Price list. Institute for Paper, Pulp and Fibre Technology. January 2015

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1 Last modification Price list Institute for Paper, Pulp and Fibre Technology January TESTING OF PAPER AND PAPERBOARD 1.0 Sample preparation Page Basic properties Page Composition Page Strength properties Page Force-deformation Behaviour Page Surface properties Page Optical properties Page Structural properties of paper Page Printability properties Page Liquid-Paper Interactions Page Barrier properties against gases and liquids Page 11 2 TESTING OF PULP AND ADDITIVES 2.0 Chemical pulp, mechanical pulp and waste paper testing Page Testing of fillers and coating pigments Page Preparation and Testing of Coating Color Page 14 3 CONDITIONS OF CONTRACT Page 15 Discounts and express or overtime pay Further information on prices and services Seite 1 von 16

2 1.0 SAMPLE PREPARATION 1 Conditioning of samples n.a. Paper and board, 23 /50% DIN EN ISO TAPPI T 402 sp V/1.1/86 20.Mär.86 Climate chamber for other testing climates described in ISO Climate Chamber per day 47, BASIC PROPERTIES 1 Grammage EN ISO ,50 Paper and board DIN EN ISO ÖNORM EN ISO ISO TAPPI T 410 om V/11/57 01.Jul.57 Corrugated board DIN ISO Tissue paper DIN EN ISO ,00 V/29.2/81 25.Mär.81 2 Grammage - CD profile 10 test points (air-dry), sampling at defined positions 19,50 10 test points (oven-dry) 13,50 3 Thickness, density, bulk EN ISO ,00 Paper and board DIN EN ISO ISO TAPPI T 411 om Tissue paper DIN EN ISO V/29.3/81 25.Mär.81 4 Measurement of hygroexpansivity, 3 climates DIN ISO ,50 2 climates 102,50 5 Dirt and shive determination in paper and board Visual estimation of impurities (mm²/m²) with TAPPI dirt count charts DIN EN ISO ,00 TAPPI T 437 om Seite 2 von 16

3 1.2 BASIC PROPERTIES Moisture content Oven-drying method (paper and board) EN ISO ,50 ISO DIN EN ISO TAPPI T 412 om Tissue paper DIN Ash DIN ,00 Paper and board, 900 C ISO T 413 om IV/40/77 15.Sep.77 Pulp, 575 C ISO C TAPPI T 211 om Fiber analysis microscopy, qualitatively with photos ISO ,00 TAPPI T 401 om IV/55/74 01.Dez.74 Fiber analysis microscopy, qualitatively without photos 34,00 4 Filler distribution in z-direction VAP-method 532,00 5 ph of aqueous extracts - hot extraction ISO ,00 DIN TAPPI T 435 om-11 (paper) 2011 TAPPI T 252 om-12 (pulp) 2012 for contact with food ÖNORM EN DIN EN Cellulosic papers for electrical purposes DIN EN n.a. 6 ph of aqueous extracts - cold extraction ISO ,50 DIN TAPPI T 509 om for contact with food ÖNORM EN Change in ph over time VAP-Method 215,00 8 Acid-insoluble ash ISO ,00 DIN IV/49/69 29.Sep.69 9 Acid-insoluble lignin in wood and pulp TAPPI T 222 om ,50 Seite 3 von 16

4 10 Acetone-soluble matter DIN EN ISO ,00 ÖNORM EN ISO SCAN-CM 49: dichloromethane-extract TAPPI T 204 cm IV/43/67 23.Okt Conductivity of aqueous extracts ISO ,50 DIN DIN EN Detection of starch Merck, S ,00 13 CMC - qualitative detection Wochenblatt d. Papierfabrikatio 17/ , STRENGTH PROPERTIES 1 Tensile strength, stretch at break, tensile index EN ISO ,50 tensile energy absorption DIN EN ISO ISO V/12/57 01.Jul.57 TAPPI T 494 om Constant rate of elongation (100 mm/min) ISO Tissue paper DIN EN ISO tensile strength of perforated lines - Calculation of perforation efficiency DIN EN ISO Tensile strength after immersion in water ISO ,00 DIN ISO SCAN-P 20: Tissue paper DIN EN ISO Initial wet tensile strength with blotting paper VAP-Method 75,50 3 Bursting strength, burst index ISO ,00 Paper DIN EN ISO TAPPI T 403 om V/12/57 01.Jul.57 Board ISO DIN EN ISO TAPPI T 807 om-11 (einwellig) 2011 TAPPI T 810 om-11 (Liner) Bursting strength after immersion in water DIN ISO ,50 ISO ZM VIII/1/ Tear resistance, tear index (Elmendorf) per direction EN ISO ,00 ÖNORM EN ISO DIN EN ISO ISO TAPPI T 414 om V/12/57 01.Jul.57 Seite 4 von 16

