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1 Page 1 of 8 Tests: The laboratory is qualified to update standards identifying the test procedures. The laboratory has a flexible scope of accreditation permitted as detailed in the Annex. Updated list of activities provided within the required flexible scope of accreditation is available at the laboratory from the Laboratory Quality Manager. The laboratory provides expert opinions and interprets test results. 1 2 Determination of humidity by gravimetry Determination of loss on ignition by gravimetry 3 Reserved 4 Determination of ash by gravimetry 5 Determination of suspended solids by gravimetry 6 Determination of dissolved substances and inorganic dissolved salts by gravimetry 7 8 Determination of sulphates by gravimetry Determination of total sulphur by gravimetry and determination of specific sulphur by calculation SOP č. OAA (ČSN , ČSN EN ISO , ČSN EN 12880, ČSN ISO 11465, ČSN , ČSN ) SOP no. OAA (ČSN , ČSN A1, ČSN EN 196-2, ČSN ) SOP no. OAA (ČSN ISO 1171) SOP no. OAA (ČSN EN 872) SOP no. OAA (ČSN ) SOP no. OAA (ČSN EN A1, ČSN EN 196-2, ČSN , ČSN ) SOP no. OAA (ČSN , ČSN , ČSN EN A1 ČSN ) soils, sediments, solid waste, solid fuels, building and silicate materials soils, sediments, solid waste, solid fuels, building and silicate materials solid fuels surface, ground and waste water, silicate materials, cement, stone aggregates, gypsum silicate materials, stone aggregates, solid fuels Page 1 of 8
2 Page 2 of 8 9 Determination of carbonate by gravimetry 10 Determination of insoluble compounds in hydrochloric acid and sodium carbonate by gravimetry Determination of ph by potentiometry Determination of electrical conductivity Determination of dissolved oxygen by oxygen electrode Determination of Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, Pb and Zn by flame AAS 15 Determination of Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, Pb and Zn by flame AAS 16 Determination of As, Be, Cd, Co, Cu, Mn, Mo, Ni, Sb, Se and Sn by electrothermal AAS 17 Determination of As, Be, Cd, Co, Cu, Mn, Mo, Ni, Sb, Se and Sn by electrothermal AAS 18 Determination of Hg by analyzer AMA 254 SOP No. OAA (ČSN ) SOP no. OAA (ČSN EN 196-2) SOP no. OAA (ČSN ISO 10523) SOP no. OAA (ČSN EN 27888) SOP no. OAA (ČSN EN 25814, Manual to the device used) 1) SOP no. OAA-05-01A (Manual to the device used, US EPA s) 2) SOP no. OAA-05-01B (Manual to the device used, US EPA s) 2) SOP no. OAA-05-02A (Manual to the device used, US EPA s) 2) SOP no. OAA-05-02B (Manual to the device used, US EPA s) 2) SOP no. OAA (Manual to AMA-254) Silicate materials, slag, fly ash, gypsum from energy production cement, acid extracts, emissions absorption solutions waste, building and silicate materials, emissions filtration medium, acid extracts, emissions absorption solutions waste, building and silicate materials, emissions filtration medium, acid extracts, waste, solid fuels, emissions absorption solutions and filtration medium Page 2 of 8
3 Page 3 of 8 19 Determination of Ag, Al, As, B, Ba, Be, Ca, Cd, Co, Cr, Cu, Fe, K, Li, Mg, Mn, Mo, Na, Ni, Pb, Sb, Se, Si, Sn, Ti, V and Zn by ICP-AES 20 Determination of Ag, Al, As, B, Ba, Be, Ca, Cd, Co, Cr, Cu, Fe, K, Li, Mg, Mn, Mo, Na, Ni, Pb, Sb, Se, Si, Sn, Ti, V and Zn by ICP-AES 21 Determination of Na, Mg, Al, Si, P, S, K, Ca, Ti, Fe, Mn, Cl, V, Cr, Co, Ni, Cu, Zn, Ga, Ge, As, Se, Br, Rb, Sr, Y, Zr, Nb, Mo, Ag, Cd, In, Sn, Sb, Te, I, Cs, Ba, La, Ce, Ta, W, Hg, Tl, Pb, Bi, Th and U by XRFS 22 Determination of P, S, Cl, K, Ca, Ti, V, Cr, Mn, Fe, Ni, Cu, Zn, Br, Mo, Ag, Cd, Sn, Ba, Pb by XRFS 23 Reserved Spectrometric determination of fluorides Spectrometric determination of fluorides 26 Spectrometric determination of total phosphorus 27 Spectrometric determination of ammonium ions and determination of inorganic nitrogen by calculation 28 Spectrometric determination of phenol index 29 Reserved SOP no. OAA-06-01A (US EPA 6010) SOP no. OAA-06-01B (US EPA 6010) SOP no. OAA (Manual to Spectro Xepos) 3) SOP no. OAA (Manual to Spectro Xepos) 3) SOP no. OAA ) SOP no. OAA ) SOP no. OAA (ČSN EN ISO 6878) SOP no. OAA (ČSN ISO ) SOP no. OAA (ČSN ISO 6439), acid extracts, emissions absorption solutions waste, building and silicate materials, emissions filtration medium soils, sediments, solid waste, solid fuels, building and silicate materials, emissions filtration medium liquid and paste waste, oils, emissions soils, sediments, solid waste, building and silicate materials Page 3 of 8
