This is to signify that

Transcription

1 This is to signify that PROFESYONEL ÇEVRE ANALIZ LAB. GIDA TARIMSAL VE KAL. HIZ. SAN. VE TIC. A.Ş TEOMANPAŞA MAH.GAZI BULVARI NO: 345 KEPEZ, ANTALYA TURKEY Testing Laboratory TL-577 has met the requirements of the IAS Accreditation Criteria for Testing Laboratories (AC89), has demonstrated compliance with ISO/IEC Standard 17025:2005, General requirements for the competence of testing and calibration laboratories, and has been accredited, commencing, for the test methods listed in the approved scope of accreditation. Patrick V. McCullen Vice, Chief Technical Officer (see attached scope of accreditation for fields of testing and accredited test methods) Print Date: 4/8/2015 Page 1 of 12

2 Profesyonel Çevre Analiz Lab. Gıda Tarımsal ve Kal. Hiz. San. ve Tic. A.Ş Ulas Goktas Teomanpaşa Mah. Gazi Bulvarı No: 345 Laboratory Manager Kepez, Antalya Turkey FIELDS OF TESTING ACCREDITED TEST METHODS Category Product Group Microbiology Food and Animal Feed ISO : Analysis of E.coli (membrane method) in food and animal feed, TS EN ISO 6579 (ISO 6579): Detection of Salmonella spp. in Food and animal feed, TS 3522: Analysis of rope spore in food and animal feed, BS ISO: : Analysis of Enterobacteriaceae in food and animal feed, TS EN ISO 7937 (ISO 7937): Analysis of Sulfite reducing anaerobes (Clostridium perfringens) in Food and animal feed, TS EN ISO (ISO ): Analysis of Mesophilicaerobicbacteria in foodandanimalfeed, ISO : Analysis of E.coli in food and animal feed, ISO / AMD 1: Detection of Listeria monocytogenes in food and animal feed, ISO 16654: Detection of E.coli O157 in food and animal feed, TS ISO 4832: Analysis of Coliform bacteria in food and animal feed, ISO : Analysis of E.coli (most probable number method-ems) in food and animal feed, ISO TS 22964: Detection of Enterobacter (Cronobacter) sakazakii in food and animal feed, TS EN ISO (ISO ): Analysis of Coagulase-positive staphylococci in food and animal feed, TS EN ISO 7932 (ISO 7932): Analysis of Bacillus cereus in food and animal feed, AOAC Official Method : Detection of Staphylococcal enterotoxinin food and animal feed, ISO : Detection of V. parahaemolyticus, V. cholerae in food and animal feed, TS ISO (ISO ): Yeast, mold analysis (water activity greater than 0.95) in food and animal feed TS ISO : Yeast, mold analysis (water activity of less than 0.95) in food and animal feed. Water XP T Membran Filter: Analysis of Pathogen Staphylococcus in water, TS EN ISO ISO 6222 (ISO 6222): Analysis of culturable water (22 C and 36 C), TS EN ISO Membrane Filter (ISO ): Analysis of E. colicoliform bacteria in water, Print Date: 4/8/2015 Page 2 of 12

3 FIELDS OF TESTING ACCREDITED TEST METHODS Category Product Group Microbiology (continued) Water ISO 16266/Membrane Filter: Analysis of Pseudomonas aeruginosa in water, TS EN ISO Membrane Filter (ISO ): Analysis of Enterococcus in water, ISO Membrane Filter: Detection of Legionella in water, BS ISO MEMBRANE FILTER: Detection of Salmonella spp.in water. Surfaces BS ISO ISO : Analysis of E. coli on all surfaces that come into contact with food, BS ISO TS EN ISO 7932: Analysis of B. cereus on all surfaces that come into contact with food, BS ISO TS EN ISO : Analysis of S. aureus on all surfaces that come into contact with food, BS ISO TS ISO 4832: Analysis of coliform bacteria on all surfaces that come into contact with food, BS ISO TS EN ISO (ISO ) Analysis of Total mesophilic aerobic bacteria on all surfaces that come into contact with food, BS ISO TS EN ISO 6579: Detection of Salmonella spp. on all surfaces that come into contact with food. Cosmetics ISO 21150: Analysis of E.coli in cosmetics, ISO 22717: Analysis of Pseudomonas aeruginosa in cosmetics, ISO 22718: Analysis of Staphylococcus aureus in cosmetics, ISO 16212: Analysis of yeast and mouldin cosmetics, ISO 21149: Analysis of Mesophilic aerobic bacteria in cosmetics, Biotechnology Meat and Meat Products DIAGEN study protocol/elisa-tek Cooked meat speciation kits:determination of types of meat and meat products Pesticide Fresh Vegetables and EN (Quechers) * Fruits Dried Vegetables and AOAC Method (Quechers): Pesticide Analysis * Fruits Whole Grains All of Feed and Feed Additives, Oil seeds All Spices All Dried Fatty Fruits (Dried Fruits) All of Feed and Feed Additives Mycotoxins All Dried Vegetables and Fruits All Spices Rapid Communications In Mass Spectrometry Rapid Commun. Mass Spectrom.2006; 20: : Analysis of Aflatoxin B1 and Total Aflatoxin (B1 + B2 + G1 + G2) Print Date: 4/8/2015 Page 3 of 12

