Invoice Description Amount Units Extension

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1 Ferthaul Florida RS LLC PO #: null 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 21, 2015 Feb 13, 2015; Invoice: Invoice Description Amount Units Extension DWPPCB-FL DWPrimarySecondary_NoGA DWVOC Paid -1, , TOTAL 0.00 This invoice is due upon receipt. VISA, MasterCard, and American Express cards will be accepted. There will be a 1.5% service charge per month on all unpaid balances.

2 Florida Department of Environmental Protection Safe Drinking Water Program Laboratory Reporting Format PUBLIC WATER SYSTEM INFORMATION (to be completed by sampler - please type or pring legibly) System Name: PWS I.D. #: System Type (check one): Community Nontransient Noncommunity Transient Noncommunity Address: City: ZIP Code: Phone #: Fax #: Address: SAMPLE INFORMATION (to be completed by sampler) Sample Number: SW1 Sample Date: Sample Time: AM PM (Circle One) Sample Location (be specific): Location Code: Treated Disinfectant Residual (required when reporting trihalomethanes and haloacetic acids): mg/l Field ph: Sample Type (Check Only One) Reason(s) for Sample (Check all that apply) Distribution Routine Compliance (with ) Replacement (of Invalidated Sample) Entry Point (to Distribution) Confirmation of MCL Exceedance* Special (not for compliance with ) Plant Tap (not for compliance with ) Composite of Multiple Sites ** Clearance (permitting) Raw (at well or intake) Max Residence Time Other: Sampling Procedure Used or Other Comments: Avg Residence Time Near First Customer * See (6) for requirements and restrictions ** See (4) for requirements and And (3) for nitrate or nitrite exceedances. attach a results page for each site. SAMPLER CERTIFICATION I,,, do HEREBY CERTIFY (Print Name) that the above public water system and collection information is complete and correct. (Print Title) Signature: Date: Certified Operator #: Phone #: Sampler's Fax: Sampler's Page 1 of 6

3 Florida Department of Environmental Protection Safe Drinking Water Program Laboratory Reporting Format LABORATORY CERTIFICATION INFORMATION (to be completed by lab - please type or print legibly) Lab Name: Flowers Chemical Laboratories, Inc. Florida DOH Certification #: E83018 Certification Expiration Date: 6/30/2015 ATTACH CURRENT DOH ANALYTE SHEET* Address: P. O. Box , Altamonte Springs, FL Phone #: Were any analyses subcontracted? Yes No If yes, please provide DOH certification number(s): ATTACH DOH ANALYTE SHEET FOR EACH SUBCONTRACTED LAB* ANALYSIS INFORMATION(to be completed by lab) Date Sample(s) Received: 01/21/15 PWS ID (From Page 1): Sample Number (From Page 1): SW1 Lab Assigned Report # or Job ID: Group(s) analyzed and results attached for compliance with Chapter , F.A.C. (check all that apply) Inorganics Synthetic Organics Volatile Organics Disinfection Byproducts Radionuclides Secondaries All Except Asbestos All 30 All 21 Trihalomethanes Single Sample All 14 Partial All Except Dioxin Partial Haloacetic Acids Qtrly Composite** Partial Nitrate Partial Chlorite Nitrite Dioxin Only Bromate Asbestos LAB CERTIFICATION I, Jefferson S. Flowers, Technical Director, do HEREBY CERTIFY that all attached analytical data are correct and unless noted meet all requirements of the National Environmental Laboratory Accreditation Conference (NELAC). Signature: Date: 02/13/15 * Failure to provide a valid and current Florida DOH certification number and a current Analyte Sheet for the attached analysis results will result in rejection of the report and possible enforcement against the public water system for failure to sample, and may result in notification of the DOH Bureau of Laboratory Services. ** Please provide radiological sample dates & locations for each quarter. CONFIRMATION AND NOTIFICATION IS REQUIRED WITHIN 24 HRS FOR NITRATE MCL EXCEEDANCES NON-DETECTS ARE TO BE REPORTED AS THE MDL WITH A "U" QUALIFIER. (Non-detects reported as "BDL" or with a "<" are not acceptable.) Compliance Determination (to be completed by DEP or DOH - attach notes as necessary) Sample Collection & Analysis Satisfactory Yes No Replacement Sample or Report Requested (circle or highlight group(s) above) Person Notified: Date Notified: DEP/DOH Reviewing Official: Page 2 of 6

4 Florida Department of Environmental Protection Safe Drinking Water Program Laboratory Reporting Format INORGANIC CONTAMINANTS Report Number / Job ID: SW (1) PWS ID (From Page 1): Lake Apopka Contam Analysis Analytical Lab Analysis Analysis DOH Lab ID Contam Name MCL Units Result Qualifier Method MDL Date Time Cert # 1040 Nitrate (as N) 10 mg/l U EPA /22/15 12:30 PM E Nitrite (as N) 1 mg/l U EPA /22/15 12:30 PM E Arsenic mg/l EPA /22/15 E Barium 2 mg/l U EPA /22/15 E Cadmium mg/l U EPA /22/15 E Chromium 0.1 mg/l U EPA /22/15 E Cyanide 0.2 mg/l U SM4500CN-E /23/15 E Fluoride 4.0 mg/l EPA /22/15 E Lead mg/l EPA /22/15 E Mercury mg/l U EPA /27/15 E Nickel 0.1 mg/l EPA /22/15 E Selenium 0.05 mg/l U EPA /22/15 E Sodium 160 mg/l 16.8 EPA /22/15 E Antimony mg/l U EPA /22/15 E Beryllium mg/l U EPA /22/15 E Thallium mg/l U EPA /22/15 E83018 Page 3 of 6

