Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 1 of 12

Transcription

1 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 1 of 12 ZINUS INC #, HUANZHU ROAD, JIMEI DISTRICT, XIAMEN, FUJIAN, CHINA The following sample(s) was / were submitted and identified on behalf of the client as: Sample Description : 100% COTTON FIBER BARRIER SGS Ref No. : CAN & GZSL TX & GZSL TX Buyer : KEETSA INC. Manufacturer : ZINUS Supplier : ZINUS Country of Destination : USA Testing Request : As requested by applicant, selected test(s) with reference to OEKO-TEX Standard 100 edition 04/2012 Sample Receiving Date : Dec.20, 2012 Test Performing Date : Dec.20, 2012 to Jan.05, 2013 Test Result(s) : For further details, please refer to the following page(s) Signed for and on behalf of SGS-CSTC Co., Ltd. Jack Yao Approved signatory

2 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 2 of 12 Part A Test Summary To determine the ph Value in the submitted sample(s) with reference to Client s requirement. Determination of Free Formaldehyde content in the submitted sample(s) with reference to Client s requirement. To determine the Extractable Heavy Metals contents in the submitted sample(s) with reference to Client s requirement. Determination of Organostannic compounds contents in the submitted sample(s) with reference to Client s requirement. Determination of O-phenylphenol (OPP) content(s) in the submitted sample(s) with reference to Client s requirement. To determine Content(s) of PBBs & PBDEs in the selected parts on the submitted To determine the Tris(2,3-Dibromopropyl) phosphate(tris) content in the submitted To determine the Tris (aziridinyl) phosphineoxide (TEPA) content in the submitted To determine the Chlorinated Organic Carriers content in the submitted sample(s) with reference to Client s requirement. Determination of Chlorinated Phenols ( TeCP, PCP) content(s) in the submitted To determine the Tris(2 chloroethyl)phosphate (TCEP) content in the submitted To determine Polynuclear Aromatic Hydrocarbons (PAHs) in the submitted To determine the Short Chained Chlorinated Paraffins (SCCP) contents in the submitted To determine the Nonylphenol (NP), Octylphenol (OP), Nonylphenol Ethoxylates (NPEOs) and Octylphenol Ethoxylates (OPEOs) content(s) in the submitted To determine the Hexabromocyclododecane (HBCDD) content in the submitted Result Part B Determination of Smell Development (SNV : 1968) Colour Fastness To Water (ISO 105 E01:2010) Part C Colour Fastness To Perspiration (ISO 105 E04:2008)

3 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 3 of 12 Part A (SGS Ref No.: CAN ) Test Results : Test Part Description : Specimen No. SGS Sample ID Description 1 CAN Beige fabric sheet Remarks : (1) 1 mg/kg = % (2) MDL = Method Detection Limit (3) ND = Not Detected ( < MDL ) (4) "-" = Not Regulated ph Value Test Method : With reference to ISO 3071, test performed by ph meter Test Item(s) Limit 001 ph value Formaldehyde Test Method : With reference to JIS L 1041:2000 Section (b) Method B, analysis was preformed by UV-Vis. Free Formaldehyde Content 300 mg/kg 20 ND

4 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 4 of 12 Extractable Heavy metal Test Method : With reference to ISO 105-E04:2008, analysis was performed by ICP-MS and UV-VIS. Arsenic (As) 1 mg/kg 0.1 ND Antimony (Sb) 30 mg/kg 1.0 ND Cadmium (Cd) 0.1 mg/kg 0.05 ND Chromium (Cr) 2 mg/kg 0.5 ND Lead (Pb) 1.0 mg/kg 0.1 ND Mercury (Hg) 0.02 mg/kg 0.01 ND Copper (Cu) 50.0 mg/kg 5.0 ND Nickel (Ni) 4 mg/kg 0.5 ND Cobalt (Co) 4 mg/kg 0.5 ND Chromium VI (Cr VI) ND mg/kg 0.5 ND Organic-tin compounds Test Method : With reference to ISO 17353: 2004 with carbamate, analysis was performed by GC-MS. Dibutyl tin (DBT) 2 mg/kg 0.02 ND Tributyl tin (TBT) 1 mg/kg 0.02 ND Dioctyl tin (DOT) 2 mg/kg 0.02 ND Triphenyl tin (TPhT) 1 mg/kg 0.02 ND OPP Test Method : SGS in house method (GZTC CHEM-TOP ), analysis was performed by GC-MS. Test Item(s) CAS_NO Limit Unit MDL 001 O-phenylphenol (OPP) mg/kg 0.5 ND