5 6 Tear test - Brecht-Imset-method, per direction DIN ,00 V/12/57 01.Jul.57 7 Folding endurance / double folds (Schopper method) ISO ,00 per direction TAPPI T 423 cm V/12/57 01.Jul.57 8 Flat crush of corrugated medium (CMT test) EN ISO ,50 DIN EN ISO ÖNORM EN ISO ISO TAPPI T 809 om Flat crush test (FCT) DIN EN ISO ,00 ISO TAPPI T 808 om Internal bond strength (z-direction) TAPPI T 541 om ,50 DIN Internal bond strength (Scott-Bond), per direction TAPPI T 569 om ,50 12 Ring crush test (RCT), per direction DIN ,00 ISO TAPPI T 822 om Surface strength of paper - wax picking test (Dennison) TAPPI T 459 om ,50 per Side 14 Folding endurance - mechanical pulp (Schopper method) ZM VI/1/66 45,00 per direction Korn Burgstaller S Ageing resistance DIN ISO ,50 Ageing resistance, climate chamber per day VAP-Method 47,00 16 Residual tensile strength after fold VAP-Method 66,50 17 E - module, per direction VAP-Method 83,00 (Zwick-Equipment Manual + Optimization of the parameters) 18 Compression strength, short span test (SCT) DIN ,50 Short-span test ISO Seite 5 von 16

6 1.4 FORCE-DEFORMATION BEHAVIOR 1 Force-elongation curves (Zwick) EN ISO ,50 2 Elastic modulus, tensile energy absorption EN ISO ,00 ISO TAPPI T 494 om (measured together with tensile strength) 8,50 3 Bending stiffness (L&W), per direction ISO ,00 SCAN-P 29: V/20/70 02.Jun.70 VIII/5/68 19.Nov.68 4 Bending resistance (Taber, conversion from L&W) TAPPI T 489 om , SURFACE PROPERTIES 1 Smoothness (Bekk), per side DIN ,00 ISO TAPPI T 479 cm V/23/73 17.Apr.73 2 Roughness/smoothness (Bendtsen), per side ISO ,00 DIN V/24/73 17.Apr.73 3 Smoothness (SPS), per side TAPPI T 460 om ,00 4 Smoothness (Gurley), per side TAPPI T 460 om ,00 5 Roughness of paper and paperboard (PPS), per side DIN ISO ,00 TAPPI T 555 om BS 6563: Hardness (Bendtsen) - according to Büchel Equipment Manual 71,00 7 Hardness (Bekk), per side Korn Burgstaller, S ,00 8 Coefficient of static friction DIN ,50 5 samples each, per side and direction (20 samples) ÖNORM A TAPPI T 815 om Seite 6 von 16

7 9 Compressibility and roughness of paper (UST) VAP-Method 130,00 Surface topography with and without load (UST) VAP-Method 77,00 rate per hour 5,00 10 Surface topography together with optical surface image (IFM) Alicona IFM VAP-Method IFM Optical Microscopy, imaging with diffusive illumination, standard: 5x5 pictures 59,50 Alicona IFM surface-topography, standard: 5x5 pictures 83,00 rate per hour 3, OPTICAL PROPERTIES 1 Brightness (Reflectance) 27,50 Basics ISO ISO-Brightness R457 Paper and board C/2 ISO D65-Brightness Paper and board D65/10 ISO Tissue D65/10 DIN EN ISO Tisuue C/2 DIN EN ISO CIE Whiteness D65/10 (outdoor daylight) ISO CIE Whiteness C/2 (indoor) ISO Florescent specimens DIN Non-flourescent speciments DIN Tablets for optical testing of pigments DIN Preparation of handsheets for the measurement ISO ,00 of brightness (reflectance) TAPPI T 525 om Opacity DIN ,00 ISO TAPPI T 519 om Lightness (Y) DIN ,50 5 CIELAB Color, per illuminant 33,50 d/0 / C/2 / L*a*b* ISO d/0 / D65/10 / L*a*b* ISO d/0 / C/2 / L,a,b, Hunter, C,h TAPPI T 527 om CIELAB Color difference (CMC) 71,00 7 ERIC 950 Effective Residual Ink Concentration Technidyne - Manual 122,50 8 Specular gloss 75, per side DIN ISO ,00 with a converging beam, TAPPI method ISO ÖNORM EN ISO TAPPI T 480 om-09 (75 ) Light-scattering and -absorption coefficients DIN ,50 SCAN-CM 27: Seite 7 von 16