5 Florida Department of Environmental Protection Safe Drinking Water Program Laboratory Reporting Format SECONDARY CONTAMINANTS Report Number / Job ID: SW PWS ID (From Page 1): Lake Apopka Contam Analysis Analytical Lab Analysis Analysis DOH Lab ID Contam Name MCL Units Result Qualifier Method MDL Date Time Cert # 1002 Aluminum 0.2 mg/l EPA /22/15 E Chloride 250 mg/l 44.0 EPA /22/15 E Copper 1 mg/l EPA /22/15 E Fluoride 4.0 mg/l EPA /22/15 E Iron 0.3 mg/l EPA /22/15 E Manganese 0.05 mg/l EPA /22/15 E Silver 0.1 mg/l U EPA /22/15 E Sulfate 250 mg/l 21.5 EPA /22/15 E Zinc 5 mg/l EPA /22/15 E Color 15 CU 50.0 SM2120 B /21/15 03:30 AM E ph ph 7.82 SM4500-H B /21/15 04:12 PM E Total Dissolved Solids 500 mg/l 322 SM2540 C /24/15 E Foaming Agents 0.5 mg/l U SM5540 C /22/15 01:00 PM E83018 Page 4 of 6

6 Florida Department of Environmental Protection Safe Drinking Water Program Laboratory Reporting Format VOLATILE ORGANICS (2)(b) Report Number / Job ID: SW1 PWS ID (From Page 1): Lake Apopka Contam Analysis Analytical Lab Analysis Analysis DOH Lab ID Contam Name MCL Units Result Qualifier Method MDL RDL Date Time Cert # ,2,4,-trichlorobenzene 70 ug/l U EPA /27/15 E cis-1,2-dichloroethylene 70 ug/l U EPA /27/15 E Xylenes ug/l U EPA /27/15 E Dichloromethane 5 ug/l U EPA /27/15 E o-dichlorobenzene 600 ug/l U EPA /27/15 E Para-dichlorobenzene 75 ug/l U EPA /27/15 E Vinyl Chloride 1 ug/l U EPA /27/15 E ,1-Dichloroethylene 7 ug/l U EPA /27/15 E trans-1,2-dichloroethylene 100 ug/l U EPA /27/15 E ,2-Dichloroethane 3 ug/l U EPA /27/15 E ,1,1-trichloroethane 200 ug/l U EPA /27/15 E Carbon tetrachloride 3 ug/l U EPA /27/15 E ,2-dichloropropane 5 ug/l U EPA /27/15 E Trichloroethylene 3 ug/l U EPA /27/15 E ,1,2-trichloroethane 5 ug/l U EPA /27/15 E Tetrachloroethylene 3 ug/l U EPA /27/15 E Monochlorobenzene 100 ug/l U EPA /27/15 E Benzene 1 ug/l U EPA /27/15 E Toluene 1000 ug/l U EPA /27/15 E Ethylbenzene 700 ug/l U EPA /27/15 E Styrene 100 ug/l U EPA /27/15 E83018 Page 5 of 6

7 Florida Department of Environmental Protection Safe Drinking Water Program Laboratory Reporting Format SYNTHETIC ORGANICS (2)(c) Report Number / Job ID: SW1 PWS ID (From Page 1): Lake Apopka Contam Analysis Analytical Lab Extraction Analysis Analysis DOH Lab ID Contam Name MCL Units Result Qualifier Method MDL RDL Date Date Time Cert # 2005 Endrin 2 ug/l U EPA /28/15 01/29/15 E Lindane 0.2 ug/l U EPA /28/15 01/29/15 E Methoxychlor 40 ug/l U EPA /28/15 01/29/15 E Toxaphene 3 ug/l U EPA /28/15 01/29/15 E Dalapon 200 ug/l U EPA /23/15 02/02/15 E Diquat 20 ug/l U EPA /26/15 01/28/15 E Endothall 100 ug/l 9.00 U EPA /03/15 02/06/15 E Glyphosate 700 ug/l 6.00 U EPA /23/15 E Di(2-ethylhexyl) adipate 400 ug/l U EPA /04/15 02/11/15 E Oxamyl (Vydate) 200 ug/l 2.00 U EPA /04/15 E Simazine 4 ug/l U EPA /29/15 02/11/15 E Di(2-ethylhexyl)phthalate 6 ug/l 10.1 EPA /04/15 02/11/15 E Picloram 500 ug/l U EPA /23/15 02/02/15 E Dinoseb 7 ug/l U EPA /23/15 02/02/15 E Hexachlorocyclopentadiene 50 ug/l U EPA /28/15 01/29/15 E Carbofuran 40 ug/l U EPA /04/15 E Atrazine 3 ug/l U EPA /29/15 02/11/15 E Alachlor 2 ug/l U EPA /29/15 02/11/15 E Heptachlor 0.4 ug/l U EPA /28/15 01/29/15 E Heptachlor epoxide 0.2 ug/l U EPA /28/15 01/29/15 E ,4-D 70 ug/l U EPA /23/15 02/02/15 E ,4,5-TP 50 ug/l U EPA /23/15 02/02/15 E Hexachlorobenzene 1 ug/l U EPA /28/15 01/29/15 E Benzo(a)pyrene 0.2 ug/l U EPA /04/15 02/11/15 E Pentachlorophenol 1 ug/l U EPA /23/15 02/02/15 E PolychlorinatedbiphenylsPCB 0.5 ug/l U EPA /28/15 01/29/15 E Dibromochloropropane 0.2 ug/l U EPA /28/15 01/29/15 E Ethylene Dibromide 0.02 ug/l U EPA /28/15 01/29/15 E Chlordane 2 ug/l U EPA /28/15 01/29/15 E83018 Page 6 of 6

