Keskin Color Kartpostalcılık A.Ş. Neslihan Sözer Chemical Laboratory Manager

Transcription

1 TEST REPORT Page 1 of 6 REPORT NUMBER : TURA APPLICANT NAME ADDRESS Keskin Color Kartpostalcılık A.Ş. Bağlar Mah. Çeşmealtı Sk.No:23 Istanbul FAX NO : Attention : Muhiddin Keskin (mkeskin@keskincolor.com) SAMPLE DESCRIPTION : BUYER : 16.5*22.5 cm Funky Designed 100 Page Notebook TÜKİD DATE IN : 26 July, 2012 (13:59) DATE OUT : 02 August, 2012 ARTICLE NO : PHOTO OF PRODUCT TESTED : Part No Tested Part 1 BEIGE COVER WITH PRINT 2 YELLOW STRIPED PAGE 3 METAL WIRE Füsun Karaoğlu Coordinator Neslihan Sözer Chemical Laboratory Manager Merkez Mahallesi Sanayi Cad. No: 23 Altındağ Plaza Yenibosna ISTANBUL / TURKEY * * ssenturk

2 R E S U L T S Page 2 of 6 REPORT : TURA August, 2012 RESULTS : Analysis Parameter Reference Analysis Method PASS FAIL Norm Limit Standard for Norm Limit Tested Part Azo Dyes 64 LFBG B P - 30 ppm 2004/21/EC Part 1-2 Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Toxic Element Cd: 75 ppm BS EN 71-3:1995 P - Analysis Cr: 60 ppm Pb: 90 ppm Hg: 60 ppm Se: 500 ppm EN 71-3 Part 1-3 Phthalate EN by GC MS P - DBP/DEHP/BBP : 1000 ppm DINP/DNOP/ DIDP :1000 ppm (27893) Notification On Market Supervision And Controls Regarding Hazardous Chemical Contents Of Some End- User Products Part 1-2 P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.

3 R E S U L T S Page 3 of 6 REPORT : TURA August, 2012 Azo Dyestuff 64 LFGB :2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis Part 1&2 Composite sample of Beige cover with red print,yellow striped page PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO 64 LFGB , LEATHER ACCORDİNG TO 64 LFGB , PES ACCORDING TO 64 LFGB , EXTRACTED BY CITRATE BUFFERED SOLUTION ph 6 AT 70 C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS. FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL BENZIDINE CHLORO-O-4-CHLOR-O-TOLUIDINE NAPHTHYLAMINE *O-AMINOAZOTOLUENE *2-AMINO-4-NITROTOLUENE P-CHLOROANILINE ,4-DIAMINOANISOLE ,4 -DIAMINOBIPHENYLMETHANE ,3 -DICHLOROBENZIDINE ,3 -DIMETHOXYBENZIDINE ,3 -DIMETHYLBENZIDINE ,3 -DİMETHYL-4,4 DIAMINOBIPHENYLMETHANE P-CRESIDINE ,4 -METHYLENE-BIS-(2 CHLOROANILINE) ,4 -OXYDIANILINE ,4 -THIODIANILINE O-TOLUIDINE ,4-TOLUYLENDIAMINE ,4,5-TRIMETHYLANILINE O-ANISIDINE **P-AMINOAZOBENZENE NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%

4 R E S U L T S Page 4 of 6 REPORT : TURA August, 2012 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 1 Antimony (Sb) <2 ppm PASS 60 Part 2 Antimony (Sb) <2 ppm PASS 60 Part 3 Antimony (Sb) <2 ppm PASS 60 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

5 R E S U L T S Page 5 of 6 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 1 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

6 R E S U L T S Page 6 of 6 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 2 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %) ## END OF TEST REPORT ##

