Bundesanstalt für Materialforschung und -prüfung
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1 Bundesanstalt für Materialforschung und -prüfung in co-operation with the Committee of Chemists of the GDMB Gesellschaft für Bergbau, Metallurgie, Rohstoff- und Umwelttechnik Certified Reference Material BAM-M382 Pure Copper Certified values Element Mass fraction Uncertainty * in µg/g in µg/g Ag 1,8 ± 0,2 Al < 2,5 Bi 0,53 ± 0,03 Cd 0,90 ± 0,09 Co 0,73 ± 0,07 Cr 0,56 ± 0,06 Fe 6,0 ± 0,4 Mn 0,76 ± 0,06 Ni 1,7 ± 0,2 Pb 1,0 ± 0,2 Sb 0,7 ± 0,2 Se 0,6 ± 0,1 Si < 6 Sn 4,29 ± 0,21 Te 0,61 ± 0,06 Zn 6,0 ± 0,5 Zr < 3 Indicatory values Element Mass fraction Uncertainty * in µg/g in µg/g As 0,6 ± 0,2 Mg 1,4 ± 0,3 S 3,2 ± 1,4 Ti 0,6 ± 0,2 *Half-width of the confidence interval of the certified value at a level of confidence of 95%, calculated from the standard deviation of mean of laboratory means BAM-M382 is intended for calibration, recalibration and checking of X-ray fluorescence and spark emission spectrometers. The reference material is available in cylindrical form (diameter: 4 cm, height: 3 cm). Date of issue: March 2006
2 Means of accepted data sets (for one method at one laboratory, respectively) Mass fraction in µg/g Certified values Indicatory values Line no. Ag Al Bi Cd Co Cr Fe Mn Ni Pb Sb Se Si Sn Te Zn Zr As Mg S Ti 1 0,95 0,19 0,48 0,74 0,59 0,413 4,51 0,592 1,286 0,512 0, ,34 3,82 0, ,05 0,432 1,0 0,447 0, ,32 0,51 0,49 0,75 0,638 0,49 5,00 0,656 1,405 0,719 0,542 0,462 1,0 3,93 0, ,22 0,437 1,098 < 1,35 0, ,40 1,3 0,51 0,76 0,66 0,502 5,15 0,710 1,447 0,823 0,577 0,540 1,35 4,145 0,586 5,21 0,8 0,445 1,20 2,20 0, ,57 1,42 0,53 0,816 0,67 0,52 5,70 0,72 1,50 0,927 0,593 0,552 2,52 4,195 0,608 5,45 0,95 0,517 1,25 3,477 0, ,76 1,96 0,54 0,83 0,70 0,530 5,85 0,725 1,554 0,970 0,602 0,56 4,90 4,20 0,660 5,97 1,13 0,541 1,45 3,598 0,68 6 1,86 0,54 0,875 0,72 0,530 5,91 0,752 1,598 1,005 0,634 0,574 4,238 0,663 5,99 1,68 < 0,63 1,51 3,679 0,68 7 1,86 0,57 0,882 0,73 0,54 6,22 0,760 1,630 1,038 0,643 0,616 4,27 0,678 6,11 1,98 0,657 1,59 3,72 0, ,89 0,58 0,94 0,81 0,570 6,30 0,762 1,722 1,10 0,657 0,73 4, ,22 2,33 0,73 1,71 5,198 < 1 9 1, ,960 0,85 0,620 6,38 0,775 1,770 1,192 0,818 4,522 6,37 2,73 0,80 2, ,93 1 0,90 0,638 6,42 0,80 1,813 1,3 0,93 4,53 6, ,96 1,08 0,682 6,48 0,833 1,82 1,352 0,98 4, ,00 1,13 0,686 6,55 0,90 2,12 1,494 1, , ,59 0,905 2, ,13 6, ,38 6, M : 1,80 < 2,5 0,528 0,90 0,725 0,56 5,98 0,76 1,68 1,039 0,71 0,58 < 6 4,29 0,61 6,02 < 3 s M : 0,356 0,036 0,128 0,098 0,082 0,668 0,088 0,273 0,280 0,185 0,083 0,299 0,070 0,510 s i : 0,142 0,042 0,036 0,040 0,073 0,319 0,038 0,172 0,127 0,070 0,052 0,167 0,036 0,378 The laboratory mean values have been examined statistically to eliminate outlying values. Where --- appears in the table it indicates that an outlying value has been omitted. A data set consists of at least 4 but usually 6 single values of one laboratory. Phosphorus was determined by three laboratories (0,24; 0,60; < 0,54 µg/g). M: mean of means of data sets s M : standard deviation of means of data sets s i : mean of standard deviations of data sets in case of repeatability