4 Page 4 of 8 30 Determination of total carbon (TC), total organic carbon (TOC) and dissolved organic carbon (DOC) by IR spectrometry 31 Determination of total carbon (TC) and total organic carbon (TOC) by IR spectrometry Determination of Mo by electrothermal AAS Determination of B, Be by ICP-AES 34 Determination of sulphur and halogens by combustion after decomposition in calorimetric reactor 35 Determination of anions by ion chromatography with conductivity detection 36 Determination of concentration of chlorides in solid phase by volumetric 37 Analyses of gases by the of gas chromatography with FID, TCD and ECD 38 Determination of PCB by the of gas chromatography with mass spectrometry detection 39 Determination of PCB by the of gas chromatography with mass spectrometry detection 40 Determination of volatile organic compounds by GC/MS SOP no. OAA (ČSN EN 1484, Manual to Multi N/C 3100) SOP no. OAA (ČSN EN 13137, Manual to Multi N/C 3100, HT1300) SOP no. OAA-05-02C (Manuals to device, US EPA s) 2) SOP no. OAA-06-01C (US EPA 6010, research papers) 3) SOP no. OOA (US EPA 5050) SOP no. OOA (US EPA 1011B, materials of Waters) SOP no. OOA (ČSN EN 196-2) SOP no. OOA (ČSN , US EPA 8000) SOP no. OOA-80-80A (US EPA 8080A) SOP no. OOA-80-80B (US EPA 8080A) SOP no. OOA-82-41A (US EPA 8240, manual to CTC CombiPal) waste, sludge, sediment solid fuels solid fuels solid and liquid fuels, waste, emission absorption solutions cement, slag, fly ash technical and waste gases, biogas, flue gases sediments, waste, oils Page 4 of 8
5 Page 5 of 8 41 Determination of volatile organic compounds by GC/MS 42 Determination of C 10 -C 40 hydrocarbons by the of gas chromatography with FID detector 43 Determination of C 10 -C 40 hydrocarbons by the of gas chromatography with FID detector 44 Determination of polycondensed aromatic hydrocarbons by HPLC/PDA/FD 45 Determination of polycondensed aromatic hydrocarbons by HPLC/PDA/FD 46 Reserved 47 Determination of volatile organic compounds by headspace/gc/ms 48 Determination of volatile organic compounds by headspace/gc/ms 49 Determination of alcohols by the of gas chromatography with FID detector 50 Determination of alcohols by the of gas chromatography with FID detector SOP no. OOA-82-41B (US EPA 8240, manual to CTC CombiPal) SOP no. OOA-80-15A (US EPA 8015C, ČSN EN ISO ) SOP no. OOA-80-15B (US EPA 8015C, ČSN EN 14039) SOP no. OOA-83-10A (US EPA 8310) SOP no. OOA-83-10B (US EPA 8310) SOP no. OOA-38-10A (Manual to CTC CombiPal, US EPA 3810) 6) SOP no. OOA-38-10B (Manual to CTC CombiPal, US EPA 3810) 6) SOP no. OOA-00-45A (ČSN , Application notes to Restek and Agilent) 7) SOP no. OOA-00-45B (ČSN , Application notes to Restek and Agilent) 7) sediments, waste waste sediments, waste sediments, waste alcoholic beverage technical ethanol, nonfreezing mixtures Page 5 of 8
6 Page 6 of 8 Annex: Flexible scope of accreditation of tests 14-17, 19, 20-22, 32, 33, 35, 37-41, The laboratory is allowed to modify the test s listed in the Annex within the specified scope of accreditation provided the measuring principle is observed. The flexible approach to the scope of accreditation cannot be applied to the tests not included in the Annex Abbreviations and explanations: AAS AMA ECD FD FID GC/MS HPLC ICP-AES IR PCB PDA SOP TCD US EPA XFRS Extracts Waste atomic absorption spectrometry atomic absorption spectrometry for Hg determination electron capture detector fluorescence detector flame ionization detector gas chromatography with mass spectrometry detection high performance liquid chromatography inductively coupled plasma atomic emission spectroscopy infrared spectrometry polychlorinated biphenyls photodiode array detector standard operation procedure, internal procedure drawn up on the basis of standardized s, legislative requirements and manuals to the devices used thermal conductivity detector United States Environmental Protection Agency X-ray fluorescence spectrometry of waste and solid samples, extracts of materials solid and liquid waste Page 6 of 8
