Large-Scale Industrial Evaporator Replacement Glassware from Ace Glass

Transcription

1 Large-Scale Industrial Evaporator Replacement Glassware from Ace Glass Ace Glass, founded in 1936, continues our long tradition of manufacturing high quality specialty glassware. We would like to introduce a new, comprehensive line of glassware to fit today s popular industrial scale rotary evaporators. This brochure outlines the more widely used glassware sets and component parts to replace your existing glass. Ace also offers both custom glass and glass repair services for all rotary evaporators. Ace Glass industrial scale rotary evaporator replacement glass, all manufactured in the USA to exacting specifications and standards. TH ACE GLASS INCORPORATED A N N I V E R S A R Y USA V I N E L A N D, N J

2 2 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS All Glassware Made in the U.S.A. Ace has been fabricating both lab scale and process scale glass for 75 years in our Vineland, NJ plant. All glass components in this catalog, for large scale industrial size rotary evaporators, are made from 33 expansion, borosilicate glass. All components are made to Ace s exacting standards and tested to insure they fit into your rotary evaporator, and for easy change over. We have improved many of the parts based on user recommendations, and have replaced hard-to-find components, such as GL and SVL threads, with Ace-Threds and Ace PTFE valve assemblies. This brochure outlines most of the components used on the 20 liter size rotary evaporators, including all types of receiving and evaporation flasks. Ace also fabricates products for this application that can meet your special requirements and special sizes. Breakage or Loss In case of Breakage: 1. Notify ACE immediately. 2. Please retain all inner and outer cartons and packing material. 3. ACE will advise you whether the carrier will report to your location for inspection or if item(s) are to be returned for inspection. In case of Shortage: 1. Notify ACE immediately. 2. A replacement will be issued upon confirming inventory discrepancy. In case of Loss: 1. First, please verify with all your receiving departments that delivery was not made. 2. Notify ACE immediately. 3. ACE will contact the carrier for tracking information as applicable. 4. A replacement will be issued upon verification that the shipment was not delivered and upon confirmation that the carrier cannot locate shipment. PLEASE NOTE: All breakages and shortages must be reported within two weeks of receipt. Returns and Repairs Incoming material (returns or repairs) must be pre-approved by our Product Return Specialist. Please follow these steps to ensure our Receiving Department does not refuse your shipment. 1 Contact ACE for an RA# (Return Authorization Number) (Vineland, NJ, USA) returns@aceglass.com 2. Once an RA# is given, properly pack the item(s) in an inner and outer box/carton and write the RA# on the outside of the box. All used items are to be thoroughly cleaned and defined in the assignment of an RA#. 3. A 20% restocking fee will be assessed for authorized returns unless arranged otherwise. ACE cannot accept responsibility for damage or destruction of glassware that occurs in your shipment to us. We strongly advise you to purchase additional insurance with your carrier. 4. For returns that are the result of your receiving the item(s) broken, ACE cannot accept responsibility for further damage or destruction of glassware that occurs in the return shipment due to improper packing. 5. Repairs will be evaluated by our technicians. You will be advised if any pieces are beyond repair or cannot be salvaged economically. ACE cannot accept responsibility for further damage or destruction of any glassware that is damaged during return shipment. by PLEASE NOTE: ACE cannot accept responsibility for material returned without proper authorization. Each item in this catalog has a two- or three-digit code in addition to the four- or five-digit number. No other ordering information is needed since each individual size, capacity, etc., has its own code. Example: /30 top 14/35 bottom would be ordered as The majority of items listed in this catalog are normally available from stock at our plant in Vineland, NJ. In the event your entire order cannot be filled immediately, a partial shipment will be sent, with the back-ordered items following shortly. If you would like the entire order to be sent in one shipment, please indicate this on your purchase order. Unless otherwise specified on the purchase order, we will ship material by what we consider the best way. Ways to Ace Glass products are also available from our many lab distribution partners, particularly VWR International, LLC and Sigma-Aldrich. PHONE CREDIT CARD FAX VISA MasterCard American Express MAIL P.O. Box 688 Vineland, NJ WEB SITE INTERNATIONAL via Sigma-Aldrich sales@aceglass.com export@aceglass.com via VWR Shipments are F.O.B. our factory in Vineland, NJ, USA. Contact ACE for current price list/pricing CD or visit our website, All item quantities in this catalog are one (1) unless otherwise noted. Specifications are subject to change without prior notice. Although they are represented to be accurate, it is best to verify product specifications with ACE prior to purchase in the event they have been changed since publication of this catalog. ing & Product Information:

3 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS , , , , , , CONDENSERS/COOLERS Replacement borosilicate glass components for Buchi R220, R220EX, and R220SE rotary evaporators. The condensers and coolers are available in either poly-coated or plain, non-coated versions. All condensers fit easily into the glass sets listed below. Ace also offers a non-jacketed version of the lower condensate cooler. Inner ball joints include CAPFE (PTFE-encapsulated silicone rubber) o-rings. Black caps (included) are SVL-22 threads; red cap (included) is GL-14 thread. Triple-Coil Condenser Triple-Coil Condenser Triple-Coil Condenser Triple-Coil Condenser Glass Condenser (Bullfrog) Glass Condenser (Bullfrog) Glass Condenser (Bullfrog) Glass Condenser (Bullfrog) Condensate Cooler, Jacketed Condensate Cooler, Jacketed Condenser Cooler, Plain Condenser Cooler, Plain Glassware Set R, D2 R, D2 D, D2 D, D2 DB, DB2 DB, DB2 RB, DB2 RB, DB2 C, RB, R C, RB, R C, RB, R C, RB, R Coated? Yes No Yes No Yes No Yes No Yes No Yes No Similar to Buchi Part No Buchi Models R220 R200EX, SE R220 R200EX, SE R220 R220EX, SE R220 R220 R220 R220EX R220 R220EX Ball/Socket DN Joint Sizes Uses O-Ring Size / 225 / / / / / / / / / / / / For Engineering Support, visit 3

4 4 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS 3967 EXPANSION TANK Replacement borosilicate glass components for Buchi R220, R220EX, and R220SE rotary evaporators. Upper expansion tanks for Buchi glass sets available in either poly-coated or plain, non-coated versions. DN40 ball joints on top and bottom. Inner bottom ball joint includes CAPFE (PTFE-encapsulated silicone rubber) o-ring, size 225. Glassware Set Coated? Buchi Part No. Buchi Models Expansion Tank D, D2, DB, DB2 Yes R Expansion Tank D, D2, DB, DB2 No R220EX, SE , , HEAD Distribution Replacement borosilicate glass components for Buchi R220, R220EX, and R220SE rotary evaporators. Lower distribution heads with improved design with easy to use Ace-Threds, PTFE stem valves PTFE 0-20mm valve stem includes three Kalrez o-rings. Stems are replaceable. Available poly-coated or plain, non-coated. Upper joint is DN40 outer ball joint. Red caps (included) are GL-14 thread; black cap (included) is SVL-15 thread. DN25 inner ball joint on and includes CAPFE (PTFE-encapsulated silicone rubber) o-ring, size 217. End thread is #15 Ace-Thred, for connection to 3978 valve assembly. Glassware Set Coated? Buchi Part No. Buchi Models Distribution Head-R C, RB, R No R Distribution Head-R C, RB, R No R220EX, SE Distribution Head-D D, D2, DB, DB2 Yes R Distribution Head-D D, D2, DB, DB2 No R220EX, SE , -10 Replacement 0-20mm PTFE valve stem (only) for / -10 distribution heads. Includes two size 116 and one size 114 Kalrez o-rings. No R220EX, SE ing & Product Information:

