LABS & TECHNOLOGICAL SERVICES AGQ S L CTRA A-423 KM24.3 BURGUILLOS (SEVILLA) SPAIN

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1 This is to signify that LABS & TECHNOLOGICAL SERVICES AGQ S L CTRA A-423 KM24.3 BURGUILLOS (SEVILLA) SPAIN Testing Laboratory TL-475 (Revision May 16, 2013) has met the requirements of the IAS Accreditation Criteria for Testing Laboratories (AC89), has demonstrated compliance with ISO/IEC Standard 17025:2005, General requirements for the competence of testing and calibration laboratories, and has been accredited, commencing, for the test methods listed in the approved scope of accreditation. Patrick V. McCullen Vice (see attached scope of accreditation for fields of testing and accredited test methods) Print Date: 8/13/2013 Page 1 of 11

2 Labs & Technological Services AGQ S L Arantxa Benito Navarro Ctra A-423 Km24.3 Lab Manager Burguillos (Sevilla) Spain Multi-Element Analysis (Ag, Al, As, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe, K, Li, Mg, Mn, Mo, Na, Ni, P, Pb, S, Sb, Sn, Sr, Ti, Tl, V, Zn) PE-4006, ICP-OES and Aqua Regia Digestión Metallic Ores and High Grade Material Metallic Ores Multi-Element Analysis (Ag, Al, As, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe, K, Li, Mg, Mn, Mo, Na, Ni, P, Pb, S, Sb, Sn, Sr, Ti, Tl, V, Zn) Gold and Silver PE-4006, ICP-OES and 4 Acid Digestion PE-4008, AA Analysis and Fire Assay PE-4014, ICP-OES Analysis and Fire Assay Print Date: 8/13/2013 Page 2 of 11

3 Metallic Ores (continued) Total S PE-4015, Elemental Analyzer Wolframium PE-4019, ICP-MS Analysis and Acid Digestion High Grade Material Gold, Silver, Palladium and Platinum PE-4014, ICP-OES Analysis Total Sulphate Metallic Ores PE-4005, Gravimetric Methods Elemental S PE-4004, Gravimetric Methods Copper PE-4009, Volumetric Methods High Grade Material Zinc PE-4010, Volumetric Methods Lead PE-4011, Volumetric Methods Iron PE-4012, Volumetric Methods Metallic Ores Total Sulphide PE-4016, Calculation Methods Print Date: 8/13/2013 Page 3 of 11

4 Metallic Ores Multi-Element Analysis (Al, Ca, Cr, Fe, K, Mg, Mn, P, Si) PE-4006, ICP-OES and Alkaline Fusion/ Acid Digestion Acid Soluble Copper PE-4020, ICP-OES Analysis and Acid Extraction Cyanide Soluble Copper PE-4021, ICP-OES Analysis and Cyanide Extraction Wolframium PE-4022, ICP-OES Analysis and Acid Digestion Uranium and Thorium PE-4023, ICP-MS Analysis and 4 Acids Digestion Matrices, Wine Acefato, Acetocloro, Acrinatrina, Alacloro, Aldrín (SP), Amitraz (SP), Atrazina, Azinfos Etil, Azinfos Metil, Benalaxil (SP), Benfluralin, Bifenazato, Bifenilo, Bifentrin, Bitertanol, Bromofos Metil, Bromopropilato, Bupirimato (SP), Buprofezin, Captan, Carbaril, Carbofenotion, Carbosulfan, Ciflutrin, Cipermetrina, Ciproconazol, Ciprodinil, Clorbenzilat, Clordano, Clorfenapir, Clorfenvinfos, Cloropropilato, Clorpirifos Etil, Clorpirifos Metil, Clorprofam (SP), Clortal- Dimetil, Clortalonil, Clortoluron, Cyhalotrin-L, PE-614 Determination of Pesticide Residue using Chromatography (GC-MS-MS) Print Date: 8/13/2013 Page 4 of 11