3 Analytical Methods Element Line no. Ag 1, 2, 8, 10 Inductively Coupled Plasma Optical Emission Spectrometry 3, 12, 14 Inductively Coupled Plasma Mass spectrometry 4 Activation Analysis with High-Energy Photons 5 Glow Discharge Optical Emission Spectrometry 6 Electrothermal Atomic Absorption Spectrometry 7 Laser Ablation Inductively Coupled Plasma Mass spectrometry 9 Globule Arc Optical Emission Spectrometry 11 Neutron Activation Analysis 13 Spark Optical Emission Spectrometry 15 Synchrotron X-ray fluorescence analysis Al 1, 5 Inductively Coupled Plasma Mass spectrometry 2, 3, 4 Inductively Coupled Plasma Optical Emission Spectrometry As 1, 4 Spark Optical Emission Spectrometry 2 Inductively Coupled Plasma Mass spectrometry 3 Laser Ablation Inductively Coupled Plasma Mass spectrometry 5 Electrothermal Atomic Absorption Spectrometry 6 Inductively Coupled Plasma Optical Emission Spectrometry 7, 9 Globule Arc Optical Emission Spectrometry 8 Activation Analysis with High-Energy Photons Bi 1, 5, 7 Inductively Coupled Plasma Mass spectrometry 2 Spark Optical Emission Spectrometry 3, 8 Globule Arc Optical Emission Spectrometry 6 Laser Ablation Inductively Coupled Plasma Mass spectrometry Cd 1, 5, 12 Inductively Coupled Plasma Optical Emission Spectrometry 2 Laser Ablation Inductively Coupled Plasma Mass spectrometry 3, 8, 11 Inductively Coupled Plasma Mass spectrometry 4, 9 Electrothermal Atomic Absorption Spectrometry 6, 7, 10 Spark Optical Emission Spectrometry Co 1 Laser Ablation Inductively Coupled Plasma Mass spectrometry 2, 3, 7 Inductively Coupled Plasma Mass spectrometry 4, 9 Inductively Coupled Plasma Optical Emission Spectrometry 5 Neutron Activation Analysis 6 Spark Optical Emission Spectrometry 8 Electrothermal Atomic Absorption Spectrometry 10 Glow Discharge Optical Emission Spectrometry Cr 1 Laser Ablation Inductively Coupled Plasma Mass spectrometry 2, 12 Inductively Coupled Plasma Optical Emission Spectrometry 3 Electrothermal Atomic Absorption Spectrometry 4, 7, 10 Spark Optical Emission Spectrometry 5, 8, 9 Inductively Coupled Plasma Mass spectrometry 6 Neutron Activation Analysis 11 Glow Discharge Optical Emission Spectrometry Fe 1, 2, 5, 6 Inductively Coupled Plasma Optical Emission Spectrometry 3 Electrothermal Atomic Absorption Spectrometry 4, 13 Inductively Coupled Plasma Mass spectrometry 7 Laser Ablation Inductively Coupled Plasma Mass spectrometry 8 Globule Arc Optical Emission Spectrometry 9 Glow Discharge Optical Emission Spectrometry 10, 11, 14 Spark Optical Emission Spectrometry 12 Photometry BAM-M382 page 3 of 6 pages
4 Element Line no. Mg 1, 2, 3, 6 Inductively Coupled Plasma Optical Emission Spectrometry 4, 8 Inductively Coupled Plasma Mass spectrometry 5, 7, 9 Spark Optical Emission Spectrometry Mn 1, 2, 9 Inductively Coupled Plasma Mass spectrometry 3, 6, 7, 13 Inductively Coupled Plasma Optical Emission Spectrometry 4 Activation Analysis with High-Energy Photons 5 Laser Ablation Inductively Coupled Plasma Mass spectrometry 8 Electrothermal Atomic Absorption Spectrometry 10, 11, 12 Spark Optical Emission Spectrometry Ni 1, 9, 13 Inductively Coupled Plasma Mass spectrometry 2, 6 Electrothermal Atomic Absorption Spectrometry 3 Globule Arc Optical Emission Spectrometry 4, 7, 11 Spark Optical Emission Spectrometry 5, 10 Inductively Coupled Plasma Optical Emission Spectrometry 8 Laser Ablation Inductively Coupled Plasma Mass spectrometry 12 Activation Analysis with High-Energy Photons Pb 1, 5, 12 Inductively Coupled Plasma Mass spectrometry 2, 6 Electrothermal Atomic Absorption Spectrometry 3 Inductively Coupled Plasma Optical Emission Spectrometry 4 Laser Ablation Inductively Coupled Plasma Mass spectrometry 7, 8 Globule Arc Optical Emission Spectrometry 9, 10 Spark Optical Emission Spectrometry 11 Neutron Activation Analysis S 1, 7 Spark Optical Emission Spectrometry 2 Inductively Coupled Plasma Optical Emission Spectrometry 