4 FIELDS OF TESTING ACCREDITED TEST METHODS Category Product Group Mycotoxins (continued) All Dried Fatty Fruits (Dried Fruits) All of Feed and Feed Additives Chemistry Vegetables and Fruits TSE 6183: Determination of nitrite-nitrate in foods All fishery Products All Water and Pool Water Rapid Communications In Mass Spectrometry Rapid Commun. Mass Spectrom.2006; 20: : Analysis of Aflatoxin B1 and Total Aflatoxin (B1 + B2 + G1 + G2) In house method Journal of Chromatography B, 693 (1997) HPLC Determination of Biogenic Amines in fish implicated in food poisoning: Analyses of histamine. TS 7159: Determination of Ammonium by spectrophotometric method, TS EN 26777: Determination of Nitrite, TS ISO 10566: Determination of aluminum by spectrophotometric method, TS 6231: Determination of Nitrate by spectrophotometric method, TS EN ISO 10523: Determination of ph, TS EN 27888: Determination of Electrical Conductivity, T.96 (SOP) In house method (using TS EN 902): Determination of hydrogen peroxide by the titrimetric method, TS EN ISO : Determination of total and composite alkalinity by the titrimetric method, Apha SM 3500-Cu C.BathoCuproine Method: Determination of copper (Cu) by spectrophotometric method, TS EN ISO : Determination of the free and bound chlorine by the colorimetric method, T.64 (SOP) In house method: "Photometric determination of the free and bound chlorine in water and pool water". T.79 (SOP) In house method (Analytical Chemistry, Vol.73, No.14:2001): Determination of cyanuric acid by HPLC, T-179 (SOP) In house method: Determination of cyanuric acid by spectrophotometric method Apha SM 2130-B Nephelometric Method: Determination of turbidity by the nephelometric method, Apha SM 2120-C: Determination of the color by spectrophotometric method - wavelength-to-multipoint, Apha SM 2550-B: Determination of temperature, T-47 (SOP) In house method: Biguanid. Chemistry Soil TS 8336: Determination of organic matter (Walkley-Black Method), TS 8333: Determination of water saturation (soil texture), TS ISO 11261: Determination of total nitrogen (Improved Kjeldahl Method), TS 8334: Determination of Salt, TS ISO 10390: Determination of ph, TS ISO 11265: Determination of Electrical Conductivity Print Date: 4/8/2015 Page 4 of 12