8 10 Transparency DIN ,50 11 Optical brighteners, quantitativ detection VAP-Method 53,50 12 Optical brighteners, qualitativ detection VAP-Method 11,00 13 Accerelerated ageing, Yellowing (climate chamber) DIN ISO n.a. ISO 5630/ ISO 5630/ ISO 5630/ TAPPI T 453 sp Yellowness index DIN ,50 15 Image analysis, optical microscope, rate per hour VAP-Method 40,00 rate per day 179,00 + report (rate per hour) 129,50 16 High definition measurement of gloss, refractive index, microroughness (Surfoptics) VAP-Method Point measurement (10) per side and sample 34,50 Grid measurement (2x2cm) per side and sample 85,50 Grid measurement (4x4cm) per side and sample 135,00 17 Print density (Gretag Densitometer) VAP-Method 33, STRUCTURAL PROPERTIES OF PAPER 1 Formation index (MK-Tester) M/K II- Manual 45,00 CD-profile per DIN A4 28,50 2 Formation; transmitted light scanner (PTS DOMAS system) VAP-Method 56,50 one DIN A4 (4 single measurements) 40,50 3 High-resolution formation measurement (beta radiography) VAP-Method 135,00 max. grammage 130 g/m² evalution by image analysis 161,00 4 Fiber orientation in z-direction; FO angle, anisotropy Cleavage of 3 strips (~30 layers), Matlab VAP-Method 590,00 Cleavage of 3 strips (~30 layers), Optimas / Excel VAP-Method 655,00 5 Layer seperation VAP-Method n.a. corresponding to A5 per layer 23,50 Basis weight of layers of corrugated board ÖNORM A Seite 8 von 16

9 6 Coating coverage (burnout test) VAP-Method 96,00 with image analysis 118,50 7 Coating thickness distribution (Microtomy images), video sequences VAP-Method n.a. 1.8 PRINTABILITY PROPERTIES 1 Resistance to picking (IGT Tester), per side and direction IGT-Manual 124,00 2 Penetration print (IGT Tester) IGT-Manual 66,00 3 Ink setting, visual assessment IGT-Manual 66,00 Ink setting for specified ink-paper combinations V/32/ Color density measurement (Gretag) Gretag - Manual 122,00 4 Print gloss (Prüfbau) Prüfbau-Manual 149,50 (incl. Gloss-Lehmann) 5 Color density measurement (Gretag) per tone level VAP-Method 33,00 6 Ink penetration on paper cross sections VAP-Method 211,50 full tone, 100mm, measurement every 5 µm 7 IASU print unevenness (Mottling index) per tone level VAP-Method 104,00 8 Printing dot analysis (single dot) per tone level (3000 dots) VAP-Method 154,50 9 PF-Method 4 stripes (1x15cm, 8points) VAP-Method 170,00 10 Structure of printing ink penetration VAP-Method 100,00 6 per side and sample 11 Ink penetration (Microtome, Image Analysis) VAP-Method 248, LIQUID-PAPER INTERACTIONS 1 Water absortion - Cobb method, per side ISO ,00 DIN EN ISO TAPPI T 441 om Oil absorption (Cobb-Unger), per side SCAN-P 37: ,00 3 Grease resistance 3M KIT Test (Castor oil) 3M - Manual n.a. Grease permeability KIT Test TAPPI T 559 cm n.a. Seite 9 von 16

