CLAN LAB METHODS COOKING WITH CHEMICALS FOR FUN AND PROFIT...
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1 1 CLAN LAB METHODS COOKING WITH CHEMICALS FOR FUN AND PROFIT...
2 2 SOME FAVORITE RECIPES...
3 3 METHODS WE LL COVER METHAMPHETAMINE RED P AMMONIA P-2-P MDMA (Ecstasy) GHB
4 4 RED PHOSPHORUS METHOD RED PHOSPHORUS WITH IODINE NICKNAMES RED P METHOD HI METHOD IODINE METHOD RED &BLACK MEXICAN NATIONAL LAB
5 RED P METHOD 5
6 6 RED P METHOD Red phosphorus can be purchased in bulk quantities and shipped in a variety of containers.
7 7 RED P METHOD Red phosphorus can be purchased in bulk quantities and shipped in a variety of containers.
8 8 RED P METHOD Red phosphorus can be purchased in bulk quantities and shipped in a variety of containers.
9 9 RED P METHOD Striker plates are usually soaked in water or alcohol to remove the red phosphorus component. Usually 33%-65% of the striker plate surface.
10 10 RED P METHOD Flares contain 30-40% red phosphorus on the striker plate (cap).
11 11 STEP 1 - TABLET EXTRACTION GRIND TABLETS PLACE IN CONTAINER ADD SOLVENT (Alcohol or water) SHAKE LET SIT SEPARATE LIQUID FROM BINDER USING FILTER PAPER USE BINDER AS CUT, USUALLY THROWN AWAY.
12 12 TABLET EXTRACTION Large scale extraction of pseudoephedrine.
13 13 TABLET EXTRACTION Coffee grinders are used to break down the tablets to extract the ephedrine or pseudoephedrine.
14 14 TABLET EXTRACTION Mixers are used to break down the tablets to extract the ephedrine or pseudoephedrine.
15 15 TABLET EXTRACTION EXTRACT EPHEDRINE PSUEDOEPHERINE
16 16 TABLET EXTRACTION Pseudoephedrine products Tablets Caplets Pills Liquid (Many gel caps are orange or green colored)
17 17 TABLET EXTRACTION- SOLVENTS ALCOHOLS ARE EXCELLENT SOLVENTS FOR EXTRACTING EPHEDRINE SELECTIVELY EXTRACT FROM TABLETING EVAPORATE QUICKLY EXAMPLES DENATURED ALCOHOL METHANOL ISOPROPYL ALCOHOL
18 TABLET EXTRACTION Lighter Fluid works, yet is a poor choice. Alcohol is the common solvent used to extract pseudoephedrine. 18
19 19 TABLET EXTRACTION Denatured alcohol is an excellent solvent, due to its rate of evaporation.
20 20 TABLET EXTRACTION- SOLVENTS Mason Jars usually are the container of choice used to extract the ephedrine or pseudoephedrine from the binder.
21 21 TABLET EXTRACTION- SOLVENTS Large-scale extraction of ephedrine or pseudoephedrine requires largescale equipment.
22 22 TABLET EXTRACTION- SOLVENTS Large-scale extraction of ephedrine or pseudoephedrine requires largescale equipment.
23 23 TABLET EXTRACTION- SOLVENTS Hot plates are a typical method used to evaporate alcohol from the dissolved ephedrine/pseudoephedrine.
24 TABLET EXTRACTION- SOLVENTS Stoves can also be used to evaporate the solvent. This is not recommended by experienced cookers. 24
25 25 TABLET EXTRACTION- SOLVENTS Mexican national organizations utilize large propane camp burners and pots for largescale extraction.
26 26 TABLET EXTRACTION- SOLVENTS Mexican national organizations utilize large propane camp burners and pots for large-scale extraction.
27 27 TABLET EXTRACTION- WATER WATER CANBE USED Pseudoephedrine Hydrochloride is water soluble Since pseudoephedrine, Red phosphorus and Iodine are all Solid compounds, water is necessary for the reduction to occur. Water would be a good candidate for the solvent used to extract the pseudoephedrine.