5 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 5 of 12 PBBs/PBDEs Test Method : With reference to US EPA 3550C:2007 for PBBs / PBDEs content, analysis was performed by GC-MS. Monobromobiphenyl ND mg/kg 5 ND Dibromobiphenyl ND mg/kg 5 ND Tribromobiphenyl ND mg/kg 5 ND Tetrabromobiphenyl ND mg/kg 5 ND Pentabromobiphenyl ND mg/kg 5 ND Hexabromobiphenyl ND mg/kg 5 ND Heptabromobiphenyl ND mg/kg 5 ND Octabromobiphenyl ND mg/kg 5 ND Nonabromobiphenyl ND mg/kg 5 ND Decabromobiphenyl ND mg/kg 5 ND Pentabromodiphenyl ether ND mg/kg 5 ND Octabromodiphenyl ether ND mg/kg 5 ND Decabromodiphenyl ether ND mg/kg 5 ND TRIS(Tris(2,3-Dibromopropyl)-phosphate) Test Method : With reference to EPA 3550C:2007. Analysis was performed by LC-MS. Test Item(s) CAS_NO Limit Unit MDL 001 Tris(2,3-Dibromopropyl) ND mg/kg 5 ND -phosphate

6 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 6 of 12 Tris-(aziridinyl) phosphineoxide (TEPA) Test Method : With reference to US EPA 3550C:2007, Analysis was performed by GC-NPD or GC-MS. Tris-(aziridinyl) phosphineoxide (TEPA) ND mg/kg 5 ND Chlorinated Organic Carriers Test Method : With reference to DIN 54232:2007, analysis was conducted with GC-MS. Sum of chlorinated organic carriers 1 mg/kg 0.1 ND 2-Chlorotoluene - mg/kg 0.1 ND 3-Chlorotoluene - mg/kg 0.1 ND 4-Chlorotoluene - mg/kg 0.1 ND 1,3-Dichlorobenzene - mg/kg 0.1 ND 1,4-Dichlorobenzene - mg/kg 0.1 ND 1,2-Dichlorobenzene - mg/kg 0.1 ND 2,4-Dichlorotoluene - mg/kg 0.1 ND 2,5-Dichlorotoluene - mg/kg 0.1 ND 2,6-Dichlorotoluene - mg/kg 0.1 ND 1,3,5-Trichlorobenzene - mg/kg 0.1 ND 1,2,4-Trichlorobenzene - mg/kg 0.1 ND 1,2,3-Trichlorobenzene - mg/kg 0.1 ND 2,4,5-Trichlorotoluene - mg/kg 0.1 ND 2,3,6-Trichlorotoluene - mg/kg 0.1 ND 1,2,3,5-Tetrachlorobenzene - mg/kg 0.1 ND 1,2,4,5-Tetrachlorobenzene - mg/kg 0.1 ND 1,2,3,4-Tetrachlorobenzene - mg/kg 0.1 ND α,α,α,4-tetrachlorotoluene - mg/kg 0.1 ND Pentachlorobenzene - mg/kg 0.1 ND Pentachlorotoluene - mg/kg 0.1 ND Hexachlorobenzene - mg/kg 0.1 ND

7 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 7 of 12 Chlorinated Phenols Test Method : With reference to LFGB 64 BVL B :2001, analysis was performed by GC-ECD or GC-MS. 2,3,4,5-Tetrachlorophenol (2,3,4,5-TeCP) - mg/kg 0.05 ND 2,3,5,6-Tetrachlorophenol (2,3,5,6-TeCP) - mg/kg 0.05 ND 2,3,4,6-Tetrachlorophenol (2,3,4,6-TeCP) - mg/kg 0.05 ND Tetrachlorophenol (TeCP) 0.5 mg/kg - ND Pentachlorophenol (PCP) 0.5 mg/kg 0.05 ND Tris(2-chloroethyl)phosphate (TCEP) Test Method : With reference to EPA 3550C :2007.Analysis was performed by HPLC-MS. Test Item(s) CAS_NO Limit Unit MDL 001 Tris(2-chloroethyl) phosphate ND mg/kg 5 ND (TCEP)