8 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 26, 2015; Invoice: Invoice Description Amount Units Extension EPA Calcium EPA Iron EPA Magnesium EPA Manganese EPA Potassium EPA Sodium EPA Aluminum EPA Arsenic EPA Barium EPA Cadmium EPA Chromium EPA Lead EPA Molybdenum EPA Nickel EPA Selenium EPA Silver EPA Zinc Paid TOTAL 0.00 This invoice is due upon receipt. VISA, MasterCard, and American Express cards will be accepted. There will be a 1.5% service charge per month on all unpaid balances. FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015

9 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 26, 2015; Invoice: Report Summary Date Received: Jan 21, 2015 FCL Project Manager: Michelle M. Garver Laboratory # Sample Description Analysis Chemist Location SampleMatrix SW1 Raw EPA200.7 EVB Main Lab Surface Water EPA200.8 EVB Main Lab SW2 Treated EPA200.7 EVB Main Lab Surface Water EPA200.8 EVB Main Lab Certificate of Results Sample integrity was certified prior to analysis. Test results meet all requirements of the NELAC Standards except as noted in the Quality Control Report. Uncertainties for these data are available on request. This report may not be reproduced in part; results relate only to items tested. FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 1 of 7

10 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 26, 2015; Invoice: Analysis Report Lab #: SW1 Sampled: 01/20/15 11:03 AM Desc: Raw Parameter Result Units DF MDL PQL QC Batch Method CAS # Analyzed Calcium 443 mg/l EPA /22/15 Iron 110 mg/l EPA /22/15 Magnesium 71.9 mg/l EPA /22/15 Manganese 1.50 mg/l EPA /22/15 Potassium 18.0 mg/l EPA /22/15 Sodium 26.8 mg/l EPA /22/15 Aluminum 47.8 mg/l EPA /22/15 Arsenic mg/l EPA /22/15 Barium mg/l EPA /22/15 Cadmium U mg/l EPA /22/15 Chromium mg/l EPA /22/15 Lead mg/l EPA /22/15 Molybdenum mg/l EPA /22/15 Nickel mg/l EPA /22/15 Selenium U mg/l EPA /22/15 Silver U mg/l EPA /22/15 Zinc 8.75 mg/l EPA /22/15 Lab #: SW2 Sampled: 01/21/15 10:30 AM Desc: Treated Parameter Result Units DF MDL PQL QC Batch Method CAS # Analyzed Calcium 37.3 mg/l EPA /22/15 Iron mg/l EPA /22/15 Magnesium 15.5 mg/l EPA /22/15 Manganese mg/l EPA /22/15 Potassium 8.36 mg/l EPA /22/15 Sodium 18.7 mg/l EPA /22/15 Aluminum mg/l EPA /22/15 FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 2 of 7

11 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 26, 2015; Invoice: Lab #: SW2 Sampled: 01/21/15 10:30 AM Desc: Treated Parameter Result Units DF MDL PQL QC Batch Method CAS # Analyzed Arsenic mg/l EPA /22/15 Barium mg/l EPA /22/15 Cadmium U mg/l EPA /22/15 Chromium U mg/l EPA /22/15 Lead mg/l EPA /22/15 Molybdenum mg/l EPA /22/15 Nickel I mg/l EPA /22/15 Selenium U mg/l EPA /22/15 Silver U mg/l EPA /22/15 Zinc mg/l EPA /22/15 FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 3 of 7

12 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 26, 2015; Invoice: Quality Control Batch: Analyst: EVB Blank Result Units Calcium 0.100U mg/l Magnesium U mg/l Potassium 0.500U mg/l Sodium 0.500U mg/l Quality Report Laboratory Control Sample Result Units Spike %REC %REC Lim Calcium 5.09 mg/l Magnesium 5.45 mg/l Potassium 5.44 mg/l Sodium 5.44 mg/l Matrix Spike Result Units Spike %REC %REC Lim Sample Calcium 65.1 mg/l Magnesium 11.6 mg/l Potassium 6.71 mg/l Sodium 20.7 mg/l Matrix Spike Duplicate Result Units Spike %REC %REC Lim Sample RPD RPD Lim Calcium 66.0 mg/l Magnesium 11.4 mg/l Potassium 6.28 mg/l Sodium 20.7 mg/l Quality Control Batch: Analyst: EVB Blank Result Units Arsenic U mg/l FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 4 of 7

13 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 26, 2015; Invoice: Quality Control Batch: Analyst: EVB Blank Result Units Barium 0.200U mg/l Cadmium U mg/l Chromium U mg/l Lead U mg/l Selenium U mg/l Silver U mg/l Zinc U mg/l Laboratory Control Sample Result Units Spike %REC %REC Lim Arsenic mg/l Barium mg/l Cadmium mg/l Chromium mg/l Lead mg/l Selenium mg/l Silver mg/l Zinc mg/l Matrix Spike Result Units Spike %REC %REC Lim Sample Arsenic mg/l U Barium mg/l U Cadmium mg/l U Chromium mg/l U Lead mg/l U Selenium mg/l U Silver mg/l U Zinc mg/l Matrix Spike Duplicate Result Units Spike %REC %REC Lim Sample RPD RPD Lim FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 5 of 7

14 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 26, 2015; Invoice: Quality Control Batch: Analyst: EVB Matrix Spike Duplicate Result Units Spike %REC %REC Lim Sample RPD RPD Lim Arsenic mg/l U Barium mg/l U Cadmium mg/l U Chromium mg/l U Lead mg/l U Selenium mg/l U Silver mg/l U Zinc mg/l FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 6 of 7