7 TEST REPORT Page 1 of 7 REPORT NUMBER : TURA APPLICANT NAME ADDRESS Keskin Color Kartpostalcılık A.Ş. Bağlar Mah. Çeşmealtı Sk.No:23 Istanbul FAX NO : Attention : Muhiddin Keskin (mkeskin@keskincolor.com) SAMPLE DESCRIPTION : BUYER : A4 Free checked Notebook 60 Page TÜKİD DATE IN : 26 July, 2012 (13:59) DATE OUT : 01 August, 2012 ARTICLE NO : PHOTO OF PRODUCT TESTED : Part No Tested Part 1 YELLOW PP COVER 2 WHITE/BLACK CHECKED PAPER 3 TRANSPARENT PLASTIC WIRE Füsun Karaoğlu Coordinator Neslihan Sözer Chemical Laboratory Manager Merkez Mahallesi Sanayi Cad. No: 23 Altındağ Plaza Yenibosna ISTANBUL / TURKEY * * ssenturk

8 R E S U L T S Page 2 of 7 REPORT : TURA August, 2012 RESULTS : Analysis Parameter Reference Analysis Method PASS FAIL Norm Limit Standard for Norm Limit Tested Part Azo Dyes 64 LFBG B P - 30 ppm 2004/21/EC Part 1-3 Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Toxic Element Cd: 75 ppm BS EN 71-3:1995 P - Analysis Cr: 60 ppm Pb: 90 ppm Hg: 60 ppm Se: 500 ppm EN 71-3 Part 1-3 Phthalate EN by GC MS P - DBP/DEHP/BBP : 1000 ppm DINP/DNOP/ DIDP :1000 ppm (27893) Notification On Market Supervision And Controls Regarding Hazardous Chemical Contents Of Some End- User Products Part 1-3 P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.

9 R E S U L T S Page 3 of 7 REPORT : TURA August, 2012 Azo Dyestuff 64 LFGB :2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis Part 1&2&3 1)Composite sample of Yellow PP cover,white/black checked paper PASS 30 ppm 2)Transparent plastic wire PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO 64 LFGB , LEATHER ACCORDİNG TO 64 LFGB , PES ACCORDING TO 64 LFGB , EXTRACTED BY CITRATE BUFFERED SOLUTION ph 6 AT 70 C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS. FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL BENZIDINE CHLORO-O-4-CHLOR-O-TOLUIDINE NAPHTHYLAMINE *O-AMINOAZOTOLUENE *2-AMINO-4-NITROTOLUENE P-CHLOROANILINE ,4-DIAMINOANISOLE ,4 -DIAMINOBIPHENYLMETHANE ,3 -DICHLOROBENZIDINE ,3 -DIMETHOXYBENZIDINE ,3 -DIMETHYLBENZIDINE ,3 -DİMETHYL-4,4 DIAMINOBIPHENYLMETHANE P-CRESIDINE ,4 -METHYLENE-BIS-(2 CHLOROANILINE) ,4 -OXYDIANILINE ,4 -THIODIANILINE O-TOLUIDINE ,4-TOLUYLENDIAMINE ,4,5-TRIMETHYLANILINE O-ANISIDINE **P-AMINOAZOBENZENE NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%

10 R E S U L T S Page 4 of 7 REPORT : TURA August, 2012 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 1 Antimony (Sb) <2 ppm PASS 60 Part 2 Antimony (Sb) <2 ppm PASS 60 Part 3 Antimony (Sb) <2 ppm PASS 60 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

11 R E S U L T S Page 5 of 7 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 1 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

12 R E S U L T S Page 6 of 7 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 2 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

13 R E S U L T S Page 7 of 7 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 3 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %) ## END OF TEST REPORT ##

14 TEST REPORT Page 1 of 6 REPORT NUMBER : TURA APPLICANT NAME ADDRESS Keskin Color Kartpostalcılık A.Ş. Bağlar Mah. Çeşmealtı Sk.No:23 Istanbul FAX NO : Attention : Muhiddin Keskin (mkeskin@keskincolor.com) SAMPLE DESCRIPTION : BUYER : Şirinler designed drawing book TÜKİD DATE IN : 26 July, 2012 (13:59) DATE OUT : 01 August, 2012 ARTICLE NO : PHOTO OF PRODUCT TESTED : Part No Tested Part 1 MULTICOLOR DESIGNED COVER 2 WHITE PAPER 3 WHITE METAL WIRE Füsun Karaoğlu Coordinator Neslihan Sözer Chemical Laboratory Manager Merkez Mahallesi Sanayi Cad. No: 23 Altındağ Plaza Yenibosna ISTANBUL / TURKEY * * ssenturk