28 28 TABLET EXTRACTION- WATER Pseudoephedrine pills Solvent Pills dissolved in Solvent. Binder sinks Pseudo suspended in solvent. Binder
29 TABLET EXTRACTION- WATER Filter out Binder Filter medium funnel Evaporate solvent Scrape out pseudoephedrine 29
30 30 STEP 2 - COOKING COMBINE PSEUDOEPHEDRINE
31 31 STEP 2 - COOKING COMBINE PSEUDOEPHEDRINE PHOSPHOROUS
32 32 STEP 2 - COOKING COMBINE PSEUDOEPHEDRINE PHOSPHOROUS IODINE
33 33 STEP 2 - COOKING COMBINE PSEUDOEPHEDRINE PHOSPHOROUS IODINE COOK (REFLUX) (amount of time depends on recipe.)
34 34 STEP 2 - COOKING COMBINE PSEUDOEPHEDRINE PHOSPHOROUS IODINE COOK (REFLUX) (amount of time depends on recipe.)
35 35 STEP 2 - COOKING COMBINE PSEUDOEPHEDRINE PHOSPHOROUS IODINE COOK (REFLUX) COOL
36 36 STEP 2 - COOKING COMBINE PHOSPHOROUS IODINE PSEUDOEPHEDRINE COOK (REFLUX) COOL SEPARATE LIQUID STRONG ACID
37 37 STEP 2 - COOKING COMBINE PHOSPHOROUS IODINE PSEUDOEPHEDRINE COOK (REFLUX) COOL SEPARATE LIQUID STRONG ACID SAVE SLUDGE (RED-P)
38 38 STEP 2 - COOKING SAVE SLUDGE (RED-P)
39 39 COOKING Red phosphorus usually will stain the reaction vessels.
40 COOKING The iodine / hydriodic acid vapors are also found at the cook location. 40
41 COOKING 41
42 42 SUBSTITUTIONS RED PHOSPHORUS... WHITE PHOSPHORUS HYPOPHOSPHORUS ACID IODINE... TINCTURE OF IODINE HYDRIODIC ACID (IF AVAILABLE)
43 43 SUBSTITUTIONS Iodine can be purchased in prill (small beads), flakes and BB size shot.
44 44 SUBSTITUTIONS Iodine very corrosive and toxic and suspect carcinogen.
45 45 SUBSTITUTIONS Household Iodine tincture has 1-3% iodine dissolved in alcohol.
46 46 SUBSTITUTIONS Veterinarian grade tincture is found in 7% to 15.5% solution.
47 47 SUBSTITUTIONS Hydrogen peroxide is mixed with tincture of iodine to precipitate the iodine in hours.
48 48 SUBSTITUTIONS Iodine crystals that have been crashed out of the tincture utilizing hydrogen peroxide.
49 49 AFTER REFLUX TO SEPARATE THE REACTION MIXTURE Filter out red phosphorous/iodine crystals Filter medium funnel RED P SLUDGE CAN BE REUSED (Meth analyte in acid)
50 50 TO SEPARATE REACTION Funnels and filter paper is typically used to separate the red phosphorus after the reflux, from the water (acid) phase.
51 ALTERNATE METHOD TO SEPARATE REACTION 51 Large labs have been known to use bed sheets and buckets.
52 52 STEP 3 - SEPARATION RAISE ph > ADD SODIUM HYDROXIDE (LYE) OIL LAYER FORMS METH BASE (meth oil) ADD ORGANIC SOLVENT (Coleman fuel or ether) SEPARATE LAYERS (Organic layer on top usually, water layer on bottom)
53 53 SEPARATION Sodium hydroxide (lye) is used to raise the ph and separate the meth oil from the aqueous phase.
54 54 SEPARATION Sodium hydroxide (lye) is used to raise the ph and separate the meth oil from the aqueous phase.