10 4 Capillary rise - Klemm method, per direction DIN ISO ,50 ISO Suction velocity sec (0-10mm) VAP-Method (UA 2755) 5 Writing properties by ink, per side DIN ,00 (pen-stroke-method) 6 Float test, per side Korn Burgstaller, S ,00 7 Water absorption and swelling, water immersion DIN ,50 VIII/2/67 01.Nov.67 8 Wet elongation, 5 per sample and direction + diagram VAP-Method 92,00 Tissue DIN V/29.5/81 25.Mär.81 Korn Burgstaller S241 9 Wet Stretching of paper under one sided Liquid contact (WSD) VAP-Method 140,50 5 measurements per side + diagram 10 Penetration measurements with aqueous solutions (PDA) VAP-Method Standard (3 min) H 2 O (10 measurements per side) 96,00 others (Slurrys, Oils) 114,50 Analysis in Excel 31,50 11 Penetration measurements with aqueous solutions (PEA) VAP-Methode Standard (2 min) H 2 O (5 measurements per side) 96,00 others (Slurrys, Oils) 114,50 Excel averaging curves 31,50 Excel per time segment 31,50 12 Contact angle measurement (FIBRO), Excel T 558 om ,50 1 liquid Only Fibro-File 66,00 13 Surface tension and polarity, Contact angle method (FIBRO) T 558 om ,50 14 Water retention value (WRV) ISO ,00 IV/33/57 01.Jän Water-absorption time and water-absorption capacity EN ISO ,00 Tissue, wire basket DIN EN ISO Dissolution behavior of tissue papers, flake content VAP-Method ,50 Seite 10 von 16

11 1.10 BARRIER PROPERTIES AGAINST GASES AND LUIQUIDS 1 Air permeability - Bendtsen method ISO ,00 DIN V/26/75 15.Sep.75 2 Air permeability - SPS method TAPPI T 460 om ,50 3 Air permeability - Gurley method ISO ,50 T 460 om Water vapour transmission rate - Dish method ISO ,00 DIN building materials and products DIN EN ISO ,50 Flexible sheets for waterproofing DIN EN TAPPI T 448 om-09, 23/ TESTING OF PULPS AND ADDITIVES 2.0 CHEMICAL PULP; MECHANICAL PULP AND WASTE PAPER TESTING 1 Laboratory cooking VAP-Method n.a. 2 Yield determination VAP-Method 71,00 3 Laboratory bleaching VAP-Method n.a. 4 Disintegration 37,00 Chemical pulps DIN EN ISO Mechanical pulps DIN EN ISO Hot-Disintegration of mechanical pulps at >= 85 C DIN EN ISO ,00 6 Laboratory beating Jokro mill DIN ,00 V/5/60 01.Nov.61 Beating to a certain freeness, all freeness levels are charged extra 161,50 7 Laboratory beating PFI-mill ÖNORM EN ISO ,00 ISO 5264/ TAPPI T 248 sp Beating to a certain freeness, all freeness levels are charged extra 161,50 8 Laboratory beating Valley beater ISO 5264/ ,50 up to 4 beating levels point any further beating level 37,00 Beating to a certain freeness 301,50 Seite 11 von 16

12 9 Drainability Schopper-Riegler-value, CSF-value EN ISO ,00 DIN ISO ISO 5267/ ÖNORM EN ISO V/7/61 01.Jul Drainage time of pulp see above 21,00 11 Fines fraction by weight of paper stock by wet screening (Britt-Jar) VAP-Method 124,50 T 261 cm ISO Washing of Pulp VAP-Method 68,00 13 Stock concentration (Rapid method) EN ISO ,00 ISO DIN EN ISO ÖNORM EN ISO Dry matter content EN ISO ,50 ISO DIN EN ISO ÖNORM EN ISO IV/42/67 23.Okt Ash in pulp (575 C) ISO ,50 16 Handsheet forming (Rapid-Köthen), 1 pulp, 5 hand sheets EN ISO up to 5 hand sheets ISO 5269/ ,00 DIN EN ISO ÖNORM EN ISO any further 3,50 each additional fiber component 41,00 5 hand sheets free shrunk VAP-Method 64,50 any further 6,50 Addition of slurry on certain filler content VAP-Method 70,50 Addition of additives, per add VAP-Method 18,00 Hand sheets for dirt in pulp, in according to TAPPI T 213 om ,00 17 Initial wet strength (g/30mm) VI/1/ ,50 18 Content of flakes V/18/62 01.Sep.62 45,50 19 Dirt in pulp TAPPI T 213 om ,00 Büchner, 200 g/m² 20 Debris in pulp, transmitted light VAP-Methode 211,50 21 Shive content and fiber classification (Brecht-Holl method) VI/1/66 03.Feb ,00 mesh 50 III/14/69 01.Dez.69 69,50 slotted screen only 69,50 22 Shive content and fiber classification (McNett method) TAPPI T 233 cm ,00 SCAN-CM 6: V/1.4/86 20.Mär.86 Seite 12 von 16