15 R E S U L T S Page 2 of 6 REPORT : TURA August, 2012 RESULTS : Analysis Parameter Reference Analysis Method PASS FAIL Norm Limit Standard for Norm Limit Tested Part Azo Dyes 64 LFBG B P - 30 ppm 2004/21/EC Part 1-2 Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Toxic Element Cd: 75 ppm BS EN 71-3:1995 P - Analysis Cr: 60 ppm Pb: 90 ppm Hg: 60 ppm Se: 500 ppm EN 71-3 Part 1-3 Phthalate EN by GC MS P - DBP/DEHP/BBP : 1000 ppm DINP/DNOP/ DIDP :1000 ppm (27893) Notification On Market Supervision And Controls Regarding Hazardous Chemical Contents Of Some End- User Products Part 1-2 P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.

16 R E S U L T S Page 3 of 6 REPORT : TURA August, 2012 Azo Dyestuff 64 LFGB :2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis Part 1&2 1)Multicolor designed cover PASS 30 ppm 2)White paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO 64 LFGB , LEATHER ACCORDİNG TO 64 LFGB , PES ACCORDING TO 64 LFGB , EXTRACTED BY CITRATE BUFFERED SOLUTION ph 6 AT 70 C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS. FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL BENZIDINE CHLORO-O-4-CHLOR-O-TOLUIDINE NAPHTHYLAMINE *O-AMINOAZOTOLUENE *2-AMINO-4-NITROTOLUENE P-CHLOROANILINE ,4-DIAMINOANISOLE ,4 -DIAMINOBIPHENYLMETHANE ,3 -DICHLOROBENZIDINE ,3 -DIMETHOXYBENZIDINE ,3 -DIMETHYLBENZIDINE ,3 -DİMETHYL-4,4 DIAMINOBIPHENYLMETHANE P-CRESIDINE ,4 -METHYLENE-BIS-(2 CHLOROANILINE) ,4 -OXYDIANILINE ,4 -THIODIANILINE O-TOLUIDINE ,4-TOLUYLENDIAMINE ,4,5-TRIMETHYLANILINE O-ANISIDINE **P-AMINOAZOBENZENE NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%

17 R E S U L T S Page 4 of 6 REPORT : TURA August, 2012 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 1 Antimony (Sb) <2 ppm PASS 60 Part 2 Antimony (Sb) <2 ppm PASS 60 Part 3 Antimony (Sb) <2 ppm PASS 60 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

18 R E S U L T S Page 5 of 6 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 1 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

19 R E S U L T S Page 6 of 6 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 2 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %) ## END OF TEST REPORT ##

20 TEST REPORT Page 1 of 5 REPORT NUMBER : TURA APPLICANT NAME ADDRESS Keskin Color Kartpostalcılık A.Ş. Bağlar Mah. Çeşmealtı Sk.No:23 Istanbul FAX NO : Attention : Muhiddin Keskin (mkeskin@keskincolor.com) SAMPLE DESCRIPTION : BUYER : Pepee Designed Weekly Course Schedule TÜKİD DATE IN : 26 July, 2012 (13:59) DATE OUT : 30 July, 2012 ARTICLE NO : PHOTO OF PRODUCT TESTED : Part No Tested Part 1 MULTICOLOR DESIGNED PAPER PP Aşkın GÜNERİ Füsun Karaoğlu Coordinator Neslihan Sözer Chemical Laboratory Manager Merkez Mahallesi Sanayi Cad. No: 23 Altındağ Plaza Yenibosna ISTANBUL / TURKEY * * ssenturk

21 R E S U L T S Page 2 of 5 REPORT : TURA July, 2012 RESULTS : Analysis Parameter Reference Analysis Method PASS FAIL Norm Limit Standard for Norm Limit Tested Part Azo Dyes 64 LFBG B P - 30 ppm 2004/21/EC Part 1 Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Toxic Element Cd: 75 ppm BS EN 71-3:1995 P - Analysis Cr: 60 ppm Pb: 90 ppm Hg: 60 ppm Se: 500 ppm EN 71-3 Part 1 Phthalate EN by GC MS P - DBP/DEHP/BBP : 1000 ppm DINP/DNOP/ DIDP :1000 ppm (27893) Notification On Market Supervision And Controls Regarding Hazardous Chemical Contents Of Some End- User Products Part 1 P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.

