ANALYTICAL RESULTS. Project: NLNA - Cistern Water Testing. Submittal Date: 04/26/2010 Group Number: State of Sample Origin: PA
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1 ANALYTICAL RESULTS Prepared by: Lancaster Laboratories 2425 New Holland Pike Lancaster, PA Prepared for: Philadelphia PA 923 May 0, 200 Project: - Cistern Water Testing Submittal Date: 04/26/200 Group Number: 9887 State of Sample Origin: PA Client Sample Description Lancaster Labs (LLI) # Grab Water Sample The specific methodologies used in obtaining the enclosed analytical results are indicated on the Laboratory Sample Analysis Record. ELECTRONIC COPY TO Philadelphia Water Department Attn: Susan Patterson Questions? Contact Environmental Client Services Respectfully Submitted,
2 Page of 3 Sample Description: Grab Water Sample - Cistern Water Testing Project Name: - Cistern Water Testing Collected: 04/26/200 08:05 by SP through 04/26/200 08:20 Submitted: 04/26/200 5:30 Reported: 05/0/200 9:50 Discard: 05/25/200 Philadelphia PA 923 LLI Sample # PW LLI Group # 9887 Account # 0907 G CAT Analysis Name CAS Number Result Limit of Quantitation GC Extractable TPH SW B modified TPH by GC/FID water C8-C40 n.a. < Metals EPA rev Cadmium < The EPA has set a maximum contaminant level of for cadmium Calcium Chromium < The EPA has set a maximum contaminant level of 0. for chromium. The state of Pennsylvania has set a maximum contaminant level of 0.05 for chromium. EPA rev Arsenic The EPA has set a maximum contaminant level of 0.0 for arsenic Lead The action level for lead in the lead and copper rule is Because health effects are possible, especially in young children, EPA guidance recommends that corrective action be taken when the action level is met or exceeded. EPA 245. rev Mercury < The EPA has set a maximum contaminant level of for mercury. Wet Chemistry EPA Total Phosphorus as P (water) EPA Chemical Oxygen Demand n.a SM B as CaCO3 as CaCO Alkalinity to ph 4.5 n.a Alkalinity to ph 8.3 n.a SM H/B Std. Units Std. Units ph n.a ph is a measure of hydrogen ion activity. An acceptable range for ph in drinking water is This parameter is not generally considered to be directly health related. In combination with solids, alkalinity and calcium levels, ph can give an indication of whether the water is corrosive to plumbing. SM NH3 D 0694 Ammonia-Nitrogen Distilled Microbiology SM B /00ml /00ml
3 Page 2 of 3 Sample Description: Grab Water Sample - Cistern Water Testing Project Name: - Cistern Water Testing Collected: 04/26/200 08:05 by SP through 04/26/200 08:20 Submitted: 04/26/200 5:30 Reported: 05/0/200 9:50 Discard: 05/25/200 Philadelphia PA 923 LLI Sample # PW LLI Group # 9887 Account # 0907 G CAT Analysis Name CAS Number Result Limit of Quantitation /00ml Microbiology SM B /00ml 086 Tot Coli/E. coli (Quanti-tray) n.a. See Below n.a. *****BACTERIOLOGICALLY CONTAMINATED**** The water this test result represents is NOT considered bacteriologically safe to drink according to standards established by the Environmental Protection Agency (EPA). It is the presence of coliform bacteria, and not the number, that is significant. If the source of your water supply is a well, we recommend that you disinfect your well and retest the water prior to consuming it. If you need information on disinfecting your well, please contact us to receive our pamphlet, "Information and General Procedures for Testing Your Water". If the well has already been disinfected, you should contact a water treatment company or your plumber for permanent options. We recommend that you retest your well