15 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 26, 2015; Invoice: Narrative Report Sample Handling Sample handling and holding time criteria were met for all samples. Samples collected by submitter. No unusual events occurred during analysis. Results are reported on a wet weight basis for aqueous matrices and on a dry weight basis for sludge and soil matrices unless otherwise noted. Sample results reported as dissolved were field filtered. Quality Control Enclosed analyses met method or FCL criteria, unless otherwise denoted on the sample results. Applied data qualifiers are defined below. Attachments Chain of Custody Qualifier U J J1 J2 J3 J4 Q L V ZTNTC A P T M G S O I B Y Meaning Compound was analyzed for but not detected. One or more QC samples associated with this data value exceeded QC limits. Surrogate recovery limits have been exceeded. No known quality control criteria exist for the component. Reported value failed to meet established quality control criteria for either precision or accuracy. Sample matrix interfered with the ability to make an accurate determination on the spiked sample. Sample held beyond the accepted holding time. Off-scale high; reported concentration exceeds the highest standard. Analyte was detected in both the sample and the associated method blank. Too numerous to count. Numeric value represents filtration volume. Absent Present Value reported is less than the statistical method detection limit. Reported for informational purposes only. Value reported is greater than the statistical method detection limit, but less than the reported MDL. The greatest of the dilutions performed did not yield sufficient oxygen depletion for valid data. The least of the dilutions performed did not yield sufficient oxygen residual for valid data. Result is greater than (over) the specified value. Reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Results based upon colony plate count outside ideal range. The laboratory analysis was from an improperly preserved sample. The data may not be accurate. FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 7 of 7

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17 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 23, 2015; Invoice: Invoice Description Amount Units Extension Paid TP TOTAL 0.00 This invoice is due upon receipt. VISA, MasterCard, and American Express cards will be accepted. There will be a 1.5% service charge per month on all unpaid balances. FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015

18 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 23, 2015; Invoice: Report Summary Date Received: Jan 21, 2015 FCL Project Manager: Michelle M. Garver Laboratory # Sample Description Analysis Chemist Location SampleMatrix SW1 Raw#1 EPA365.4 VLB Main Lab Surface Water SW2 Raw#2 EPA365.4 VLB Main Lab Surface Water SW3 Treated#1 EPA365.4 VLB Main Lab Surface Water SW4 Treated#2 EPA365.4 VLB Main Lab Surface Water Certificate of Results Sample integrity was certified prior to analysis. Test results meet all requirements of the NELAC Standards except as noted in the Quality Control Report. Uncertainties for these data are available on request. This report may not be reproduced in part; results relate only to items tested. FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 1 of 4

19 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 23, 2015; Invoice: Analysis Report Lab #: SW1 Sampled: 01/20/15 11:00 AM Desc: Raw#1 Parameter Result Units DF MDL PQL QC Batch Method CAS # Analyzed Total Phosphorus(as P) 7.58 mg/l EPA /23/15 Lab #: SW2 Sampled: 01/20/15 11:00 AM Desc: Raw#2 Parameter Result Units DF MDL PQL QC Batch Method CAS # Analyzed Total Phosphorus(as P) 7.58 mg/l EPA /23/15 Lab #: SW3 Sampled: 01/21/15 10:00 AM Desc: Treated#1 Parameter Result Units DF MDL PQL QC Batch Method CAS # Analyzed Total Phosphorus(as P) mg/l EPA /23/15 Lab #: SW4 Sampled: 01/21/15 10:00 AM Desc: Treated#2 Parameter Result Units DF MDL PQL QC Batch Method CAS # Analyzed Total Phosphorus(as P) mg/l EPA /23/15 FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 2 of 4

20 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 23, 2015; Invoice: FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 3 of 4

21 Ferthaul Florida RS LLC PO #: n/a 6311 Inducon Corporate Drive, Ste. 5 Client Project #: Lake Apopka Sanborn,NY Date Sampled: Jan 20, 2015 Jan 23, 2015; Invoice: Narrative Report Sample Handling Sample handling and holding time criteria were met for all samples. Samples collected by submitter. No unusual events occurred during analysis. Results are reported on a wet weight basis for aqueous matrices and on a dry weight basis for sludge and soil matrices unless otherwise noted. Sample results reported as dissolved were field filtered. Quality Control Enclosed analyses met method or FCL criteria, unless otherwise denoted on the sample results. Applied data qualifiers are defined below. Attachments Chain of Custody Qualifier U J J1 J2 J3 J4 Q L V ZTNTC A P T M G S O I B Y Meaning Compound was analyzed for but not detected. One or more QC samples associated with this data value exceeded QC limits. Surrogate recovery limits have been exceeded. No known quality control criteria exist for the component. Reported value failed to meet established quality control criteria for either precision or accuracy. Sample matrix interfered with the ability to make an accurate determination on the spiked sample. Sample held beyond the accepted holding time. Off-scale high; reported concentration exceeds the highest standard. Analyte was detected in both the sample and the associated method blank. Too numerous to count. Numeric value represents filtration volume. Absent Present Value reported is less than the statistical method detection limit. Reported for informational purposes only. Value reported is greater than the statistical method detection limit, but less than the reported MDL. The greatest of the dilutions performed did not yield sufficient oxygen depletion for valid data. The least of the dilutions performed did not yield sufficient oxygen residual for valid data. Result is greater than (over) the specified value. Reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Results based upon colony plate count outside ideal range. The laboratory analysis was from an improperly preserved sample. The data may not be accurate. FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 4 of 4