22 R E S U L T S Page 3 of 5 REPORT : TURA July, 2012 Azo Dyestuff 64 LFGB :2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis Part 1 Multicolor designed paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO 64 LFGB , LEATHER ACCORDİNG TO 64 LFGB , PES ACCORDING TO 64 LFGB , EXTRACTED BY CITRATE BUFFERED SOLUTION ph 6 AT 70 C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS. FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL BENZIDINE CHLORO-O-4-CHLOR-O-TOLUIDINE NAPHTHYLAMINE *O-AMINOAZOTOLUENE *2-AMINO-4-NITROTOLUENE P-CHLOROANILINE ,4-DIAMINOANISOLE ,4 -DIAMINOBIPHENYLMETHANE ,3 -DICHLOROBENZIDINE ,3 -DIMETHOXYBENZIDINE ,3 -DIMETHYLBENZIDINE ,3 -DİMETHYL-4,4 DIAMINOBIPHENYLMETHANE P-CRESIDINE ,4 -METHYLENE-BIS-(2 CHLOROANILINE) ,4 -OXYDIANILINE ,4 -THIODIANILINE O-TOLUIDINE ,4-TOLUYLENDIAMINE ,4,5-TRIMETHYLANILINE O-ANISIDINE **P-AMINOAZOBENZENE NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%

23 R E S U L T S Page 4 of 5 REPORT : TURA July, 2012 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 1 Antimony (Sb) <2 ppm PASS 60 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

24 R E S U L T S Page 5 of 5 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 1 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %) ## END OF TEST REPORT ##

25 TEST REPORT Page 1 of 17 REPORT NUMBER : TURA APPLICANT NAME ADDRESS Keskin Color Kartpostalcılık A.Ş. Bağlar Mah. Çeşmealtı Sk.No:23 Istanbul FAX NO : Attention : Muhiddin Keskin (mkeskin@keskincolor.com) SAMPLE DESCRIPTION : BUYER : Pepee Construction paper TÜKİD DATE IN : 26 July, 2012 (13:59) DATE OUT : 30 July, 2012 ARTICLE NO : PHOTO OF PRODUCT TESTED : Part No Tested Part 1 RED PAPER 2 GREEN PAPER 3 BLUE PAPER 4 BROWN PAPER 5 PINK PAPER 6 ORANGE PAPER 7 BLACK PAPER 8 NAVY PAPER 9 YELLOW PAPER 10 GREY PAPER 11 MULTICOLOR PEPEE DESIGNED COVER Füsun Karaoğlu Coordinator Neslihan Sözer Chemical Laboratory Manager Merkez Mahallesi Sanayi Cad. No: 23 Altındağ Plaza Yenibosna ISTANBUL / TURKEY * * ssenturk

26 R E S U L T S Page 2 of 17 REPORT : TURA July, 2012 RESULTS : Analysis Parameter Reference Analysis Method PASS FAIL Norm Limit Standard for Norm Limit Tested Part Azo Dyes 64 LFBG B P - 30 ppm 2004/21/EC Part 1-11 Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Toxic Element Cd: 75 ppm BS EN 71-3:1995 P - Analysis Cr: 60 ppm Pb: 90 ppm Hg: 60 ppm Se: 500 ppm EN 71-3 Part 1-11 Phthalate EN by GC MS P - DBP/DEHP/BBP : 1000 ppm DINP/DNOP/ DIDP :1000 ppm (27893) Notification On Market Supervision And Controls Regarding Hazardous Chemical Contents Of Some End- User Products Part 1-11 P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.

