Schedule of Accreditation United Kingdom Accreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK
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1 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK Issue No: 032 Issue date: 21 June 2016 Unit 6 Parkhead Greencroft Industrial Park Stanley County Durham DH9 7YB Contact: Mr J Burbeck Tel: +44 (0) Fax: +44 (0) jamieburbeck@chemtech-env.co.uk Website: Testing performed at the above address only DETAIL OF ACCREDITATION SOILS, SLUDGES AND ASSOCIATED MATERIALS Chemical Tests Documented In-House Methods based on BS 1377:Part 3:1990 Loss on ignition at 440 C Method No CE 006 ph value Method No CE 004 Anions (fluoride, chloride, nitrate sulphate,) Metals: Metals Mercury Arsenic Beryllium Cadmium Antimony Selenium Barium Cobalt Chromium Copper Molybdenum Nickel Lead Tin Vanadium Zinc Iron Method No CE 049 2:1 Water soluble anions by Ion Chromatography Documented In-House Methods based on ISO and Blue Book Methods for the Examination of Waters and Associated Materials In House Method CE127 by ICPMS Assessment Manager: JY Page 1 of 9
2 SOILS, SLUDGES AND ASSOCIATED MATERIALS (cont d) Chemical Tests (cont d) Water Soluble Boron Documented In-House Methods In house method CE063 by ICP- OES Electrical conductivity Method No CE 007 (ISBN ) Thiocyanate Method No CE 014 (ISBN X) SOILS BTEX and MTBE: Benzene Toluene Ethylbenzene (m+p)-xylene o-xylene MTBE Total Organic Carbon Organic Matter Content by calculation Extractable Petroleum Hydrocarbons (EPH) in the range, with banding >C10-C40 >C10-C44 >C10-C12 >C10-C20 >C10-C21 >C10-C25 >C10-C28 >C12-C16 >C16-C21 >C16-C35 >C20-C40 >C21-C35 >C21-C40 >C25-C40 >C28-C40 >C35-C40 >C35-C44 Method CE057 by GC-FID Documented In-House Method CE072 using Eltra carbon analyser CE033 using GC-FID Assessment Manager: JY Page 2 of 9
3 SOILS (cont d) Chemical Tests (cont d) Documented In-House Methods Polyaromatic Hydrocarbons Naphthalene, Acenaphthylene Acenaphthene, Fluorene, Phenanthrene, Anthracene, Fluoranthene Pyrene Chrysene, Benzo(a)anthracene, Benzo(k)fluoranthene, Benzo(b)fluoranthene Benzo(a)pyrene, Indeno(1,2,3,c,d)pyrene, Dibenz(a,h)anthracene, Benzo(g,h,i)perylene CE087 USING GCMS detection SOILS (cont d) Chemical Tests (cont d) Documented In-House Methods PolyChlorinated Biphenyl Congeners: PCB 28 PCB 52 PCB 101 PCB 118 PCB 138 PCB 153 PCB 180 PCB Total of ICES 7 Elemental Sulphur Total Cyanide CE137 using GCMS detection In house method CE034 using HPLC In house method CE077 using continuous flow analyser Assessment Manager: JY Page 3 of 9
4 SOILS Chemical Tests Documented In-House Methods to meet the requirements of the Environment Agency MCERTS performance standard - chemical testing of soil ph Method CE 004 Acid soluble sulphate Water soluble sulphate (2:1) Method CE 062 using ICP-OES Method CE 061 using ICP-OES Thiocyanate Method CE 014 Total Organic Carbon Organic Matter Content by calculation Documented In-House Method CE072 using Eltra carbon analyser Assessment Manager: JY Page 4 of 9
5 SOILS (cont d) Chemical Tests (cont d) Documented In-House Methods to meet the requirements of the Environment Agency MCERTS performance standard - chemical testing of soil Metals Mercury Arsenic Cadmium Antimony Selenium Barium Cobalt Chromium Copper Molybdenum Nickel Lead Tin Vanadium Zinc Iron Water Soluble Boron Polyaromatic Hydrocarbons Naphthalene, Acenaphthylene Acenaphthene, Phenanthrene, Fluoranthene Pyrene Chrysene, Benzo(k)fluoranthene, Benzo(b)fluoranthene Indeno(1,2,3,c,d)pyrene, Dibenz(a,h)anthracene, Benzo(g,h,i)perylene In House Method CE127 by ICPMS In house method CE063 by ICP- OES CE087 using GCMS detection Assessment Manager: JY Page 5 of 9
6 SOILS (cont d) Chemical Tests (cont d) Documented In-House Methods to meet the requirements of the Environment Agency MCERTS performance standard - chemical testing of soil Extractable Petroleum Hydrocarbons (EPH) in the range, with banding CE033 using GC-FID >C10-C40 >C10-C44 >C10-C12 >C10-C20 >C10-C21 >C10-C25 >C10-C28 >C12-C16 >C16-C21 >C16-C35 >C20-C40 >C21-C35 >C21-C40 >C25-C40 >C28-C40 >C35-C40 >C35-C44 PolyChlorinated Biphenyl Congeners: PCB 28 PCB 52 PCB 101 PCB 118 PCB 138 PCB 153 PCB 180 PCB Total of ICES 7 Elemental Sulphur Total Cyanide CE137 using GCMS detection In house method CE034 using HPLC In house method CE077 using continuous flow analyser Assessment Manager: JY Page 6 of 9
7 WATERS Chemical Tests Documented In-House Methods based on BS 1377:Part 3:1990 ph value Method No CE 004 Ammonia Method No CE 012 by Colorimetry Electrical conductivity Method No CE 007 (ISBN ) Alkalinity Method No CE 035 (ISBN ) surface water, landfill leachate and industrial effluent Chemical Oxygen Demand (Total, Settled, Filtered) Documented In house method CE037 Assessment Manager: JY Page 7 of 9
8 WATERS Chemical Tests Documented In-House Methods Groundwater, Surface water, Landfill leachate, Leachate prepared from soils, Effluent Filtered Metals: Aluminium Antimony Arsenic Barium Beryllium Boron Cadmium Cobalt Chromium Copper Iron Mercury Manganese Molybdenum Nickel Lead Selenium Strontium Tin Vanadium Zinc Calcium Magnesium Phosphorus Potassium Sulphur Sodium BTEX and MTBE: Benzene Toluene Ethylbenzene (m+p)-xylene o-xylene MTBE Documented In house method CE128 by ICPMS Method CE057 by GC-FID leachate from landfill, effluent Suspended solids Method No CE 038 (ISBN ) Assessment Manager: JY Page 8 of 9
9 WATERS (cont d) Chemical Tests (cont d) Documented In-House Methods leachate from landfill Groundwater, leachate prepared from soil, effluent Chromium (hexavalent) Anions (fluoride, chloride, bromide, nitrite, nitrate, sulphate, phosphate) Method No CE 050 by Colorimetry Method No CE 049 by Ion Chromatography Groundwater, surface water Thiocyanate Method No CE 014 (ISBN X) END Assessment Manager: JY Page 9 of 9
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