3 Carrier gas hot extraction with IR-detection (gas calibration) 4 Titration 5, 6 Photometry 8 Glow Discharge Optical Emission Spectrometry Sb 1, 5 Electrothermal Atomic Absorption Spectrometry 2 Synchrotron X-ray fluorescence analysis 3 Laser Ablation Inductively Coupled Plasma Mass spectrometry 4, 7 Inductively Coupled Plasma Mass spectrometry 6 Neutron Activation Analysis 8 Photometry 9, 11 Globule Arc Optical Emission Spectrometry 10 Activation Analysis with High-Energy Photons 12 Spark Optical Emission Spectrometry Se 2, 3 Electrothermal Atomic Absorption Spectrometry 4 Laser Ablation Inductively Coupled Plasma Mass spectrometry 5, 7, 8 Spark Optical Emission Spectrometry 6 Neutron Activation Analysis Si 1, 2, 3 Spark Optical Emission Spectrometry 4 Glow Discharge Optical Emission Spectrometry 5 Inductively Coupled Plasma Optical Emission Spectrometry Sn 1, 9 Inductively Coupled Plasma Mass spectrometry 2 Globule Arc Optical Emission Spectrometry 3, 4, 7 Inductively Coupled Plasma Optical Emission Spectrometry 5 Activation Analysis with High-Energy Photons 6 Laser Ablation Inductively Coupled Plasma Mass spectrometry 8 Electrothermal Atomic Absorption Spectrometry 10, 11 Spark Optical Emission Spectrometry BAM-M382 page 4 of 6 pages
5 Element Line no. Te 1, 5 Electrothermal Atomic Absorption Spectrometry 2, 6, 8 Inductively Coupled Plasma Mass spectrometry 3 Laser Ablation Inductively Coupled Plasma Mass spectrometry 4 Synchrotron X-ray fluorescence analysis 7 Globule Arc Optical Emission Spectrometry Ti 1, 3, 4 Inductively Coupled Plasma Optical Emission Spectrometry 2, 7, 8 Inductively Coupled Plasma Mass spectrometry 5, 6 Spark Optical Emission Spectrometry Zn 3 Glow Discharge Optical Emission Spectrometry 4, 10 Spark Optical Emission Spectrometry 5, 8, 9 Inductively Coupled Plasma Optical Emission Spectrometry 6 Laser Ablation Inductively Coupled Plasma Mass spectrometry 7 Inductively Coupled Plasma Mass spectrometry Zr 1, 6 Inductively Coupled Plasma Mass spectrometry 2, 3, 4 Inductively Coupled Plasma Optical Emission Spectrometry 5, 8, 9 Spark Optical Emission Spectrometry 7 Activation Analysis with High-Energy Photons BAM-M382 page 5 of 6 pages
6 Participating Laboratories Boliden Mineral AB, Boliden, Sweden Bundesanstalt für Materialforschung und -prüfung (BAM), Berlin, Germany Laboratory I.11 (Metal Analysis) Laboratory I.43 (Activation Analysis, Gas Analysis) Project Group I.1902 Copper Refineries Pty. Ltd, Xstrata Copper, Brisbane, Australia Diehl Metall Stiftung & Co. KG, Röthenbach a. d. Pegnitz, Germany Institut für Kernchemie, University of Mainz, Germany Institut für NE-Metallurgie und Reinststoffe, TU Bergakademie Freiberg, Germany Korrosions- och Metallforskningsinstitutet AB (KIMAB), Stockholm, Sweden KM Europa Metal AG, Osnabrück, Germany LECO Instrumente GmbH, Mönchengladbach, Germany Montanwerke Brixlegg AG, Brixlegg, Austria Norddeutsche Affinerie AG, Hamburg, Germany Outukumpu Poricopper Oy, Pori, Finland Ridsdale & Co. Ltd., Middlesbrough, UK Tréfimétaux SA, Sérifontaine, France Umicore, Olen, Belgium Wieland-Werke AG, Ulm, Germany BAM Berlin BAM Berlin Department I Division I.1 Analytical Chemistry; Inorganic-chemical Analysis; Reference Materials Reference Materials Prof. Dr. U. Panne (Head of Department) Dr. R. Matschat (Head of Division) Berlin, Sale: Bundesanstalt für Materialforschung und -prüfung Richard-Willstätter-Straße Berlin Phone: Fax: sales.crm@bam.de BAM-M382 page 6 of 6 pages
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