27 R E S U L T S Page 3 of 17 REPORT : TURA July, 2012 Azo Dyestuff 64 LFGB :2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis Part 1&2&3&4&5&6&7&8&9&10&11 1)Composite sample of Red,Green,Blue paper PASS 30 ppm 2)Composite sample of Brown,Pink,Orange paper PASS 30 ppm 3)Composite sample of Black,navy,yellow paper PASS 30 ppm 4)Grey paper PASS 30 ppm 5)Multicolor pepee designed cover PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO 64 LFGB , LEATHER ACCORDİNG TO 64 LFGB , PES ACCORDING TO 64 LFGB , EXTRACTED BY CITRATE BUFFERED SOLUTION ph 6 AT 70 C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS. FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL BENZIDINE CHLORO-O-4-CHLOR-O-TOLUIDINE NAPHTHYLAMINE *O-AMINOAZOTOLUENE *2-AMINO-4-NITROTOLUENE P-CHLOROANILINE ,4-DIAMINOANISOLE ,4 -DIAMINOBIPHENYLMETHANE ,3 -DICHLOROBENZIDINE ,3 -DIMETHOXYBENZIDINE ,3 -DIMETHYLBENZIDINE ,3 -DİMETHYL-4,4 DIAMINOBIPHENYLMETHANE P-CRESIDINE ,4 -METHYLENE-BIS-(2 CHLOROANILINE) ,4 -OXYDIANILINE ,4 -THIODIANILINE O-TOLUIDINE ,4-TOLUYLENDIAMINE ,4,5-TRIMETHYLANILINE O-ANISIDINE **P-AMINOAZOBENZENE NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%

28 R E S U L T S Page 4 of 17 REPORT : TURA July, 2012 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 1 Antimony (Sb) <2 ppm PASS 60 Part 2 Antimony (Sb) <2 ppm PASS 60 Part 3 Antimony (Sb) <2 ppm PASS 60 Part 4 Antimony (Sb) <2 ppm PASS 60 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

29 R E S U L T S Page 5 of 17 REPORT : TURA July, 2012 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 5 Antimony (Sb) <2 ppm PASS 60 Part 6 Antimony (Sb) <2 ppm PASS 60 Part 7 Antimony (Sb) <2 ppm PASS 60 Part 8 Antimony (Sb) <2 ppm PASS 60 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

30 R E S U L T S Page 6 of 17 REPORT : TURA July, 2012 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 9 Antimony (Sb) <2 ppm PASS 60 Part 10 Antimony (Sb) <2 ppm PASS 60 Part 11 Antimony (Sb) <2 ppm PASS 60 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

31 R E S U L T S Page 7 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 1 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

32 R E S U L T S Page 8 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 2 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

33 R E S U L T S Page 9 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 3 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

34 R E S U L T S Page 10 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 4 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

35 R E S U L T S Page 11 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 5 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

36 R E S U L T S Page 12 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 6 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

37 R E S U L T S Page 13 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 7 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

38 R E S U L T S Page 14 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 8 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

39 R E S U L T S Page 15 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 9 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

40 R E S U L T S Page 16 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 10 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

41 R E S U L T S Page 17 of 17 REPORT : TURA July, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 11 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %) ## END OF TEST REPORT ##

42 TEST REPORT Page 1 of 6 REPORT NUMBER : TURA APPLICANT NAME ADDRESS Keskin Color Kartpostalcılık A.Ş. Bağlar Mah. Çeşmealtı Sk.No:23 Istanbul FAX NO : Attention : Muhiddin Keskin (mkeskin@keskincolor.com) SAMPLE DESCRIPTION : BUYER : Spiderman A5 Metallize Checked Designed Notebook 80 Page TÜKİD DATE IN : 26 July, 2012 (13:59) DATE OUT : 01 August, 2012 ARTICLE NO : PHOTO OF PRODUCT TESTED : Part No Tested Part 1 SPIDERMAN DESIGNED MULTICOLOR COVER 2 MULTICOLOR CHECKED PAPER 3 METAL WIRE Füsun Karaoğlu Coordinator Neslihan Sözer Chemical Laboratory Manager Merkez Mahallesi Sanayi Cad. No: 23 Altındağ Plaza Yenibosna ISTANBUL / TURKEY * * ssenturk