5 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS TRAPS C Set Replacement borosilicate glass components for Buchi R220, R220EX, and R220SE rotary evaporators. Inner and outer cold trap components for Buchi C glassware Set. Available poly-coated or plain, non-coated. DN40 inner ball joint includes CAPFE (PTFE-encapsulated silicone rubber) o-rings, size 225. Black cap (included) is SVL-22 thread. Top CAPFE o-ring (included) for and is for 150mm grooved top flat flange. 150mm clamp and PFA cap, listed below, must be ordered separately. Glassware Set Buchi Part No. Buchi Coated? Models Inner Cold Trap C No , 220EX, 220SE Outer Cold Trap C Yes Outer Cold Trap C No EX, 220SE PFA Cap (Lid) C No All Duran Quick Clamp C No All , TUBES Vapor Duct Steam Tube, Glass Replacement borosilicate glass vapor tubes for Buchi R220, R220EX, and R220SE rotary evaporators contains a Porosity C (25-50 micron) glass frit. Glassware Set Buchi Part No. Buchi Coated? Models Vapor Duct Tube All No R Vapor Duct Tube w/c Frit All No R TUBE Vapor Duct Steam Tube, Stainless Steel Replacement 316 stainless steel vapor tube for Buchi R220, R220EX, and R220SE rotary evaporators. Glassware Set Coated? Buchi Part No. Buchi Models Vapor Duct Tube All No R For Engineering Support, visit

6 6 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS , , , TUBES Connecting Tubes, Receiving Replacement borosilicate glass tubes for Buchi R220, R220EX, and R220SE rotary evaporators. Connecting glass tubes for Buchi receiver assembly. Available either poly-coated or plain, non-coated PTFE 0-20mm valve stem includes three Kalrez o-rings. See page nine for 6726 receiver flasks. DN25 inner ball joints have CAPFE (PTFE-encapsulated silicone rubber) o-rings, size 217. Buchi Part No. Buchi Models Coated? For Double Receiver Assembly Upper Branching Piece #1 Right, Ace Valve Yes R Upper Branching Piece #1 Right, Ace Valve No R220EX, SE Upper Branching Piece #2 Left, Ace Valve Yes / R Upper Branching Piece #2 Left, Ace Valve No R220EX, SE For Single Receiver Assembly Upper Branching Piece Ace Valve Yes R Upper Branching Piece Ace Valve No R220EX, SE Replacement 0-20mm PTFE valve stem (only) for 3973 branching tubes only. Includes two size 116 and one size 114 Kalrez o-rings. No All See our Laboratory Glassware & Equipment Catalog for replacement Kalrez, CAPFE and FETFE o-rings. ing & Product Information:

7 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS , , , , , TUBES Connecting, Glass Sets Replacement borosilicate glass tubes for Buchi R220, R220EX, and R220SE rotary evaporators. Upper and lower connecting tubes for glass distillation sets available poly-coated or plain, non-coated. The codes through -27 have two GL14 thread ports (with red caps) on top for thermosensor, or for easy clean out. DN40 inner ball joints on -12, -13, -20, -22, -25, and -27 include CAPFE (PTFE-encapsulated silicone rubber) o-rings, size 225. Bottom DN25 ball joint on -15 and -18 includes CAPFE o-ring, size and -13 both include an SVL-22 thread black cap and a GL 14 thread red cap. Glassware Set Coated? Buchi Part No. Buchi Models Vacuum Connector Tube DB, D Yes R Vacuum Connector Tube DB, D No R220EX, SE Y Bottom Tube DB, D2, D Yes R Y Bottom Tube DB, D2, D No R220EX, SE U Top Connect Tube DB, DB2 Yes R U Top Connect Tube DB, DB2 No R220EX, SE U Top Connect Tube D, D2 Yes R U Top Connect Tube D, D2 No R220EX, SE Y Bottom Tube DB2 Yes R Y Bottom Tube DB2 No R220EX, SE For Engineering Support, visit