7 Page 7 of 8 Additional explanations to SOP: Listed s were also drawn up using the following documents: 1) 2) 3) 4) 5) 6) 7) Manual to Multimetr P4 device. The SOLAAR Series Cookbook, AAS ATI Unicam, US EPA s, SW 846, Vol.1, Section A, chapter 3. Krakovská, E., Kuss H.M. Rozklady v analytickej chemii, VIENALA Košice, WANG, J.; NAKAZATO, T.; SAKANISHI, K.; YAMADA, O.; SAITO, I. Microwave digestion with HNO 3 /H 2 O 2 mixture at high temperatures for determination of trace elements in coal by ICP-OES and ICP-MS. Analytica Chimica Acta. 2004, s WANG, J.; NAKAZATO, T.; SAKANISHI, K.; YAMADA, O.; TAO, H.; SAITO, I. Single-step microwave digestion with HNO 3 alone for determination of trace elements in coal by ICP spectrometry. Talanta. 2006, 5. ed., s Greenberg, A.E., Clesceri, L.S., Eaton, A.D. Standard Methods for the Examination of Water and Wastewater, 18th edition, 1992, Washington. ČSN , ČSN , ČSN Zýka, J. Analytical Guide, 1st Volume, SNTL/ALFA, 1988, Prague. Píša, J. Methods for the determination of fluorine with focus on fuel analysis. ÚPV Monography No. 68. Fuel Research Institute. Běchovice. Manuals to CTC CombiPal Headspace US EPA s, SW 846, Vol.1, Section B, Chapter 4. Application lists for Restek and Agilent headspace. Range of determined parameters: Ord. range of parameters 8 Determination of total sulphur by gravimetry and determination of specific sulphur by calculation The calculation of specific sulphur applies to solid fuels only 21 Determination of Na, Mg, Al, Si, P, S, K, Ca, Ti, Fe, Mn, Cl, V, Cr, Co, Ni, Cu, Zn, Ga, Ge, As, Se, Br, Rb, Sr, Y, Zr, Nb, Mo, Ag, Cd, In, Sn, Sb, Te, I, Cs, Ba, La, Ce, Ta, W, Hg, Tl, Pb, Bi, Th and U by XRFS Expressed in the form of listed elements or in the form of oxides: Na 2 O, MgO, Al 2 O 3, SiO 2, P 2 O 5, SO 3, K 2 O, CaO, TiO 2, MnO, Fe 2 O 3, BaO, SrO Page 7 of 8
8 Page 8 of 8 Ord. range of parameters 34 Determination of sulphur and halogens by combustion after decomposition in calorimetric reactor Fluorine, chlorine, bromine, combustible sulphur 35 Determination of anions by ion chromatography with conductivity detection Fluorides F -, chlorides Cl -, nitrites NO 2 -, bromides Br -, nitrates NO 3 -, phosphates PO 4 3-, sulphates SO Analyses of gases by the of gas chromatography with FID, TCD and ECD Carbon oxide, nitrous oxide, sulphide, hydrogen, methane, ethane, ethene, ethyne, propane, propene, butane, isobutane 38, 39 Determination of PCB by the of gas chromatography with mass spectrometry detection Congeners 28,52,101,118,138,153,180 40, 41 Determination of volatile organic compounds by GC/MS Benzene, tetrachloromethane, chloroform, trans-1,2-dichloroethene, ethylbenzene, methylchloride, styrene, 1,1,2,2-tetrachloroethane, tetrachloroethene, toluene, 1,1,1- trichlorethane, 1,1,2-trichlorethane, trichlorethene, xylenes 44, 45 Determination of polycondensed aromatic hydrocarbons by HPLC/PDA/FD Naphthalene, acenaphthylene, acenaphthene, fluorene, phenanthrene, anthracene, fluoranthene, pyrene, benzo[a]anthracene, chrysene, benzo[b]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene, indeno[1,2,3-cd]pyrene, dibenzo[ah]anthracene, benzo[ghi]perylene 47, 48 Determination of volatile organic compounds by headspace/gc/ms Benzene, toluene, ethylbenzene, xylenes, chloroform, trichloroethene, tetrachloroethene 49, 50 Determination of alcohols by the of gas chromatography with FID detector Methanol, ethanol, isopropanol Page 8 of 8
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