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24 DIVISN-EAR Serial Number: Page 1 of 16 DIVISN-EAR Florida Department of Environmental Protection Central Laboratory 2600 Blair Stone Road Tallahassee, FL DOH Accreditation E31780 Event Description: Request ID: Customer: Project ID: Lake Apopka Project-ORL RQ DIVISN-EAR OTHER-EAR Send Reports to: FL Dept. of Environmental Protection 3319 Maguire Blvd Orlando, FL Attn: Rob Renk For additional information please contact Timothy W. Fitzpatrick Liang-Tsair Lin, Ph.D. Colin Wright, Ph.D. Thekkekalathil Chandrasekhar, PhD, QA Officer Phone (850) Certified by: Liang Lin, Environmental Administrator Date Certified: 05-FEB :56

25 DIVISN-EAR Serial Number: Page 2 of 16 Job: TLH Job: TLH Job: TLH Group: Metals Group: Nutrients Group: Pesticides

26 DIVISN-EAR Serial Number: Page 3 of 16 Sample Location: LAKE APOPKA INFLUENT Collection Date/Time: 01/20/ :20 Field ID: LAKE APOPKA INFLUENT Matrix: W-SURF-FRH Sample ID Ref. Method Component Result Code Units Batch ID QC Failures EPA Rev. 4.4 Iron 2.91E+04 ug/l EPA Rev. 5.4 Aluminum 1.79E+04 ug/l Arsenic 61.5 ug/l Lead 85.1 ug/l EPA Rev. 2.0 Ammonia-N 0.29 mg N/L EPA Rev. 2.0 Kjeldahl Nitrogen 150 mg N/L EPA Rev. 2.0 NO2NO3-N I mg N/L EPA Rev. 2.0 Total-P 8.0 mg P/L SM 2540 D-97 TSS 5.30E+03 A mg/l DEP SOP: GC (based on EPA 608 and 617) Aldrin U ug/l Alpha-BHC U ug/l Beta-BHC U ug/l Delta-BHC U ug/l Gamma-BHC U ug/l P P P P P P P P P Carbophenothion UJ ug/l CCV Chlordane 0.44 ug/l Chlorothalonil UJ ug/l CCV Cypermethrin U ug/l DDD-p,p' U ug/l DDE-p,p' 0.29 ug/l DDT-p,p' U ug/l Dicofol UJ ug/l CCV Dieldrin U ug/l Endosulfan I U ug/l Endosulfan II U ug/l Endosulfan Sulfate U ug/l Endrin U ug/l Endrin Aldehyde U ug/l Heptachlor U ug/l Heptachlor Epoxide U ug/l Methoxychlor U ug/l Mirex U ug/l Permethrin U ug/l Toxaphene U ug/l PCB U ug/l PCB U ug/l PCB U ug/l PCB U ug/l PCB U ug/l PCB U ug/l PCB U ug/l Trifluralin U ug/l EPA 8270D Ametryn** 2.0 U ng/l MS

27 DIVISN-EAR Serial Number: Page 4 of 16 Field ID: LAKE APOPKA INFLUENT Matrix: W-SURF-FRH Sample ID Ref. Method Component Result Code Units Batch ID QC Failures EPA 8270D Atrazine** 6.5 I ng/l Chlorpyrifos Ethyl** 0.98 U ng/l Chlorpyrifos Methyl** 1.2 U ng/l Disulfoton** 4.9 U ng/l Ethion** 0.98 U ng/l Ethoprop** 0.98 U ng/l Hexazinone** 9.8 U ng/l Malathion** 1.2 U ng/l Metribuzin** 2.5 U ng/l Mevinphos** 2.5 U ng/l MS Norflurazon** 9.8 U ng/l MS Phorate** 2.5 U ng/l Prometryn** 2.5 U ng/l Simazine** 2.5 U ng/l Atrazine Desethyl** 2.5 U ng/l MS Fipronil** 4.9 U ng/l MS Molinate** 2.9 U ng/l Pendimethalin** 4.9 U ng/l Terbufos** 0.98 U ng/l EPTC** 2.9 U ng/l Terbuthylazine** 2.0 U ng/l Bromacil** 4.9 U ng/l Fipronil Sulfide** 2.0 U ng/l Fipronil Sulfone** 2.0 U ng/l Ref. Method and Comment: EPA Rev. 5.4: The arsenic and lead results were confirmed on 02/03/2015. SM 2540 D-97: Sample has large amount of particulate matter. DEP SOP: GC (based on EPA 608 and 617): MDL for Dicofol, Endrin aldehyde, Dieldrin, DDD-p,p' and DDT-p,p' elevated due to matrix interference. Quality control failure(s) observed. EPA 8270D: MDLs are elevated due to sample dilution. MS accuracy for Atrazine could not be assessed due to high content of the analyte in the spiked sample. Quality Assurance Report Method Blank Results Reference Method: DEP SOP: GC (based on EPA 608 and 617) Batch ID: Component Result Code Units Aldrin U ug/l Alpha-BHC U ug/l Beta-BHC U ug/l Carbophenothion U ug/l Chlordane U ug/l Chlorothalonil U ug/l Cypermethrin U ug/l DDD-p,p' U ug/l DDE-p,p' U ug/l DDT-p,p' U ug/l Delta-BHC U ug/l Dicofol U ug/l