8 PAHs Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 8 of 12 Test Method : With reference to ZEK of German ZLS and its amendments, analysis was performed by GC-MS. Naphthalene(NAP) - mg/kg 0.2 ND Acenaphthylene(ANY) - mg/kg 0.2 ND Acenaphthene(ANA) - mg/kg 0.2 ND Fluorene(FLU) - mg/kg 0.2 ND Phenanthrene(PHE) - mg/kg 0.2 ND Anthracene(ANT) - mg/kg 0.2 ND Fluoranthene(FLT) - mg/kg 0.2 ND Pyrene(PYR) - mg/kg 0.2 ND Benzo(a)anthracene(BaA) - mg/kg 0.2 ND Chrysene(CHR) - mg/kg 0.2 ND Benzo(b)fluoranthene(BbF) + - mg/kg 0.4 ND Benzo(j)fluoranthene(BjF) Benzo(k)fluoranthene(BkF) - mg/kg 0.2 ND Benzo(e)pyrene(BeP) - mg/kg 0.2 ND Benzo(a)pyrene(BaP) 1 mg/kg 0.2 ND Indeno(1,2,3-c,d)pyrene(IPY) - mg/kg 0.2 ND Dibenzo(a,h)anthracene(DBA) - mg/kg 0.2 ND Benzo(g,h,i)perylene(BPE) - mg/kg 0.2 ND Sum of 18 PAHs 10 mg/kg - ND

9 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 9 of 12 Short Chained Chlorinated Paraffin (SCCP) Test Method : With reference to US EPA 3550C: 2007, analysis was performed by GC-ECD. Short Chained Chlorinated Paraffin (SCCP) ND mg/kg 50 ND Nonylphenol (NP), Octylphenol (OP), Nonylphenol Ethoxylates (NPEOs) and Octylphenol Ethoxylates (OPEOs) Test Method : With reference to US EPA Method 3550C:2007, analysis was performed by LC-MS. Nonylphenol ethoxylates (NPEOs) 1000 mg/kg 10 ND Octylphenol ethoxylates (OPEOs) 1000 mg/kg 10 ND Nonylphenol(NP) 100 mg/kg 10 ND Octyphenol(OP) 100 mg/kg 10 ND Hexabromocyclododecane (HBCDD) Test Method : With reference to US EPA 3550C: 2007, analysis was performed by GC-MS. Hexabromocyclododecane (HBCDD) ND mg/kg 5 ND

10 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 10 of 12 Photo Appendix Part B (SGS Ref No.: GZSL TX) Test Result: Determination of Smell Development Of Shoes (SNV : 1968) Test Procedure: The samples was kept in a hermetically closed space with 37 C±1 C for a duration of 15 hours, in this status the smell independently judge by at least 3 persons and described by possibility of its type. The judgement 1 End Result Sample blank End Result Weak odour Odourless Photo Appendix

11 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 11 of 12 Part C (SGS Ref No.: GZSL TX) Test Result: Colour Fastness To Water (ISO 105 E01:2010) Requirement Change in shade 4-5 Min 3 Staining on multi-fiber Min 3 stripe Acetate 4-5 Cotton 4-5 Nylon 4-5 Polyester 4-5 Acrylic 4-5 Wool 4-5 Colour Fastness To Perspiration (ISO 105 E04:2008) Acidic Change in shade 4-5 Min 3-4 Staining on multi-fiber Min 3-4 stripe Acetate 4-5 Cotton 4-5 Nylon 4-5 Polyester 4-5 Acrylic 4-5 Wool 4-5 Alkaline Change in shade 4-5 Min 3-4 Staining on multi-fiber Min 3-4 stripe Acetate 4-5 Cotton 4-5 Nylon 4-5 Polyester 4-5 Acrylic 4-5 Wool 4-5 Remark: Grey Scale Rating is based on the 5-step scale of 1 to 5, where 1 is bad and 5 is good.

12 Test Report No.: SDHGR CM Date: Jan.07, 2013 Page 12 of 12 Photo Appendix Remark: This test was conducted at 198 Kezhu Road, Scientech Park Guangzhou Economic & Technology Development District, Guangdong Province, China. *** End of Report ***