ASTM Volume 09.01, July 2015 Rubber, Natural and Synthetic -- General Test Methods; Carbon Black



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1 D297-13 Standard Test Methods for Rubber Products Chemical Analysis 2 D395-14 Standard Test Methods for Rubber Property Compression Set 3 D412-06a(2013) Standard Test Methods for Vulcanized Rubber and Thermoplastic Elastomers Tension 4 D413-98(2013) Standard Test Methods for Rubber Property Adhesion to Flexible Substrate 5 D429-14 Standard Test Methods for Rubber Property Adhesion to Rigid Substrates 6 D430-06(2012) Standard Test Methods for Rubber Deterioration Dynamic Fatigue 7 D454-04(2010) Standard Test Method for Rubber Deterioration by Heat and Air Pressure 8 D471-12a Standard Test Method for Rubber Property Effect of Liquids 9 D531-00(2010) Standard Test Method for Rubber Property-Pusey and Jones Indentation 10 D572-04(2010) Standard Test Method for Rubber-Deterioration by Heat and Oxygen 11 D573-04(2010) Standard Test Method for Rubber Deterioration in an Air Oven 12 D575-91(2012) Standard Test Methods for Rubber Properties in Compression 13 D623-07(2014) Standard Test Methods for Rubber Property Heat Generation and Flexing Fatigue In Compression 14 D624-00(2012) Standard Test Method for Tear Strength of Conventional Vulcanized Rubber and Thermoplastic Elastomers 15 D750-12 Standard Practice for Rubber Deterioration Using Artificial Weathering Apparatus 16 D813-07(2014) Standard Test Method for Rubber Deterioration Crack Growth 17 D814-95(2014) Standard Test Method for Rubber Property Vapor Transmission of Volatile Liquids 18 D816-06(2011) Standard Test Methods for Rubber Cements 19 D832-07(2012) Standard Practice for Rubber Conditioning For Low Temperature Testing 20 D865-11 Standard Test Method for Rubber - Deterioration by Heating in Air (Test Tube Enclosure) 21 D925-14 Standard Test Methods for Rubber Property Staining of Surfaces (Contact, Migration, and Diffusion) 22 D926-08(2013) Standard Test Method for Rubber Property Plasticity and Recovery (Parallel Plate Method) 23 D945-06(2012) Standard Test Methods for Rubber Properties in Compression or Shear (Mechanical Oscillograph) 24 D991-89(2014) Standard Test Method for Rubber Property Volume Resistivity Of Electrically Conductive and Antistatic Products 25 D1052-09(2014) Standard Test Method for Measuring Rubber Deterioration Cut Growth Using Ross Flexing Apparatus 26 D1053-92a(2012) Standard Test Methods for Rubber Property Stiffening at Low Temperatures: Flexible Polymers and Coated Fabrics 27 D1076-14 Standard Specification for Rubber Concentrated, Ammonia Preserved, Creamed, and Centrifuged Natural Latex 28 D1148-13 Standard Test Method for Rubber Deterioration Discoloration from Ultraviolet (UV) or UV/Visible Radiation and Heat Exposure of Light-Colored Surfaces 29 D1149-07(2012) Standard Test Methods for Rubber Deterioration Cracking in an Ozone Controlled Environment 30 D1171-99(2007) Standard Test Method for Rubber Deterioration Surface Ozone Cracking Outdoors or Chamber (Triangular Specimens) 31 D1229-03(2008) Standard Test Method for Rubber Property-Compression Set at Low Temperatures 32 D1278-91a(2011) Standard Test Methods for Rubber from Natural Sources Chemical Analysis 33 D1329-08 Standard Test Method for Evaluating Rubber Property Retraction at Lower Temperatures (TR Test) 34 D1349-14 Standard Practice for Rubber Standard Conditions for Testing 35 D1415-06(2012) Standard Test Method for Rubber Property International Hardness 36 D1417-10 Standard Test Methods for Rubber Latices-Synthetic 37 D1418-10a Standard Practice for Rubber and Rubber Latices-Nomenclature 38 D1456-86(2014) Standard Test Method for Rubber Property Elongation at Specific Stress 39 D1460-86(2014) Standard Test Method for Rubber Property Change in Length During Liquid Immersion 40 D1485-07(2011) Standard Practice for Rubber from Natural Sources Sampling and Sample Preparation 41 D1506-99(2013) Standard Test Methods for Carbon Black Ash Content 42 D1508-12 Standard Test Method for Carbon Black, Pelleted Fines and Attrition 43 D1509-95(2012) Standard Test Methods for Carbon Black Heating Loss 44 D1510-13 Standard Test Method for Carbon Black Iodine Adsorption Number 45 D1511-12 Standard Test Method for Carbon Black Pellet Size Distribution 1/5