55 55 STEP 3 - SEPARATION RAISE ph > ADD SODIUM HYDROXIDE (LYE) OIL LAYER FORMS METH BASE (meth oil) ADD ORGANIC SOLVENT (Coleman fuel or ether) SEPARATE LAYERS (Organic layer on top, water layer on bottom)
56 56 SEPARATION Ether is a common candidate for dissolving meth base (oil) prior to separating the oil and ether from the water phase.
57 57 SEPARATION White gas (camp fuel) is the other most common solvent used to help extract the meth oil and separate from the water phase.
58 58 SEPARATION White gas (camp fuel) is the other most common solvent used to help extract the meth oil and separate from the water phase.
59 59 METH SOLUBILITY METH BASE METH HCL WATER INSOLUBLE SOLUBLE SOLVENTS SOLUBLE INSOLUBLE
60 60 REVIEW - SEPARATION STEP = METH OIL SOLVENT WATER WATER WATER AMBER LIQUID ADD NaOH (OIL FORMS) ADD SOLVENT
61 61 SEPARATE LAYERS POUR THE LIQUIDS INTO A SEPARATORY FUNNEL DRAINS FROM THE BOTTOM
62 62 ALTERNATE METHODS FOR SEPARATING LIQUIDS USE ANY CONTAINER WITH A SPIGOT WATER BOTTLES ARE ALSO VERY COMMON.
63 63 STEP 4 - SALTING OUT BUBBLE HYDROGEN CHLORIDE GAS THROUGH SOLVENT CRYSTALS FORM METH HYDROCHLORIDE
64 64 STEP 4 - SALTING OUT BUBBLE HYDROGEN CHLORIDE GAS THROUGH SOLVENT CRYSTALS FORM METH HYDROCHLORIDE
65 65 STEP 4 - SALTING OUT Separate through filter
66 SALTING OUT HCL acid gas generators are typically plastic gas cans, or plastic soda bottles. 66
67 67 SALTING OUT HCL acid gas generator may be a 1 liter soda bottle or similar vessel.
68 68 SALTING OUT HCL acid gas generator may be a 1 liter soda bottle or similar vessel.
69 69 SALTING OUT The tip of the tubing is an excellent place to typically find meth HCL product notice the residue.
70 70 SALTING OUT Large Mexican National Labs are great candidates for supers labs (10lbs/day) and are referred to as Ranches.
71 71 METHODS FOR SALTING OUT SULFURIC ACID + ROCK SALT MURIATIC ACID + ALUMINUM FOIL GAS CAN HCL GAS HCL GAS ACID SOLID
72 72 METHODS FOR SALTING OUT Sulfuric acid is the most common means of producing an HCL gas generator.
73 73 METHODS FOR SALTING OUT Rock salt (NaCl) is commonly used in a gas generator with sulfuric acid (H 2 SO 4 ) to produce HCL gas.
74 74 ALTERNATE RED P METHODS SPORTS BOTTLE COLD COOK NO HEAT APPLIED EXPLOSIVE!!! POOR YIELD PHOSPHINE IS PRODUCED
75 75 ALTERNATE RED P METHODS SPORTS BOTTLE COLD COOK NO HEAT APPLIED EXPLOSIVE!!! POOR YIELD PHOSPHINE IS PRODUCED
76 76 ALTERNATE RED P METHOD PRESSURE COOKER JELLY JARS WITH CHEMICALS PLACED IN COOKER HEAT WHEN ALL BOTTLES HAVE EXPLODED- DONE!
77 77 ALTERNATE RED P METHOD PRESSURE COOKER JELLY JARS WITH CHEMICALS PLACED IN COOKER HEAT WHEN ALL BOTTLES HAVE EXPLODED- DONE!