5 FIELDS OF TESTING Category Product Group Chemistry Fertilizer (continued) ACCREDITED TEST METHODS TS ISO 5073: Determination of Humic-Fulvic, TS EN TS EN Turkish Gazette No Regulation of Market Surveillance and Control of fertilizer charter an additional 3 or annex 3,AOAC : Determination of ammonium nitrogen, nitrate nitrogen in chemical fertilizers, TS ISO 10390: Determination of ph in chemical and organic fertilizers, TS ISO 11265: Determination of Electrical Conductivity, AOAC AOAC TS 2832: Determination of organic matter in organic fertilizers, TS 2832, Kacar- Kütük 2009:Determination of moisture content of fertilizers, TS 6798-DUMAS 1962 BREMNER 1965: Determination of total nitrogen (Dumas Method), Turkish Official Gazette No Regulation of Market Surveillance and Control of fertilizer charter an additional 3 or annex 3, TS 2832, TS EN 15958: Determination of water soluble phosphorus in chemical fertilizer, TS 2832, Turkish Official Gazette No Regulation of Market Surveillance and Control of fertilizer (annex 3), TS EN 15604: Determination of urea nitrogen, Turkish Official Gazette No Regulation of Market Surveillance and Control of fertilizer (annex 3), TS EN 15961: Determination of water soluble sulfur dioxide in chemical fertilizers, Turkish Official Gazette No Regulation of Market Surveillance and Control of fertilizer (annex 3), TS EN 15925: Determination of total sulfur, Turkish Official Gazette No Regulation of Market Surveillance and Control of fertilizer (annex 3), TS 2832/ TS EN 15477: Determination of water-soluble potassium in chemical fertilizer Chemicals Cosmetics T.188 (SOP) In house method: About required Composition Analysis Methods for the Control of Cosmetic Products Notification No:İEG/2005/2: Analysis of Alcohol (methanol) in cosmetics (non-aerosol samples only) T.189 (SOP) In house method (J.Chem.Pharm.Res.,2010,2(6):92-97): Analysis of Heavy Metal ; Lead(Pb), Cadmium(Cd), Arsenic(As), Tin(Sn), Nickel(Ni), Mercury(Hg) in cosmetics Sampling Water TS EN ISO TS EN ISO TS EN ISO : Taking Water samples Microbiological Sampling Notes: TS - Turkish Standards Water TS EN ISO 19458: Taking Water Sampling for microbiological analysis Print Date: 4/8/2015 Page 5 of 12

6 Table 1. List of pesticides that can be traced. 1 2,4,D LC-MS/MS 2 2,4-5T GC-MSD Dichlorobenzophenone GC-MSD 4 Acephate LC-MS/MS 5 Acetamiprid LC-MS/MS 6 Acetochlor LC-MS/MS 7 Acibenzolar-S-methyl LC-MS/MS 8 Aclonifen LC-MS/MS 9 Acrinathrin LC-MS/MS 10 Alachlor LC-MS/MS 11 Aldicarb LC-MS/MS 12 Aldicarb-sulfone LC-MS/MS 13 Aldicarb-sulfoxide LC-MS/MS 14 Aldrin (HHDN) GC-MSD 15 Alpha-Cypermethrin GC-MSD 16 Alpha-Endosulfan GC-MSD 17 Amitraz LC-MS/MS 18 Anilazine LC-MS/MS 19 Atrazine LC-MS/MS 20 Azinphos-ethyl LC-MS/MS 21 Azinphos-methyl LC-MS/MS 22 Azimsulfuron LC-MS/MS 23 Azoxystrobin LC-MS/MS 24 Bendiocarb LC-MS/MS 25 Benfuracarb LC-MS/MS 26 Beta-Cyfluthrin GC-MSD 27 Beta-Endosulfan GC-MSD 28 Bifenthrin LC-MS/MS 29 Bitertanol LC-MS/MS 30 Bromacil LC-MS/MS 31 Bromophos-ethyl LC-MS/MS 32 Bromopropylate GC-MSD 33 Bromoxynl LC-MS/MS 34 Bromuconazole LC-MS/MS 35 Bupirimate LC-MS/MS 36 Buprofezin LC-MS/MS 37 Butralin LC-MS/MS 38 Cadusafos LC-MS/MS 39 Captafol GC-MSD 40 Captan GC-MSD Print Date: 4/8/2015 Page 6 of 12

7 41 Carbaryl LC-MS/MS 42 Carbendazim,Benomyl LC-MS/MS 43 Carbofuran LC-MS/MS 44 Carbosulfan LC-MS/MS 45 Carboxin LC-MS/MS 46 Carfentrazone-ethyl LC-MS/MS 47 Chlorfenson GC-MSD 48 Chlorfenvinphos LC-MS/MS 49 Chlorfluazuron LC-MS/MS 50 Chloridazon LC-MS/MS 51 Chlorobenzilate GC-MSD 52 Chlorothalonil GC-MSD 53 Chloroxuron LC-MS/MS 54 Chlorpropham LC-MS/MS 55 Chlorpyrifos LC-MS/MS 56 Chlorpyrifos-methyl LC-MS/MS 57 Chlorsulfuron LC-MS/MS 58 Cinidon-ethyl LC-MS/MS 59 Clofentezine LC-MS/MS 60 Cyanazine LC-MS/MS 61 Cycloate GC-MSD 62 Cyfluthrin GC-MSD 63 Cymoxanil LC-MS/MS 64 Cypermethrin GC-MSD 65 Cyproconazole LC-MS/MS 66 Cyprodinil LC-MS/MS 67 Cyromazine LC-MS/MS 68 Daminozide LC-MS/MS 69 Dazomet GC-MSD 70 Deltamethrin GC-MSD 71 DDD-2.4'- GC-MSD 72 DDD-4.4'- GC-MSD 73 DDE-2.4'- GC-MSD 74 DDE-4.4'- GC-MSD 75 DDT-2.4'- GC-MSD 76 DDT-4.4'- GC-MSD 77 Dialifos LC-MS/MS 78 Diazinon LC-MS/MS 79 Dicamba GC-MSD 80 Dichlofluanıde LC-MS/MS 81 Dichlorvos (DDVP) LC-MS/MS 82 Diclofop-methyl LC-MS/MS Print Date: 4/8/2015 Page 7 of 12

