Poland Ukraine Finland Russia-Federation United Kingdom France Slovakia United States European and international institutions: IRMM/BCR IAEA WHO 7
8 Distribution of CRM by fields of application - September 2003 Industrial 18% Ferrous 13% Quality of life 11% Non ferrous 25% Biological 3% Physical properties 15% Organic 5% Inorganic 10% 8
9 Contained CRM information Producer complete address of the producer Additional information (purchase, experts, QMS) (pdf files, if available) CRM name e.g. BAM-376 Description e.g. pure copper, Cu 99,5 Application description e.g. intended use Packaging / storage e.g. 40 g bottle; storage at -20 C Form of material e.g. disc Chemical composition Elements e.g. Ag µg/g Molecules (CAS-No.) e.g. alpha-hch ( ) 32.0 µg/kg Physical/conventional properties Physical properties (ISO-No.) e.g. Activity / kbq Conventional properties e.g. Flash point /ISO C Data files certificate, report, references (if available) Quality CRM, RM, setting-up sample, pharmacopoeia Status available, out of stock, under development 9
10 Login screen click button "Sign Up" 10
11 Sign Up Screen for registration 11
12 Start screen for users 12
13 Search by CRM name 13
14 Search by CRM name % = wildcard click button "Show Results" click button "Apply Filter" to start the search 14
15 Search by CRM name - show results 15
16 Search by CRM name - print preview 16
17 Search by CRM name - show results 17
18 Detailed information of the CRM (1) 18
19 Additional producer information 19
20 Detailed information of the CRM (2) 20
21 Certificate of the CRM "BAM-P123" 21
22 CRM search by description e.g. soil and sediment click button "+" to open input fields 22
23 CRM search by description e.g. soil and sediment type soil in the field description click button "Apply Filter" to start the search 23
24 CRM search by description e.g. soil and sediment button "+" to open the description fields 24
25 CRM search by description e.g. soil and sediment Boolean operators: A = and N = not O = or note: in the first line A and O = and button "Apply Filter" to start the search 25
26 Search by country or producer mark country and producer and click button "Apply Filter" to open the catalogues 26
27 Search by country or producer e.g. Germany select the country click button "+" 27
28 Search by country or producer select the producer click button "+" 28
29 Search by country or producer 29
30 Search by physical property e.g. dynamic viscosity ISO No [30-70Pa.s] select the physical property from the catalogue click button "+" 30
31 Search by physical property e.g. dynamic viscosity ISO No [30-70Pa.s] limit the search by the criteria minimum and maximum value click button "Apply Filter" to start search 31
32 Search by physical property e.g. dynamic viscosity ISO No [30-70Pa.s] 32
33 Search by fields of application e.g. quality of life / foodstuffs select "quality of life" from the catalogue click button "+" 33
34 Search by fields of application e.g. quality of life / foodstuffs select "foodstuffs" from the catalogue click button "+" 34
35 Search by fields of application e.g. quality of life / foodstuffs mark country and producer click button "Apply Filter" to open the catalogues 35
36 Search by fields of application e.g. quality of life / foodstuffs 36
37 Search by Fields of Application e.g. Quality of Life / Foodstuffs 37
38 Search by composition / element e.g. oxygen and nitrogen in steel select "O" from the catalogue click button "+" 38
39 Search by composition / element e.g. oxygen and nitrogen in steel select "N" from the catalogue click button "+" 39
40 Search by composition / element e.g. oxygen and nitrogen in steel limit the search by the criteria minimum and maximum value click the button "Apply Filter" 40
41 Search by composition / element e.g. oxygen and nitrogen in steel mark "Main Application" and click the button "Apply Filter" 41
42 Search by composition / element e.g. oxygen and nitrogen in steel 42
43 Search by composition / element e.g. oxygen and nitrogen in steel 43
44 Search by composition / molecule name e.g. alpha-hch and beta-hch mark "Molecule / CAS_No." and click button "Apply Filter" to open the catalogue 44
45 Search by composition / molecule name e.g. alpha-hch and beta-hch type "HCH" and click button "+" select "alpha-hch/ " from the catalogue click button "+" 45
46 Search by composition / molecule name e.g. alpha-hch and beta-hch select "beta-hch/ " from the catalogue click button "+" 46
47 Search by composition / molecule name e.g. alpha-hch and beta-hch 47
48 Search by composition / CAS_No. e.g. p,p -DDE CAS mark "Molecule / CAS-No." type the CAS_No. click button "Apply Filter" 48
49 Search by composition / CAS_No. e.g. p,p -DDE CAS select "p.p'-dde / " click button "+" 49
50 Search by composition / CAS_No. e.g. p,p -DDE CAS select "4,4'-DDE/ " click button "+" 50
51 Search by composition / CAS_No. e.g. p,p -DDE CAS change the operator and click "Apply Filter" 51
52 Amount of CRM Country Australia 4 Austria 93 Brazil 61 Bulgaria 212 Canada 377 China 1008 European Union (IRMM) 714 Finland 3 France 1188 Germany 888 India 59 Japan 870 Mexico 27 Mongolia 17 Poland 76 Russian Federation 708 Slovakia 233 South Africa 59 Spain 14 Sweden 253 Switzerland 253 The Netherlands 81 UK 2265 Ukraine 12 USA 1031 SUM of CRMs
53 Development of user accounts date number of users
54 User's origin Argentina Estonia Korea South Korea Australia Finland Latvia Slovakia Austria France Luxemburg Slovenia Belgium Germany Malaysia Spain Brazil Greece Mexico Sweden Bulgaria Guatemala Mongolia Switzerland Canada Hong Kong Netherlands Taiwan Chile India New Zealand Turkey China Ireland Norway UK Cuba Israel Poland Ukraine Czechia Italy Portugal USA Denmark Japan Russia Vietnam further users of unknown origin (e.g.:.com,.org) 54
55 Access and search date COMAR login and search approx. number of access COMAR login viewed search results COMAR login viewed search results COMAR login viewed search results COMAR login viewed search results COMAR login viewed search results
56 You are kindly invited to visit and use COMAR! 56
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