8 8 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS VALVES Replacement borosilicate glass for Buchi R220, R220EX, and R220SE rotary evaporators. PTFE valve stem parts and valve assemblies, with Kalrez o-rings, for receiving flasks and 3970 lower distribution heads. Socket joint on is DN25. Joints on are PTFE, Ace-Thred #11 and #15, and they include CAPFE (PTFE-encapsulated silicone rubber) o-rings. Hose coupling on -07 is size G, for 5/8-inch I.D. tubing. Replacement o-rings for the bushings on are CAPFE size 110 ( ) for side port and CAPFE size 112 ( ) on end. Glassware Set Coated? Buchi Part No. Buchi Models Glass Body (only) for Inlet Valve All No All Complete Inlet Valve Assembly for Distribution Head All No All Bottom Drain Valve (Receiver) No All Replacement PTFE valve stem (only) for valves. Includes two size 011 and one size 111 Kalrez o-rings. No All ACE Glass introduces... A full line of Replacement Glassware for Bench-Scale Rotary Evaporators! Ace Glass, founded in 1936, continues our long tradition of manufacturing high quality specialty glassware. We would like to introduce a new, comprehensive line of glassware to fit today s popular bench-scale rotary evaporators. Ace also offers both custom glass and glass repair services for rotary evaporators. Ace Glass rotary evaporator replacement glass, all manufactured in the USA to exacting specifications and standards. Toll-free: Toll-free fax: Fax: sales@aceglass.com Contact us today for a copy of our new brochure! P.O. Box 688 Vineland, NJ ing & Product Information:

9 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS FLASKS Receiving Replacement borosilicate glass for Buchi R220, R220EX, and R220SE rotary evaporators. Receiving flasks are designed to fit all large-scale rotary evaporators. Now available in coated, plain, non-coated, amberized, and 6727 jacketed versions. Side necks include SVL-22 threaded black vent caps. Top and bottom socket joints are DN25, and bottom joint includes CAPFE (PTFE-encapsulated silicone rubber) o-ring, size 217. Coated? Buchi Part No. Buchi Models Receiving Flask 10L Yes All Receiving Flask 10L No All Receiving Flask 20L Yes All Receiving Flask 20L No All Receiving Flask 10L Amber No All Receiving Flask 20L Amber No All SVL-22 vent cap with PTFE insert For o-ring/ball joint connectors, see the Ace Laboratory Glassware & Equipment Catalog FLASKS Receiving, Jacketed Standard receiving flask for all rotary evaporators except, with outer jacket for cooling/heating of contents. Inlet/outlet connections are 28/15 o-ring ball joints and include FETFE o-rings, size 116. Top and bottom joints are DN25. Bottom inner ball joint includes CAPFE (PTFE-encapsulated silicone rubber) o-ring, size 217. Side joint is SVL-22 thread, with black vent cap included. Rotavap Coated? Models Receiving Flask 8L No All SVL-22 vent cap with PTFE insert ACE Custom Glass Design Service For Engineering Support, visit

10 10 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS Large Evaporator Flasks for All Rotary Evaporators 6702 FLASKS Evaporation, Large Scale These large sized evaporation flasks are fabricated from heavy wall flask blanks selected for balance and quality. Necks are carefully fabricated to prevent rotational whip. Flasks are now available in clear plain glass, poly-coated, or amberized. Amber coated flask can protect light sensitive contents. The XL size flange (see table) is compatible with the 150mm, and is standard for Buchi Model R220 rotary evaporators. OVERALL HEIGHT C A B 1. Select Flange Size A O.D., mm (Inches) B I.D., mm (Inches) C Thickness (mm) Flange Size Designation S (Small) 90 (3.5) 67 (2.7) 18 M (Medium) 100 (3.9) 72 (2.8) 19 L (Large) 110 (4.3) 83 (3.3) 23 XL (Extra Large) (5.9) (4.7) Select Flask Capacity and match with Flange Size Easy Instructions 1. Determine flange size (A) O.D., (B) I.D., (C) thickness (see diagram). 2. Match flask capacity with overall height and flange size. Capacity, Liters Buchi Part No. Overall Height, mm Flange Size S M M L L XL S M M L XL M M L XL COVER For Evaporating Flask, Polyethylene Polyethylene dust cover for evaporating flasks with 149.5mm I.D. XL flange has integral o ring to keep a tight seal. Comes complete with Viton o-ring. Buchi Part No ing & Product Information:

11 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS FLASKS Evaporation, Large Scale, Poly-Coated Same as 6702 on previous page, but poly-coated for added safety. Plastic coated flasks are clear and will withstand temperatures up to 100 C. Capacity, Liters Buchi Part No. Overall Height, mm Flange Size S M M L L XL S M M L XL M M L XL FLASKS Evaporation, Amberized Same as 6702 above, except with an amber coating to protect light sensitive contents. The XL size matches Buchi large scale rotary evaporators. Plain, not coated Capacity, Liters Buchi Part No. Overall Height, mm Flange Size XL/ XL/ XL/ FLASKS Evaporation, Indented These flasks are also referred to as drying flasks. They are particularly suited for drying of powdered samples. The baffles, indented into the glass, provide better circulation and mixing of the powders while rotating. Plain, not coated. Capacity, Liters Buchi Part No. Overall Height, mm Flange Size XL/ XL/ For Engineering Support, visit

12 12 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS Replacement Items for Use with Heidolph Rotary Evaporators LARGE EVAPORATOR FLASKS Used with Heidolph 20L rotary evaporators. These large flasks are fabricated from blanks selected for balance and quality. Necks are carefully welded to prevent rotational whip. Flasks can be plastic coated upon request. Cap., Liters Overall Height, mm A O.D., mm Flange B I.D., mm C mm LARGE RECEIVER FLASKS Used with Heidolph 20L rotary evaporators. This receiver flask is fabricated from blanks selected for balance and quality. Center neck is a polished S J 40/25 joint; side neck is a GL-18 thread, supplied with solid cap. At bottom is a 0-10mm Easy-Action stopcock with a GL-18 side arm, supplied with a 3/8-inch hose connection tube. Flasks can be plastic coated upon request. Cap., Liters Overall Hght., mm Center Neck Side Neck Bottom Outlet J40/25 S GL mm/GL Replacement GL-18 cap VAPOR TUBE for Heidolph Bench-Top Series Used as replacements with Heidolph Bench-Top Series rotary evaporators. Tube is secured in rotary drive with low-stress plastic clip that seats into groove behind joint. Available plain or with Firestone splash guard to protect against splash-up. The vapor tube comes standard with all Heidolph bench-scale rotary evaporators. Type Joint Plain 24/ Plain 24/ Plain 29/ Plain 45/ w/splash Guard 24/ w/splash Guard 29/ Color Coated Glassware Ace Glass offers many of our existing glass vessels in various coated versions. Flasks, Pressure Bottles, Beakers, Bottles and many other items listed in this catalog can be amber or color coated on request. The coating is a proprietary process and gives excellent UV protection characteristics. Contact Ace for more details and pricing. ing & Product Information:

13 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS CAPS GL Thread, With Hole Red polybutylterapthalate (PBT) replacement caps with open tops for use with GL threads and with 7623 hose barbs. Temperature range to GL Thread Size CAPS GL Thread, Solid Red polybutylterapthalate (PBT) replacement caps with solid tops for use with GL threads. Temperature range to GL Thread Size HOSE CONNECTIONS GL with Rubber Seal Polypropylene hose connections with a silicone rubber seal for use with 7621 open-top caps. Available in either straight or bent styles. GL Thread Size CAPS Solid, SVL Replacement caps, solid with SVL thread, for Buchi glassware SVL Thread Size CAP Vent, SVL Replacement caps with open top and PTFE insert, retainer clip with SVL thread for Buchi glassware SVL Thread Size Buchi Part No For Engineering Support, visit

14 14 LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS Spare Parts, Glassware Assemblies R RB , , , , -32 C Interchangeable Receiver (W) , , , Series Single Receiver (E) , , Series ing & Product Information:

15 Spare Parts, Glassware Assemblies LARGE-SCALE INDUSTRIAL EVAPORATOR REPLACEMENT GLASSWARE COMPONENTS 15 D , -27 D , , , , , , , , , , , DB , -22 DB , , , , , , , , , , -18 For Engineering Support, visit

16 0115 P.O. Box 688 Vineland, NJ Fax: TOLL-FREE: FAX: