CONTENTS. GENERAL INTRODUCTION... 3 Welcome at ENSCL...4 I- INFORMATION ON THE INSTITUTION... 5

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2 2 CONTENTS GENERAL INTRODUCTION... 3 Welcome at ENSCL...4 I- INFORMATION ON THE INSTITUTION... 5 A. THE FRENCH EDUCATION SYSTEM... 5 B. NAME AND ADDRESS OF THE INSTITUTION... 5 C. GENERAL DESCRIPTION OF THE INSTITUTION... 6 D. REGISTRATION REQUIREMENTS FOR ECTS STUDENTS... 7 E. PREREQUISITE IN FRENCH... 7 F. ACADEMIC CALENDAR... 8 II- GENERAL INFORMATION... 9 A. HOW TO REACH THE ECOLE NATIONALE SUPERIEURE DE CHIMIE DE LILLE? 9 B. ACCOMMODATION C. RESIDENCE PERMIT D. SOCIAL SECURITY E. UNIVERSITY LIBRARY F. ASSOCIATIONS G. SPORT H. LEISURE I. MISCELLANEOUS J. TELEPHONE K L. USEFUL ADDRESSES III- GENERAL DESCRIPTION OF THE INSTITUTION A. TEACHING B. RESEARCH C. PROGRAMME OF STUDY FOR "LE CYCLE INGENIEUR" /09 version APPENDIX (Application process) 130

3 3 GENERAL INTRODUCTION This "Information Package" describes the Ecole Nationale Supérieure de Chimie de Lille and the programmes available for European students who will spend 1 or 2 semesters in the school within the ERASMUS LIFE LONG LEARNING programme. The objective of ECTS (European Credit Transfer System) is to guarantee academic recognition of studies abroad, enabling students to have access to regular courses alongside local students, with the benefit of full participation in the academic life of the host institution. It guarantees curriculum transparency by providing detailed information on the curricula and their relevance towards a degree. ECTS helps academics to make academic recognition decisions thanks to prior agreements on the content of study programmes abroad between students and their home and host institutions. ECTS credits are a value allocated to course units to describe the student workload required to complete them. They reflect the quantity of work each course requires in relation to the total quantity of work required to complete a full year of academic study at the institution, that is, lectures, practical work, seminars, private work- in the library or at home- and examinations or other assessment activities. Credits thus express a relative value. In ECTS, 60 credits represent the workload of a year of study; normally 30 credits are given for a semester, and 20 credits for a term. ECTS credits can be allocated to practical placements, and to thesis preparation when these activities are an assessed part of the official programme of study. ECTS credits are allocated to courses and awarded to students who successfully complete those courses by passing the examinations or other assessments. To help institutions interpret the grades awarded to ECTS students, the ECTS grading scale has been developed by the institution participating in the pilot scheme. This provides additional information to the student's performance to that provided by the institution's grade, but does not replace the local grade. Higher education institutions make their own decisions on how to apply the ECTS grading scale to their own system. The transcript of records shows the learning achievements of the student prior to and after the period of study abroad. Every course taken by the student is recorded on the transcript of records with not only the ECTS credits but also the grade awarded according to the local grading scale and, when available, the ECTS grading scale. The combination of grades and ECTS credits represents the performance of the students in qualitative and quantitative terms respectively. The learning agreement, which describes the programme of study abroad and is drawn up by the individual student and the institution involved before the student goes abroad. ECTS enables further studies abroad. A student may prefer not to go back to the home institution after the study period abroad, but rather stay at the host institution - possibly to gain a degree- or move on to a third institution. The institutions themselves will decide whether or not this is acceptable and what conditions the student must fulfil in order to transfer registration and/or to get a diploma.

4 4 Welcome at ENSCL! Since 1894, The Ecole Nationale Supérieure de Chimie de Lille (ENSCL), or the National Graduate School of Chemistry and Chemical Engineering of Lille, has been closely following scientific and technological developments in the training of its graduates. ENSCL provides its students with a solid grounding in chemistry, essentially based on chemical engineering, materials, formulation, bioprocesses and catalysis. To help them fit perfectly into today s industrial world and become responsible engineers, ENSCL offers effective tuition in foreign languages, social sciences, management, economics and administration. Being open to the entire world is also a priority for us. ENSCL has trained over 3,600 graduates whose qualities and skills are recognised worldwide. The openness of the school can also be seen in its diversified national and international recruitment policy. If the idea of becoming a graduate chemist appeals to you, then join us and share our values! Our Euroregion of Nord - Pas de Calais has a reputation for its hospitality. We will be no exception to the rule and be delighted to welcome you. We are looking forward to hearing from you! Jean Grimblot Director of the ENSCL Welcome day for international students- September 2009

5 5 I- INFORMATION ON THE INSTITUTION A. THE FRENCH EDUCATION SYSTEM Scientific university curricula are divided into three levels : - First level ( three years), leading to the Bachelor s degree - Second level (two years), leading to the Master s degree - Third level (up to three years), with the Doctoral degree Some peculiarities of the Fench higher education system may first surprise foreign students : - it does not only take place in universities, but also sometimes in High Schools ("lycées") even after having obtained a Baccalauréat (special courses preparing for specialized colleges, special technical sections - "STS"), and many Engineering Schools are compared to foreign equivalents (from 30 to 500 students per year). - French universities themselves normally do not select among candidates : the Baccalauréat (bac) itself opens the doors to Higher Education. Competition among students occurs for the entry into smaller colleges, like IUT (technical institutes), STS (special technical sections), "classes préparatoires" 1 for Engineering Schools. Competitive examinations are organized at the Baccalauréat level, or two years thereafter when leaving the "classes préparatoires" (bac + 2 level). There are a lot of engineering studies in France. They differ from one another on several grounds : programme duration, kind of entrance examination, areas covered. Foreign students cannot easily grasp a clear picture with such a great amount of sometimes small schools. The common characteristic of those Graduate Engineering Schools is the engineering degree (bac + 5 level). The classical model of specifically French engineering education system includes two stages : - two years of "classes préparatoires" - three years of higher technical education within schools. B. NAME AND ADDRESS OF THE INSTITUTION Ecole Nationale Supérieure de Chimie de Lille Cité Scientifique Bât C7 BP FRANCE VILLENEUVE D'ASCQ CEDEX Tel. (33) Fax. (33) World Wide Web Address : Director Jean GRIMBLOT tel : + 33 (0) fax : + 33 (0) Preparation for the nationwide competitive entrance examination to French Engineering Schools

6 6 [email protected] Director of Studies Jean MARKO tel : + 33 (0) fax : + 33(0) [email protected] International Department Zahia TURPIN, Director ECTS/SOCRATES Coordinator tel/fax : + 33 (0) [email protected] Mélanie CHARPENTIER, Incoming students Tel/fax : [email protected] Location Welcome to the Nord-Pas-de-Calais region, with its 4 million inhabitants, where the mercantile and industrial tradition is bordering the challenge of innovation. A land of progress strengthened by its enthusiastic youth (42 % of its population is less than 25), this region relies on an avant-garde infrastructure. Thanks to the Channel Tunnel, the North European TGV and its precious human resources, the Nord-Pas-de-Calais region has become the first European platform of exchanges, innovations and new technologies. All these achievements have combined with a huge development of the regional higher education with 7 universities. Lille is a cross-border metropolis of 1.5 million inhabitants. Its schools and 4 universities, whose foundation dates back to Philip II of Spain in 1562, have set up a common means of consultation and of common actions : the Pôle Universitaire Européen de Lille Nord Pas-de-Calais. The Ecole Nationale Supérieure de Chimie de Lille is located on the campus of the University of Sciences and Technology of Lille (Chemistry, building C7), 11 km from the centre of Lille in Villeneuve d'ascq. Today, the town of Villeneuve d'ascq has more than 68,000 inhabitants. It offers all the facilities of a modern town, enriched by 3 universities, Grandes Ecoles, many research laboratories, successful companies... It also offers a quality of clean life likely to attract young and entreprising people. C. GENERAL DESCRIPTION OF THE INSTITUTION 1. Introduction Founded in 1894, the Ecole Nationale Supérieure de Chimie (at that time Institut de Chimie de la faculté des sciences de Lille) is a state run higher education institution under the supervision of the French Ministry of Education. It is entitled to award engineer's degrees, which are recognised by the national committee. A lot is at stake : meeting today's needs of the industry while anticipating tomorrow's evolutions.

7 7 Like in every Engineering School, the duration of the studies is 3 years, after 2 or 3 years of preparation. 2. General structure of study Graduate Schools French Universities Anglo Saxon universities D. REGISTRATION REQUIREMENTS FOR ECTS STUDENTS ECTS students can either follow first, second, or third-year courses, or make their own programme from the courses taught in several years, or do a practical placement in a laboratory or in a company. The registration form, the learning agreement together with a transcript of records and a detailed curriculum vitae have to be sent to Mrs Zahia TURPIN. The duration of the practical placement can vary and the credits allocated to them are defined according to ECTS rules (1 semester=30 credits). For the curricula programme, ECTS students should first get in touch with their home Socrates supervisor and then the Director of studies of ENSCL. Students shall not be required to pay tuition fees at the host institution ; the student may however be required to continue to pay his/her normal tuition fees to the home institution during the study period abroad. E. PREREQUISITE IN FRENCH All the courses are given in French. A good level of French is thus absolutely required. Each ERASMUS foreign student should be able to attend courses taken in French as well as work with books or documents written in French.

8 8 Linguistic preparation (39 hours): - French courses are planned : - evaluation test in mid -September - courses start at the beginning of October (3 hours/week) 3 ECTS Credits per semester are allocated for this course. The course takes place on campus. At the end of this course, students can take an examen called "Diplôme Universitaire de Lille en Français Langue Etrangère". F. ACADEMIC CALENDAR The academic year at the Ecole Nationale Supérieure de Chimie de Lille is divided into 2 semesters : First semester : mid-september to end of January Second semester : end of January to the end of June Exams : First semester : January Second semester : end of may Holidays : - 1 week at the end of October - 2 weeks at Christmas (mid-december - January) - 1 week in February - 2 weeks at Easter (April) II- GENERAL INFORMATION A. HOW TO REACH THE ECOLE NATIONALE SUPERIEURE DE CHIMIE DE LILLE? 1) By plane - If you arrive at Paris : - From Orly airport : The "ORLYVAL" underground links only the airport with - Line B of the RER at Antony. From "Antony" station, take the underground and stop at the "Gare du Nord" station. - timetable : from 6.00 am to pm - duration : 30 minutes - price : 8,80 - there are trains every 7 minutes - From Roissy-Charles de Gaulle Airport : There is a rail link between this airport and Lille (T.G.V)

9 9 - If you arrive at Brussels airport : A shuttle regularly links the airport and the Brussels central train station - duration : 25 minutes - price : 2,50 - If you arrive at Lille-Lesquin airport : A shuttle regularly links the airport and the town centre. - duration : 20 minutes - price : 3 2) By train + underground - Departure from Paris-Gare du Nord : For schedule and price : - Departure from Brussels : For schedule and price : - In Lille train station : To reach the University of Lille I, take line n 1 of the underground, direction "4 cantons", get off at "Cité Scientifique". - duration : 15 minutes - price of a ticket : 1,25 - price of 10 tickets : 10,30 - first and last train : 5.12 am pm (Sunday, first train at 6.24 am) There are vending machines in every station (take a supply of change) REDUCTIONS SNCF (train) "Carte 12-25" This card is sold 48. It is intended for people aged from 12 to 25 and is valid one year. With this card you can have a reduction of 50% on the price. REDUCTIONS FOR THE UNDERGROUND - "Carte VIVA" This card is delivered to students who are less than 25 years old. It costs 1,50 francs and entitles them to a reduction of 25% on subscriptions (unlimited journeys) :

10 10 - weekly coupon : 8,25 - monthly coupon : 30 - coupon for 7 to 10 months : 28,65 3) By car - By the motorway, direction Lille-Villeneuve d'ascq - take the Villeneuve d'ascq - Cité Scientifique exit. B. ACCOMMODATION The Ecole Nationale Supérieure de Chimie de Lille has a few rooms available in university halls of residence. However, there are some conditions that the student has to follow. 1 The students accepted in Lille have to fill their ECTS accommodation form and send it to : ENSCL Service logements "ERASMUS" Cité Scientifique Bât C7 BP FRANCE VILLENEUVE D'ASCQ CEDEX 2 It is very difficult to find accommodation in Lille on arrival in September. However, in order to meet the ERASMUS students' specific needs, the Ecole Nationale Supérieure de Chimie de Lille has signed an agreement with the University Accommodation Office, enabling the students to get a room. Prices for ERASMUS student : «Chambre rénovée» 165,17 per month «Chambre non rénovée» 130,91 per month As soon as the student has been awarded a room, he/she has to live in this room for the whole period of his/her stay. If he/she ever wants to move, he/she will have to find another student to rent the room for the same period. No moving is allowed without the agreement of the International Relations Office. These rooms are entirely under the supervision of ENSCL. Contact : Ms Melanie CHARPENTIER Tel./Fax (0) [email protected]/[email protected] Room 17 Deposit : Every student has to give a deposit equivalent to one month rent.

11 11 This cheque will only be cashed if the room has been damaged or if you don't pay your rent. This money will be refunded to you upon proof from the caretaker that no damage has been declared, and if payments have been regular. Payment : The rent must be paid before the 5 of every month by cheque (no cash). Return of the deposit : Make an appointment with the secretary of the residence in order to make an inventory of fixtures the day before your departure. Present the certificate of the inventory of fixtures to him/her to return your deposit. Insurance : Every student must take out fire and water damage insurance and civil liability insurance (about 15 a year). The management accepts no liability for loss or damage to residents' personal effects. So, insurance for personal property is recommended. Rooms : Renovated rooms in halls of residence have a surface of 9 m², with a single bed, a washbasin, a fitted cupboard, a work table, a fridge, two hot plates, a plug for TV reception and a plug for telephone connection. Sheets and blankets can be rented. Shower rooms are located in the corridor (one shower for 10 students). Halls of residence are located on the university campus, close to the university restaurants and to the underground stations. Students are posted to their room in September. Generally, students have a room in the hall of residence called "Residence BOUCHER" which is very close to the ENSCL. Booking : Send the accommodation form (see in annex) before 1st May for an arrival in September and 1 st November for an arrival from the second semester. ALLOCATION LOGEMENT SOCIALE (A.L.S.)* In order to help you to pay your rent, you can benefit from the so called "Allocation Logement Sociale" delivered by the French Minsitry of Health Social affairs. To be eligible, you must have been living in France for more than three months, have a regular residence permit and have the following documents : - a birth certificate translated into French - particulars of your bank account - a certified copy of your identity card or passport

12 12 - a copy of your student identity card from your home university - a registration certificate - a certified copy of the accommodation certificate - a certified copy of the first month rent receipt established at the name of the tenant mentioning the name and address of the landlords. If you live in Lille, you should make your request to : Caisse d'allocations Familiales de Lille 82, rue Brûle Maison BP LILLE If you live in Villeneuve d'ascq, you should make your request to : Caisse d'allocations Familiales de Roubaix-Tourcoing 124, boulevard Gambetta BP ROUBAIX CEDEX 1 Attention : in order to get the ALS grant, your residence permit should be issued but it can take a long time to get it. Besides the ALS grant is not guaranteed for short period stays (less than six months). * the French law can cancel this financial aid. This information must therefore be considered as simple information. C. RESIDENCE PERMIT Students from the EC who stay in France for less than three months do not require a residence permit. However, if the student stays longer, he/she must go to the building A3 on the campus to obtain an extended study visa ("un visa long séjour pour Etudes"). It will cost 55. More information will be given to you at your arrival.

13 13 To obtain a residence permit, you must have an appointment and bring with you the following documents : - 4 recent photographs (with a light background) - a copy of your valid passport or identity card - your Birth Certificate translated into French - a record of Civil Status indicating the filiation - a declaration stating that you have sufficient resources to live in France during the academic year (for example your letter proving that you are a SOCRATES student and a letter from your parents declaring that they are responsible for your finances). The letter must be translated into French and include the original signature. - a copy of the ENSCL enrolment certificate - an accommodation certificate to prove your residence in France Students coming from outside the European Economic Space must apply for a visa to the French Embassy in their home country. D. SOCIAL SECURITY 1. European Union students On his/her arrival in France, the student should bring the E111, E106, E121 ou E128 form he/she got from his Social Security Office or private insurance in his/her country. The student will have to pay for any medical costs (doctor, medicine...) of the place he/she lives in France. If the student lives in Lille or Villeneuve d'ascq, he/she should send his/her prescriptions to : CPAM Relations Internationales - Service migrants 6 rue Rémi Cooghe BP ROUBAIX CEDEX 1 When sending the first request for refund, the student should enclose : - the care slip together with the medical prescription - the price labels on medicines - the original of the E111 or E128 form (it will be sent back to you later) - some particulars of his/her bank account (in France or abroad) - a letter stating that he/she is a SOCRATES student Your consultation will be refunded at 70% and your medicine between 35% and 65%. If you wish to be refunded at 100%, you can subscribe for a complementary insurance ("Mutuelle", between 132 and 264 /year (SMENO) and between 47 and 451 (LMDE)).

14 14 SMENO Furet du Nord Galerie du Ventoux Centre commercial V VILLENEUVE D'ASCQ LMDE 96/98 rue de l'hôpital Militaire Lille If the student cannot provide an E111 or E128 form or any insurance certificate recognized by the French State, he/she will be able to subscribe for the student social security system on the condition that he/she is registered as a student in France, and he/she is under 28. It will cost him/her about 174. If this is not possible, the student will have to subscribe for a private insurance (contact the CPAM). Civil liability Generally the E111 or E128 form or any other insurance does not cover third-party damage. Every European student has to subscribe for : - physical injury caused in private life - material damage The SMENO offers students this type of insurance which covers the civil liability for 20 /year. Insurance for the housing : from 16 /year.

15 15 2. Students without a European form (outside EEE) Any student coming from a country outside the European Economic Space will have to subscribe for the French Student Security System even if he/she is already covered by his/her social security system in his/her country or a French private insurance. It will cost him/her around 180 /year.

16 16 E. UNIVERSITY LIBRARY It is divided into three sections (Law, Literature and Medical Sciences-Pharmacy, Sciences). The students can use any of these sections, whatever their specialization. They just have to register, with their student card, at the library. The registration is free. Opening hours (from November to June) : 8.00 am pm from Monday to Friday 9.00 am am Saturday Closure during : - the Christmas holidays - the Easter holidays - August Lending : 5 documents Lending duration : - books, thesis, periodicals : one fortnight - periodicals in the reading room (except the latest number) : one week Other libraries : Bibliothèque Municipale de Lille, 32/34 rue E. Delesalle. Bibliothèque Municipale de Villeneuve d'ascq, 96 chaussée de l'hôtel de Ville. F. ASSOCIATIONS 1. The "Association des élèves-ingénieurs" The Association's target is to represent its members, to improve the students' working conditions, to organize activities for them, and in particular annual galas, to participate in student events, to help maintain close links between the ENSCL, its students and the former students (each student is sponsored by a former student). 2. "ENSCL-ACTIVITES" Association Created in 1983, it is a non-profit-making organization. It is an association which type is the "Junior Entreprise", managed by the students who put their knowhow and ultramodern equipment at the service of companies.

17 17 3. INTERNATION STUDENTS CLUB Our international students club readily welcomes international exchange students. Your programme manager will put you in contact with them. Here is the address of the association which welcomes international students : Club d Accueil International ENSCL Bureau des Elèves Cité scientifique tel : [email protected] always put us in cc ([email protected]) The association helps international students adapt to the French way of life. Its main aims are : - to welcome foreign students from the day of their arrival : accommodation, introduction to the campus, evenings out, conferences... - to promote the Northern region with a view to its tourist attractions, innovative companies, cultural entertainment... - to solve the problems of everyday life (medical care, medicines, travel discounts...) and university life (lecture notes, teacher contact...) - to put international exchange students in contact with French students. G. SPORT The University of Lille I favours the practise of sport for its students, including the promotion of competition. Through an important sport center, it provides the students with the means to participate in great number of sport activities (football, rugby, basket, volley, handball, swimming-pool, field hockey, athletics, cross-country, tennis...). H. LEISURE Tourist Office in Lille 42, place Rihour LILLE Tourist book of Lille (in French or in English) : get it from the International Office. Tourist Office in Villeneuve d'ascq : Allée du Chat Botté VILLENEUVE D'ASCQ Cultural places in Villeneuve d'ascq : - The Theatre : l'espace Rose des Vents

18 18 - The Ferme St-Sauveur - The cinemas - The Musée d'art Moderne - The Centre de Culture Scientifique - The bibliothèque municipale (library) - the Espace Concorde - The Maison d'activités Culturelles et de Colloques (MACC) I. MISCELLANEOUS Cost of miscellaneous expenses : University Restaurant about 2.60 /meal University residence about 200 /month Books and stationery about 65 Private room from 230 to 305 /month Underground tickets (a book of 10) 10,20 J. TELEPHONE You need phonecards for allmost all public telephones. You can buy them in post offices and at tobacconists. - When phoning abroad from France, dial 00 + country code + phone number - When phoning France from abroad, dial phone number (without the first "0") Numbers to dial in emergency : - police : 17 - fire brigade : 18 - SAMU (mobile emergency medical service) : 15 - SOS "mains et doigts" : (clinique de Lille Sud, 96 rue G. Delory LESQUIN) - Centre Hospitalier Régional (CHR) : (2 rue Oscar Lambret à Lille - metro line n 1) - Treatment Centre for poisoning cases : (rue du professeur J. Leclerc à Lille) K. An electronic address is given to each foreign student a few weeks after arrival at ENSCL.

19 19 L. USEFUL ADDRESSES Town Councils : Hôtel de Ville de Lille Place R. Salengro LILLE Hôtel de Ville de Villeneuve d'ascq Place S. Allende VILLENEUVE D'ASCQ Post Offices : In Villeneuve d'ascq : - la Poste Centrale de Villeneuve d'ascq, rue de Lille tél : et la Poste du Triolo, rue Traversière tél : In Lille : - la Poste Centrale de Lille, 7 place de la République tél : Banks : - Scalbert Dupont, rue Trudaine, Villeneuve d'ascq tél : Banque Populaire du Nord, 12 place de la République Villeneuve d'ascq tél : BNP, 20 place S. Allende, Villeneuve d'ascq tél : contact Karine BLONDEAU tél : Crédit Lyonnais : 28 rue Nationale - Lille tél : Crédit Lyonnais : Centre Commercial V2 Villeneuve d'ascq tél :

20 20 III- GENERAL DESCRIPTION OF THE INSTITUTION A. TEACHING The teaching at ENSCL aims at training engineers with expertise in chemistry, and physico-chemistry as well as chemical engineering, and geared to the various requirements of firms in the fields of chemistry, parachemistry and metallurgy. The students are put in touch with the different aspects of their future jobs through courses in economics and management, visits to factories, work placements, and eventually a research project involving practical applications in a firm. The core courses are metallurgy, solid state chemistry and chemical engineering. A strong emphasis is laid on languages - English, German, in which all the graduates are expected to be fluent, and optional Japanese. B. RESEARCH In order to maintain a high level of training for its students, the school has to integrate the latest developments in research and technology into its curriculum. This can only be made possible if the institution can make use of a competitive infrastructure within its own laboratories. This is the reason why for many years the ENSCL has developed a research policy which is particularly active in the fundamental field as well as in applied sciences. This development takes place in full collaboration with the USTL as part of the close links between the two structures. The research teams of the school have been awarded the status of CNRS-associated units, which is a recognition of the scientific expertise of the work carried out. Each one of the teams has established fruitful relations with the industrial world and the scientific community at a national level, be it private or public, through the registration of patents and the publication every year of a great number of articles in international reviews. It is thanks to the financial help provided by the Ministry of Education that ENSCL can follow a policy requiring both high technology equipment and motivated and dynamic teams. This help will enable it to increase its contribution to the development of the Nord-Pas-de-Calais region.

21 21 RESEARCH LABORATORIES LABORATOIRE DE CRISTALLOCHIMIE ET PHYSICOCHIMIE DU SOLIDE UPRESA CNRS N 8012 Permanent staff: 22 Total number: 37 Address : Phone : + 33 (0) Director : École Nationale Supérieure de Chimie de Lille Avenue Mendeleïev Bâtiment C7a BP VILLENEUVE D ASCQ CEDEX M. le Professeur Francis ABRAHAM [email protected] Research Fields: Solid State Chemistry Ionic, electronic and mixed conductors Mixed Valence Materials Electrochemical separation of oxygen gas Tetrahedral anion based materials Conductive glasses Precursors and new routes for oxide synthesis Scientific equipment: X-ray powder diffractometers Four circle and CCD X-ray single crystal diffractometers High temperature x-ray diffraction (up to 1600 C) Impedance spectroscopy Ionic transport number measurements Thermogravimetry Differential Scanning Calorimetry, Differential Thermal Analysis Solid State NMR Electron microscopy Key-words : Ceramics Electronic conductivity Ionic conductivity Structure determination Phosphates Magnetic properties Main fields of applications: Gas separation Energy storage and savings Electrochemical membranes Refractory materials and glasses Environment

22 22 LABORATOIRE DE CATALYSE DE LILLE Permanent staff: 55 Total number: 100 Addresses : Phone : + 33 (0) Director : Université des Sciences et Technologies de Lille Bâtiment C3 École Nationale Supérieure de Chimie de Lille Bâtiment C7 Ecole Centrale de Lille Cité Scientifique VILLENEUVE D ASCQ Prof Edmond PAYEN [email protected] Research Fields : Heterogeneous catalysis : synthesis and characterization of catalysts, catalytic tests and kinetic studies, modelization. Hydrotreatment, oxidation, environment, Fischer-Tropsch synthesis. Homogenous catalysis : catalytic reactions using organometallic complexes for organic synthesis, synthesis of enantiomerically pure synthons via asymmetric catalysis, mechanisms and modelisation, biphasis catalysis, carbon monoxide chemistry, polymerization reactions, surface and interface science and analysis by physical methods Chemical engineering : catalytic reactors, fluidized beds, powdered material. Scientific equipment : Surface analysis : XPS, AES, ISS Catalytic tests under atmospheric pressure or under high pressure with analytical systems. Devices for the preparation and analysis of powders Devices for the synthesis and characterization of sensitive organometallic compounds Electrochemical apparatus for the synthesis of unusual complexes Thermogravimetry X-ray diffraction Key words : Hydrocarbon activation and transformation, atmospheric depollution, hydroformylation and CO chemistry, hydrogenation, asymmetric catalysis, chiral ligands, hydrotreatments, oxidation, oxidehydrogenation, biphasic catalysis Main fields of applications: Petrochemistry, Carbochemistry and Fine chemicals Energy production, pollution treatments Synthesis of specialties and Fine Chemicals for the pharmaceutical industry Polymer synthesis

23 23 LABORATOIRE DE CHIMIE ORGANIQUE ET MACROMOLÉCULAIRE Permanent staff : 41 Total : 70 Adress : Phone : + 33 (0) Director : Université des Sciences et Technologies de Lille UFR de Chimie Bâtiment C VILLENEUVE D ASCQ CEDEX Dr. Christian ROLANDO [email protected] Research Fields : Pro and anti oxidant molecules Organic synthesis, reactivity, functionnalization Water soluble polymers with complexing properties Photo and radiochemistry on polymers Studies of photochemical reactions by NMR Singlet Oxygen Free radicals Formulation Polyphenols Scientific equipment : UV, Visible, IR and IRTF spectrophotometers Spectrofluorimetry Phosphorimeter Photoreactive cells Chromatographic devices Potentiostat. Galvanostat Electron beam (175kV) UV sources Dynamometers Goniometry Specific area measurements Treatments of textile EPR NMR Key-words : Alcaloïds Macromolecules Antioxidant molecules Singlet oygen Pro-oxidant complexes - Photochemistry Water soluble polymers Free radicals Main fields of applications : Polymeric materials Pharmaceutical industry Surfactants Cosmetics Paints and varnishes

24 24 LABORATOIRE DE METALLURGIE PHYSIQUE ET GENIE DES MATERIAUX Laboratory associated to the CNRS (National Scientific Research Center) : UMR N 8517 in partnership with EDF Permanent staff : 18 Total number : 30 Adress : Phone : + 33 (0) Director : Université des Sciences et Technologies de Lille Bâtiment C VILLENEUVE D ASCQ CEDEX Prof. Jean-Paul MORNIROLI : [email protected] Research Fields : Thermodynamics of alloys and surface treatments Mechanical properties and environmental effects Mechanical alloying and nanomaterials Behaviour and damage mechanism of metallic alloys Synthesis and mastering of microstructures Electron microscopy Modelling, calculation and simulations Scientific equipment : X Ray diffractometer Transmission and reflection Mössbauer Spectrometer Scanning and transmission electron microscopes Optical microscope and image collection system Dilatometer Electrochemical equipment Micro- et macro-indentation Tensile, fatigue and impact machines Nitriding facilities and galvanisation unit High energy mill, cold roller Heat treatment furnaces Gold and carbon sputtering Keys-words : Mechanical tests and fracture analysis Microscopies -metallography Mössbauer spectroscopy Corrosion Microstructure-galvanisation Main fields of applications : Metallurgy Steel making Energy Transportation industry Battery

25 25 LABORATOIRE DES PROCEDES D ELABORATION DES REVETEMENTS FONCTIONNELS (PERF) Permanent staff : 12 Total staff : 20 Adress : Laboratory is located on the University of Science and Technology of Lille (USTL) campus in Villeneue d Ascq and has sites : At ENSCL, Building C7a, directed by Prof.Rene DELOBEL [email protected] Phone : +33 (0) Fax : +33 (0) Research Fields : Physical and chemical processes of surface treatments Corrosion and interactions between reactive fluids and materials Remote cold plasma phenomena and reactor design Design of microwave couplers Activation of polymer surfaces Plasma enhanced Chemical Vapour Deposition using nitrogen plasma Processes of manufacturing of fire resistant polymers Characterization of polymer degradation products and assessment of their toxicity Scientific equipment : Plasma generators Plasma reactors including high volume reactors Laser : excimer and CO 2 pulsed laser Electron Micro Probe Analysis (EMPA) using Comebax setup Thermal analyses DTA, DSC, TG Spectrometers : UV, visible, IR, IRTF Rheometers for high temperature Electrochemical cells Impedance measurements Texture elaboration of powders; Extruders Key words : Microwave couplers PECVD Plasma spectroscopy Corrosion Fire retardant properties Thermal analyses Films and coatings Toxicity Main fields of application : Metallurgy. Biomaterials Automobile industry Plastics transformation industry Paint.

26 26 C. PROGRAMME OF STUDY FOR THE ENGINEERING CYCLE During the first year (3 rd academic year, semesters S5-S6), you will consolidate your fundamental knowledge and the basic practices of chemistry, physical chemistry, kinetics, thermodynamics, analytical chemistry, as well as inorganic and organic chemistry. The second year (semesters S7-S8) focuses on the applied aspects of chemistry: organic chemistry, polymer chemistry, solid-state chemistry, materials science, and chemical engineering. Practicals, some of which are genuine mini-projects, will allow you to familiarise yourself with a scientific approach and to take initiatives. For semester S8, you will choose a field of study: Molecules or Materials. The third year (semesters S9-S10) offers you three areas of specialisation: - Bioprocesses - Pharmacochemistry - Environment, - Formulation Chemistry, - Materials science/metallurgy It is possible to take your third year abroad (80 partnership universities); or take an option in another school in the FGL; or take a double degree abroad (at one of the 8 partner institutions) or with the IFP School (Graduate School of the French Petroleum Institute). You can also take a research master s degree at the same time as continuing your curriculum, and then follow it up with a doctorate, in particular in one of the 4 research laboratories associated with the ENSCL. A strong emphasis is laid on languages - English, German, in which all the graduates are expected to be fluent, and optional Japanese. The students have the opportunity to spend their third and final year in American, Dutch, German, Irish or British universities, a testimony of the School's international commitment. The school has a full range of modern research equipment. It also benefits from a highly qualified teaching staff and researchers and is thus able to adapt easily to the evolution of sciences and technologies. COURSE OF STUDIES AT ENSCL Science A levels (Bac) International Undergraduate Preparatory Programme of the FGL Preparatory classes Bachelor s 2 year (CPI) By continuous assessment By entry examination By qualification and application Fundamental chemistry Industrial placement (6 weeks) The applications of chemistry Degree holders: Master s 1 Molecules OR Materials Industrial placement with responsibilities (2 3 months) Bioprocesses (Pharmacochemistry, Environment) OR Formulation chemistry OR Optimisation and Reliability of materials OR Option in another FGL Graduat School, in a foreign partner university, Double Degree (IFP School, Germany, UK, USA, Brazil, ) End of studies placement project (6 months) ENGINEERING DEGREE, equivalent to the Master s degree

27 27 ECTS scale of notation French mark ECTS mark Definition >15 A EXCELLENT : outstanding performance with only minor errors B VERY GOOD : above the average standard but with some errors C GOOD : generally sound work with a number of notable errors D SATISFACTORY : fair but with significant shortcomings. 8-6 E FAIL : performance meets the minimum criteria. <6 F FAIL : some more work required before the credit can be awarded. Masters by Research (instruction in French) : See details on : Materials Science : Prof. Patrick Cordier ([email protected]) or [email protected] Organic Chemistry :Prof André Mortreux ([email protected]) Catalyse et Procédés : Prof. Edmond Payen ([email protected]) Formulation Chemistry :Prof.Jean-Marie Aubry ([email protected]) Advanced Master in Drug Design : Prof. Patrick Depreux ([email protected])

28 28 3 rd academic year programme Semester 5 Semester 6 ECTS Code ECTS Code ECTS Credits Fundamental Chemistry Sciences Organic Chemistry 5,0 General Organic Chemistry CH1101 Multi-step organic synthesis CH1201 Inorganic Chemistry 4,0 Solid state Chemistry CH1102 Cristallography CH1102 CH1102 Inorganic Chemistry CH1202 Analytical sciences 8,0 Equilibria in Solution CH1103 Electrochemistry CH1203 Applied Molecular Spectroscopies CH1107 CH1107 General Chemistry 6,0 Thermodynamics CH1106 CH1206 Kinetics CH1205 Practicals Organic Chemistry TP1201 4,0 Inorganic Chemistry TP1202 4,0 Analytical Chemistry TP1103 5,0 Physical Chemistry TP1104 4,0 Industrial Chemical Sciences and Technologies Computer science and applied statistics: CI1101 2,0 Data systems and treatment Qualtity, Health and safety CI1102 3,0 Sustainable developpment Security in Laboratory Professional Risk prevention CI1202 Entrepreneurial Training Economics FE1101 2,0 Sport FE1102 FE1102 1,0 Personal and professional project Seminars, visits of industrial places International Training - Languages French as a Foreign Language LV1105 LV1105 6,0 English LV1101 LV1101 6,0 German LV1102 LV1102 Dutch LV1103 LV1103 Japanese (optional) LV1104 LV1104 FMP Industrial placement FMPO 5,0 TOTAL 65

29 29 4 th academic year programme Semestrer 7 Semester 8 ECTS Code ECTS Code ECTS Credits Fundamental Chemistry Sciences Oganic Chemistry 5,0 Organic compounds of sulfur CH2301 Heterocycles CH2401 Applied spectroscopy CH2307 Polymer chemistry CH2309 3,0 Practicals Organic Chemistry (project) TP2301 4,0 inorganic Chemistry (project) TP2302 4,0 Industrial Chemistry : analatycal methodes security TP2303 3,0 Polymer Chemistry TP2405 2,0 Metallurgy TP2406 2,0 Chemical Engineering TP2407 1,0 Industrial Chemical Sciences and Technologies Functional Polymers CI2409 Formulation Physical Chemistry CI2307 Experimental Design CI2407 Catalysis 3,0 Homogeneous catalysis CI2403 Heterogeneous catalysis CI2303 Organometallic chemistry CI2301 Chemical Engineering 5,0 Unit Operations 1 CI2304 Unit Operations 2 CI2304 Reactors CI2405 Materials Science 5,0 Classes of Materials Mechanical Behaviour of Materials CI2309 Applied Metallurgy CI2408 Glasses-Ceramics CI2310 Analysis of Solids CI2312 Corrosion CI2411 Specializations (Choose 2 units) Option 1 : Bioorganic Chemistry Biomolecules Organometallic Chemistry Homogeneous Catalysis Option 2 : Formulation Chemistry Formulation Chemistry Experimental Design Option 3 : Materials Science Advanced Analysis Techniques Plasticity - Fractures Mechanisms Physical Metallurgy CI2307 STCIB CI2401 CI2301 CI2403 STCIF CI2407 STCIM CI2413 CI2414 CI2415 (2 x 3,0) Entrepreneurial Training Economics FE2401 Management FE2402 Law FE2403 Production Activities FE2304 Industrial Property FE2305 Industrial placement Report and oral examination Personal Professional Project Crédit d'activités Collectives (CAC 50) FECAC FECAC Seminars, visits of factories International Training - Languages French as a Foreign Language LV2305 LV2305 6,0 English LV2301 LV2301 6,0 German LV2302 LV2302 Dutch LV2303 LV2303 Japanese (optional) LV2304 LV2304 Industrial engineering placement FMPT 10,0 TOTAL 70

30 30 5 th academic year programme Semestre 9 Semestre 10 ECTS Code ECTS Code ECTS Credits Pratical Experimental Physico-chemistry of polymers TP Chemical Engineering TP Industrial Chemical Sciences and Technologies Main aera 1 "Bioprocess, Pharmacochemistry, Environment OP Biotechnologies Fundamental Microbiology Industrial Microbiology and Fermentation Bioprocess et Industriel Engineering Drug design ("Pharmaco.2") Water treatment (" Environment2") Transversal project Main aera 2 "Formulation Engineering OP Colloïds, dispersed systems Seminars Transversal project Main aera 3 "Optimization and Reliability of Materials OP Reliability and damage mechanisms of structural materials Composite materials Surface treatment Surface treatment- Advanced lecture Metallic Alloys Study of Techniques in material science Recycling of end-of-life materials CES : a numeric tool in material selection Transversal project Chemical Engineering Physico-chemistry of Polymers5 CI3504 CI3509 Entrepreneurial Training Quality, Health, Safety FE Sustainable developpment Industrial security Transversal project Economics FE3501 Busines Simulation Transversal project Management FE3503 Entrepreneurship Project management Strategy and Marketing Production management Simulation/interviews International Training Foreign Languages French as a foreign language LV3505 LV3505 4,0 English LV3501 LV3501 4,0 German LV3502 LV3502 Dutch LV3503 LV3503 Japanese (or other languages- optional) LV3504 LV3504 Final-year project Industrial engineering placement FMPI 30,0 TOTAL 60

31 31 MODULES DESCRIPTION 3 rd ACADEMIC YEAR Semesters 5 and 6 Module : CH1101 S5 ORGANIC CHEMISTRY COORDINATOR : P. COTELLE SCHEDULE : 16 COURSES HOURS + 14 DIRECTED STUDIES HOURS TEACHERS : Pr P. COTELLE, Courses 8h, directed studies 7h. Dr M. LAGRENEE. Courses 8h, directed studies 7h. PREREQUISITE : Elementary knowledge gained in preparatory classes (CPGE, CPI, DEUG, DUT, BTS, ATS) Paul Arnaud : Courses de chimie organique, Dunod 15 ème édition, 1990, ISBN ASSESSMENT : Control of the pre-requisite qualifications + a single examination LEARNING OUTCOMES : Upgrade the knowledge gained previously Vollhardt, Schore : Traité de chimie organique, 2ème édition, 1995, ISBN DETAILED PROGRAMME : Addition to carbone-carbone multiple bonds Aliphatic substitutions Eliminations Aromatic substitutions Organometallics : synthesis and reactions Carbonyl compounds : keto-enol tautomeric equilibrium, condensations, transpositions. Nitrogen compounds Claisen reaction, Michael addition, Robinson annellation

32 32 Module : CH1102 S5 INORGANIC CHEMISTRY : STRUCTURE AND PROPERTIES OF MATTER COORDINATOR: ROSE-NOËLLE VANNIER SCHEDULE : 16 HOURS TEACHER: MURIELLE RIVENET, LECTURER, COURSES 16 HOURS PREREQUISITES: No prerequisites LEARNING OUTCOMES: This lecture is an introduction to the study of the mineral and inorganic compounds. It aims at bringing the basic concepts which are necessary to approach the materials properties. ASSESSMENT: a written exam an oral exam for those who have chosen this subject BIBLIOGRAPHY: Chimie physique, Paul Arnaud, Ed. Dunod - Chimie générale, Steven S. Zumdahl, Ed. CEC inc. - Introduction à la cristallographie et à la chimie structurale, Maurice Van Meerssche, Janine Feneau-Dupont, Ed. Peeters - Eléments de chimie générale, Michèle Suard, Brigitte Praud, Lionel Praud, Ed. Flammarion Médecine-Sciences - Structure électronique des molécules. 1 De l atome aux molécules simples, Yves Jean, François Volatron, Ed. Dunod - Intermolecular and surface forces, Jacob Israelachvili, Ed. Academic Press - Introduction à la chimie du solide, Lesley Smart, Elaine Moore, Ed. Masson DETAILED PROGRAMME: The first part of the lecture aims to revise some concepts on atoms and cores. A large part is devoted to the radioactivity and its applications, in particular in the medical and energetic fields. The second part aims to give a better understanding of the behavior of the elements and their combinations. In order to fulfil the purpose, various physicochemical parameters (atomic parameters, electronegativity, rays atomic, polarizability, chemical bond...) of the elements are considered. The last part relates to the main structural buildings which are described and analysed in relation to their potential properties.

33 33 Module : CH1102 CRYSTALLOCHEMISTRY S5 COORDINATOR : ROSE-NOËLLE VANNIER TIME SCHEDULE : 24 HOURS: LECTURES LECTURER : ROSE-NOËLLE VANNIER, PROFESSOR PREREQUISITES : NO PREREQUISITE LEARNING OUTCOMES The aim of this lecture is to give the basics in crystallography in the field of materials science. EVALUATION: A WRITTEN EXAM AN ORAL EXAM FOR THOSE WHO HAVE CHOSEN THIS SUBJECT REFERENCES: Eléments de radiocristallographie, R. Ouahes, Ed. Publisud, Analyse structurale et chimique des matériaux, J.P. Eberhart, Dunod, Les rayons X, A. Guinier, Collection "Que sais-je?", Presses universitaires de France, International Tables for Crystallography, Volume A, edited by Theo Hahn, by Kluwer Academic Publishers, Dordrecht/Boston/London (1989). DETAILED PROGRAMME: The aim of this lecture is the description of the main tools of crystallography to learn material science. In a first part, the lattice and symmetry in crystals are explained. Then, the international tables of crystallography are introduced. In a second part, X-ray diffraction and the derived techniques are described.

34 34 Module : CH1103 ANALYTICAL SCIENCES : EQUILIBRIA IN SOLUTION S5 COORDINATOR : E. BORDES SCHEDULE : COURSES 16 HOURS + DS 14 HOURS TEACHERS : ELISABETH BORDES-RICHARD, PROFESSEUR, COURSES 16 HOURS, DS 14 HOURS CAROLINE PIROVANO, MAÎTRE OF CONFERENCES, DS 14 HOURS PREREQUISITE : Bases from CPGE, CPI, DEUG, DUT, BTS, ATS Chemistry of aqueous solutions (acids and bases, precipitation-solubility, complexes) LEARNING OUTCOMES : ASSESSMENT : Examination of prerequisites Written examination Facultative oral examination (choice among several fields) Chimie analytique, Skoog, West, Holler, DeBoeck Univ. Equilibres chimiques en solution, M.O. Delcourt, N. Bois, F. Chouais, DeBoeck Univ. Physico-chimie of solutions, R. Gaboriaud, Masson. Solutions aqueuses and non aqueuses, G. Charlot, Masson DETAILED PROGRAMME: Chap. 1. General considerations: Solutions, non aqueous solvents, comparaison of solvents and phenomena (4 h) Chap. 2. Reactions of proton transfer in proto-active solvent (acids and bases, ph, equilibrium diagrams) (5 h) Chap. 3. Equilibria and reactions of complexation (ligands, quantitative previsions, conditionnal constants, graphical representations) (3 h) Chap. 4. Solid-solution equilibria (solubility products, conditionnal constants, graphical representations) (2 h) Chap. 5. Solvent extraction and exchange of ions (conditionnal constants, graphical representations) (2 h)

35 35 Module : CH1106 THERMODYNAMICS S5 COORDINATOR : SERGUEI GORIATCHEV SCHEDULE : 45 HOURS TEACHERS : Serguei GORIATCHEV, Professeur Charaffeddine JAMA, Maître de Conférences PREREQUISITE : Fluid mechanics. Statistical physics. Thermodynamics. Chemical thermodynamics. LEARNING OUTCOMES : 1. Can to use the main thermodynamic functions and relations in Chemical Engineering and Material Sciences. 2. Know the behaviour, the equations of state and the thermodynamic diagrams of real gases, fluids and solids. 3. Be able to deal with the phase transformations. 4.Know how to calculate a chemical equilibrium state of thermodynamic system. ASSESSMENT : Written exam 1. Perrot P. - Thermodynamique chimique, Problèmes corrigés et commentés avec rappels de Courses, Dunod, Paris, Landau L., Lifchitz E. - Physique statistique, Ellips, Paris, Durupthy A., Mesnil C. et Zobiri T. - Thermodynamique chimique, Courses avec exercices corrigés, Hachette, Brénon-Audat F., Mesnil C. et Durupthy A. - Thermodynamique chimique, Exercices et problèmes corrigés, Hachette, Brébec J.-M. - Thermodynamique, Courses avec exercices corrigés, Hachette, Favier A. - Thermodynamique, Exercices et problèmes corrigés, Hachette, DETAILED PROGRAMME : Courses 1. Statistical thermodynamics. 2. Thermodynamics quantities. 3. Perfect gases and real gases. 4. Phase equilibrium 5. Solutions 6. Chemical reactions Directed studies 1. Thermodynamics principles. 2. Functions of state. 3. Chemical potential. 4. Reaction quantities. 5. Evolution and equilibrium of a system. 6. Variance. 7. Displacement of chemical equilibrium. 8. Binary solid-liquid equilibrium. 9. Binary equilibrium.

36 36 Module : CH1107 COORDINATOR : ERIC BUISINE SCHEDULE : 55 HOURS TEACHERS : MOLECULAR SPECTROSCOPY S5 & S6 ERIC BUISINE, MAÎTRE DE CONFÉRENCES : COURSES, 21 H ALAIN MOISSETTE, MAITRE DE CONFERENCES : DIRECTED STUDIES, 10 H CAROLINE TOKARSKI, MAITRE DE CONFERENCES : COURSES 16H ; DIRECTED STUDIES TD 8 H PREREQUISITE : None LEARNING OUTCOMES : ASSESSMENT : Written 2 hour exam DETAILED PROGRAMME : Molecular spectroscopy provides an important method for probing the structure of molecules. The aim of this module is to develop knowledge and understanding of the main molecular spectroscopy techniques used in analytical chemistry. The principles, applications and limitations of UV/Vis electronic spectroscopy, Infra-Red spectroscopy, Micro-Wave rotational spectroscopy and mass spectrometry will be presented. This module comprises also the study of separation processes by chromatography analysis (gas and liquid). The courses will introduce fundamental aspects while directed studies will be especially devoted to the interpretation and analysis of experimental spectra. Concrete examples will be presented and discussed.

37 37 Module : TP1103 ANALYTICAL CHEMISTRY (Practicals) S5 COORDINATOR : C. PIROVANO SCHEDULE : 85 HOURS TEACHERS : RENE DELOBEL CAROLINE PIROVANO GERARD POUILLARD AURELIE ROLLE PREREQUISITE : Classical methods learnt in preparatory classes LEARNING OUTCOMES : Acquisitions of specific methods of analytical Chemistry ASSESSMENT : Report, preparation test DETAILED PROGRAMME : This teaching aims at acquiring a good scientific rigour, qualities of reasoning, initiative, autonomy, and the conceptual control of the phenomena involved. This Practical Work of Analytical Chemistry begins with a initiation cycle to the classical laboratory techniques Once this preparatory cycle accomplished in small groups, the students begin the analytical Chemistry practicals during which each student works individually at fixed station ; having his own material, he prepares his solutions, titrates and calibrates them. During these practicals, each student must conceive and justify their experimental protocol. The studied titrations are : - acid-base titration - gravimetric titration - complexometric titration - redox titration These practical works must lead to the acquisition of good laboratory practices through the development of care, initiative and rigour.

38 38 Module : TP1104 PHYSICAL CHEMISTRY (Practicals) S5 COORDINATOR : C. PIROVANO SCHEDULE : 70 HOURS TEACHERS : CHARLOTTE BECQUART RENE DELOBEL SERGUEI GORIATCHEV JEAN-PAUL MORNIROLI CAROLINE PIROVANO GERARD POUILLARD LUDOVIC THUINET PREREQUISITE : Methods and bases learnt in preparatory classes Analytical chemistry practical works LEARNING OUTCOMES : Acquisitions of the specific methods of physical Chemistry ASSESSMENT : Report, preparation test DETAILED PROGRAMME : This cycle of practical works, realized in direct relationship to the Courses of general chemistry (analytical chemistry, thermodynamic, spectroscopy, chemical kinetics...) led the students to check concretely the fundamental laws, the theoretical principles and the specific methods of physical chemistry. The students work in group. They are so accustomed to their future task of supervising, the roles of each one evolving between each practical work of simple performer to writer and then to director, which shows them the diversity of the professions they will afterward be confronted with. The use of data processing allows them to acquire the control of these tools and to perform a precise exploitation of the results (traced curves, simulations of experiments, modellings of experimental phenomena). With these methods are thus approached: - electrochemistry (phmetry, potentiometry, conductimetry, polarography...) - chemical kinetics - spectroscopic methods (spectroscopy U.V. and atomic spectroscopy) - thermic analyses

39 39 Module : CI1101 APPLIED STATISTICS S5 COORDINATOR : SERGUEI GORIATCHEV SCHEDULE : 15 HOURS Teachers : Serguei GORIATCHEV, Professor. Courses. PREREQUIS : Probabilities. Discrete and continuous random variables. Distribution and repartition functions. Familiar distributions. Joint random variables. Linear regression. Central limit theorem. LEARNING OUTCOMES : Every measure involves inevitable errors, and above all in an industrial context, it matters to be able to evaluate their importance. In that course, practical indications are given on methods of errors estimation. Assessment : Written exam 1. Dress F. - Probabilités et Statistique, Rappels de cours, Dunod, Paris, Couty F., Debord J. et Fredon D. - Probabilités - Statistique, Résumés de cours et 157 exercices et problèmes corrigés, Dunod, Paris, Renault J.- Formulaire de probabilités et de statistiques, Dunod, Paris, R. Veysseyre, Statistique et probabilités pour l ingénieur, Dunod, Paris (2004). DETAILED PROGRAMME : 1. Probability and statistics. 2. Data description. 3. Point parameter estimation. 4. Parameter estimation by confiidence interval method. 5. Tests of hypotheses. 6. Correlation. 7. Linear regression.

40 40 Module : CI1102 COORDINATOR : ELISABETH BORDES SCHEDULE : 15 HOURS CHEMICAL RISK S5 TEACHERS : ELISABETH BORDES-RICHARD, PROFESSEUR ; Cours, 15 h PREREQUISITES : none LEARNING OUTCOMES : ASSESSMENT : Bibliographical project La sécurité en laboratoire de chimie et de biologie, A. Picot et P. Grenouillet, Editions Tec&Doc, Paris Sécurité des procédés chimiques, A. Laurent, Editions Tec&Doc, Paris Guide d analyse du risque chimique, B. Martel, Dunod, 1999 DETAILED PROGRAMME : Any human action is done with risks which must be controlled if not reduced. Prevention is today a concern in all domains of industry as well as for ecosystems. This course is an initiation into the general methodology of risk prevention and assessment, with an application to chemical risks. Notion of industrial and ecological risk. Methodology of risk analysis and assessment : identification of potential hazards (Preliminary Risk Analysis, HAZOP, etc.), methods of modelisation (failure tree), the human factor. The chemical risk in laboratory : risks linked to chemical products, to processes and operations, notions of toxicology, and other risks.

41 41 Module : FE1101 COORDINATOR : A. GRITLI SCHEDULE : 20 HOURS TEACHERS : A. GRITLI, CONSULTANT ; Cours, 20 h ECONOMICS S5 PREREQUISITE : none ASSESSMENT : SALVATORE Dominick : Microéconomie : cours et problèmes ; série SCHAUM. Groupe Mc- GRAW- HILL, 1998 CLERGEAU Cécile. Microéconomie ; Théorie du marché. Edition, seuil 1999 MALABOU Denis : l essentiel de la microéconomie. GUALINO Editeur 1999 MEDAN Pierre. Microéconomie. Travaux dirigés. DUNOD 2002 DETAILED PROGRAMME : The choice of investment Supply, demand and equilibrium The production theory : the production function and the producer equilibrium The choice of the company and the production costs The firm and the market equilibrium in perfect competition The monopoly market

42 42 LV1105 LECTURER : UNKNOWN YET FRENCH AS A FOREIGN LANGUAGE (FLE) S5 WORKLOAD :3 HOURS A WEEK ECTS CREDITS :6 ASSESSMENT : written and oral exam LEARNING OUTCOMES : Maîtrise efficace de la langue en particulier sur un plan professionnel : comprendre l essentiel d un texte, prendre des notes en cours, donner son avis de façon brève mais claire sur un sujet général ou professionnel. DETAILED PROGRAMME: 3 hours lessons on a weekly basis, completed by an individual self-training under the teacher s supervision, according to the background and the needs of the student.

43 43 Modules : LV1101- LV1102 and LV1103 S5 ENGLISH GERMAN or DUTCH COORDINATOR :P. RIBAUCOUR SCHEDULE : 80 HOURS IN EACH STUDIED LANGUAGE TEACHERS : ANNE GUEGAND, ENGLISH ABDEL BENAÏSSA, ENGLISH CLAUDINE MELY, GERMAN PASCAL RIBAUCOUR, GERMAN PREREQUISITES : LEARNING OUTCOMES : Language tuition at the ENSCL has a double objective : - to give all students adequate communication skills in English and German and eventually the same fluency in both languages. - to encourage prospective engineers to develop an international opening onto foreign firms and uni ASSESSMENT : Continuous language assessment is carried out through at least two written tests and one interview in each language DETAILED PROGRAMME : The students who reach the required level can take the following exams : German : - ZdaF, - Zertifikat Deutsch Für den Beruf - Zentrale Mittelstufenprüfung English : - TOEFL (USA) - Cambridge First, Advanced and Proficency (UK) - TOEIC (USA)

44 44 Module : LV1104 JAPANESE S5 COORDINATOR : JEAN-LUC RIGAL SCHEDULE : 5 MODULES DE 60 HEURES (TD) TEACHERS : AKIKO FUKAGAWA, LV1204 ET LV2304 JEAN-LUC RIGAL, LV1104, LV1204 ET LV2304 KAZUKO SCENNER, LV1104 ET LV1204 KIYONOBU TEDO, LV2404 ET LV3504 PREREQUISITE : none, other than that the desire to learn japanese (written include) ASSESSMENT : oral and written exam continuous assessment Minna no Nihongo, Nihongo Shoho, Nihongo Chûkyû, Nelson Kan ei Jiten, Kana Nyûmon DETAILED PROGRAMME : The main object of this course is to give basic communication tools to the students who intend to do their first, second or/and third year industrial placements in Japan, but also to complete the curriculum of future managers of a branch of industry which has many relations with Japan. One third of the course is devoted to civilization and two thirds to language. Because of the very particular writing system of Japanese, in which two syllabaries and at least 2000 ideograms are combined, reading and writing are given the same importance as oral work. In addition to the learning and systematic use of the two syllabaries, strong emphasis is put on the logic of ideograms, the objective being, through the study of a few hundreds of them, to facilitate the subsequent assimilation of those - much more numerous - which are necessary to everyday life. The course is divided into 5 levels, and not according to the three years of the curriculum. As a matter of fact, if Level I is mainly attended by first year students, Level II by second year students and Level III by third year students, some students start the study of Japanese in their second/third year, whereas other students - especially those who come from the "CPI" - may have been studying Japanese for two years or more when they start their engineering studies.

45 45 3 rd ACADEMIC YEAR CYCLE INGÉNIEUR Semester S6 Module CH1201 S6 COORDINATOR : P. GRANDCLAUDON SCHEDULE : 45 HOURS TEACHERS : MULTI STEP ORGANIC CHEMISTRY Pierre GRANDCLAUDON, Professeur; Courses : 20hours ; directed studies: 20 hours Adina RYCKEBUSCH, Maître de Conférences; Courses : 5 hours PREREQUISITE : Elementary knowledge gained in preparatory classes (CPGE, CPI, DEUG, DUT, BTS, ATS) Organic chemistry semester 1 LEARNING OUTCOMES : ASSESSMENT : Single written exam Oral exam on students choices DETAILED PROGRAMME : Orientation : multi-step strategy in organic synthesis Applications in directed studies: strategy in organic synthesis - synthesis and use of polyfunctional molecules - protecting and activating groups

46 46 Module : CH1202 S6 INORGANIC CHEMISTRY : INORGANIC AND INDUSTRIAL CHEMISTRY COORDINATOR : ROSE-NOËLLE VANNIER SCHEDULE : 20 HOURS TEACHERS : ROSE-NOËLLE VANNIER, PROFESSOR, COURSES 20 HOURS PREREQUISITES : No prerequisite LEARNING OUTCOMES : The aim of this lecture is the description of the preparation and use of the main inorganic compounds. ASSESSMENT: a written exam an oral exam for those who have chosen this subject Techniques de l'ingénieur, Actualité chimique, Cours de chimie minérale, Maurice Bernard, Ed. Dunod, Chimie industrielle, Robert Perrin, Jean-Pierre Scharff, ed. Masson DETAILED PROGRAMME: The first chapter is devoted to hydrogen and its combinations, oxides are described in a second part and halogens and their combinations in a third. Applications such as batteries and fuel cells are described. The preparations of common compounds like ammonia, chlorine, soda,. are also detailed.

47 47 Module : CH1203 ANALYTICAL SCIENCES : ELECTROCHEMISTRY S6 COORDINATOR : E. BORDES SCHEDULE : COURSES 16 HOURS + DS 14 HOURS TEACHERS : ELISABETH BORDES-RICHARD, PROFESSOR, COURSES 16 HOURS, DS 14 HOURS SERGE BOURBIGOT, PROFESSOR, DS 14 HOURS PREREQUISITES : Bases from CPGE, CPI, DEUG, DUT, BTS, ATS Redox phenomena in aqueous solutions (Nernst equation, redox equilibria) Module CH1103 LEARNING OUTCOMES : Assessment : Written examination Facultative oral examination (choice among several fields) Chimie analytique, Skoog, West, Holler, DeBoeck Univ. Equilibres chimiques en solution, M.O. Delcourt, N. Bois, F. Chouais, DeBoeck Univ. Equilibres chimiques en solution, M.O. Delcourt, N. Bois, F. Chouais, DeBoeck Univ. Of l oxydoreduction à l electrochimie, Y. Verchier, F. Lemaître, Ellipses 2006 Electrochimie ; of concepts aux applications, F. Miomandre, S. Sadki, P. Audebert, R. Meallet-Renault, Dunod, Paris 2005 DETAILED PROGRAMME: Chap. 1. Redox reactions (5 h) - qualitative and quantitative previsions (electrochemical fonctions) - conditional potentials (acidity, complexation, precipitation) - potential-ph diagrams, potential-px, etc. Chap. 2. Piles and electrolysers (4 h) - principles, - electrodes (types of, indicators, membrane) - types of pile and electrolyser, - piles of concentration without and with transport, flux diagrams Chap. 3. Electrochemical kinetics (voltamperometry) (7 h) - Fast reactions, intensity-potential curves and formulae - Slow reactions, intensity-potential curves and formulae - applications (corrosion etc.)

48 48 Module : CH1205 COORDINATOR : JEAN GRIMBLOT SCHEDULE : 20 HOURS IN SELFTRAINING TEACHER : KINETICS S6 Anne-Sophie MAMEDE, Maître de Conférences, Courses : 20 hours PREREQUISITE : Mathématics : integration of differential equations Basic knowledge in physical chemistry ASSESSMENT : 1 or 2 written exam with course packets 1 oral exam (depending on results) LEARNING OUTCOMES : DETAILED PROGRAMME : The objective of the course is to give the students the basic knowledge about different aspects of chemical kinetics. In a first step, they should be able to identify and use all the parameters which may take part in the equations relative to the rate of the chemical transformations. Different reaction mechanisms are also explored as well as some basic elements about rate theories. A large part of the course deals with the kinetic laws on chemical processes performed in a homogeneous medium (successive, parallel, chain reactions, etc.). Another chapter is relevant to kinetic aspects of reactions conducted in liquid phase. Influences of chemical diffusion, dielectric permittivity of the solvent or ionic strength of the solution are examined. Homogeneous catalytic reactions, namely acid-base catalysis, are also studied. The last chapter deals with some kinetic aspects of heterogeneous catalysis. Molecular adsorption, desorption from a surface and the Langmuir isotherm are explained, as well as the BET isotherm for physisorption. Several mechanisms of heterogeneous catalysis are reviewed with emphasis on the Langmuir-Hinshelwood and Eley-Rideal models.

49 49 Module : CH1206 Applied Thermodynamics S6 COORDINATOR : SERGUEI GORIATCHEV SCHEDULE : 11 HOURS TEACHERS : Charlotte BECQUART, Professor. Courses. Serguei GORIATCHEV, Professor. Courses. PREREQUISITE : Thermodynamics (S5) LEARNING OUTCOMES : Use of Ellingham diagramm Knowledge of how a blast furnace operates Knowledge of the processing of Al ASSESSMENT : Written exam 1. J. Barralis & G. Maeder, Métallurgie, Tome 2: alliages ferreux, ENSAM (1983), Editions communications actives, ISBN J. Philibert, A. Vignes, Y. Bréchet & P. Combrade, Métallurgie : du minerai au matériau, DUNOD, Paris 2002, ISBN G. Béranger, G. Henry & G. Sanz, Le livre de l acier, techniques & documentation- Lavoisier,1994, ISBN P. Perrot, Dictionnaire de thermodynamique, 1994, InterEditions, Paris DETAILED PROGRAMME : 1. Thermodynamic data. 2. Processing methods of metals and alloys. 3. Which method should one use? 4. Steel processing 5. Al processing

50 50 Module : CH1206 COORDINATOR : S. GORIATCHEV Applied Thermodynamics S6 SCHEDULE: 11 HEURES (11HEURS DE COURS) TEACHERS : CHARLOTTE BECQUART, Professeur, Cours. SERGUEI GORIATCHEV, Professeur, Cours. PREREQUISITE : Thermodynamique (S5) OBJECTIFS DE FORMATION : Savoir utiliser un diagramme d Ellingham. Connaître le fonctionnement d un haut fourneau Connaître les bases de la fabrication de l aluminum Examen écrit BIBLIOGRAPHIE : 1/ J. Barralis & G. Maeder, Métallurgie, Tome 2: alliages ferreux, ENSAM (1983), Editions communications actives, ISBN / J. Philibert, A. Vignes, Y. Bréchet & P. Combrade, Métallurgie : du minerai au matériau, DUNOD, Paris 2002, ISBN / G. Béranger, G. Henry & G. Sanz, Le livre de l acier, techniques & documentation- Lavoisier,1994, ISBN / P. Perrot, Dictionnaire de thermodynamique, 1994, InterEditions, Paris DETAILED PROGRAMME : 1. Les données thermodynamique 2. Les procédés industriels d élaboration des métaux et alliages. 3. Quelle famille de transformations utiliser? 4. Elaboration de l acier. 5. Elaboration de Al.

51 51 Module : TP1201 COORDINATOR : M. LAGRÉNÉE SCHEDULE : 65 HOURS TEACHERS : Sophie Duquesne, MdC. Gaëlle Fontaine, MdC. Michel Lagrenée, MdC. ORGANIC CHEMISTRY (practicals) S6 PREREQUISITE : Elementary knowledge gained in preparatory classes (CPGE, CPI, DEUG, DUT, BTS, ATS) ASSESSMENT Continuous assessment (one mark per practicals), 4 prepatory praticals + 7 synthesis practicals DETAILED PROGRAMME : Preparatory practicals : - Distillation and analysis techniques (gas phase chromatography, IRTF) - Cristillation, Determination of the fusion point - Chromatography ( CCM, Column, HPLC) - Extraction techniques (en continuous, soxhlet) Synthesis

52 52 Module : TP1202 INORGANIC CHEMISTRY : PRACTICAL S6 COORDINATORS : MURIELLE RIVENET / NATHALIE TANCRET SCHEDULE : 60 HOURS TEACHERS : MARIE COLMONT, LECTURER CATHERINE RENARD, LECTURER MURIELLE RIVENET, LECTURER NATHALIE TANCRET, LECTURER TECHNICAL STAFF : CATHERINE CANDELIER PREREQUISITES : Designation and use of vessel Basic knowledge of analytical and physical chemistry LEARNING OUTCOMES : The practical aims to synthesise numerous inorganic compounds using a large number of synthesis methods solid-solid, hydrothermal, sol-gel and to characterise them. ASSESSMENT : Assessment is based both on the students behaviour during practical and on practical reports. DETAILED PROGRAMME : Numerous inorganic compounds are synthesised using various synthesis methods solidsolid, hydrothermal, sol-gel. A special emphasise is devoted to the synthesis of some basic compounds of the inorganic industry (synthesis of sodium carbonate using Solvay process, synthesis of soda and chlorine by means of electrolysis)... The obtained compounds are characterised by means of analytical chemistry and by means of physico-chemical methods as X-ray diffraction, thermal analyses, atomic absorption spectroscopy...

53 53 Module : CI1202 PROFESSIONNEL RISKS PREVENTION (project) S6 COORDINATOR : ELISABETH BORDES SCHEDULE : 15 HEURES TEACHERS : ELISABETH BORDES-RICHARD, PROFESSEUR ; Projet 15 h PREREQUISITES : none ASSESSMENT : Written bibliographic report LEARNING OUTCOMES : La sécurité en laboratoire de chimie et de biologie, A. Picot et P. Grenouillet, Editions Tec&Doc, Paris Sécurité des procédés chimiques, A. Laurent, Editions Tec&Doc, Paris Guide d analyse du risque chimique, B. Martel, Dunod, 1999 DETAILED PROGRAMME : Any human action is done with risks which must be controlled if not reduced. Prevention is today a concern in all domains of industry as well as for ecosystems. This course is an initiation into the general methodology of risk prevention and assessment, with an application to chemical risks. Notion of industrial and ecological risk. Methodology of risk analysis and assessment : identification of potential hazards (Preliminary Risk Analysis, HAZOP, etc.), methods of modelisation (failure tree), the human factor. The chemical risk in laboratory : risks linked to chemical products, to processes and operations, notions of toxicology.

55 55 Modules : LV1201- LV1202 LV1103 S6 ENGLISH GERMAN or DUTCH COORDINATOR : SCHEDULE : 80 ENGLISH HOURS AND 80 GERMAN HOURS TEACHERS : ANNE GUEGAND, ENGLISH MARTINE HERRIQUET, ENGLISH CLAUDINE MELY, GERMAN PASCAL RIBAUCOUR, GERMAN PREREQUISITE : ASSESSMENT : DETAILED PROGRAMME : Language tuition at the ENSCL has a double objective : - to give all students adequate communication skills in English and German and eventually the same fluency in both languages. - to encourage prospective engineers to develop an international opening onto foreign firms and universities. Continuous language assessment is carried out through at least two written tests and one interview in each language. The students who reach the required level can take the following exams : German : ZDaF English : TOEFL (USA) Cambridge First, Advanced and Proficency (UK) TOEIC (USA)

57 57 4 th academic year Semester S7 Module CH2301 S7 COORDINATOR : PIERRE GRANDCLAUDON ORGANIC CHEMISTRY SCHEDULE : 30 HOURS TEACHERS : Pierre GRANDCLAUDON, Professeur; Courses et directed studies chimie organique (C: 14h; directed studies: 14h) Adina RYCKEBUSCH, Maître de Conférences; Courses biomolécules (C: 2h). PREREQUISITE : Elementary knowledge gained in preparatory classes (CPGE, CPI, DEUG, DUT, BTS, ATS) Organic chemistry : semesters 1 & 2, CH1101 and CH1201 ASSESSMENT: Single written exam Rabasso, N.: Chimie organique; hétéroéléments, stratégies de synthèse et chimie organomerallique; De Boeck, DETAILED PROGRAMME : Orientation: la stratégie en synthèse organique multi-étapes (2) Mise en évidence des propriétés particulières liées à l'atome S et de l'intérêt des dérivés organiques contenant S en tant qu'auxiliaires en synthèse. Applications développées au cours des TD. Fonctions organiques contenant un ou des atomes de S (préparation, propriétés, applications): Thiols Sulfures - Disulfures Sulfoxydes Sulfones Acides sulféniques et sulfiniques Composés intégrant le groupement thione (thiones, thionesters, thionamides, composés dérivant de CS 2 ) Au cours de ce programme les propriétés originales liées aux hétéroatomes de la troisième période de la classification périodique (Si, P, S) seront développées et permettront d'aborder l'aménagement fonctionnel en synthèse (Umpolung...).

58 58 Module : CH2307 COORDINATOR : ERIC BUISINE SCHEDULE : 28 HOURS TEACHERS : MOLECULAR SPECTROSCOPY S7 ERIC BUISINE, MAITRE DE CONFERENCES : COURSES, 20 H ; DIRECTED STUDIES, 8H. PREREQUISITE : None LEARNING OUTCOMES : ASSESSMENT : Written 2 hour exam DETAILED PROGRAMME : The aim of this module is to teach students how to use Nuclear Magnetic Resonance (NMR) spectroscopy for solving structural problems in organic chemistry. The module is specifically devoted to the study of 1D-NMR spectroscopy applied to 1 H and 13 C nuclei in solution. The course will introduce the fundamental and practical aspects of Fourier Transform NMR techniques. The directed studies will consist in the interpretation of experimental 1 H and 13 C NMR spectra of small organic molecules.

59 59 Module : CH2309 COORDINATOR : Patrice Woisel POLYMER CHEMISTRY S7 SCHEDULE : 28 Courses hours, 12 Directed Studies hours TEACHERS : Patrice Woisel, Professor, Courses 10 hours Frédéric Cazaux, Maître de Conférences, Directed Studies 12 hours PREREQUISITE : General organic chemistry Kinetics and chemical thermodynamics LEARNING OUTCOMES : The student should obtain a broad theoretical knowledge about structure and properties of poly about the methods and techniques that are used in polymer chemistry. ASSESSMENT : Written exam - La polymérisation : Principes et applications George ODIAN Polytechnica, 1994 ISBN Chimie et physico-chimie des polymères Michel FONTANILLE, Yves GNANOU Dunod, 2002 ISBN Polymers : Chemistry & Physics of Modern Materials, 2 nd edition J. M. G. COWIE Blackie Academic & Professional - Chapman & Hall, 1997 ISBN X - Exercices et problèmes de chimie macromoléculaire Thierry HAMAIDE, Michel BARTHOLIN Editions TEC & DOC, 1999 ISBN

60 60 DETAILED PROGRAMME : Course: The purpose of this course is to introduce the basic concepts and leading features of polymer synthesis and structure at a molecular level. Introduction to polymer chemistry: historical and economic backgrounds Polyadditions: free radical, anionic and cationic polymerizations-mechanisms, kinetics, thermodynamics, stereoregularity, average molecular weights and distribution. Living polymerization. Free radical copolymerization: kinetics, reactivity ratios, Q-e scheme. Step-growth polymerizations: linear polycondensation Cross-linking and gelation of tridimensional polycondensates Industrial polymerization processes Directed Studies: The aim of this teaching is to illustrate and to complete main aspects tackled in course: Generalities : polydispersity, polymerization stereochemistry, efficacity factor Radicalar polymerization Radicalar copolymerization three dimensional and linear polycondensation Industrial polymerization processes (mass, solution, suspension, emulsion) Cationic polymerization Anionic polymerization

61 61 Module TP2301 COORDINATOR : M. LAGRÉNÉE ORGANIC CHEMISTRY (project) S7 SCHEDULE : 25 HOURS OF BIBLIOGRAPHICAL SEARCH, 40 HOURS OF PRACTICAL TEACHERS : Philippe Cotelle, Pr. Gaëlle Fontaine, MdC. Michel Lagrenée, MdC. Adina Ryckebusch, MdC. PREREQUISITE : 1 st year practicals (TP1201), 1 st year organic chemistry courses (CH1101 et CH1201), Spectroscopy courses (CH1107 et CH2307). ASSESSMENT : Bibliographical report, pratical report, oral exam,continuous assessment

62 62 Module : TP2302 INORGANIC CHEMISTRY : RESEARCH PROJECTS S7 COORDINATORS : MURIELLE RIVENET / NATHALIE TANCRET SCHEDULE : HOURS (BIBLIOGRAPHIC SEARCHING + PRACTICAL) TEACHERS : LECH PAWLOWSKI, PROFESSOR CATHERINE RENARD, LECTURER MURIELLE RIVENET, LECTURER NATHALIE TANCRET, LECTURER TECHNICAL STAFF : CATHERINE CANDELIER MAXENCE VANDEWALLE PREREQUISITE : How to deal with a bibliographic searching How to write a scientific report The characterisation methods used in solid-state chemistry LEARNING OUTCOMES : The research projects aim to improve the students self-sufficiency in preparing, choosing, organising and realising their experiments. ASSESSMENT : Assessment is based on the scientific reports (bibliographical + practical), oral presentation and investment in the research project. DETAILED PROGRAMME : The first step of the projects is a bibliographic searching. The students are helped in this task by frequent discussions with the teachers so as to determine the best ways of synthesis and characterisation. The students are encouraged to use the characterisation methods available at the ENSCL and to widen their field of investigation with the characterisation methods available within the research laboratories of the USTL. Finally, the experiments must be carried within one week (40 hours). The subjects of the research projects are renewed every year so as to match the course of "ceramics and glasses" and to show an industrial and/or a fundamental interest.

63 63 Module : TP2303 INDUSTRIAL CHEMISTRY (PRACTICALS) : ANALYTICAL METHODS AND SECURITY S7 COORDINATOR : ERIC BUISINE SCHEDULE : 45 HOURS TEACHERS : SERGE BOURBIGOT, PROFESSEUR MARIE COLMONT, MAITRE DE CONFERENCES ERIC BUISINE, MAITRE DE CONFERENCES CAROLINE TOKARSKI, MAITRE DE CONFERENCES PRÉREQUISITE : None LEARNING OUTCOMES : ASSESSMENT : Participation during the practical and result reports Techniques de l'ingénieur DETAILED PROGRAMME : The aim of these practicals is the presentation of analytical techniques frequently used in industry : calorimetry, mass spectroscopy, chromatography gas and liquid (HPLC), X-ray diffraction, X-ray fluorescence analysis, NMR. Quantitative, qualitative aspects and limits of each technique are underlined. With these practicals, students have also the opportunity to be sensitized to security problems and the means deployed in industry: study of the thermal stability of chemical reactions, resistance to fire and to heat of materials

64 64 Module : CI2301 ORGANOMETALLIC CHEMISTRY S7 & S8 COORDINATOR : LYDIE PELINSKI SCHEDULE : 20 HEURES TEACHERS : Lydie PELINSKI, Professeur ; cours 20 heures. PREREQUISITE : ASSESSMENT : DETAILED PROGRAMME : Introduction and preparations Organometallics protecting and stabilising Organometallics as electrophiles Organometallics as nucleophiles Coupling and cyclisation Organometallics in biochemistry and biology

65 65 Module : CI2303 COORDINATOR : E. BORDES SCHEDULE : COURSES 20 HOURS TEACHERS : HETEROGENEOUS CATALYSIS S7 ELISABETH BORDES-RICHARD, PROFESSEUR, COURSES 16 HOURS, DS 14 HOURS PREREQUISITE : Inorganic and organic chemistry, physical chemistry LEARNING OUTCOMES : ASSESSMENT : Written examination Cinetique and catalyse, G. Scacchi, M. Bouchy, J.F. Foucaut, O. Zahraa, TecDoc Lavoisier, 1996 Chimie of surfaces and catalyse, G.A. Somorjai, M.P. Delplancke, Ediscience, DETAILED PROGRAMME: A catalyst is necessary in 90 % of chemical processes, for at least one reaction step. Heterogeneous catalysis is a pluridisciplinary field in which several types of chemistry (organic, inorganic, physical, etc.) as well as chemical engineering, are involved. Thanks to the solid catalyst, gas and/or liquid phase reactions are faster (activity), energetically cheaper and «cleaner» (economy of atoms, selectivity). The structural properties being prominent, the preparation and the main physicochemical properties of solid inorganic catalysts, as well as their uses in large industrial processes (refining and petrochemistry) andin pollution abatement are studied. Typical properties of catalysts (adsorption, surface reactivity), preparation and shaping, reactors. Physicochemical properties and applications of the three types of catalysts (6h) : 1) Acid-base catalysts (refining, catalytic cracking, alkylation, etc) (4h) 2) Metallic catalysts and bifonctional catalysts (hydrogenation, reforming, pollution abatement, etc.) (5h) 3) Oxidic catalysts (mild and total oxidations, hydrodesulfuration, polymerisations) (4h)

66 66 Module : CI2304 CHEMICAL ENGINEERING UNIT OPERATIONS 1 S7 COORDINATOR : NOURIA FATAH SCHEDULE : 60 HOURS TEACHERS : ANDRÉ ACLOQUE, VACATAIRE ; Courses, 60h PREREQUISITE : Unit operations : Elementary knowledge gained in preparatory classes (CPGE, CPI, DEUG, DUT, BTS, ATS) LEARNING OUTCOMES : ASSESSMENT : Unit operations : two hours exam with documentation in january General book on chemical engineering : P. Wuithier : Raffinage et Génie Chimique, ed. Technip Perry : Chemical Engineers Handbook, Mc Graw Hill Mc Cabe & Smith : Unit Operations of Chemical Engineering, Mc Graw Hill Detailed programme : UNIT OPERATIONS Fluid mechanics : Fluid statics. Ideal and real fluid dynamics. Basic relations. Viscosity, pressure drop (on line and miscellaneous). Piping design and specifications. Fluid pumping, centrifugal pump specification. Heat transfer : General. Heat transmission by radiation, conduction. Different types of heat exchangers. General relations for heat transfer coefficients. Design of shell and tube exchangers. Special study of evaporators, reaction vessels - steady and unsteady operation. Mass transfer and unit operations : Distillation, adsorption liquid-liquid extraction. Humidification and drying. Fluid and particle systems : gas-solid - flow conditions, separations : liquid-solid, centrifugation, filtration. Special care is taken to point out industrial applications and economic impact. Specific courses devoted to chemical companies and industrial project management, technical documents for plant erection or technology transfer, safety and environment.

67 67 Module : CI2307 FORMULATION CHEMISTRY S7 COORDINATOR : JEAN-MARIE AUBRY SCHEDULE : 25 HEURES TEACHERS : Jean-Marie AUBRY, Professeur, cours 25 heures PREREQUISITE : ASSESSMENT : DETAILED PROGRAMME : This course aims to give students the main concepts necessary to understand, to design and to characterise formulated compounds. These concepts are illustrated through examples taken from various industrial fields, detergency, hard surface treatment and human care products. 1) Interactions of a liquid with another phase - Miscibility, solubilization (solvent choice), solubility parameters (degreasing) - Surface tension, wetting (contact angle, hydrophobation, rolling-up) 2) Surfactants in aqueous solution - Adsorption to interfaces (Gibb's equation, cmc, HLB) - Auto-aggregation (micelles, temperature effect, phase diagrams) 3) Surfactants in dispersed systems - Microemulsions, emulsions, foams

68 68 Module: CI2309 MECHANICAL PROPERTIES OF MATERIALS S7 COORDINATOR : JEAN-BERNARD VOGT SCHEDULE : 15 HOURS TEACHER: Jean-Bernard VOGT, Professor PREREQUISITES o Mathematics and physics Learning outcomes : EXAMINATION one written examination at semester end Des matériaux, J.-P. Baïlon et J.-M. Dorlot, Presses Internationales Polytechnique, (2000) Science et génie des matériaux, W.D. Callister, Modulo Editeur (2000) Engineering materials, an introduction to their properties and applications, M.A. Ashby and D.R.H. Jones, materials Science and technology, Vol.34, Pergamon press (1982) Mechanical behaviour of materials, T.H. Courtney, Mc Graw Hill Publishing Company (1990) PROGRAMME : The purpose of this course is to introduce students to the various methods for the evaluation of the mechanical behaviour of solid materials. The first part of the course deals with the notions of stress and strain and their relationship: elastic behaviour (Hooke's law), plastic and inelastic behaviour. The mechanical behaviour is discussed according to the class of materials. The second part gives a description of the different tests aiming at the characterization of the mechanical strength and of the characterization of the damage resistance. This lecture can be complemented by the lecture Plasticity-Fracture given during semester 4 A Mechanical behaviour of solids 1. Definition of stress and strain 2. The relation between stress and strain Elasticity Plasticity Anelasticity 3. Solicitation modes: Uniaxial loading Shear Torsion Bending B Mechanical test 1. Characterisation of the mechanical response hardness test monotonic tensile test Creep test 2. Characterisation of damage résistance Impact test Toughness test Fatigue test Friction and wear

69 69 Module : CI2310 COORDINATOR : JEAN-BERNARD VOGT TIME SCHEDULE : 20 HOURS Glasses - Ceramics S7 Lecturer : NATHALIE TANCRET, ASSOCIATE PROFESSOR PREREQUISITES Inorganic chemistry Physical chemistry Cristallography EVALUATION final examination LEARNING OUTCOMES : REFERENCES : Solid State Chemistry : An Introduction, seconde édition, Lesley SMART et Eliane MOORE, publié par Chapman et Hall (UK ). Chimie Industrielle, Robert PERRIN et Jean-Pierre SCHARFF, 2ème édition, Masson (Paris ). Matériaux 2 : Microstructure et Mise en Oeuvre, Michael ASHBY et David Rayner Hunkin JONES, traduit de l'anglais par Yves BRECHET, Joël COURBON et Michel DUPREUX, Editions Dunod (Paris ). DETAILED PROGRAMME : The aim of this course is to present to students the great families of ceramics (and glasses) and their functions. From the divided solid to the melted solid, we will define what is a cement, a zeolithe, a ceramic, a glass, as well as their synthesis methods, their physical properties and their uses. We will begin by the definition of each type of materials by a chemical point of view (composition, structure). The following part will be dedicated to the different methods of elaboration which directly influence the nature of the material and, consequently, its physical properties. We will see the methods of synthesis the more currently used in industry (ceramic, micro-wave, sol-gel process, ) and the importance of techniques allowing energy savings. Another chapter will be dedicated to properties of materials and, particularly, the dielectric and magnetic properties. This will allow to see the basis of ferromagnetism, paramagnetism, ferroelectric effect, as well as superconductivity. Finally, a particular attention will be given to uses of materials on the level of industry and in the daily life of everyone. Even if all aspects will not be considered in this lesson, the more important points will be developed to give to the students good basis concerning solid state matter. This knowledge will be able to be thorough during the third school year in the specific option or by preparing a Master.

70 70 Module : CI2312 ANALYSES OF SOLIDS S7 COORDINATOR: JEAN-BERNARD VOGT TIME SCHEDULE: 15 HOURS: lectures Lecturers : ROSE-NOËLLE VANNIER (10 hours), Professor, MARIE COLMONT (5 hours), Lecturer PREREQUISITE : Lectures of cristallochemistry S6 EVALUATION written exam LEARNING OUTCOMES : REFERENCES: Techniques de l'ingénieur, Analyse structurale et chimique des matériaux, J.P. Eberhart, Dunod, Analyses chimiques, Francis Rouessac et Annick Rouessac, Dunod, DETAILED PROGRAMME: In this lecture techniques like X-ray fluorescence, SEM, TEM, EDS are described in a first step. Quantitative analysis using X-ray diffraction is detailed in a second step. The way to derive micro-strains and crystallite size is also described.

71 71 Module : CI2403 HOMOGENEOUS CATALYSIS S7 & S8 COORDINATOR : ANDRÉ MORTREUX SCHEDULE : 20 HEURES TEACHERS : ANDRE MORTREUX, PROFESSEUR ; Cours, 20h PREREQUISITE : Organic chemistry M1 1 st year Organic chemistry ASSESSMENT : Written exam JM Brégeault : Catalyse Homogène par Complexes de métaux de transition, Masson, 1992 Didier Astruc :Chimie Organométallique EDP Sciences, 2000 DETAILED PROGRAMME : Fundamental principles of organometallic chemistry directed towards homogeneous catalysis by transition metal complexes. * The catalytic cycle : principles of catalytic species generation and determination of fundamental pathways. * Selected examples of homogeneously catalyzed reactions : hydrogeneration - asymmetric synthesis, hydroformulation - carbonylation reactions, olefin oligomerization and polymerization oxidation reactions All these reactions are illustrated by typical industrial processes using homogeous catalysis

72 72 Module : FE2304 COORDINATOR: LECH PAWLOWSKI PRODUCTION ACTIVITIES S7 SCHEDULE : 10 HEURES TEACHERS: LECH PAWLOWSKI, PROFESSEUR ; Courses, 10 h PREREQUISITE : Elementary knowledge in organic chemistry and inorganic chemistry General knowledge in industrial chemistry ASSESSMENT : Exam without documents and calculator R. Perrin, J.P. Scharff, Chime industrielle, Dunod, Paris,1999. L. Pawlowski, Dépôts Physiques, PPUR, Lausanne, Suisse, Articles consacrés à l actualité de la chimie industrielle dans de journaux professionnels et quotidiens (Galvano-Organo, Der Spiegel-Wirtschaft Seiten, Figaro-pages jaunes, ) Articles scientifiques de : International Journal of Hydrogen Energy, Chemical Engineering Journal, Journal of Physics D : Applied Physics, Surface and Coatings Technology DETAILED PROGRAMME : 1. Actual industrial chemistry Growth sectors Fields of industrial chemistry Raw materials and energy 2. Oil Refining Raw oil Distillation of raw oil Cracking et reforming 3. Petrochemistry Olefins and di-olefins Preparation of organic compounds with C4 carbon content Preparation of aromatic hydrocarbons 4. Alumina: preparation of material and product thereof Raw materials Technical alumina Plasma spraying of alumina 5. Titnia: preparation of material and products thereof Raw materials Classical processes: "using sulphates" and "using chlore" Processes in development: using low pressure and thermal plasmas

74 74 Modules : LV2301-LV2302-LV2303 ENGLISH GERMAN or DUTCH COORDINATOR : S7 SCHEDULE : 80 ENGLISH HOURS AND 80 GERMAN HOURS TEACHERS : ANNE GUEGAND, ENGLISH MARTINE HERRIQUET, ENGLISH CLAUDINE MELY, GERMAN PASCAL RIBAUCOUR, GERMAN PREREQUISITE : ASSESSMENT : DETAILED PROGRAMME : Language tuition at the ENSCL has a double objective : - to give all students adequate communication skills in English and German and eventually the same fluency in both languages. - to encourage prospective engineers to develop an international opening onto foreign firms and universities. Continuous language assessment is carried out through at least two written tests and one interview in each language. The students who reach the required level can take the following exams : German : ZDaF English : TOEFL (USA) Cambridge First, Advanced and Proficency (UK) TOEIC (USA)

76 76 4 th academic year Semester S8 Module : Module CH2401 S8 CHIMIE ORGANIQUE : HÉTÉROCYCLES COORDINATOR : P. GRANDCLAUDON SCHEDULE : 17 HEURES TEACHERS : Pierre GRANDCLAUDON, Professeur; C: 10 H, TD: 7 H. PREREQUISITE : Bases acquises en années préparatoires (CPGE, CPI, DEUG, DUT, BTS, ATS) Chimie organique: semestres S5, S6 & S7, CH1101, CH1201 & CH2301 ASSESSMENT : Examen unique, écrit. David T. Davies: Chimie des Heterocycles Aromatiques, Oxford Chemistry Primers Les essentiels en Chimie, 1997 (1992 pour la version anglaise), De Boeck Université. DETAILED PROGRAMME : Orientation: la stratégie en synthèse organique multi-étapes (3) Particularités liées à la construction et à la réactivité des composés hétérocycliques aromatiques. Exemples d'applications en TD. Hétérocycles aromatiques π déficitaires ou électrophiles: Azines (Pyridines, Quinoléines, Isoquinoléines) et polyazines. Hétérocycles aromatiques π excédentaires ou nucléophiles: Azoles (Pyrroles, Indoles) Diazoles Thiophènes et Furanes.

77 77 Module : TP2405 COORDINATOR : Frédéric CAZAUX SCHEDULE : 25 hours TEACHERS : POLYMER CHEMISTRY S8 Frédéric CAZAUX, Maître de conférences, Practicals 25 hours PREREQUISITE : Modules CH2309 et CI2409 LEARNING OUTCOMES : To put into practice knowledge acquired in courses and directed studies upon various synthesis me as molecular weights determination and kinetics parameters during a polymerization reaction ASSESSMENT : 5 practical reports - La polymérisation : Principes et applications George ODIAN Polytechnica, 1994 ISBN Chimie et physico-chimie des polymères Michel FONTANILLE, Yves GNANOU Dunod, 2002 ISBN Exercices et problèmes de chimie macromoléculaire Thierry HAMAIDE, Michel BARTHOLIN Editions TEC & DOC, 1999 ISBN DETAILED PROGRAMME : - Synthesis of a styrene / methyl methacrylate copolymer - Production of a plate of poly(methyl methacrylate) by a thermal or a photochemical process - Synthesis of a polyamide-6,6, a polyurethane, and a phenolic thermoset - Curing of a stratified composite material - Suspension and emulsion polymerization of styrene - Mass distribution characterization by Gel Permeation Chromatography analysis (GPC) - Kinetics of free radical bulk polymerization of styrene by dilatometry - Kinetics of polycondensation of amino-11 undecanoic acid

78 78 Module : TP2406 METALLURGY (Practicals) S8 COORDINATOR : JEAN-BERNARD VOGT SCHEDULE: 20 HOURS TEACHERS : Ludovic THUINET (assistant professor) and Jean-Bernard VOGT (Professor) PREREQUISITES : Metallurgy, mechanical properties, corrosion, industrial analytical chemistry EXAMINATION based on oral participation and written reports Des matériaux, J.-P. Baïlon et J.-M. Dorlot, Presses Internationales Polytechnique, (2000) Science et génie des matériaux, W.D. Callister, Modulo Editeur (2000) Métallurgie, du minerai au matériau, J. Philibert, A. Vignnes, Y. Bréchet et P. Combrade, Masson Paris,(1998) Le livre de l acier, G. Béranger, G. Henry et G. Sanz, Technique et Documentation Lavoisier (1994) PROGRAMME : AIMS The purpose of the practical training in metallurgy is to improve the fundamental background with experiments in structural metallurgy, in mechanical properties, plasticity, fracture and corrosion Techniques frequently used in industry are presented. EXPERIMENTS and TOPICS 1 - Recrystallisation of aluminium *To analyse the effect of thermomechanical treatments on the microstructure *To understand the recrystallisation phenomena *To learn the metallographic methods : polishing, etching, optical microscopy, grain size 2 - Tensile test *To be able to use with a modern tensile machine *To analyse a tensile test diagram *To study the effect of restraining, recovery and recrystallisation on the plasticity of aluminium 3 - Corrosion *To understand the electrochemical corrosion phenomena of metallic materials in aqueous solutions *To become familiar with general methods of corrosion protection *To master the potentiostat method of corrosion control 4 - Heat treatments of steels *To be able to use the equilibrium diagrams (Fe-C), the TTT and CCT diagrams for predicting the microstructures of steels *To study phase transformation phenomena in steels *Effect of heat treatments on mechanical properties and brittleness of steels *To know the hardness test and impact test experiments

79 79 Module : TP2407 CHEMICAL ENGINEERING : EXPERIMENTAL TRAINING S8 COORDINATOR : NOURIA FATAH SCHEDULE: 54 HEURES TEACHERS : R. BECHARA, M. CZERNICKI, F. DHAINAUT et N. FATAH PREREQUISITE : HEAT TRANSFER, THERMODYNAMIC, MASS TRANSFER, POWDER TECHNOLOGY, Fluid Dynamics ASSESSMENT : Oral presentation Teachers documents P. Wuithier : Raffinage et Génie Chimique, ed. Technip Perry : Chemical Engineers Handbook, Mc Graw Hill Mc Cabe & Smith : Unit Operations of Chemical Engineering, Mc Graw Hill DETAILED PROGRAMME : Practical work of Chemical engineering gathers theory, practical program, simulation and numerical modelling. They try to carry out an harmonization accentuated between the basic disciplines of chemistry and those of Chemical engineering and target three objectives: - to supplement the course of the teaching of Chemical engineering. - to confront the students with semi-industrial scale pilots during a sufficient working time in order to obtain results of good quality and into practice to put the theoretical teaching exempted at the time of the courses and directed work. - to put in interaction the characterization, the properties of the divided solids and the processes of Chemical engineering. The unit operations of Chemical engineering implemented are: - distillation and simulation with ASPEN software, - absorption on columns, - gas-solid and liquid-solid fluidization, - evaporator and numerical modelling - filtration - physical adsorption, - characterization of the divided solids, measurement of the real density, the size distribution (method of diffraction-diffusion) and texture of particle, - liquid-liquid extraction, -Numerical Modelling : The purpose of this study is to introduce the modelling possibilities offered by Comsol. In the first part, the design of a heat exchanger allows to review the fundamental of technical drawing in 3D. Then, flows across a cylinder are modelled, in laminar state according to the Navier-Stokes equations, but also in turbulent state with the k- model. In the last part, a multiphysics phenomenon, between 2 equation systems is accomplished by considering the convection and conduction phenomena in order to take into account the heat transfer.

80 80 Module : CI2401 Option Bioorganic chemistry : Biomolécules S8 COORDINATOR : P. GRANDCLAUDON SCHEDULE : 15 HOURS TEACHERS : Adina RYCKEBUSCH, Assistant Professor C: 15 H. PREREQUISITE : Organic Chemistry : semesters S5 & S6, CH1101 et CH1201 LEARNING OUTCOMES : the aim of this course is to provide students with basic notions in stru functions of biomolecules such as proteins, sugars, lipids and nucleic acids ASSESSMENT : written examination C. Moussard, Biochimie structurale et métabolique: médecine, pharmacie, sciences: 2ème édition, De Boeck, 2002 DETAILED PROGRAMME : Structure et functions of biomolecules Protides: Amino-acids (physical proprieties, methods for analysis) - Peptides : peptide bond and peptide chain, peptides of biological interes - Proteins : primary, secondary, tertiary, quaternary structure; methods for analysis and separation. Carbohydrates: Monosaccharides (structure, properties, representations, derivatives of biological interest Polysaccharides (glycosidic linkage, stockage polysacchardies, structural polysaccharides, biological functions and industrial applications) - Heteropolysaccharides : peptidoglycans, proteoglycans. Lipids: Classification Saturated and unsaturated natural fatty acides Simple lipids (acylglycerols, cerids, sterids) Complex lipids (glycerophospholipids, sphingolipids) Lipidic character compounds (isoprenoids, steroids, vitamins) Plasmic membrane Nucleic acids: Primary structure (sugars, bases) DNA secondary structure Genetic code.

81 81 Module : CI2405 COORDINATOR : N.FATAH SCHEDULE : 20 HOURS TEACHERS : RAFEH BECHARA REACTORS S8 PREREQUISITE : 1st year chemical kinetics basic knowledge, and thermodynamics basic knowledge ASSESSMENT : written exam LEARNING OUTCOMES : General book on chemical engineering : P. Wuithier : Raffinage et Génie Chimique, ed. Technip Perry : Chemical Engineers Handbook, Mc Graw Hill Mc Cabe & Smith : Unit Operations of Chemical Engineering, Mc Graw Hill J. Villermaux : Génie de la réaction chimique, Tec & Doc Lavoisier DETAILED PROGRAMM : Reactors are equipment in which the chemical transformations are performed. The way they work is very important for all the equipment placed upstream and downstream in an industrial process. The objectives of the present course are to give the students basic knowledge of different kinds of reactors. In order to make the reactor design calculations clearer, only homogeneous reactive mixtures are considered. After a description of the fundamental aspects needed for reactor calculations, such as mass and heat transfers, several kinds of reactors are examined in more detail. They are respectively the well-mixed batch reactor, the continous stirred tank reactor, the continous tubular plug flow reactor and the cascade of tank reactors. A selection of problems with numerical calculations is proposed to illustrate the importance of the choice of the reactor for given chemical transformation(s).

82 82 Module : CI2304 GÉNIE CHIMIQUE : OPERATIONS UNITAIRES 2 S8 COORDONNATEUR : NOURIA FATAH, ROFESSEUR VOLUME HORAIRE : 32 HEURES ENSEIGNANT : ANDRE ACLOQUE, VACATAIRE ; COURS, 32 H PRÉREQUIS : Bases acquises en années préparatoires (CPGE, CPI, DEUG, DUT, BTS, ATS). Thermodynamique des équilibres entre phase. ÉVALUATION : Examens de deux heures avec documents en janvier et en février. BIBLIOGRAPHIE : Ouvrages généraux de Génie Chimique : P. Wuithier : Raffinage et Génie Chimique, ed. Technip Perry : Chemical Engineers Handbook, Mc Graw Hill Mc Cabe & Smith : Unit Operations of Chemical Engineering, Mc Graw Hill PROGRAMME DÉTAILLÉ : 1. Transfert de matière Loi de la diffusion de Fick Mesure et estimation des coefficients de diffusion Introduction aux calculs des coefficients de diffusion à partir des relations en nombres adimensionnels (Schmidt, Sherwood) Cuves agitées : calcul des puissances d agitation, transfert thermique en cuve agitée Technologie des mélangeurs discontinus et continus 2. Distillation Historique, schéma type d une installation, mesures et estimation des grandeurs physiques nécessaires Rappel sur les équilibres liquide-vapeur, azéotropes et hétéazéotropes Bilans matière et thermique autour d une colonne à distiller Calcul du nombre de plateaux et du reflux : - Méthode de Ponchon et Savarit - Hypothèses simplificatrices de Lewis - Mélanges complexes : méthodes de Fenske et de Gilliland Dimensionnement des colonnes à distiller : diamètre, espacement entre les plateaux, hauteur de garnissage Exploitation d une colonne à distiller continue Distillation discontinue : dimensionnement et exploitation

83 83 Module : CI2407 EXPERIMENTAL DESIGN S8 COORDINATOR : JEAN-MARIE AUBRY SCHEDULE : 24 HEURES TEACHERS : CHRISTEL PIERLOT, PROFESSEUR ; Cours, 16 heures ; TD, 2 heures JEAN-MARIE AUBRY, PROFESSEUR ; TD, 6 heures PREREQUISITE : ASSESSMENT : Exam (2 hours) DETAILED PROGRAMME : COURSES a) Problems depending on many independent parameters b) Problems depending on interacting parameters Complete factorial designs with two levels Fractional factorial designs c) 3 - Simplex d) 4 - Response surfaces (composite and Doehlert designs) DIRECTED STUDIES a) Application execices b) Studies by using NEMROD Software

84 84 Module : CI2409 COORDINATOR : Patrice WOISEL SCHEDULE : 10 hours TEACHERS : FUNCTIONAL POLYMERS S8 Patrice Woisel, Professor, Courses 10 hours PREREQUISITE : Polymer chemistry General organic chemistry Kinetics and chemical thermodynamics LEARNING OUTCOMES : After completing this unit the student should be able to: - Understand the principles of chemical modification of polymer structure and the effect on the polymer properties - Be aware of methods by which polymer structure can be controlled - Explain the factors that cause polymers to degrade ASSESSMENT : Written exam - La polymérisation : Principes et applications George ODIAN Polytechnica, 1994 ISBN Traité des Matériaux. 13. Chimie des Polymères : Synthèses, réactions, dégradations Jean-Pierre MERCIER, Ernest MARECHAL Presses polytechniques et Universitaires Romandes, 1993 ISBN DETAILED PROGRAMME : The main purpose of this course is to introduce modern synthetic concepts which allow the preparation of polymers with well defined structures and properties. Chemical modification of polymers Technology to control polymer formation: ATRP (Atom Transfer Radical Polymerization), RAFT (Reversible Addition-Fragmentation chain Transfer) polymerizations Stereospecific polymerizations Supramolecular polymers: synthesis, characterization and properties Degradation and stability of polymers Environmental aspects

85 85 Module : CI2408 COORDINATOR : JEAN-BERNARD VOGT Applied Metallurgy S8 TIME SCHEDULE : 15 HOURS: lectures 15h Lecturer : CHARLOTTE BECQUART, Associate Professor PREREQUISITES Thermodynamics, crystallography. LEARNING OUTCOMES : EVALUATION written exam REFERENCES : J. Barralis & G. Maeder, Métallurgie, Tome 2: alliages ferreux, ENSAM (1983), Editions communications actives, ISBN J. Philibert, A. Vignes, Y. Bréchet & P. Combrade, Métallurgie : du minerai au matériau, DUNOD, Paris 2002, ISBN G. Béranger, G. Henry & G. Sanz, Le livre de l acier, techniques & documentation- Lavoisier,1994, ISBN DETAILED PROGRAMME: From the liquid to the solid : - equilibrium diagrams - solidification - segregation in ingots - dendritic growth and equiaxed grains - recrystallisation and restoration Steels and cast Irons : - designation - heat treatments - TTT diagrams - TRC diagrams Phase transformations : - Nucleation and growth - precipitation - Displacive transformations : martensite and bainite - Relationship between mechanisms of phase transformations and steels Processing : - Processing of steels and cast irons : blast furnaces - Processing of aluminium : electrolysis Aluminium alloys

86 86 Module : CI2411 COORDINATOR : JEAN-BERNARD VOGT CORROSION S8 TIME SCHEDULE : 15 HOURS - lectures Lecturer : INGRID SERRE, CNRS researcher PREREQUISITES Electochemistry, metallurgy, materials science knowledge LEARNING OUTCOMES : EVALUATION Written test REFERENCES : Métallurgie, du minerai au matériau, J. Philibert et al, Éditeur MASSON Corrosion et chimie de surface des métaux, D. Landolt, Traité des Matériaux, Volume 12, Presses polytechniques et universitaires Romandes Atlas électrochimiques à 25 C, M. Pourbaix, Gauthier Villars Corrosion et protection des métaux, G. Béranger et F. Dabosi, Editions de Physique Des matériaux, J-P. Baïlon, J-M Dorlot, Presses intrenationales polytechnique Traitements de surface et protection contre la corrosion, S. Audisio et al, Editions de Physique Corrosion des matériaux à haute température, G. Béranger, JC. Colson, F. Dabosi, Editions de Physique Les aciers inoxydables, P. Lacombe, B. Baroux, G. Béranger, Editions de Physique Corrosion et protection, HH. Uhlig, Dunod La protection cathodique, guide pratique, TECHNIP Corrosion des métaux et alliages, G. Béranger, H. Mazille, Mécanique et Ingénerie des matériaux, Hermes, Lavoisier Corrosion et anticorrosion, ibid above Précis de corrosion, J-J. Lanoureux, Sciences des matériaux, MASSON Corrosion Engineering Handbook, Edited by Philip A. Schweitzer, P. E., Marcel Dekker, Inc. Principles and prevention of corrosion, Denny A. Jones, printed by Quinn-Woodbine, 1991 DETAILED PROGRAMME: Introduction : definition of corrosion impacts of corrosion in industry Electrochemical aspects and types of corrosion : electrochemical reactions, Ellingham diagram, dry corrosion, aqueous corrosion (Nernst law, Pourbaix diagram, electrochemical lectro, Bulter-Volmer equation, Tafel extrapolation method, corrosion potential, potential / current density curves), factors influencing corrosion phenomena, types of corrosion General corrosion : atmospheric corrosion, uniform aqueous corrosion, passive materials Localized corrosion : galvanic corrosion, pitting corrosion, crevice corrosion, intergranular corrosion, erosion corrosion and caviatation corrosion Corrosion at elevated temperature Corrosion prevention : materials selection, structures design, layer protection (coatings, paints, surface treatments), use of corrosion inhibitors, lectrochemical protection (sacrificial anode, impressed current protection), service corrosion tests

87 87 Module : CI2413 ADVANCED ANALYTICAL TECHNIQUES S8 COORDINATOR: JEAN-BERNARD VOGT TIME SCHEDULE: 5 HOURS: lectures Lecturer : ROSE-NOËLLE VANNIER, Professor PRÉREQUISITE : Lectures of cristallochemistry S6 and Analyses of Solids S7 LEARNING OUTCOMES : EVALUATION REFERENCES: Techniques de l'ingénieur, Analyse structurale et chimique des matériaux, J.P. Eberhart, Dunod Determination of residual stresses by neutron diffraction in materials and technological components, F. Rustichelli, Metallurgical Science and Technology, vol. 14 (1) 1996, Fullprof, J. Rodriguez-Carjaval, (cours de Yves Epelboin) DETAILED PROGRAMME: This lecture is devoted to advanced techniques and complete the lecture given on the analyses of solids in S7. It is presented to students which have chosen Material Science as speciality. The first part of the lecture is the presentation of non conventional sources (synchrotron, neutrons). The techniques which are described are: Measurement of residual strains in materials Textures Absorption techniques (EXAFS, XANES, Mössbauer). Surface techniques (AFM, STM).

88 88 Module : CI2414 PLASTICITY - FRACTURE MECHANISMS S8 COORDINATOR : JEAN-BERNARD VOGT SCHEDULE: 10 HOURS TEACHER: Jean-Bernard VOGT, Professor Prerequisites : Mechanical properties of materials - crystallography LEARNING OUTCOMES : EXAMINATION : Written test BIBLIOGRAPHY Des matériaux, J.-P. Baïlon et J.-M. Dorlot, Presses Internationales Polytechnique, (2000) Science et génie des matériaux, W.D. Callister, Modulo Editeur (2000) Engineering materials, an introduction to their properties and applications, M.A. Ashby and D.R.H. Jones, materials Science and technology, Vol.34, Pergamon press (1982) Mechanical behaviour of materials, T.H. Courtney, Mc Graw Hill Publishing Company (1990) DETAILED PROGRAMME : This lecture is an extension of the lecture entitled «Mechanical Properties of Materials» delivered at semester 7. It aims at giving an interpretation of plastic deformation mechanisms of metals and metallic alloys on the basis of the dislocation theory. The role of plasticity is shown through a presentation of some metal working processes and a description of rupture mechanisms. A Mechanism of plasticity of solids 1. Dislocations 2. Plasticity of single crystals and transition to polycristals B Metalworking of solid state alloys 1. Rolling 2. Wire drawing 3. Deep drawing C Rupture Mechanisms 1. Brittle fracture 2. Ductile fracture 3. Fatigue fracture

89 89 Module : CI2415 PHYSICAL METALLURGY S8 COORDINATOR : JEAN-BERNARD VOGT TIME SCHEDULE : 15 HOURS : Lectures LECTURER : JEAN-PAUL MORNIROLI, Professor PREREQUISITES 1 st year lectures on crystallography. LEARNING OUTCOMES : The aim of these lectures is to give a description of the structural and microstructural features of the and alloys in order to understand the relationships with the mechanical properties. EXAMINATION : Written test Jean Philibert, Alain Vignes, Yves Bréchet, Pierre Combrade, Métallurgie, du minerai au matériau, Dunod, Paris, 2002, Broché, 1177 p. (ISBN ) DETAILED PROGRAMME: I - Structural features - Structure of the fcc, hcp and bcc pure metals Glide systems Allotropy - Structure of the alloys Substitutional solid solutions. Order-disorder phenomena Interstitial solid solutions Intermediate phases, intermetallic compounds II - Microstructural features - Point defects - Dislocations - Stacking faults, antiphase boundaries - Grain boundaries, coincidence grain boundaries, twins

90 90 Module : FE2401 GESTION (ÉCONOMIE ) COORDINATOR : A. GRITLI VOLUME HORAIRE : 30 HEURES TEACHER: A GRITLI, CONSULTANT ; COURS 30H PREREQUISITES : aucun EXAMINATION : CADIC Jean-Yves : Gestion comptable de l entreprise : cours et exercices corrigés, édition Jean-Yves CADIC, septembre DORIATH. B et GOUJET. CH ; Comptabilité de gestion. DUNOD 2001 DETAILED PROGRAMME : I ) COMPTABILITE GENERALE Objectif du cours : «sensibiliser l élève ingénieur à la lecture, l analyse et l interprétation des documents comptables : le bilan et le compte de résultat» Thèmes abordés : L entreprise, ses opérations et ses flux. La traduction comptable des flux : le principe de la partie double : le jeu des comptes. Analyse et modèles comptables le plan comptable. Mécanismes et contrôles comptables : le journal, grand livre, Balance. Analyse de situation : le bilan. Analyse d de l exploitation : le compte de résultat. Détermination du résultat ; documents de synthèses (Bilan, compte de résultat, annexe). Analyse du bilan : les grandes masses du bilan : Fonds de roulement, Besoins en fonds de roulement, Trésorerie. Analyse du compte de résultat : les SIG II ) COMPTABILITE ANALYTIQUE Objectif du cours : «sensibiliser l élève ingénieur au calcul des coûts et prix de revient d un ou plusieurs produits» Thèmes abordés : I - Les coûts partiels 1- La nature des charges : Les charges fixes ; les charges variables ; combinaison de ces notions avec charges directes et indirectes ; les charges retenues, etc. 2- La méthode des coûts spécifiques 3 - La méthode de l imputation rationnelle des charges fixes 4- Le seuil de rentabilité 5 - Le coût marginal 6- Exercices d application.

91 II Les coûts complets L enchaînement des calculs des coûts Les éléments constitutifs des coûts La prise en compte des charges dans les coûts ; La répartition des charges indirectes ; Les sections auxiliaires, principales, l unité d œuvre, les prestations réciproques,etc La concordance avec la comptabilité générale ; Exercices d application. 91

92 92 Module : FE2402 TEACHERS : Robert Vazille, consultant SCHEDULE : PREREQUISITE : none MANAGEMENT S8 Peter Senge, La V discipline Michael Porter, Competitive Advantage Michael Porter, Competitive Edge of Nations Patrick Lagadec, Le Management des crises Elihayu Goldratt, La théorie des contraintes Harry Mikel, Six Sigma Elihayu Goldratt, La théorie des contraintes Ouakin Mark Alain, Lire aux éclats Daniel Goleman, L intelligence émotionnelle Covey Stephen, The 7 habits of highly efective people Gordon, Cadres efficaces Barbara de Angela, Real Moments Michael Treacy, L exigence du choix Jack Welch, Jack Carlos Ghosn, Turn round Emmanuelle Laborit, Le cri de la mouette Byham William, Zapp Michel Hammer, Le re engineering Tom Peters, Liberation Management DETAILED PROGRAMME : SESSION 1: overall survey of the different styles of management through different case studies. SESSION 2: Quality ISO 9001 Processus EFQM SESSION 3: Knowledge Management Transformer of information key concepts explicit and tacit knowledge KM for individual application KM within a team SESSION 4: Crisis Management, - conflicts - acquisition

93 93 Module : FE2403 COORDINATOR : J.J. TRIPLET VOLUME HORAIRE : 12 HEURES TEACHER : LAW S8 J.J. TRIPLET, ANCIEN BATONNIER, AVOCAT HONORAIRE ; COURS 12H PREREQUISITES : EXAMINATION : Examen écrit (1h) DETAILED PROGRAMME : Introduction : l intérêt du Droit La relation entre le Droit et la Justice 1 Les sources du Droit Le Droit écrit, le Droit oral Le Droit conventionnel, le Droit institutionnel le Droit institutionnel : le Droit International, le Droit Communautaire, le Droit Interne (la Constitution, la Loi, les règlements, la jurisprudence, la Doctrine) 2- Les catégories de Droit Droit public, Droit privé, Droit civil, Droit pénal 3 Les institutions judiciaires Les acteurs Les institutions : suivant la nature des affaires, suivant le degré 4 La procédure L intégration Européenne 4.1 Les Institutions Européennes Les caractéristiques du Droit Communautaire et son évolution Les institutions actuelles et le Traité Constitutionnel 4.2 Le Droit Européen La Primauté Les caractéristiques L applicabilité directe Le recours préjudiciel Les sources Les Juridictions N.B. La Cour Européenne des Droits de l Homme Conclusion : La coopération judiciare

95 95 Modules : LV2401- LV2402-LV2403 S8 ENGLISH GERMAN or DUTCH COORDINATOR : SCHEDULE : 80 ENGLISH HOURS AND 80 GERMAN HOURS TEACHERS : ANNE GUEGAND, ENGLISH MARTINE HERRIQUET, ENGLISH CLAUDINE MELY, GERMAN PASCAL RIBAUCOUR, GERMAN PREREQUISITE : ASSESSMENT : DETAILED PROGRAMME : Language tuition at the ENSCL has a double objective : - to give all students adequate communication skills in English and German and eventually the same fluency in both languages. - to encourage prospective engineers to develop an international opening onto foreign firms and universities. Continuous language assessment is carried out through at least two written tests and one interview in each language. The students who reach the required level can take the following exams : German : ZDaF English : TOEFL (USA) Cambridge First, Advanced and Proficency (UK) TOEIC (USA)

97 97 5 th academic year Semester S9 Module : TP3504 S9 COORDINATOR : PROF. NOURIA FATAH CHEMICAL ENGINEERING (praticals) SCHEDULE : COURS, 100 HEURES TEACHERS : RAFEH BECHARA, PROFESSEUR MAREK CZERNICKI, PROFESSEUR NOURIA FATAH,, MAITRE DE CONFERENCES ; Cours, 10h PREREQUISITE : ASSESSMENT : 3 oral presentations 1 written report DETAILED PROGRAMME : 8 training sessions/group Each group (option) subdivided into teams of 2 to 4 students Manipulations adapted to the specific character of each option ; chosen among the following : 1) Double-pipe heat exchanger 2) Evaporator 3) Filter press 4) Drum (continuous) filter 5) Distillation in a tray column 6) Distillation in a packed column 7) Absorption in a falling film column 8) Absorption in a packed column 9) Desorption in a packed column 10) Gas-solid fluidisation 11) Liquid-solid fluidisation 12) Characterization of solids (textural, granulometric) 13) Measure of the powders flow

98 98 Module : TP3505 PHYSICOCHEMISTRY OF POLYMERS S9 COORDINATOR : Frédéric CAZAUX SCHEDULE : 20 hours TEACHERS : Frédéric CAZAUX, Maître de conférences, Practicals 20 hours PREREQUISITE : Module CI3509, Basic knowledge in analytical chemistry and physic chemistry (conductimetry, UV spectrocopy, infrared spectroscopy) LEARNING OUTCOMES : To know the main physicochemical techniques of characterization of polymers ASSESSMENT : 4 practical reports - Polymers : Chemistry & Physics of Modern Materials, 2 nd edition J. M. G. COWIE Blackie Academic & Professional - Chapman & Hall, 1997 ISBN X - Fundamentals of Polymer Sciences: An Introductory Text, 2 nd edition Paul C. PAINTER, Michael M. COLEMAN Technomic Publication, 1997 ISBN Initiation à la rhéologie Guy COUARRAZE, Jean-Louis GROSSIORD TEC & DOC 2000 ISBN DETAILED PROGRAMME : - Capillary viscosimetry - Couette viscosimetry - Determination of the molecular weight of a polymer by tonometry - Ultraviolet spectrophotometry and conductimetry: Determination of the composition of a styrene / maleique anhydride copolymer - Infrared spectrophotometry and ThermoGravimetric Analysis: Determination of an Ethylene / Vinyl Acetate copolymer composition

99 99 Module : OP3501 S9 "BIOPROCESS, PHARMACOCHEMISTRY, ENVIRONNEMENT" COORDINATOR : ADINA RYCKBUSCH SCHEDULE : 170 HOURS TEACHERS : Pierre GRANDCLAUDON, Professeur; Courses et directed studies chimie organique (C: 14h; directed studies: 14h) Adina RYCKEBUSCH, Maître de Conférences; Courses biotechnologie (C: 20h), projets (40h). Claude DEFIVES, Maître de Conférences IUT A - USTL, Courses et TP microbiologie (C: 16h; TP: 12h). Jean-Pierre HORNEZ, Professeur IUT A - USTL, Courses microbiologie industrielle (C: 16h + 6h) Pascal DHULSTER, Professeur IUT A - USTL, Courses bioprocédés, génie industriel (C: 12h) Nouriah FATAH, Maître de Conférences, Courses et TP génie chimique (C: 4h + 32h) Marek CZERNICKI, Maître de Conférences, TP génie chimique (C: 32h) Alain HURE, Ingénieur, Courses traitement de l'eau (C: 10h) Jean-Pierre HÉNICHART, Professeur Lille 2, Courses pharmacochimie (C: 20h) PREREQUISITE : Elementary knowledge in biochemistry ASSESSMENT : Written reports and oral exam about practicals and project DETAILED PROGRAMME : Courses in common(120h) Biotechnology (20h) Fundamental microbiology (16h + 12h): Industrial and fermentation microbiology (16h) Bioprocesses and industrial engineering (12h + 32h) Option : "pharmacochemistry" (60h) Option : "Environnement" (60h)

100 100 Module : OP3502 FORMULATION ENGINEERING S9 COORDINATOR : JEAN-MARIE AUBRY SCHEDULE : 170 HOURS TEACHERS : CHRISTEL PIERLOT, PROFESSEUR, Travaux pratiques 60h STANISLAS PIETRZYK, PROFESSEUR, Cours 5h JEAN-MARIE AUBRY, PROFESSEUR, Cours 105h NOURIA FATAH, PROFESSEUR, Cours 6h PREREQUISITE : Assessment : Bibliography : DETAILED PROGRAMME : Formulation engineering (praticals) Technical and analytical methods used in formulation industries are presented. - Emulsions (notion of HLB, Windsor I,II,III) - Microemulsions (ternary diagram) - Surfactants (cloud point, Krafft point) - Detergents (separation and analysis of surfactants) - Paints (color, opacity, brightness, rheology) - Lipsticks (optimization with experimental design) - Toothpaste and shaving cream formulation - Sensorial analysis Viscosity and surface tension of liquids, structure properties correlations This lecture concerns the properties of liquids in relation to their applications in commercial products, which were not presented within the Applied Thermodynamic 1 (second year, third semester). The viscosity and surface tension of liquids are defined and the corresponding molecular models discussed. The best estimation method for the two properties (additivity methods, generalized correlations) are presented. Chemistry and formulation engineering This course, illustrated by lectures, goes deeply into the physicochemical concepts involved in formulation and includes processes used with heterogeneous mixtures and strategies used to elaborate, optimize and characterize formulated specialties. - Physical chemistry : Dispersed systems, colloïds, foams Rheology of complex fluids - Formulation processes - Strategies : Chemometry in formulation - Lectures : Sensorial analysis, colorimetry, cosmetology, detergency, fluorinated finishes - Formulation report : Bibliographical study by two students of formulation problem Divided solids technology

101 101 Module : OP3503 S9 RELIABILITY AND DAMAGE MECHANISMS OF STRUCTURAL MATERIALS COORDINATOR : JEAN-BERNARD VOGT TIME SCHEDULE : 15 HOURS - COURS LECTURER : JEAN-BERNARD, professor PREREQUISITES : Metallurgy, mechanical properties, corrosion, analytical chemistry LEARNING OUTCOMES : EVALUATION written exam REFERENCES : Mechanical behaviour of materials, Thomas H. Courtney, McGraw-Hill Publishing Company (1990) Stress-Corrosion cracking : materials performance and evaluation, Russel H. Jones, ASM International (1992) Solution to Hydrogen Attack in Steels, P.F. Timmins, ASM International (1997) Fatigue of Materials, S. Suresh, Cambridge University Press (1991 DETAILED PROGRAMME: The objective of the lecture is to identify and to understand damage mechanisms of structural materials (especially those employed in the chemical industry) that result from mechanical solicitations and from environmental effect. The lecture is divided into 3 parts : In the first one, the different types of fracture are presented: cleavage, ductile rupture, creep type rupture, ruptures maps and the influence of temperature and stress is examined. The second one is devoted to fatigue fracture (initiation and propagation) : stress response to strain cycling, fatigue resistance diagrams, dislocations structures, extrusions-intrusions and microcrack initiation, classification and behaviour of short cracks, long crack propagation, Crack growth rate regimes, crack tip plasticity, fatigue crack closure Environmentally-assisted fracture mechanisms: liquid metal embrittlement, hydrogen embrittlement, stress corrosion cracking, corrosion - fatigue, cavitation erosion, are studied in the third part.

102 102 Module : OP3503 COMPOSITES MATERIALS S9 COORDINATOR : JEAN-BERNARD VOGT TIME SCHEDULE : 6 HOURS : Lectures Lecturer : JEAN-PAUL MORNIROLI, Professor PREREQUISITES 2 nd year lectures on materials LEARNING OUTCOMES : EVALUATION Without References An introduction to composites materials D. Hull, Cambridge University Press, 1985 The main aim of these lectures is to give a general description of the composites materials and of eir main ap applications - Definition and classification of composite materials - Description and role of the fibres - Description and role of the matrix - Geometrical aspects - Mechanical properties (elastic properties, plastic properties, failure) - Conception and elaboration - Main applications

103 103 Module : OP3503 SURFACE TREATMENT S9 COORDINATOR : JEAN-BERNARD VOGT TIME SCHEDULE : 15 HOURS: lectures 6h + 9h oral reports Lecturer : CHARLOTTE BECQUART, Associate Professor PREREQUISITES 2 nd year lectures in material science, in particular, the corrosion lecture. LEARNING OUTCOMES : EVALUATION : oral report REFERENCES : Y. Adda, J.M. Dupouy, J. Philibert et Y. Quéré, Eléments de Métallurgie Physique, Vol.6, INSTN, CEA, collection enseignement S. Audisio, M. Cailler, A. Galerie et H. Mazille, Traitements de Surface et Protection contre la Corrosion, Ecole d'été, Aussois 1987, les éditions de physique. Manuel des traitements de surface à l'usage des bureaux d'études, Club des traitements de surface, CETIM. J. Barralis et G. Maeder, Métallurgie, Tome 2: alliages ferreux, ENSAM (1983), Editions communications actives, ISBN Groupe de recherches sur l'usure des matériaux industriels, Organisation de Coopération et de Développements Economiques, Glossaire des termes et définitions dans le domaine du frottement, de l'usure et de la lubrification (tribologie). Le livre de l'acier, éditeurs Gérard Béranger, Guy Henry, Germain Sanz (1994) Principes de base du traitement thermique, Pyc édition, Publications Yves Colombot. Advances of surface treatments, Proceedings of the AST World Conference Advances in Surface Treatments and Surface finishing (Paris 1986), A. Niku-Lari director, volume 5, Pergamon Press Surface Treatments for Improved Performance and Properties, Edited by J.J. Burje and V. Weiss, Plenum Press, New York and London (1982) Friction and Wear, A.D. Sarkar, Academic Press, a Subsidiary of Harcourt Brace Jovanovitch, Publishers, London. New York. Toronto. Sydney. San Fransisco (1980) Tribology: Principles and Design Applications, R. D. Arnell, P.B. Davies, J. Halling and T.L. Whomes, Published by Macmillan Education Ltd (1991) Surface Engineering, Edited by S.A. Meguid, Elsevier Applied Science, London and New York (1990) Théorie et pratique industrielle du frottement, J.J. Caubet, Technip Paris, Dunod Paris (1964) Matériaux : propriétés et applications, M.F. Ashby et D.R. Jones, Dunod Paris 1996 Various papers in "Traitement Thermique", "Galvano-Organo-Traitement de Surface", "News on Coatings and Corrosion", "Annual Review of Material Science", "Journal of Metals", "MRS Bulletin". Précis de Métallurgie J. Barralis et G. Maeder, AFNOR 6 ème édition. Les Aciers, Ben Simon, Pyc-édition, cours professé au C.E.S.T.O Principles of the surface treatments of steels, C.R. Brooks, Technomic publishing Co. Inc. Lancaster Basel Le vide les couches minces les couches dures, A. Richardt et A.M. Durand, éditions IN FINE. HEF Mécanique des surfaces. Catalogue de cas concrets. Centre Stéphanois de recherches mécaniques.hydrodynamique et Frottement Guide d emploi des traitements de surfaces appliqués aux problèmes de frottement. Editions TEC & DOC. HEF groupe

104 104 DETAILED PROGRAMME: The purpose of this course is introducing the students to the various methods, physical, mechanical, or electrochemical, which can be used to modify a materials surface. Most of the time, these treatments aim at protecting the material from an external attack, however they can have other purposes : increase wear, erosion or friction resistance, electrical properties modifications, optical properties modifications...in a first part, the course presents what is a surface, which processes can be responsible for its degradation, which methods can be used to improve the surface properties, what are pre-treatments, what are the methods which can be used to characterize the surface. In a second part, some of the most commonly used processes are studied in more details : Physical Vapour Deposition (PVD) and Chemical Vapour Deposition (CVD), thermochemical treatments, galvanization, ion Implantation, mechanical treatments... This second part is done in the form of oral reports prepared by the students from lecture material given by the instructor.

105 105 Module : OP3503 SURFACE TREATMENT ADVANCED LECTURE S9 COORDINATOR : JEAN-BERNARD VOGT SCHEDULE : 10 HOURS COURS Students involved in the «Optimisation and Reliability of Materials have to choose either this cours on metallic alloys (Pr. J.-B. VOGT) TEACHER: LECH PAWLOWSKI, Professor PREREQUISITE : Properties of materials Chemical engineering (basic) Fluids mechanics (basic) LEARNING OUTCOMES : ASSESSMENT no specific exam L. Pawlowski, The Science and Engineering of Thermal Spray Coatings, Wiley, Chichester, 1995 L. Pawlowski, Dépôts Physiques : Techniques, Microstructures et Propriétés, PPUR, Lausanne, DETAILED PROGRAMME : The lecture presents the modern methods of surface treatment and engineering and, in particular, the physical methods of films and coatings deposition. These methods are, in general, more environmental friendly than the galvanic ones are being presently extensively used. The lecture starts with on an overview of substrate preparation methods such as e.g. cleaning and activation. Subsequently, the methods of deposition by: (i) atomistic; (ii) granular; (iii) and massive are described. The microstructure of each type of film and coating are carefully analyzed. Finally, the methods of deposits characterizations and some of their properties are shown. The lecture bases on the textbooks written by Professor Pawlowski..

106 106 Module : OP3503 COORDINATOR : JEAN-BERNARD VOGT SCHEDULE : 10 HOURS COURS METALLIC ALLOYS S9 Students involved in the «Optimisation and Reliability of Materials have to choose either this cour on Advanced Surface Treatments (Pr. L. PAWLOWSKI) TEACHER: JEAN-Bernard VOGT, Professor PREREQUISITE : Metallurgy, mechanical properties, corrosion LEARNING OUTCOMES : ASSESSMENT no specific exam Les aciers inoxydables, P. Lacombe, B. Baroux, G. Béranger, Les éditions de physique (1990) Le zirconium, G. Béranger, P. Lacombe, R. Tricot, Les éditions de physique (1990) Matériaux industriels-matériaux métalliques, M. Colombié et coll., Dunod (2000) DETAILED PROGRAMME : The course aims at a description of the main classes metallic alloys highly resistant to mechanical strength and corrosion : * stainless steels * nickel alloys *zirconium alloys *titanium alloys *aluminium alloys.

107 107 Module : OP3503 STUDY OF TECHNIQUES IN MATERIAL SCIENCE S9 COORDINATOR : JEAN-BERNARD VOGT SCHEDULE :30 HOURS TEACHERS : Jean-Bernard VOGT, Jean-Paul MORNIROLI, Jean GRIMBLOT, Lech PAWLOWSKI, Ingrid SERRE, Courses & Practicals PREREQUISITE : Physics and analytical l chemistry technics LEARNING OUTCOMES : ASSESSMENT no specific exam Méthodes usuelles de caractérisation des surfaces, D. David, R. Caplain, Eyrolles (1988) Microcaractérisation des solides, M. Ammou, CRAM-LPSES-CNRS (1989) DETAILED PROGRAMME The course starts first with a consideration of the physical processes that are on the basis of the most popular analytical techniques used in the field of material science. The principle of : Scanning Electron Microscope (SEM), Atomic Force Microscopy (AFM) Transmission Electron Microscope (TEM) Energy Dispersive Sprectrometry (EDS) Xray Photoelectron Spectroscopy (XPS) are then theoretically described. An experimental approach of these techniques is finally carried out with small group of students in co-operation with ENSCL research units known to be efficient in this area.

108 108 Module : OP3503 RECYCLING OF END-OF-LIFE MATERIALS S9 COORDINATOR: JEAN-BERNARD VOGT TIME SCHEDULE: 10 HOURS: lectures Lecturer : CAROLINE PIROVANO PRÉREQUISITE : Lectures Material Science S7, S8 - General Chemistry LEARNING OUTCOMES : Evaluation : none REFERENCES: Techniques de l'ingénieur ( Publications de l'ademe DETAILED PROGRAMME: The objectives of this lecture is to present, from an economic and technologic point of view, the principles of recycling and beneficiation of materials (metals, glass, polymers, ) and of end-of-life products (end-of-life vehicle, waste from electrical and electronic equipment, ). Content : - waste and recuperation - recycling of metals - recycling of polymers - recycling of glass and ceramic - recuperation of energy - end-of-life products

109 109 Module : OP3503 CES: A NUMERICAL TOOL in MATERIAL SELECTION S9 COORDINATOR : JEAN-BERNARD VOGT TIME SCHEDULE: 8 HOURS. LECTURER: CHARLOTTE BECQUART, Associate Professor. PREREQUISITES: Materials science, mechanical properties, reliability of materials, corrosion LEARNING OUTCOMES : EVALUATION written report. REFERENCES Materials selection in Mechanical Design, M.F. Ashby, Butterworth et Heinemann Matériaux : propriétés et applications, M.F. Ashby et D.R. Jones, Dunod Paris 1996 DETAILED PROGRAMME: The purpose of this lecture is to show the students how the software CES can be used to ass selecting a material for a given application. Introduction : designing a component implies 3 problems which are not independent: (i) selecting the materials, (ii) selecting the shape, and (iii) selecting the process to make the component. Writing the specifications is difficult as some criteria are hard to quantify (aesthetics ) and as there exists an hyper choice of materials and processes. Materials : recalls Metallic materials Organic materials Mineral materials Composite materials Fundamental properties : recalls Shaping processes For metallic materials For organic materials For mineral materials For composite materials Material indices. What is a material index? How do we determine a material index? case studies (CES selector)

110 110 Module : OP3503 COORDINATOR : JEAN-BERNARD VOGT MINI LAB PROJECT S9 SCHEDULE : 50 HOURS - Practicals, project TEACHER: Each ENSCL teacher involved in the field of materials PREREQUISITE : Materials science, chemistry of materials, analytical techniques LEARNING OUTCOMES : ASSESSMENT : written report and oral presentation Specific documents related to the project DETAILED PROGRAMME : Each professor involved in the Material Science program can submit to a group of 2 or 3 students a project that reflects a specific application field (surface treatment, metallurgy, cristallochemistry, catalysis materials, chemical engineering materials, software assisted selection of materials ). The project takes place inside ENSCL laboratories and can be connected with an industrial partner. It includes a literature survey, a proposal and a realisation of an experimental procedure suitable for solving the problem and then a discussion of the obtained results. A condensed report associated with an oral presentation in front of the students and the teachers are then given. Laboratories involved : Unité de Catalyse et Chimie du Solide Laboratoire de Métallurgie Physique et Génie des Matériaux Laboratoire des Procédés d Elaboration des Revêtements Fonctionnels

111 111 Module : CI3504_a CHEMICAL ENGINEERING : fluidized BED- multi-media teaching COORDINATOR : NOURIA FATAH S9 SCHEDULE : 2 HOURS TEACHERS : Nouria FATAH, Professeur (Courses) PREREQUISITE : FLUIDS MECANICS Porous media LEARNING OUTCOMES : ASSESSMENT : Oral presentation Documents of the teachers Gas Fluidization technology, D. Geldart, John Wiley and Sons, 1986 M. RHODES, «PRINCIPLES OF POWDER TECHNOLOGY», John Wiley and Sons, 1990 DETAILED PROGRAMME : This course illustrates the gas fluidization technology, the hydrodynamics properties of fluidized bed are defined like minimum fluidization velocity, porosity, height, the bubble phenomenon, the different hydrodynamics behaviour of fluidized bed and fluidization quality.

112 112 Module : CI3504_a CHEMICAL ENGINEERING : ABSORPTION S9 COORDINATOR : NOURIA FATAH, PROFESSOR SCHEDULE : Courses, 4h; Directed Studies; 4h TEACHERS : MAREK CZERNICKI, ASSOCIATED PROFESSOR ; Courses, 4h NOURIA FATAH, PROFESSOR, Directed Studies, 4h PREREQUISITE : Chemical Engineering Courses ASSESSMENT : Oral exam about chemical engineering practical Coulson J.M., Richardson J.F., Chemical Engineering, Pergamon Press 1990 Hobler T., Mass Transfer and Absorbers, Pergamon Press 1966 Bachmann P., Tissot P., Précis de Génie chimique, Georg- Librairie de l Université, Genève 1981 Anglaret P., Filippi J., Kazmierczak S., Technologie - Génie chimique, Centre Régional de Documentation Pédagogique de l Académie d Amiens, Amiens 1998 Lefrançois B., Chimie Industrielle, Technique et Documentation Lavoisier, Paris 1995 Techniques de l Ingénieur Perry R., Green D., Perry s Chemical Engineering Handbook, Mc Graw Hill 11. J.L. Humphrey, G.E. Keller, Procédés de séparation, Dunod, Paris Emilian Koller, Aide-Memoire, Génie chimique, Dunod, Paris 2001 DETAILED PROGRAMME : This main object of this course is to give basic concepts of the absorption process. This lecture covers the methods used to calculate the absorbers (Diffusive and convective mass transfer, mass transfer coefficients).

113 113 Module : CI3504_a CHEMICAL ENGINEERING : ADVANCED DISTILLATION S9 COORDINATOR : MAREK CZERNICKI SCHEDULE : Courses, 5 hours; TEACHERS : MAREK CZERNICKI, ASSOCIATED PROFESSOR; Courses, 5h PREREQUISITE : Notions of heat transfer, mass transfer and unit operations Chemical engineering courses ASSESSMENT : Oral exam about chemical engineering practical H.Z. Kister, «Distillation Design», McGraw-Hill, 1992 H.Z. Kister, «Distillation Operation», McGraw-Hill, 1989 J.G. Stichlmair, J.R. Fair, «Distillation Principles and Practices», WILEY-VCH, 1998 Perry R., Green D., Perry s «Chemical Engineering Handbook», Mc Graw Hill Techniques de l Ingénieur, Génie des Procédés C.D. Holland, «Fundamentals of Multicomponenet Distillation», McGraw-Hill, 1981 L.M. Rose, «Distillation Designe Practice», Elservier, 1985 K. Sundmacher, A. Kienle, «Reactive Distillation», WILEY-VCH, 2003 DETAILED PROGRAMME : Rigorous multicomponent distillation calculation for tray columns - Basic concepts - Numerical modelling of distillation column Distillations systems - Multiple columns - Complex columns Hybrid process - Extractive distillation - Azeotropic distillation - Reactive distillation Batch distillation - Basic concepts - Optimal reflux rate policy for batch distillation columns

114 114 Module : CI3504_a CHEMICAL ENGINEERING : LIQUID-VAPOUR EQUILIBRIUM S9 COORDINATOR : MAREK CZERNICKI SCHEDULE : Courses, 4 hours; Directed Studies; 8 hours TEACHERS : MAREK CZERNICKI, ASSOCIATED PROFESSOR; Courses, 4h ; directed studies, 8h PREREQUISITE : Notions of applied thermodynamics Liquid-vapour equilibrium for ideal systems ASSESSMENT : Oral exam about chemical engineering practical 1. Jean VIDAL, «Thermodynamique», Editions Technip, B.E.Poling, J.M.Prausnitz, J.P.O Connell, «The Properties of Gases and Liquids», McGraw-Hill, J.M.Prausnitz, R.N.Lichtenthaler, E.G.de Azevedo, «Molecular Thermodynamics of Fluid-Phase Equilibria», Pretince-Hall Inc., Pierre Perrot, «Thermodynamique Chimique», Dunod, Paris,1998 DETAILED PROGRAMME : The phase equilibrium liquid-vapour problems for multicomponent systems are discussed. Equations of state and liquid solution models: The Van Laar, Scatchard-Hildebrand, Flory- Huggins, Wilson, NRTL, UNIQUAC, UNIFAC methods for estimation of activity coefficients in liquid phase are presented.

115 115 Module : CI3504_a CHEMICAL ENGINEERING : ASPEN PLUS SIMULATION S9 COORDINATOR : MAREK CZERNICKI SCHEDULE: Courses, 4 hours; Directed Studies; 8 hours TEACHERS : MAREK CZERNICKI, ASSOCIATED PROFESSOR; Courses, 4h ; directed studies, 8h PREREQUISITE : Notions of applied thermodynamics Notions of heat transfer, mass transfer and unit operations Courses : Chemical Engineering, Advanced Distillation, Liquid-Vapour Equilibrium ASSESSMENT : project : simulation of an industrial installation Aspen Plus documents DETAILED PROGRAMME : Introduction to the computing environment, solution of typical engineering problems using computer tools. The purpose of this course is to provide to the using with Aspen Plus to built and use a steady state process simulation model. Several unit operations (distillation columns, heat exchangers, etc.) and thermodynamic databanks are presented. The course explains with examples how to perform the basic task for creating and running simulation. After the introduction course, students use Aspen Plus to solve chemical engineering problems: calculation of the thermodynamic property of ternary mixture and the separation of multicomponent mixture using distillation column sequencing.

116 116 Module : CI3504_a COORDINATOR : NOURIA FATAH SCHEDULE : 16 HOURS Adsorption & Catalysis S9 TEACHERS : RAFEH BECHARA PREREQUISITE : Courses of Reactors (Second year) and thermodynamics basic knowledge ASSESSMENT : Supervised exam + oral presentation Chemical engineering kinetics, J.M. Smith, Third edition, McGraw-Hill (1981) Particle size measurement, Terence Allen, Fifth edition, Chapman and Hall (1997) Adsorption by powders and porous solids, F. Rouquerol, J. Rouquerol, K. Sing, Academic press (1999) Adsorption, surface area and porosity, S. j. Gregg, K. S. W. Sing, Second edition, Academic press (1997) DETAILED PROGRAMME : Adsorption is of great technological importance. Thus, some porous adsorbents are widely employed for the separation of gases, the purification of liquids or for pollution control. Another reason for the widespread use of adsorption techniques is the importance now attached to the characterization of the surface properties and texture of porous materials. The aim of this course is to propose some methods for the assessment of the surface specific area and pore size distribution of a diverse range of powders and porous materials. Also, adsorption phenomena play a vital role in heterogeneous catalysis and in much solid state reaction. Then, we present the effect of physical processes on observed rates of reaction, mass and heat transfer coefficients.

117 117 Module : CI3504_b CHEMICAL ENGINEERING : POWDER TECHNOLOGY S9 COORDINATOR : NOURIA FATAH SCHEDULE : 10 HOURS TEACHERS : Nouria FATAH, Professeur (Courses) PREREQUISITE : Solids physics LEARNING OUTCOMES : ASSESSMENT : oral presentation -Documents of the teachers -M. RHODES, «PRINCIPLES OF POWDER TECHNOLOGY», John Wiley and Sons, 1990 DETAILED PROGRAMME : This lecture regroups two parts: Particle size measurement: -This course covers the theory and techniques to analyse the sampling, particle size (light scattering laser, image analysis, sieving), definition of size, size distribution and diameter of particle. This lecture covers the theory and techniques to measure:, porosity, density, specific area, shape factor, particle size (light scattering laser, image analysis, sieving) and definition of size, distribution, diameter of particle, agglomeration phenomenon and the interaction between fluid and particles. Powder flowability: This lecture concern the presentation of the different methods to measure the rheological parameters of powders and the importance of the interaction between particles, the influence of the physical properties of particles, the agglomeration phenomenon on the powder flow.

118 118 Module : CI3509 PHYSICO CHEMISTRY OF POLYMERS S9 COORDINATOR : PR. XAVIER COQUERET SCHEDULE : 20 HOURS TEACHERS : Xavier COQUERET, Professeur, Courses 20 hours PREREQUISITE : Modules CH2309 and CH2409 ASSESSMENT : Written exam - Polymers : Chemistry & Physics of Modern Materials, 2 nd edition J. M. G. COWIE Blackie Academic & Professional - Chapman & Hall, 1997 ISBN X - Initiation à la chimie et à la physico-chimie macromoléculaires Vol.12 : Chimie de l élaboration du matériau polymère Collectif Groupe Français des Polymères, 2001 ISBN - - Introduction to Polymer Science F. W. BILLMEYER Wiley, 1984 ISBN DETAILED PROGRAMME : - Introduction to the physico-chemistry of polymers - Chain dimensions and statistics - Thermodynamics of polymer solutions ans blends : Flory-Huggins and Flory-Krigbaum theories, solubility parameters, predicting polymer solubility - Determination of molecular weights: osmometry and tonometry, size exclusion chromatography, universal calibration - Light scattering : principle, experimental method, Zimm plot, MW determination and radius of giration - Viscosity of polymer solutions: Einstein s law, capillary viscosimetry, Mark-Houwink relation, Couette viscosimetry - Structure properties relations, use properties of polymers - Surface properties and surface treatments of polymers: surface characterisation, modification by physical and chemical methods, applications

119 119 Module : FE3502 SAFETY AND HAZARD IN CHEMICAL ENGINEERING S9 COORDINATOR : SERGE BOURBIGOT SCHEDULE : 20 HOURS TEACHERS : Serge Bourbigot PREREQUISITE : Chemistry and Physics at the undergraduate level LEARNING OUTCOMES : Safety in the industry ASSESSMENT : Scientific project with defence and report Guide d Analyse du Risque Chimique, B. Martel, Dunod, Paris, Fiches toxicologiques INRS et Toxicité Procédés Propres et Sûrs, André Laurent, Nancy, ENSIC. La qualité des produits industriels, C. Maria, Dunod, Paris, DETAILED PROGRAMME : 1. Basic of safety in chemical engineering Safety in chemical industry Danger process Blowhole dimension Atmospheric dispersion Combustions explosions Dust explosions Chemical reactors Domino effect 2. Safety in the industry Safety and legislation for chemicals in the hyper market Safety and hazard in chemical engineering Technical gases Safety on industrial site Reaction and resistance to fire: legislation, testing and solutions

120 120 Module : FE3501 (1) COORDINATOR : A. GRITLI SCHEDULE : TEACHERS : A. GRITLI, CONSULTANT ; Cours BUSINESS SIMULATION S9 PREREQUISITE : ASSESSMENT : DETAILED PROGRAMME : 1. Fundamentals of industrial security General hazards in chemical industry Hazard process Design of venting systems Gas evolution measurement Fire and explosion hazards Dust explosion Chemical reaction hazards (thermal runaway chemical reactions) Domino effect 2. Problems of security in industry Safety and regulation for chemicals Safety and chemical reaction engineering Industrial use of technical gases (invited conference) Safety in industrial plants Reaction to fire of materials : assessment, regulation and solutions

121 121 FE3503 COORDINATOR : ENTRPREUNERSHIP S9 WORKLOAD : 15 HOURS LECTURERS : REMI BACHELET, MAITRE DE CONFERENCES, ECOLE CENTRALE DE LILLE; 8h DOMINIQUE FRUGIER, CONSULTANT ; 7h PREREQUISITES ASSESSMENT : MULTIPLE CHOICE QUESTIONS (MCQ) LEARNING OUTCOMES : - Roles in project management Project profiling actors and stakes in a project - Business plan design REFERENCES : Project management course DETAILED PROGRAMM : Introduction to project and innovation management. Projects typology, basic concepts of project management : production vs. projects, project and innovation. Systems and project organisation : e.g. matrix organisation, tiger teams.. organisation for system design, from Over-the-wall to concurrent engineering. Project management tools and methods : pert, Gantt, WBS, groupware with an emphasis on functional analysis. Risk management and human factor analysis using sociology of organisations. Linking project management and technological innovation using a project design methodology. Business creation and business plans will also be tackled. Innovation management, from the global firm strategy to its daily implementation. Innovation marketing

122 122 Module : FE3503 COORDINATOR : PROJECT MANAGEMENT S9 SCHEDULE : 15 HOURS TEACHERS : REMI BACHELET, MAITRE DE CONFERENCE, ECOLE CENTRALE DE LILLE; Courses 7h DOMINIQUE FRUGIER, CONSULTANT ; Courses 4h ALAIN DORAT, CONSULTANT ; Courses 4h PREREQUISITE : ASSESSMENT : Exam with short and open answers

123 123 Module : FE3503 (4) COORDINATOR : A. PLOUVIER SCHEDULE : 18H TEACHERS : STRATEGY AND MARKETING S9 A. PLOUVIER, CONSULTANT ; Courses 18h PREREQUISITE : ASSESSMENT :

124 124 Module : FE3503 (4) PRODUCTION MANAGEMENT S9 COORDINATOR : EMMANUEL CASTELAIN SCHEDULE : 12H TEACHERS : EMMANUEL CASTELAIN, MAITRE DE CONFERENCE, ECOLE CENTRALE DE LILLE ; Courses 12h PREREQUISITE : ASSESSMENT : Exam with short and open answers

126 126 Modules : LV3501-LV3502-LV3503 S9 ENGLISH GERMAN or DUTCH COORDINATOR : SCHEDULE : 80 ENGLISH HOURS AND 80 GERMAN HOURS TEACHERS : ANNE GUEGAND, ENGLISH MARTINE HERRIQUET, ENGLISH CLAUDINE MELY, GERMAN PASCAL RIBAUCOUR, GERMAN PREREQUISITE : ASSESSMENT : DETAILED PROGRAMME : Language tuition at the ENSCL has a double objective : - to give all students adequate communication skills in English and German and eventually the same fluency in both languages. - to encourage prospective engineers to develop an international opening onto foreign firms and universities. Continuous language assessment is carried out through at least two written tests and one interview in each language. The students who reach the required level can take the following exams : German : ZDaF English : TOEFL (USA) Cambridge First, Advanced and Proficency (UK) TOEIC (USA)

128 APPENDIX 128

129 ENSCL ECOLE NATIONALE SUPERIEURE DE CHIMIE DE LILLE (F) SOCRATES/ERASMUS PROGRAMME STUDENT APPLICATION FORM ACADEMIC YEAR / Attach 2 Recent photographs FIELD OF STUDY:.... This application should be completed in BLACK PRINT in order to be easily copied and/or faxed. SENDING INSTITUTION Name and full address: ERASMUS ID... Department co-ordinator - name, telephone and fax numbers, Institutional co-ordinator - name, telephone and fax numbers, STUDENT S PERSONAL DATA Family name: Title: (Mr/Mrs/Miss):. Place of Birth:... Address for correspondence: Tel.: First name (s):... Date of birth: (day/month/year)... Sex:... Nationality:... Permanent address (if different): Tel.:

130 Current address is valid until: SPECIAL NEEDS If you have special needs that might require additional support please tick this box and we will contact you. Our aim is to support you. If we are unaware of special needs when you apply it may prove difficult to meet them. Briefly state the reasons why you wish to study abroad? DATES OF STUDY EXCHANGE Period of Study (give actual dates) From To Length of Stay (months) Number of Expected ECTS Credits (if applicable).. day/month/year.. day/month/year Declaration: I am sending this application, together with a Transcript of Records and provisional Learning Agreement and two recent photographs. Signature of Applicant:... Date:...

131 2 PROPOSED STUDY Taught Modules (list titles) Project (outline topic briefly) Please attach a Learning Agreement even if only provisional at this stage. Please use another sheet if necessary LANGUAGE COMPETENCE Mother tongue:... Language of instruction at home institution (if different):... English I have sufficient knowledge to follow lectures I need some extra language preparation Yes No Yes No PREVIOUS AND CURRENT STUDY Diploma/Degree for which you are currently studying:... Title of Course: Number of higher education study years prior to departure abroad:...have you studied abroad before? Yes No If Yes, when? at which institution? Please attach a Transcript of Records including full details of previous and current higher education study. Details not known at the time of application can be provided at a later stage, before registration. Return form to the SOCRATES Co-ordinator in the School in which you wish to study, who will complete the section below: UNIVERSITY OF SURREY: DECLARATION BY SCHOOL School/Department : I acknowledge receipt of the Application, proposed Learning Agreement and Transcript of Records. The above-mentioned student is: accepted at our institution 1 not accepted at our

132 3 institution 1 Level of registration: Undergraduate 1 Postgraduate Taught 1 Course against which student should be registered: [PG Taught only].. Postgraduate Research 1 Doctoral level 1 ECTS credits to apply Yes 1 No 1 School SOCRATES Co-ordinator s name:... Date:... Signature:... For office use only: Received by Socrates Institutional Co-ordinator Signature... Date... Sent to UG Office Sent to PG Office Accommodation Office form Date... Date... If received, date sent to Accommodation Office.. Date last revised: January

133 LEARNING AGREEMENT ACADEMIC YEAR 20 /20 - FIELD OF STUDY: CHEMISTRY Name of student: Sending institution:... Country:... DETAILS OF THE PROPOSED STUDY PROGRAMME ABROAD/LEARNING AGREEMENT Receiving institution:... Country:.. Course unit code (if any) and page no. of the information package if necessary, continue the list on a separate sheet Course unit title (as indicated in the information package) Number of credits Student s signature... Date:... SENDING INSTITUTION We confirm that the proposed programme of study/learning agreement is approved. Departmental coordinator s signature Institutional coordinator s signature Date: Date:...

134 5 RECEIVING INSTITUTION We confirm that this proposed programme of study/learning agreement is approved. Departmental coordinator s signature Institutional coordinator s signature Date:... Date: Name of student: Sending institution: CHANGES TO ORIGINAL PROPOSED STUDY PROGRAMME/LEARNING AGREEMENT (to be filled in ONLY if appropriate) Course unit code (if any) and page no. of the information package Course unit title (as indicated in the information package) Deleted course unit Added course unit Number of credits if necessary, continue this list on a separate sheet

135 6 Student s signature Date:... SENDING INSTITUTION We confirm that the above-listed changes to the initially agreed programme of study/learning agreement are approved. Departmental coordinator s signature Date:... Institutional coordinator s signature Date:... RECEIVING INSTITUTION We confirm bye the above-listed changes to the initially agreed programme of study/learning agreement are approved. Departmental coordinator s signature Date:... Institutional coordinator s signature Date:...

136 RELEVE DE NOTES Transcript of records NOM DE L'ETABLISSEMENT D'ORIGINE :... Faculté/Département :... Coordonnateur ECTS départemental :... NOM DE L'ETUDIANT(E) :... Prénom :... Date et lieu de naissance :...sexe :... Date d'inscription :... Numéro d'inscription :... NOM DE L'ETABLISSEMENT D'ACCUEIL :... Faculté/Département :... Coordonnateur ECTS départemental :... Tél. :...Télécopie : Code du cours (1) Intitulé du cours Durée du cours (2) Note locale (3) Note ECTS (4) Crédits ECTS (5) Suite sur une feuille séparée Total :... (1) (2) (3) (4) (5) voir explications au verso Diplôme décerné :... Date : Signature du secrétaire général/doyen/responsable administratif : Cachet de l'établissement NB : ce document n'est pas valable sans signature

137 (1) Code du cours Voir le dossier d'information ECTS (2) Durée du cours Y = 1 année universitaire 1S = 1 semestre 1T = 1 trimestre 2S = 2 semestres 2T = 2 trimestres (3) Description du système de notation de l'établissement (4) Echelle de notation ECTS Note ECTS Pourcentage d'étudiants admis qui devraient obtenir la note Définition A 10 EXCELLENT - résultat remarquable, avec seulement quelques insuffisances mineures B 25 TRES BIEN - résultat supérieur à la moyenne, malgré un certain nombre d'insuffisances notables C 30 BIEN - travail généralement bon, malgré un certain nombre d'insuffisances notables D 25 SATISFAISANT - travail honnête, mais comportant des lacunes importantes E FX 10 - PASSABLE - le résultat satisfait aux critères minimaux

138 9 INSUFFISANT - un travail supplémentaire est nécessaire pour l'octroi d'un crédit F - INSUFFISANT - un travail supplémentaire considérable est nécessaire (5) Crédits ECTS 1 année universitaire = 60 crédits 1 semestre = 30 crédits 1 trimestre = 20 crédits RELEVE DE NOTES - Page 2

139 10 ACCOMMODATION FORM Please fill it in with black ink and send it by at or by fax : To be returned before 1 st May for the 1 st semester (starting from September) And 30 th November for the 2 nd semester (starting from February) 1) Sending Institution : Coordinator s name :... Phone :... Fax : Name and address of the institution : ) Personal information : Student name and forename :... Date of birth :...Sex : M F Country of birth :...Nationality :... Permanent address abroad : valid until:... 3) Accomodation Kind of accommodation Rent per month hall of residence : traditional room standard B 130,91 hall of residence : renovated room standard A 165,17 Hall of residence : studio 281,77 Studéa Lille I : studio (private residence) 405 Private (accomodation research by the student) - * Sort by your accomodation type preference from 1 to 3 Sort by preference* Period of stay : from to 4) Need help from the Mentor Club : yes no If yes :Date, place and time of arrival :... VERY IMPORTANT NOTICE For the room attribution in hall of residence, it is imperative to arrive before 15 h at the residence