28 Quality Assurance Report Method Blank Results DIVISN-EAR Serial Number: Page 5 of 16 Reference Method: DEP SOP: GC (based on EPA 608 and 617) Batch ID: Component Result Code Units Dieldrin U ug/l Endosulfan I U ug/l Endosulfan II U ug/l Endosulfan Sulfate U ug/l Endrin U ug/l Endrin Aldehyde U ug/l Gamma-BHC U ug/l Heptachlor U ug/l Heptachlor Epoxide U ug/l Methoxychlor U ug/l Mirex U ug/l PCB U ug/l PCB U ug/l PCB U ug/l PCB U ug/l PCB U ug/l PCB U ug/l PCB U ug/l Permethrin U ug/l Toxaphene 0.10 U ug/l Trifluralin U ug/l Reference Method: EPA Rev. 4.4 Batch ID: P Component Result Code Units Iron 30 U ug/l Reference Method: EPA Rev. 5.4 Batch ID: P Component Result Code Units Aluminum 5.0 U ug/l Arsenic 0.25 U ug/l Lead 0.20 U ug/l Reference Method: EPA Rev. 2.0 Batch ID: P Component Result Code Units Ammonia-N U mg N/L Reference Method: EPA Rev. 2.0 Batch ID: P Component Result Code Units Kjeldahl Nitrogen U mg N/L Reference Method: EPA Rev. 2.0 Batch ID: P Component Result Code Units

29 Quality Assurance Report Method Blank Results DIVISN-EAR Serial Number: Page 6 of 16 Reference Method: EPA Rev. 2.0 Batch ID: P Component Result Code Units NO2NO3-N U mg N/L Reference Method: EPA Rev. 2.0 Batch ID: P Component Result Code Units Total-P U mg P/L Reference Method: EPA 8270D Batch ID: Component Result Code Units Ametryn 0.20 U ng/l Atrazine 0.25 U ng/l Atrazine Desethyl 0.25 U ng/l Bromacil 0.50 U ng/l Chlorpyrifos Ethyl 0.10 U ng/l Chlorpyrifos Methyl 0.12 U ng/l Disulfoton 0.50 U ng/l EPTC 0.30 U ng/l Ethion 0.10 U ng/l Ethoprop 0.10 U ng/l Fipronil 0.50 U ng/l Fipronil Sulfide 0.20 U ng/l Fipronil Sulfone 0.20 U ng/l Hexazinone 1.0 U ng/l Malathion 0.12 U ng/l Metribuzin 0.25 U ng/l Mevinphos 0.25 U ng/l Molinate 0.30 U ng/l Norflurazon 1.0 U ng/l Pendimethalin 0.50 U ng/l Phorate 0.25 U ng/l Prometryn 0.25 U ng/l Simazine 0.25 U ng/l Terbufos 0.10 U ng/l Terbuthylazine 0.20 U ng/l Reference Method: SM 2540 D-97 Batch ID: P Component Result Code Units TSS 2 U mg/l Quality Assurance Report Laboratory Control Sample Accuracy Reference Method: DEP SOP: GC (based on EPA 608 and 617) Batch ID:

30 Quality Assurance Report Laboratory Control Sample Accuracy DIVISN-EAR Serial Number: Page 7 of 16 Reference Method: DEP SOP: GC (based on EPA 608 and 617) Batch ID: Toxaphene P/P Reference Method: EPA Rev. 4.4 Batch ID: P Iron 105 P Reference Method: EPA Rev. 5.4 Batch ID: P Aluminum 91.1 P Arsenic 90.2 P Lead 90.8 P Reference Method: EPA Rev. 2.0 Batch ID: P Ammonia-N 103 P Reference Method: EPA Rev. 2.0 Batch ID: P Kjeldahl Nitrogen 101 P Reference Method: EPA Rev. 2.0 Batch ID: P NO2NO3-N 102 P Reference Method: EPA Rev. 2.0 Batch ID: P Total-P 95.7 P Reference Method: EPA 8270D Batch ID: Ametryn P/P Atrazine P/P Atrazine Desethyl P/P Bromacil P/P Chlorpyrifos Ethyl P/P Chlorpyrifos Methyl P/P Disulfoton P/P EPTC P/P

31 DIVISN-EAR Serial Number: Page 8 of 16 Quality Assurance Report Laboratory Control Sample Accuracy Reference Method: EPA 8270D Batch ID: Ethion P/P Ethoprop P/P Fipronil P/P Fipronil Sulfide P/P Fipronil Sulfone P/P Hexazinone P/P Malathion P/P Metribuzin P/P Mevinphos P/P Molinate P/P Norflurazon P/P Pendimethalin P/P Phorate P/P Prometryn P/P Simazine P/P Terbufos P/P Terbuthylazine P/P Quality Assurance Report Matrix Spike Accuracy Reference Method: DEP SOP: GC (based on EPA 608 and 617) Batch ID: Spiked Sample Toxaphene P/P Reference Method: EPA Rev. 4.4 Batch ID: P Spiked Sample Iron P/P Iron 108 P Reference Method: EPA Rev. 5.4 Batch ID: P Spiked Sample Aluminum P/P Arsenic P/P Lead P/P Aluminum 93.0 P Arsenic 92.4 P Lead 93.6 P Reference Method: EPA Rev. 2.0 Batch ID: P Spiked Sample Ammonia-N P/P

32 Quality Assurance Report Matrix Spike Accuracy DIVISN-EAR Serial Number: Page 9 of 16 Reference Method: EPA Rev. 2.0 Batch ID: P Spiked Sample Kjeldahl Nitrogen P/P Reference Method: EPA Rev. 2.0 Batch ID: P Spiked Sample NO2NO3-N 99.0 P Reference Method: EPA Rev. 2.0 Batch ID: P Spiked Sample Total-P P/P Reference Method: EPA 8270D Batch ID: Spiked Sample Ametryn 136 F Atrazine Desethyl 113 F Bromacil 76.8 P Chlorpyrifos Ethyl 62.7 P Chlorpyrifos Methyl 47.8 P Disulfoton 113 P EPTC 92.3 P Ethion 81.1 P Ethoprop 96.8 P Fipronil 42.9 F Fipronil Sulfide 126 P Fipronil Sulfone 90.9 P Hexazinone 102 P Malathion 89.3 P Metribuzin 99.4 P Mevinphos 112 F Molinate 111 P Norflurazon 163 F Pendimethalin 128 P Phorate 94.2 P Prometryn 121 P Simazine 124 P Terbufos 89.3 P Terbuthylazine 107 P Quality Assurance Report Precision Reference Method: DEP SOP: GC (based on EPA 608 and 617) Batch ID: Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits

33 DIVISN-EAR Serial Number: Page 10 of 16 Quality Assurance Report Precision Reference Method: DEP SOP: GC (based on EPA 608 and 617) Batch ID: Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits Toxaphene 1.51 Spike P 0-30 Toxaphene 6.17 LCS P 0-30 Reference Method: EPA Rev. 4.4 Batch ID: P Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits Iron Spike P 0-20 Reference Method: EPA Rev. 5.4 Batch ID: P Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits Aluminum 2.03 Spike P 0-20 Arsenic Spike P 0-20 Lead 1.08 Spike P 0-20 Reference Method: EPA Rev. 2.0 Batch ID: P Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits Ammonia-N 1.58 Spike P 0-20 Reference Method: EPA Rev. 2.0 Batch ID: P Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits Kjeldahl Nitrogen 1.11 Spike P 0-20 Reference Method: EPA Rev. 2.0 Batch ID: P Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits NO2NO3-N Spike P 0-20 Reference Method: EPA Rev. 2.0 Batch ID: P Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits Total-P 4.42 Spike P 0-20

34 DIVISN-EAR Serial Number: Page 11 of 16 Quality Assurance Report Precision Reference Method: EPA 8270D Batch ID: Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits Ametryn 4.20 LCS P 0-30 Atrazine 1.20 LCS P 0-30 Atrazine Desethyl 3.71 LCS P 0-30 Bromacil 3.41 LCS P 0-30 Chlorpyrifos Ethyl 1.41 LCS P 0-30 Chlorpyrifos Methyl LCS P 0-30 Disulfoton 1.60 LCS P 0-30 EPTC 11.2 LCS P 0-30 Ethion 1.62 LCS P 0-30 Ethoprop 1.56 LCS P 0-30 Fipronil 2.27 LCS P 0-30 Fipronil Sulfide 1.55 LCS P 0-30 Fipronil Sulfone 2.18 LCS P 0-30 Hexazinone 6.44 LCS P 0-30 Malathion 1.06 LCS P 0-30 Metribuzin 2.09 LCS P 0-30 Mevinphos 6.94 LCS P 0-30 Molinate 8.11 LCS P 0-30 Norflurazon LCS P 0-30 Pendimethalin 1.95 LCS P 0-30 Phorate LCS P 0-30 Prometryn 3.37 LCS P 0-30 Simazine 15.3 LCS P 0-30 Terbufos 2.73 LCS P 0-30 Terbuthylazine 3.85 LCS P 0-30 Reference Method: SM 2540 D-97 Batch ID: P Replicated Lab Sample Component % RSD/RPD Sample/Spike/LCS* Pass/Fail Control Limits TSS 1.51 Sample P 0-10 * Sample, spike and/or laboratory control sample precision (LCS) is reported. Replicate spike precision may be reported when sample results are below quantifiable levels. Quality Assurance Report Surrogates Lab Sample ID: Field Sample ID: LAKE APOPKA INFLUENT Reference Method Surrogate % Rec. Pass/Fail Control Limits DEP SOP: GC (based on EPA 608 and Decachlorobiphenyl 57.5 P ) Lab Sample ID: Field Sample ID: LAKE APOPKA INFLUENT Reference Method Surrogate % Rec. Pass/Fail Control Limits EPA 8270D 5-Nitroquinoline 94.6 P

35 Quality Assurance Report Calibration Verification DIVISN-EAR Serial Number: Page 12 of 16 Reference Method: EPA Rev. 2.0 Run ID: A60722 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits NO2NO3-N P/P Reference Method: EPA Rev. 2.0 Run ID: A60753 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Ammonia-N P/P Reference Method: EPA Rev. 4.4 Run ID: A60762 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Iron P/P Reference Method: EPA Rev. 2.0 Run ID: A60785 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Total-P P/P Reference Method: EPA Rev. 5.4 Run ID: A60812 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Arsenic P/P Lead P/P Reference Method: EPA Rev. 2.0 Run ID: A60829 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Kjeldahl Nitrogen P/P Reference Method: EPA Rev. 5.4 Run ID: A60839 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Aluminum P/P Reference Method: DEP SOP: GC (based on EPA 608 and 617) Run ID: A60866 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Aldrin P/P

36 Quality Assurance Report Calibration Verification DIVISN-EAR Serial Number: Page 13 of 16 Reference Method: DEP SOP: GC (based on EPA 608 and 617) Run ID: A60866 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Alpha-BHC P/P Beta-BHC P/P Carbophenothion 88.9* 97.6 F/P Chlordane P/P Chlorothalonil * P/F Cypermethrin P/P DDD-p,p' P/P DDE-p,p' P/P DDT-p,p' P/P Delta-BHC P/P Dicofol * P/F Dieldrin P/P Endosulfan I P/P Endosulfan II P/P Endosulfan Sulfate P/P Endrin P/P Endrin Aldehyde P/P Gamma-BHC P/P Heptachlor P/P Heptachlor Epoxide P/P Methoxychlor P/P Mirex P/P Permethrin P/P Toxaphene P/P Trifluralin P/P Reference Method: EPA 8270D Run ID: A60914 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Ametryn 95.3 P Atrazine 97.2 P Atrazine Desethyl 88.8 P Bromacil 99.2 P Chlorpyrifos Ethyl 97.0 P Chlorpyrifos Methyl 97.1 P Disulfoton 87.8 P EPTC 98.1 P Ethion 99.8 P Ethoprop 90.8 P Fipronil 110 P Fipronil Sulfide 99.4 P Fipronil Sulfone 102 P Hexazinone 103 P Malathion 86.4 P Metribuzin 93.5 P Mevinphos 80.1 P Molinate 101 P Norflurazon 102 P Pendimethalin 93.7 P