13 23 Screening of pulp (Somerville) TAPPI T 275 sp ,00 24 Fiber length distribution, Coarseness (optical) ISO Kajaani FS200 Kajaani-Manual 90,00 Excel without Coarseness 106,50 Excel with Coarseness 140,50 25 Fiber dimensions - Curl Fiber Tester ISO ,00 Excel without Coarseness (Standard) 160,00 Excel with Coarseness (Standard) 211,50 26 Vessel cell content of pulps VAP-Methode 147,00 Disintegration DIN EN ISO ,00 Coarseness Kajaani Kajaani-Manual 90,00 27 Kappa-number, with known dry matter content ISO ,00 DIN TAPPI T 236 om IV/37/80 07.Jul Viscosity of pulp (CED) ISO ,00 TAPPI T 230 om Measurement of the average viscometric degree of polymerization of new DIN EN and aged cellulosic electrical insulating materials 29 Alphacellulose in pulp ISO ,00 TAPPI T 203 cm IV/39/67 20.Feb.67 Alkali resistance DIN ,00 Betacellulose in pulp 5,50 Gamma-cellulose in pulp 53,50 30 Alkali reserve (volumetric) ISO ,50 31 Copper number Zellcheming IV/8/ , TESTING OF FILLERS AND COATING PIGMENTS 1 Moisture content of fillers (oven dry method) VAP-Method 30,50 2 Dry matter content of fillers VAP-Method 30,50 3 Slurry preparation of dry fillers VAP-Method 44,00 4 Tablets for optical testing of pigments DIN ,00 SCAN-P 89: TAPPI T 534 om Test for pigments and fillers - ph value of an aqueous suspension DIN EN ISO ,00 Seite 13 von 16

14 2.2 PREPARATION AND TESTING OF COATING COLOR 1 Preparation of coating colors VAP-Method n.a. 2 Rheological properties (Paar Physica) VAP-Method n.a. Standard tests (amplitude sweep, jump test, flow curve) 85,50 3 Viscosity of slurrys (Brookfield) TAPPI T 648 om ,50 Starch TAPPI T 676 cm SCAN-P 50: Anionic and nonionic dispersing V/27.9/ Coating with automatic hand blade instrument VAP-Method n.a. 5 Pilot Coater Trials, per hour VAP-Method 185,00 6 Calendering, 5 sheets VAP-Method 27,00 any further 3,50 Calendering with pre-wetting in a climate chamber VAP-Method 53,50 Seite 14 von 16

15 3 CONTRACT CONDITIONS 3.1 The acceptance of the order made on the basis of a written order. 3.2 All orders will be treated as confidential, the results of the investigation will be communicated only to the client. 3.3 All prices are without VAT (TU Graz charged by the Universities Act 2002, no VAT). 3.4 A lump sum for issuing the report (currently 27) will be charged. 3.5 Accretion of Discount percent discount 1-4 samples 0% 5-9 samples 10% samples 20% samples 30% 40 - mehr samples 40% Beispiel: 22 Bestimmungen (á 23 ) samples with 0% discount samples with 10% discount 103, samples with 20% discount samples with 30% discount 48,3 Price 427,8 Discount 78,2 3.6 Express or overtime pay If overtime (working longer than until 17:00h or weekends) is necessary it will be charged with the double hourly rate of our laboratory technicians. 3.7 The with N. A. marked (according to expenditure) examinations will be charged at the hourly rate of the laboratory technicians. This also concerns additional time due to for example lack of sample size. 3.8 If procedures are not feasible or if the customer withdraws from the contract, the services and expenses to this point have to be paid by the customer. 3.9 The standards blue and bold in the price list are to be understood as the main standards corresponding to the ISO accreditation. Preis Seite 15 von 16

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