78 78 ANHYDROUS AMMONIA METHOD AMMONIA WITH LITHIUM OR SODIUM NICKNAMES AMMONIA METHOD NAZI METHOD BIRCH METHOD LITHIUM METHOD
79 79 ANHYDROUS AMMONIA ANHYDROUS MEANS WITHOUT WATER = CONCENTRATED FORM OF CHEMICAL
80 80 AMMONIA SOURCES COMPRESSED GAS CYLINDERS LIQUID AMMONIA FERTILIZER REFRIGERANT GAS AMMONIUM NITRATE/SULFATE AND LYE LOOK FOR PROPANE TANKS CAN FAIL IN LESS THAN THREE WEEKS!!! THERMOS JUGS FIRE EXTINGUISHERS
81 81 AMMONIA SOURCES Ammonia is often placed in propane cylinders for transport and storage.
82 82 AMMONIA SOURCES Illegal anhydrous Ammonia tank
83 83 AMMONIA SOURCES Anhydrous ammonia tanks vessels.
84 84 AMMONIA SOURCES Replacement valves for ammonia tanks.
85 AMMONIA SOURCES Lye can be mixed with ammonium nitrate and water to produce ammonia gas. 85
86 86 AMMONIA SOURCES Lye can be mixed with ammonium sulfate or ammonium nitrate and water to produce ammonia gas.
87 87 LITHIUM & SODIUM HIGHLY WATER REACTIVE REACTIVE WITH MOISTURE IN AIR CHEMICAL SUPPLY PACKED IN OIL OR MINERAL SPIRITS TO EXCLUDE AIR WIRE OR SOLID CHUNKS GROCERY STORE CAMERA BATTERIES - LITHIUM CAN MAKE SODIUM FROM LYE/DRANO!!
88 LITHIUM & SODIUM Lithium batteries are the most common reactive metal used in ammonia labs. 88
89 89 LITHIUM & SODIUM Stripped lithium batteries are common wastes in the ammonia method of manufacturing meth.
90 LITHIUM & SODIUM Lithium battery stripes will oxidize to a darker color if not placed in some type of mineral spirit before use. 90
91 91 SODIUM FROM LYE/DRANO NaOH - + Na + - OH BATTERY HEAT LYE LYE ELECTROPLATE METAL
92 SODIUM FROM LYE/DRANO 92
93 SODIUM FROM LYE/DRANO 93
94 SODIUM FROM LYE/DRANO 94
95 95 STEP 1 - TABLET EXTRACTION SAME AS OTHER METHODS EXCEPT WATER IS NOT AN OPTION!! WATER REACTS WITH THE METALS
96 96 STEP 2 - REACTION TO A CONTAINER ADD EPHEDRINE ANHYDROUS AMMONIA LITHIUM OR SODIUM METAL MIX
97 97 STEP 2 - REACTION TO A CONTAINER ADD EPHEDRINE ANHYDROUS AMMONIA LITHIUM OR SODIUM METAL MIX
98 98 REACTION Pseudoephedrine with lithium metal in Pyrex dish.
99 99 REACTION CONTINUED... ALLOW AMMONIA TO EVAPORATE ADD WATER DECOMPOSE METAL OUCH!!! LET COOL OIL LAYER FORMS METH BASE!
100 100 REACTION CONTINUED... ALLOW AMMONIA TO EVAPORATE ADD WATER DECOMPOSE METAL OUCH!!! LET COOL OIL LAYER FORMS METH BASE!
101 101 REACTION CONTINUED... ALLOW AMMONIA TO EVAPORATE ADD WATER DECOMPOSE METAL OUCH!!! LET COOL OIL LAYER FORMS METH BASE!
102 102 STEP 3 - SEPARATION ADD ORGANIC SOLVENT (Top Layers) SEPARATE THE LAYERS
103 103 STEP 3 - SEPARATION ADD ORGANIC SOLVENT (Top Layers) SEPARATE THE LAYERS
104 104 STEP 3 - SEPARATION ADD ORGANIC SOLVENT (Top Layers) SEPARATE THE LAYERS
105 105 STEP 4 - SALTING OUT BUBBLE HYDROGEN CHLORIDE GAS THROUGH SOLVENT METH PRECIPITATE FORMS METH HCL
106 106 STEP 4 - SALTING OUT BUBBLE HYDROGEN CHLORIDE GAS THROUGH SOLVENT METH PRECIPITATE FORMS METH HCL
107 107 SALTING OUT Epsom salt (magnesium sulfate) is sometimes used as a drying agent to dry the wet HCL gas.