8 83 Dicofol GC-MSD 84 Dicrotophos LC-MS/MS 85 Diethofencarb LC-MS/MS 86 Difenconazole LC-MS/MS 87 Diflubenzuron LC-MS/MS 88 Dimethoate LC-MS/MS 89 Dimethomorph LC-MS/MS 90 Diniconazole LC-MS/MS 91 Dinobuton GC-MSD 92 Dinocap LC-MS/MS 93 Diphenamid LC-MS/MS 94 Diphenylamine GC-MSD 95 Disulfoton LC-MS/MS 96 Ditalimfos LC-MS/MS 97 Dithianon LC-MS/MS 98 Diuron LC-MS/MS 99 Dodine LC-MS/MS 100 Endrin GC-MSD 101 Endosulfan GC-MSD 102 Epoxiconazole LC-MS/MS 103 Esfenvalerate GC-MSD 104 Ethalfluralin GC-MSD 105 Ethiofencarb LC-MS/MS 106 Ethion LC-MS/MS 107 Ethofumesate LC-MS/MS 108 Ethoprophos LC-MS/MS 109 Etofenprox LC-MS/MS 110 Etrimfos LC-MS/MS 111 Famoxadone LC-MS/MS 112 Fenamıdone LC-MS/MS 113 Fenamiphos LC-MS/MS 114 Fenarimol LC-MS/MS 115 Fenbuconazole LC-MS/MS 116 Fenazaquın LC-MS/MS 117 Fenhexamid LC-MS/MS 118 Fenitrothion LC-MS/MS 119 Fenoxycarb LC-MS/MS 120 Fenpropathrin LC-MS/MS 121 Fenpropimorph LC-MS/MS 122 Fenthion LC-MS/MS 123 Fenvelarate GC-MSD 121 Fenpropimorph LC-MS/MS Print Date: 4/8/2015 Page 8 of 12

9 122 Fenthion LC-MS/MS 123 Fenvelarate GC-MSD 124 Fipronil LC-MS/MS 125 Flubenzimine LC-MS/MS 126 Flucythrinate LC-MS/MS 127 Fludioxonil LC-MS/MS 128 Flufenoxuron LC-MS/MS 129 Fluorochloridone LC-MS/MS 130 Fluroxypyr LC-MS/MS 131 Flusilazole LC-MS/MS 132 Folpet GC-MSD 133 Formetanate-hydroclor LC-MS/MS 134 Formothion GC-MSD 135 Furathiocarb LC-MS/MS 136 gamma-hch (Lindane) GC-MSD 137 Haloxyfop-2-ethoxy-ethyl LC-MS/MS 138 Hexachlorobenzene GC-MSD 139 Hexaconazole LC-MS/MS 140 Hexaflumuron LC-MS/MS 141 Hexythiazox LC-MS/MS 142 Imazalil LC-MS/MS 143 Imiadcloprid LC-MS/MS 144 Ioxynil LC-MS/MS 145 Iprodione LC-MS/MS 146 Iprovalicarb LC-MS/MS 147 Isoproturon LC-MS/MS 148 Isoxafluate LC-MS/MS 149 Kresoxim-methyl LC-MS/MS 150 Lambda-Cyhalothrin GC-MSD 151 Lenacil LC-MS/MS 152 Linuron LC-MS/MS 153 Lufenuron LC-MS/MS 154 Malaoxon LC-MS/MS 155 Malathion LC-MS/MS 156 Mecarbam LC-MS/MS 157 Mesotrione LC-MS/MS 158 Metobromuron LC-MS/MS 159 Metalaxyl-Metalaxyl M LC-MS/MS 160 Metamitron LC-MS/MS 161 Methacrifos LC-MS/MS 162 Methamidophos LC-MS/MS 163 Methidathion LC-MS/MS Print Date: 4/8/2015 Page 9 of 12