43 R E S U L T S Page 2 of 6 REPORT : TURA August, 2012 RESULTS : Analysis Parameter Reference Analysis Method PASS FAIL Norm Limit Standard for Norm Limit Tested Part Azo Dyes 64 LFBG B P - 30 ppm 2004/21/EC Part 1-2 Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Toxic Element Cd: 75 ppm BS EN 71-3:1995 P - Analysis Cr: 60 ppm Pb: 90 ppm Hg: 60 ppm Se: 500 ppm EN 71-3 Part 1-3 Phthalate EN by GC MS P - DBP/DEHP/BBP : 1000 ppm DINP/DNOP/ DIDP :1000 ppm (27893) Notification On Market Supervision And Controls Regarding Hazardous Chemical Contents Of Some End- User Products Part 1-2 P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.

44 R E S U L T S Page 3 of 6 REPORT : TURA August, 2012 Azo Dyestuff 64 LFGB :2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis Part 1&2 1)Spiderman designed multicolor cover PASS 30 ppm 2)Multicolor checked paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO 64 LFGB , LEATHER ACCORDİNG TO 64 LFGB , PES ACCORDING TO 64 LFGB , EXTRACTED BY CITRATE BUFFERED SOLUTION ph 6 AT 70 C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS. FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL BENZIDINE CHLORO-O-4-CHLOR-O-TOLUIDINE NAPHTHYLAMINE *O-AMINOAZOTOLUENE *2-AMINO-4-NITROTOLUENE P-CHLOROANILINE ,4-DIAMINOANISOLE ,4 -DIAMINOBIPHENYLMETHANE ,3 -DICHLOROBENZIDINE ,3 -DIMETHOXYBENZIDINE ,3 -DIMETHYLBENZIDINE ,3 -DİMETHYL-4,4 DIAMINOBIPHENYLMETHANE P-CRESIDINE ,4 -METHYLENE-BIS-(2 CHLOROANILINE) ,4 -OXYDIANILINE ,4 -THIODIANILINE O-TOLUIDINE ,4-TOLUYLENDIAMINE ,4,5-TRIMETHYLANILINE O-ANISIDINE **P-AMINOAZOBENZENE NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%

45 R E S U L T S Page 4 of 6 REPORT : TURA August, 2012 Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma- ICP_OES. RESULT IN ppm PASS/FAIL Requirement (ppm) Part 1 Antimony (Sb) <2 ppm PASS 60 Part 2 Antimony (Sb) <2 ppm PASS 60 Part 3 Antimony (Sb) <2 ppm PASS 60 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=results quoted have been corrected for uncertainty. -)

46 R E S U L T S Page 5 of 6 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 1 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)

47 R E S U L T S Page 6 of 6 REPORT : TURA August, 2012 TOTAL PHTHALATE CONTENT EN : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 2 DIBUTYL PHTHALATE (DBP) DIETHYL HEXYL PHTHALATE (DEHP) BENZYL BUTYL PHTHALATE (BBP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) DI-ISO-NONYL PHTHALATE (DINP) DI-N-OCTYL PHTHALATE (DNOP) DI-ISO-DECYL PHTHALATE (DIDP) SUM OF THREE PHTHALATES LIMIT (MAX.) RESULT (%, w/w) 1000 ppm (0.1% (w/w)) REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %) ## END OF TEST REPORT ##