5 DDD-pp+DDT-pp, Deltametrina, Diafenturion, Diazinon, Diclobenil, Diclofluanida Diclofention, Dicloran, Diclorvos, Dicofol, Dicrotofos, Dieldrin (SP), Dieldrin Suma (SP), Difenilamina, Difenoconazol, Diflufenican, Diniconazol, Dinobuton, Disulfuton, Disulfuton (Sum), Ditalimfos, Diuron, Endosulfan (A+B+Sulf), Endosulfan Alfa, Endosulfan Beta, Endosulfan Sulfato, Endrin, Etalfluralin, Etion, Etofumesato Disulfuton Sulfona, Disulfuton Sulfoxido, (SP), Etoprofos, Etoxiquina, Etrimfos, Fenamifos, Fenarimol, Fenazaquin, Fenitrotion, Fenoxicarb, Fenpropatrin, Fensulfotion, Fention (SP), Fentoato, Fenv+Esfenvalerato, Fluazifop-Butil, Flucitrinato, Fludioxonil, Fluquinconazol, Flusilazol, Flutriafol, Fluvalinato Tau, Folpet, Fonofos, Fosalone, Fosmet (SP), Furalaxil, Heptacloro (SP), Heptenofos, Hexaclorobenceno, Hexaclorobutadieno, Hexaconazol, Imazalil, Iprodiona, Iprovalicarb, Isazofos, Isofenfos, Isofenfos Metil, Kresoxim Metil, Lindano, Malation (SP), Mecarbam, Mepronil, Metacrifos, Metalaxil (SP), PE-614 Determination of Pesticide Residue using Chromatography (GC-MS-MS) Print Date: 8/13/2013 Page 5 of 11

6 Metamidofos, Metazaclor, Metidation, Metiocarb (SP), Metoxiclor, Metribuzin, Mevinfos, Miclobutanilo, Mirex, Molinato, Naled, Napropamida, Nuarimol, o,p-ddt, Ofurace, Ortofenilfenol, Oxadiazon, Oxadixil, Oxifluorfen, p,p-dde, Paclobutrazol, Paration Etil, Paration Metil (SP), Penconazol, Pendimetalina, Pentacloroanilina, Pentacloroanisol, Pentaclorobenceno, Permetrina, Piperonil Butoxido, Pirazofos, Piridaben, Piridafention Pirifenox, Pirimetanil, Pirimicarb (SP), Pirimifos Etil, Pirimifos Metil, Piriproxifen, Procimidona, Procloraz (SP), Profam, Profenofos, Profluralin, Prometrina, Propargita, Propiconazol, Propizamida, Protiofos, Quinalfos, Quinometionato, Quintoceno, Quintoceno Suma, Simazina, Sulfotep, Tebuconazol, Tebufenpirad, Tecnazen, Teflutrin, Terbacil, Terbufos, Terbutilazina, Terbutrin, Tetraclorvinfos, Tetraconazol, Tetradifon, Tetrametrina, Tiometon, Tolclofos Metil, Tolilfluanida (SP), Transflutrin, Triadimefon (SP), Triadimenol (SP), PE-614 Determination of Pesticide Residue using Chromatography (GC-MS-MS) Print Date: 8/13/2013 Page 6 of 11

7 Triazofos, Triciclazol, Triclorfon, Trifluralin, Uniconazol-p, Vinclozolina (SP), Zoxamida. Pirifenox, Pirimetanil, Pirimicarb (SP), Pirimifos Etil, Pirimifos Metil, Piriproxifen, Procimidona, Procloraz (SP), Profam, Profenofos, Profluralin, Prometrina, Propargita, Propiconazol, Propizamida, Protiofos, Quinalfos, Quinometionato, Quintoceno, Quintoceno Suma, Simazina, Sulfotep, Tebuconazol, Tebufenpirad, Tecnazen, Teflutrin, Terbacil, Terbufos, Terbutilazina, Terbutrin, Tetraclorvinfos, Tetraconazol, Tetradifon, Tetrametrina, Tiometon, Tolclofos Metil, Tolilfluanida (SP), Transflutrin, Triadimefon (SP), Triadimenol (SP), Triazofos, Triciclazol, Triclorfon, Trifluralin, Uniconazol-p, Vinclozolina (SP), Zoxamida. 2,4-D, Abamectina, Acetamiprid (SP), Aclonifen, Aldicarb, Aldicarb (Sum), Aldicarb Sulfona, Aldicarb Sulfoxido, Azoxistrobin, Bendiocarb, Benfuracarb, Benomilo-Carbendazima, Bentazona (SP), Bentiavalicarb Isopropil, Boscalid, Bromacilo, Bromoxinil, Bromuconazol, Butoxicarboxim, Cadusafos, Captafol, PE-614 Determination of Pesticide Residue using Chromatography (GC-MS-MS) Print Date: 8/13/2013 Page 7 of 11

8 Carbofuran (SP), Chlorantraniliprole, Ciazofamida, Cicloxidim (SP), Cimoxanilo, Ciromazina, Cletodim, Clofentezina, Clomazona, Clopiralid, Cloridazon, Clothianidin (SP), Demeton S-Metil (SP), Demeton-S-Metil Sulfoxido (SP), Desmedifam, Diclofop, Diclormid, Diclorprop, Dietofencarb, Diflubenzuron, Dimetoato (SP), Dimetoato Suma, Dimetomorf, Dinocap (SP), Dodemorf, Dodina, Emamectina Benzoato, Epoxiconazol, Espinetoram, Espinosad (A+D), Espirodiclofen, Espiromesifen, Espirotetramat, Espiroxamina, Etiprol, Etofenprox, Etoxazol, Famoxadona, Fenamidona, Fenbuconazol, Fenexamida, Fenmedifam, Fenpiroximato, Fenpropidin, Fenpropimorf, Fipronil (SP), Flazasulfuron, Flonicamid (SP), Fluacinam, Flubendiamida, Flufenacet, Flufenoxuron, Fluometuron, PE-614 Determination of Pesticide Residue using Chromatography (GC-MS-MS) Print Date: 8/13/2013 Page 8 of 11