108 THIONYL CHLORIDE METHOD- HAZARDS ONLY 108 PSEUDOEPHEDRINE IS PRECURSOR THIONYL CHLORIDE WITH CHLOROFORM NICKNAMED HYDROGENATION METHOD SHAKE-N-BAKE REACTIVE CATALYSTS RANEY NICKEL PALLADIUM BLACK
109 109 THIONYL HAZARDS THIONYL CHLORIDE WATER REACTIVE- FORMS HYDROCHLORIC AND SULFURIC ACIDS HYDROGEN GAS PRESSURE FLAMMABLE CATALYST WATER REACTIVE CHLOROFORM SUSPECTED CARCINOGEN
110 110 HYDROGENATION PRESSURE GAUGE HYDROGEN FILL HOSE HYDROGEN GAS SHAKE PRESSURIZE REPEAT METH in ALCOHOL HYDROGENATOR PRESSURE VESSEL WASTE CATALYST SLUDGE
111 111 HOMEMADE HYDROGENATOR
112 112 HOMEMADE HYDROGENATOR
113 113 HOMEMADE HYDROGENATOR
114 114 PHENYL-2-PROPANONE MANUFACTURE BENZYL CHLORIDE TO BENZYL CYANIDE BENZYL CYANIDE TO PAA PAA TO P2P
115 115 PHENYL-2-PROPANONE METHOD PHENYL-2-PROPANONE (P-2-P) WITH METHYLAMINE AND ALUMINUM FOIL NICKNAMED P-2-P METHOD FOIL METHOD BIKER METHOD PROP DOPE METHOD
116 116 FOIL PREPARATION COOKERS WILL OFTEN WASH FOIL IN SODIUM HYDROXIDE RED DEVIL LYE DRANO CRYSTALS SHRED FOIL INCREASES SURFACE AREA OF FOIL
117 117 P-2-P REACTION REACTION IS SLIGHTLY EXOTHERMIC REACTION OCCURS ON FOIL SURFACE FOIL CONSUMED IN REACTION GREY SLUDGE AT BOTTOM OF FLASK
118 118 STEP 1 - REACTION COMBINE P-2-P METHYLAMINE MERCURIC CHLORIDE ALCOHOL ALUMINUM FOIL ALLOW TO REACT LET COOL
119 119 STEP 2 - SEPARATION OIL LAYER FORMS - METH BASE FILTER REACTION TO REMOVE GREY SLUDGE (ALUMINUM) ADD ORGANIC SOLVENT SEPARATE SOLVENT LAYER
120 120 STEP 3 - SALTING OUT BUBBLE HYDROGEN CHLORIDE GAS THROUGH SOLVENT CRYSTALS FORM METH HYDROCHLORIDE
121 121 HAZARD COMPARISON METHOD RED PHOSPHOROUS AMMONIA THIONYL CHLORIDE P-2-P HAZARDS PHOSPHINE GAS IODINE IRRITANT/FLAM GAS WATER RX METALS ACID GASES CARCINOGEN IRRITANT/FLAM GAS CNS TOXICANT
122 122 PRODUCTION COMPARISON METHOD RED PHOSPHOROUS AMMONIA THIONYL CHLORIDE P-2-P TIME / YIELD 1-11/2 DAYS % 1-2 HOURS 95 PLUS % 2-2 1/2 DAYS % 1-11/2 DAYS %
123 123 Begin with Safrole Sassafras oil contains 80% safrole DEA placed sassafras oil on watched list. Sassafras tree grows naturally in the south, southeast, eastern seaboard, and in the Appalachian Mountain regions.