48 TEST REPOR Page 1 of 8 REPORT NUMBER : APPLICANT NAME ADDRESS SAMPLE DESCRIPTION : BUYER : TURA Keskin Color Kartpostalcılık A.Ş. Bağlar Mah. Çeşmealtı Sk. No: Güneşli Đstanbul TÜRKĐYE FAX NO : Attention :Muhiddin Keskin (mkeskin@keskincolor.com) Ten samples of Ground color carton TÜKĐD DATE IN : 04 August, 2011 (13:59) DATE OUT : 10 August, 2011 PHOTO OF PRODUCT TESTED : Part No Tested Part Part No Tested Part 1 RED CARDBOARD 6 GREY CARDBOARD 2 YELLOW CARDBOARD 7 PINK CARDBOARD 3 BLACK CARDBOARD 8 ORANGE CARTBOARD 4 BLUE CARDBOARD 9 GREEN CARDBOARD 5 WHITE CARDBOARD 10 BROWN CARDBOARD Zeynep Akın Assistant Chemical Laboratory Manager Neslihan Sözer Chemical Laboratory Manager Merkez Mahallesi Sanayi Cad. No: 23 Altındağ Plaza Yenibosna ISTANBUL / TURKEY * * tugcekomurcu

49 R E S U L T S Page 2 of 8 REPORT : TURA August, 2011 RESULTS : Analysis Parameter Reference Analysis Method PASS FAIL Norm Limit Standard for Norm Limit Tested Part Azo Dyes 64 LFBG B P - 30 ppm 2004/21/EC Part 1-10 Determination of perfluorooctane sulfonates (PFOS) & perfluorooctanoic acıd (PFOA) Formaldehyde Toxic Element Analysis INTERTEK IHTM AL by LC/MS/MS JIS LAW 112 (Textile) 35 LFBG (Leather) BS EN 71-3:1995 P - P - 1 µg/m² 2006/122/EC Part 1-10 P - 20 ppm 2002/371/EC Part 1-10 Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Cd: 75 ppm Cr: 60 ppm Pb: 90 ppm Hg: 60 ppm Se: 500 ppm EN 71-3 Part 1-10 P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.

50 R E S U L T S Page 3 of 8 REPORT : TURA August, 2011 Azo Dyestuff 64 LFGB :2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis Part 1&2&3&4&5&6&7&8&9&10 1) Composite sample of Red, Yellow, Black cardboard PASS 30 ppm 2) Composite sample of Blue, White, Grey cardboard PASS 30 ppm 3) Composite sample of Pink, Orange, Green cardboard PASS 30 ppm 4) Brown cardboard PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO 64 LFGB , LEATHER ACCORDĐNG TO 64 LFGB , PES ACCORDING TO 64 LFGB , EXTRACTED BY CITRATE BUFFERED SOLUTION ph 6 AT 70 C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS. FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL BENZIDINE CHLORO-O-4-CHLOR-O-TOLUIDINE NAPHTHYLAMINE *O-AMINOAZOTOLUENE *2-AMINO-4-NITROTOLUENE P-CHLOROANILINE ,4-DIAMINOANISOLE ,4 -DIAMINOBIPHENYLMETHANE ,3 -DICHLOROBENZIDINE ,3 -DIMETHOXYBENZIDINE ,3 -DIMETHYLBENZIDINE ,3 -DĐMETHYL-4,4 DIAMINOBIPHENYLMETHANE P-CRESIDINE ,4 -METHYLENE-BIS-(2 CHLOROANILINE) ,4 -OXYDIANILINE ,4 -THIODIANILINE O-TOLUIDINE ,4-TOLUYLENDIAMINE ,4,5-TRIMETHYLANILINE O-ANISIDINE **P-AMINOAZOBENZENE NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%

51 R E S U L T S Page 4 of 8 REPORT : TURA August, 2011 Determination of Perfluorooctane sulfonates (PFOS) & Perfluorooctanoic Acid (PFOA) INTERTEK IHTM AL : Solvent Extraction Followed By Liquid Chromotographic- Mass Spectrometric(LS-MS-MS) Analysis Part 1 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 2 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 3 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 4 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 5 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 6 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 7 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 8 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 9 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Part 10 PFOS (Perfluorooctane sulfonates) PFOA (Perfluorooctanoic Acid) Result Result Result Result Result Result Result Result Result Result Detection Limit ND =0.25 ppb /0.5 µg/m² (<0,25 ppb / <0.5 µg/m²) Requirement (Total Uncertainty=±4 %) 1µg/m² according to 2006/122/EC