9 Fluopicolid, Fluotrimizole, Flutolanil, Forato, Forato (Sum), Forato Sulfona, Forato Sulfoxido, Forclorfenuron, Formetanato, Fostiazato, Furatiocarb, Hexaflumuron, Hexitiazox, Himexazol, Imazamox, Imidacloprid (SP), Indoxacarb, Ioxinil (SP), Isocarbofos, Isoproturon, Isoxaben, Lenacilo, Linurón, Lufenuron, MCPA, Mepanipirim (SP), Metaflumizona, Metamitron, Metil Tiofanato (SP) Metoalacloro, Metolcarb, Metomilo (SP), Metomilo Suma, Metoxifenoxida, Metoxuron, Metrafenona, Milbectina, Monocrotofos, Monolinuron, Nicosulfuron, Nitenpiram, Novaluron, Ometoato (SP), Oxadiargil, Oxamilo, Oxicarboxina, Pencicuron, Picoxistrobin, Pimetrocina, Piraclostrobin, Pirididato, Propamocarb, Propanilo, Propaquizafop, Propoxur, Proquinazida, Prosulfocarb, Quinclorac, Quinmerac, Quinoxifen, PE-618 Determination of Pesticide Residue using Chromatography (LC-MS-MS) Print Date: 8/13/2013 Page 9 of 11

10 Labs & Technological Services AGQ S L TL-475 Quizalofop-Ethyl (SP), Rimsulfuron, Rotenona, Sulcotriona, Tebufenocida, Teflubenzuron, Thiametoxam Suma, Thiametoxan (SP), Tiabendazol, Tiacloprid, Tiociclam, Tiodicarb (SP), Triclopir, Tridemorf, Trifloxistrobin, Triflumizol (SP), Triflumuron, Triforina. Fish, Canned Fish and Wine Hystamine Nuts Aflatoxins (B1, B2, G1, G2) Coffee, Wine, Beer and Dried Fruits Cereal, Nuts Ocratoxin A Micotoxins Fruits, Vegetables Dithiocarbamates (as CS 2) PE-618 Determination of Pesticide Residue using Chromatography (LC-MS-MS) PE-516 Determination of Residues of Hystamine by LC/MS-MS Chromatography PE-519 Determination of Aflatoxins B & G by LC/MS-MS Chromatography PE-520 Determination of Ochratoxin by LC/MS-MS Chromatography PE-505 Determination of Micotoxins by LC/MS-MS Chromatography PEC-032 Determination of Dithiocarbomates through Spectrophotometric ultraviolet visible spectrophotometry Print Date: 8/13/2013 Page 10 of 11

11 Wine, Cork Trichloroanisole (TCA) (2,4,6-Trichloroanisole 2,3,4,6-Tetrachloroanisole PE 657 Anisoles Determination in wine and cork by extraction with PDM/S (Twisters TM ) Stirring Bars 2,4,6-Tribromoanisole, Pentachloroanisole) Drinking Water Plate Count of Aerobic Microorganisms at 22ºC PE-401 Total Bacterial count at 22 o C, 31 0 C and 37 0 C in water Water (all type) Total Coliform Count (Filtration) PE-402 Total Coliforms count in Waters (Filtration) Fecal Coliform Count (Filtration) PE-403 Fecal Coliforms in Waters (Filtration) Escherichia coli Count (Filtration) PE-425 Escherichia coli count in water Intestinal Enterococci Counts (Filtration) PE-423 Intestinal Enterococci Count in Waters (Filtration) Clostridiums Perfringens Count (Filtration) PE-433 Clostridiums perfringens count in Waters (Filtration) Food Plate Count of Aerobic Microorganisms at 30º C PE-407 Plate Count of Aerobic Microorganisms in Food Plate Count of Staphilococcus Aureus PE-417 Count Coagulase-positive Staphylococci in Food Plate Count of Escherichia Coli PE-410 Count glucuronidase positive Escherichia coli in Food Sallmonella Spp Investigation PE-413 Sallmonella Spp Investigation in Food Listeria Monocytogenes Investigation PE-428 Listeria Monocytogenes Investigation in Food Print Date: 8/13/2013 Page 11 of 11

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