10 164 Methoxychlor GC-MSD 165 Metolachlor LC-MS/MS 166 Metribuzin LC-MS/MS 167 Metsulfuron-methyl LC-MS/MS 168 Mevinphos LC-MS/MS 169 Molinate LC-MS/MS 170 Monocrotophos LC-MS/MS 171 Monolinuron LC-MS/MS 172 Myclobutanil LC-MS/MS 173 Nicosulfuron LC-MS/MS 174 Nitrofen GC-MSD 175 Nitrothal-isopropyl GC-MSD 176 Nuarimol LC-MS/MS 177 Omethoate LC-MS/MS 178 Oxadiazon LC-MS/MS 179 Oxadixyl LC-MS/MS 180 Oxamyl LC-MS/MS 181 Oxyfluorfen LC-MS/MS 182 Parathion-ethyl LC-MS/MS 183 Parathion-methyl LC-MS/MS 184 Penconazole LC-MS/MS 185 Pencycuron LC-MS/MS 186 Pendimethalin LC-MS/MS 187 Permethrin GC-MSD 188 Phenmedipham GC-MSD 189 Phenthoate LC-MS/MS 190 Phorate LC-MS/MS 191 Phosalone LC-MS/MS 192 Phosmet LC-MS/MS 193 Phoxim LC-MS/MS 194 Picolinafen LC-MS/MS 195 Pirimicarb LC-MS/MS 196 Pirimiphos methyl LC-MS/MS 197 Pirimiphos-ethyl LC-MS/MS 198 Prochloroz LC-MS/MS 199 Procymidone GC-MSD 200 Profenofos LC-MS/MS 201 Profoxydim-lithium LC-MS/MS 202 Propargite LC-MS/MS 203 Propazine LC-MS/MS 204 Propham LC-MS/MS 205 Propiconazole LC-MS/MS Print Date: 4/8/2015 Page 10 of 12

11 206 Propoxur LC-MS/MS 207 Propyzamide LC-MS/MS 208 Prosulfuron LC-MS/MS 209 Prothiopfos LC-MS/MS 210 Pyrazophos LC-MS/MS 211 Pyridaben LC-MS/MS 212 Pyridaphenthion LC-MS/MS 213 Pyrıdate LC-MS/MS 214 Pyriproxyfen LC-MS/MS 215 Quaizalofop_p_ethyl LC-MS/MS 216 Quinalphos LC-MS/MS 217 Qunomethionate GC-MSD 218 Quintozene GC-MSD 219 Resmethrin LC-MS/MS 220 Rimsulfuron LC-MS/MS 221 Simazine LC-MS/MS 222 Spiroxamine LC-MS/MS 223 Tau-fluvalinate GC-MSD 224 Tebuconazole LC-MS/MS 225 Tebufenozide LC-MS/MS 226 Tecnazene GC-MSD 227 Teflubenzuron LC-MS/MS 228 Terbuthylazine LC-MS/MS 229 Terbutryn LC-MS/MS 230 Tetradiphon GC-MSD 231 Tetrasul GC-MSD 232 Thiabendazole LC-MS/MS 233 Thiamethoxam LC-MS/MS 234 Thiodicarb LC-MS/MS 235 Thiophanate-methyl LC-MS/MS 236 Tolyfluanid GC-MSD 237 Tralkoxydim LC-MS/MS 238 Triadimefon LC-MS/MS 239 Triadimenol LC-MS/MS 240 Triallate (Tri-allate) LC-MS/MS 241 Triazophos LC-MS/MS 242 Tribenuron-methyl LC-MS/MS 243 Trichlorfon LC-MS/MS 244 Tridemorph LC-MS/MS 245 Trifloxystrobin LC-MS/MS 246 Triflumizole LC-MS/MS 247 Trifluralin GC-MSD Print Date: 4/8/2015 Page 11 of 12

12 248 Triphenylphosphate LC-MS/MS 249 Vamidothion LC-MS/MS 250 Vinclozolin GC-MSD 251 α (alpha)- HCH GC-MSD 252 β (beta) - HCH GC-MSD *List of pesticides that can be traced is on Table 1 Print Date: 4/8/2015 Page 12 of 12