37 Quality Assurance Report Calibration Verification DIVISN-EAR Serial Number: Page 14 of 16 Reference Method: EPA 8270D Run ID: A60914 Included Lab Sample IDs: Component % Rec.1 % Rec.2 Pass/Fail* Control Limits Phorate 98.4 P Prometryn 99.7 P Simazine 92.6 P Terbufos 92.3 P Terbuthylazine 97.7 P * Pass/Fail determinations are made for each bracketing calibration verification check. Control limits for initial calibration checks may be different from those for continuing checks, depending on method requirements. Where they are different, both control limits are provided. Quality Assurance Report Summary Ref. Method Analyte LCS % Recovery MS % Recovery Precision LCS SMP MS DEP SOP: GC (based on Toxaphene EPA 608 and 617) EPA Rev. 4.4 Iron EPA Rev. 5.4 Aluminum Arsenic Lead EPA Rev. 2.0 Ammonia-N EPA Rev. 2.0 Kjeldahl Nitrogen EPA Rev. 2.0 NO2NO3-N EPA Rev. 2.0 Total-P EPA 8270D Ametryn Atrazine Atrazine Desethyl Bromacil Chlorpyrifos Ethyl Chlorpyrifos Methyl Disulfoton EPTC Ethion Ethoprop Fipronil Fipronil Sulfide Fipronil Sulfone Hexazinone Malathion Metribuzin Mevinphos Molinate Norflurazon Pendimethalin Phorate Prometryn Simazine Terbufos Terbuthylazine

38 DIVISN-EAR Serial Number: Page 15 of 16 Quality Assurance Report Summary Ref. Method Analyte LCS % Recovery MS % Recovery Precision LCS SMP MS SM 2540 D-97 TSS 1.51 Reference Method Descriptions Method / NELAC Cert. # Description Associated Samples DEP SOP: GC (based on EPA 608 and 617) / E31780 EPA Rev. 4.4 / E31780 EPA Rev. 5.4 / E31780 EPA Rev. 2.0 / E31780 EPA Rev. 2.0 / E31780 EPA Rev. 2.0 / E31780 EPA Rev. 2.0 / E31780 EPA 8270D / E31780 Organochlorine pesticides (low levels) in water matrices by GC/ECD Total Recoverable Metals analysis using ICP emission spectroscopy for aqueous samples supporting Clean Water Act Projects Total Recoverable Metals analysis using ICP-MS for aqueous samples supporting Clean Water Act Projects Ammonia in aqueous matrices as mg N/L Total Kjeldahl Nitrogen in aqueous matrices Nitrite/Nitrate in aqueous matrices as mg N/L Total Phosphorus in aqueous matrices as mg P/L Organonitrogen and phosphorus pesticides (ultra trace level) in water matrices by GC/MS/MS SM 2540 D-97 / E31780 Total Suspended Solids in aqueous matrices

39 DIVISN-EAR Serial Number: Page 16 of 16 Preparation and Analysis Log Ref. Method Received Date Prep Date/Time Prepared By Analysis Date/Time Analyzed By Associated Samples DEP SOP: GC (based on 01/21/ /23/2015 Rasheda Ghaffari 01/28/2015 Vandana T. Nagar EPA 608 and 617) 01/21/ /23/2015 Rasheda Ghaffari 01/29/2015 Vandana T. Nagar EPA Rev /21/ /21/2015 Elliott D. Healy 01/23/2015 Joshua Ayres EPA Rev /21/ /21/2015 Elliott D. Healy 01/27/2015 Charles J. Peterson /21/ /21/2015 Elliott D. Healy 01/28/2015 Charles J. Peterson EPA Rev /21/ /23/2015 Diana M. Turner EPA Rev /21/ /28/2015 Christopher Armour 01/28/2015 Bryan A. Werth EPA Rev /21/ /22/2015 Peter D. Kaus EPA Rev /21/ /26/2015 Christopher Armour 01/27/2015 Lipi Saha EPA 8270D 01/21/ /26/2015 Fe-Val Siddell 01/29/2015 Irina Carbone SM 2540 D-97 01/21/ /26/2015 Sima Feizi

40 DIVISN-EAR Serial Number: Page 1 of 16 DIVISN-EAR Florida Department of Environmental Protection Central Laboratory 2600 Blair Stone Road Tallahassee, FL DOH Accreditation E31780 Event Description: Request ID: Customer: Project ID: Lake Apopka Project-ORL RQ DIVISN-EAR OTHER-EAR Send Reports to: FL Dept. of Environmental Protection 3319 Maguire Blvd Orlando, FL Attn: Rob Renk For additional information please contact Timothy W. Fitzpatrick Liang-Tsair Lin, Ph.D. Colin Wright, Ph.D. Thekkekalathil Chandrasekhar, PhD, QA Officer Phone (850) Certified by: Timothy Fitzpatrick, Program Administrator Date Certified: 04-FEB :06

41 DIVISN-EAR Serial Number: Page 2 of 16 Job: TLH Job: TLH Job: TLH Group: Metals Group: Nutrients Group: Pesticides