water every 6 to 2 months to verify that it continues to be bacteriologically safe. Total Coliform > /00ml E. coli <.0 /00ml General Sample Comments PA DEP Lab Certification ID , Expiration Date: /3/ All QC is compliant unless otherwise noted. Please refer to the Quality Control Summary for overall QC performance data and associated samples. Laboratory Sample Analysis Record CAT Analysis Name TPH by GC/FID water C8-C40 Extraction - DRO (Waters) Cadmium Calcium Chromium Arsenic Lead Mercury EPA 600 ICP Digest (tot rec) ICP/MS EPA-600 Digest PW/WW Hg Digest Total Phosphorus as P (water) Total Phos as P Prep (water) Chemical Oxygen Demand Alkalinity to ph 4.5 Alkalinity to ph 8.3 ph Method Trial# SW B modified SW C EPA rev 4.4 EPA rev 4.4 EPA rev 4.4 EPA rev 5.4 EPA rev 5.4 EPA 245. rev 3 EPA rev 4.4 EPA rev 5.4 EPA 245. rev 3 EPA 365. EPA 365. EPA 40.4 SM B SM B SM H/B Batch# A A A A A 07090A B A A B Analysis Date and Time 04/29/200 3:56 04/28/200 09:35 05/03/200 07:30 05/03/200 07:30 05/03/200 07:30 05/0/200 4:48 05/0/200 4:48 04/29/200 9:33 05/02/200 09:20 05/06/200 4:02 04/29/200 09:50 04/28/200 8:0 04/27/200 2:00 05/04/200 07:3 05/04/200 2:25 05/04/200 2:25 04/26/200 22:00 Analyst Heather E Williams Karen R Rettew Joanne M Gates Joanne M Gates Joanne M Gates Choon Y Tian Choon Y Tian Nelli S Markaryan James L Mertz James L Mertz Denise K Conners Joseph E McKenzie Nancy J Shoop Susan A Engle Geraldine C Smith Geraldine C Smith Luz M Groff
4 Page 3 of 3 Sample Description: Grab Water Sample - Cistern Water Testing Project Name: - Cistern Water Testing Collected: 04/26/200 08:05 by SP through 04/26/200 08:20 Submitted: 04/26/200 5:30 Reported: 05/0/200 9:50 Discard: 05/25/200 Philadelphia PA 923 LLI Sample # PW LLI Group # 9887 Account # 0907 G Laboratory Sample Analysis Record CAT Analysis Name 0694 Ammonia-Nitrogen Distilled 0429 Ammonia Distillation 086 Tot Coli/E. coli (Quantitray) Method SM NH3 D SM NH3 B SM B Trial# Batch# A A 04260LMH Analysis Date and Time 05/04/200 08:50 05/03/200 07:45 04/27/200 20:55 Analyst Michele L Graham Michele L Graham Keith A Hoover n.a.
5 Page of 2 Quality Control Summary Client Name: Group Number: 9887 Reported: 05/0/0 at 07:50 PM Matrix QC may not be reported if site-specific QC samples were not submitted. In these situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise specified in the method. Laboratory Compliance Quality Control Blank Blank Report LCS LCSD LCS/LCSD Analysis Name Result LOQ Units %REC %REC Limits RPD RPD Max Batch number: A Sample number(s): TPH by GC/FID water C8-C40 < Batch number: Sample number(s): Mercury < Batch number: Sample number(s): Cadmium < Calcium < Chromium < Batch number: A Sample number(s): Arsenic < Lead < Batch number: 07090A Sample number(s): Total Phosphorus as P (water) < Batch number: B Sample number(s): ph Batch number: A Sample number(s): Ammonia-Nitrogen Distilled < Batch number: A Sample number(s): Alkalinity to ph 4.5 < as CaCO Batch number: B Sample number(s): Chemical Oxygen Demand Sample Matrix Quality Control Unspiked (UNSPK) = the sample used in conjunction with the matrix spike Background (BKG) = the sample used in conjunction with the duplicate MS MSD MS/MSD RPD BKG DUP DUP Dup RPD Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max Batch number: Sample number(s): UNSPK: BKG: Mercury < < () 20 Batch number: Sample number(s): UNSPK: P BKG: P Cadmium < < () 20 *- Outside of specification () The result for one or both determinations was less than five times the LOQ. (2) The unspiked result was more than four times the spike added.
6 Page 2 of 2 Quality Control Summary Client Name: Group Number: 9887 Reported: 05/0/0 at 07:50 PM Sample Matrix Quality Control Unspiked (UNSPK) = the sample used in conjunction with the matrix spike Background (BKG) = the sample used in conjunction with the duplicate MS MSD MS/MSD RPD BKG DUP DUP Dup RPD Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max Calcium 35 (2) Chromium < < () 20 Batch number: A Sample number(s): UNSPK: BKG: Arsenic () 20 Lead () 20 Batch number: 07090A Sample number(s): UNSPK: P BKG: P Total Phosphorus as P (water) < 0.0 < () 3 Batch number: B Sample number(s): BKG: P ph Batch number: A Sample number(s): BKG: P96785 Ammonia-Nitrogen Distilled Batch number: A Sample number(s): UNSPK: BKG: Alkalinity to ph Alkalinity to ph Batch number: B Sample number(s): UNSPK: P BKG: P Chemical Oxygen Demand ,070 3, Surrogate Quality Control Surrogate recoveries which are outside of the QC window are confirmed unless attributed to dilution or otherwise noted on the Analysis Report. Analysis Name: TPH by GC/FID water C8-C40 Batch number: A Chlorobenzene Orthoterphenyl Blank LCS LCSD Limits: *- Outside of specification () The result for one or both determinations was less than five times the LOQ. (2) The unspiked result was more than four times the spike added.
7 Lancaster Laboratories Explanation of Symbols and Abbreviations The following defines common symbols and abbreviations used in reporting technical data: N.D. none detected BMQL Below Minimum Quantitation Level TNTC Too Numerous To Count MPN Most Probable Number IU International Units CP Units cobalt-chloroplatinate units umhos/cm micromhos/cm NTU nephelometric turbidity units C degrees Celsius F degrees Fahrenheit Cal (diet) calories lb. pound(s) meq milliequivalents kg kilogram(s) g gram(s) mg milligram(s) ug microgram(s) l liter(s) ml milliliter(s) ul microliter(s) m3 cubic meter(s) fib >5 um/ml fibers greater than 5 microns in length per ml ppm ppb Dry weight basis < less than The number following the sign is the limit of quantitation, the smallest amount of analyte which can be reliably determined using this specific test. > greater than parts per million One ppm is equivalent to one milligram per kilogram (mg/kg), or one gram per million grams. For aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter (), because one liter of water has a weight very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter of gas per liter of gas. parts per billion U.S. EPA data qualifiers: Results printed under this heading have been adjusted for moisture content. This increases the analyte weight concentration to approximate the value present in a similar sample without moisture. Organic Qualifiers Inorganic Qualifiers A TIC is a possible aldol-condensation product B Value is <CRDL, but IDL B Analyte was also detected in the blank E Estimated due to interference C Pesticide result confirmed by GC/MS M Duplicate injection precision not met D Compound quatitated on a diluted sample N Spike amount not within control limits E Concentration exceeds the calibration range of S Method of standard additions (MSA) used the instrument for calculation J Estimated value U Compound was not detected N Presumptive evidence of a compound (TICs only) W Post digestion spike out of control limits P Concentration difference between primary and * Duplicate analysis not within control limits confirmation columns >25% + Correlation coefficient for MSA <0.995 U Compound was not detected X,Y,Z Defined in case narrative Analytical test results for methods listed on the laboratories accreditation scope meet all requirements of NELAC unless otherwise noted under the individual analysis. Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our staff. This report shall not be reproduced except in full, without the written approval of the laboratory. WARRANTY AND LIMITS OF LIABILITY In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF MERCHANTABILITY. IN NO EVENT SHALL LANCASTER LABORATORIES BE LIABLE FOR INDIRECT, SPECIAL, CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF LANCASTER LABORATORIES AND (B) WHETHER LANCASTER LABORATORIES HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Lancaster Laboratories which includes any conditions that vary from the Standard Terms and Conditions of Lancaster Laboratories and we hereby object to any conflicting terms contained in any acceptance or order submitted by client.
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