124 Ecstasy 124
125 125 Components of Sassafras Oil Component % Composition 1atm ( C) Pinene 2 10% 154 Phelladrene 2 10% 175 D-Camphor 0 5% 204 Safrole 80 90% 234 Eugenol 0 10 % 252
126 126 Separate Safrole Oil Easiest method: 1. Wash sassafras oil with 28% acetic acid to removed eugenol, pinene, and camphor oils. 2. Wash remaining oil with water to remove other contaminants. 3. Wash oil with denatured alcohol to dissolve safrole (leaving phelladrene behind). 4. Heat denatured alcohol until alcohol has evaporated leaving safrole behind.
127 127 Safrole to Isosafrole Combine Safrole oil Sodium or potassium hydroxide Denatured alcohol Reflux at C for hours Dark colored mixture is isosafrole
128 128 MDP-2-P Production 1. Place a large flask or container with 30% hydrogen peroxide and 88% formic acid in an ice bath. 2. Combine isosafrole and acetone in a seperatory funnel. 3. Slowly add the isosafrole/acetone solution drop wise to the chilled hydrogen peroxide/formic acid solution. Ensure temperature stays below 20 C. Solution will turn from yellow to orange. 4. Let solution sit and warm to room temperature. Solution will turn to dark red.
129 129 MDP-2-P Production Cont. 5. Distill or allow acetone and formic acid to evaporate. A thick black liquid should remain. 6. Add methanol and 15% sulfuric acid to the thick black liquid and reflux for three hours. 7. Allow liquid to cool (oil layer will develop on bottom of container) and add an organic solvent. 8. Transfer organic solvent to another container and wash solvent with 5% sodium hydroxide to neutralize any formic acid still left. 9. Evaporate organic solvent. Remaining oil is MDP-2-P.
130 130 MDMA (ECSTASY) MANUFACTURING MULTIPLE ROUTES POSSIBLE USING MDP-2-P COMMON ROUTE FOLLOWS P-2-P/ METHYLAMINE PROCEDURE USES SAME CHEMICALS FOLLOWS SAME STEPS
131 131 STEP ONE - REACTION COMBINE THE FOLLOWING MDP-2-P METHYLAMINE MERCURIC CHLORIDE ALCOHOL FOIL LET REACT TO COMPLETION EXOTHERMIC
132 132 STEP 2 - SEPARATION WHEN REACTION IS COMPLETE OIL LAYER FORMS - MDMA BASE FILTER REACTION TO REMOVE GREY SLUDGE (ALUMINUM) ADD ORGANIC SOLVENT SEPARATE SOLVENT LAYER MDMA OIL IS IN SOLVENT LAYER
133 133 STEP 3 - SALTING OUT BUBBLE HYDROGEN CHLORIDE GAS THROUGH SOLVENT CRYSTALS FORM MDMA HYDROCHLORIDE
134 134 GHB MANUFACTURING GAMMA HYDROXYBUTYRATE ONE STEP REACTION COMBINE GAMMABUTYROLACTONE (GBL) WITH LYE HEAT
135 135 GHB MANUFACTURING Butyrolactone is the common precursor for GHB.
136 136 GHB MANUFACTURING Baking soda is a buffered base that can be used to convert GBL to GHB
137 137 GHB ALTERNATIVES USERS DISCOVERED: DON T NEED TO MAKE GHB, JUST INGEST GBL BODY CONVERTS INTO GHB CAN ALSO INGEST 1,4-BUTANEDIOL BODY CONVERTS INTO GHB SAME PATHWAY AS ALCOHOL DEHYDROGENASE
138 GHB ALTERNATIVES 138
139 GHB ALTERNATIVES 139
140 140 CONVERSIONS 1 GRAM = 1000mg 3.5 GRAMS = 1/8 th OUNCE (EIGHTBALL) 14 GRAMS = ½ OUNCE 28 GRAMS = 1 OUNCE 454 GRAMS = 1 POUND
141 141 CLAN LAB METHODS WHAT WILL THEY THINK OF NEXT?...
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