46 D1512-15 Standard Test Methods for Carbon Black ph Value 47 D1513-05(2012) Standard Test Method for Carbon Black, Pelleted Pour Density 48 D1514-04(2011) Standard Test Method for Carbon Black - Sieve Residue 49 D1519-95(2014) Standard Test Methods for Rubber Chemicals Determination of Melting Range 50 D1566-14 Standard Terminology Relating to Rubber 51 D1618-99(2011) Standard Test Method for Carbon Black Extractables - Transmittance of Toluene Extract 52 D1619-11 Standard Test Methods for Carbon Black Sulfur Content 53 D1630-06(2012) Standard Test Method for Rubber Property Abrasion Resistance (Footwear Abrader) 54 D1646-07(2012) Standard Test Methods for Rubber Viscosity, Stress Relaxation, and Pre-Vulcanization Characteristics (Mooney Viscometer) 55 D1765-14 Standard Classification System for Carbon Blacks Used in Rubber Products 56 D1766-05(2011) Standard Test Method for Rubber Chemicals - Solubility 57 D1799-03a(2014) Standard Practice for Carbon Black Sampling Packaged Shipments 58 D1817-05(2011) Standard Test Method for Rubber Chemicals Density 59 D1900-06(2011) Standard Practice for Carbon Black - Sampling Bulk Shipments 60 D1917-03(2012) Standard Test Methods for Rubber Property Shrinkage of Raw and Compounded Hot- Polymerized Styrene-Butadiene Rubber (SBR) 61 D1937-13 Standard Test Method for Carbon Black, Pelleted Mass Strength 62 D1991-05(2010) Standard Test Method for Rubber Chemicals 2-Mercaptobenzothiazole (MBT) Assay 63 D1992-91(2013) Standard Guide for Testing Synthetic Plasticizers Used in Rubber 64 D1993-03(2013) Standard Test Method for Precipitated Silica-Surface Area by Multipoint BET Nitrogen Adsorption 65 D2084-11 Standard Test Method for Rubber Property Vulcanization Using Oscillating Disk Cure Meter 66 D2136-02(2012) Standard Test Method for Coated Fabrics Low-Temperature Bend Test 67 D2137-11 Standard Test Methods for Rubber Property - Brittleness Point of Flexible Polymers and Coated Fabrics 68 D2226-93(2012) Standard Classification for Various Types of Petroleum Oils for Rubber Compounding Use 69 D2227-96(2011) Standard Specification for Natural Rubber (NR) Technical Grades 70 D2228-04(2009) Standard Test Method for Rubber Property-Relative Abrasion Resistance by the Pico Abrader Method 71 D2230-96(2012) Standard Test Method for Rubber Property Extrudability of Unvulcanized Compounds 72 D2240-05(2010) Standard Test Method for Rubber Property Durometer Hardness 73 D2414-14 Standard Test Method for Carbon Black Oil Absorption Number (OAN) 74 D2449-88(2011) Standard Specification for Rubber Bales From Natural Sources Limit on Coating 75 D2632-14 Standard Test Method for Rubber Property Resilience by Vertical Rebound 76 D2663-14 Standard Test Methods for Carbon Black Dispersion in Rubber 77 D2702-05(2011) Standard Practice for Rubber Chemicals Determination of Infrared Absorption Characteristics 78 D3053-13a Standard Terminology Relating to Carbon Black 79 D3137-81(2013) Standard Test Method for Rubber Property Hydrolytic Stability 80 D3156-96(2011) Standard Practice for Rubber Chromatographic Analysis of Antidegradants (Antioxidants, Antiozonants and Stabilizers) 81 D3157-05(2010)e1 Standard Test Method for Rubber from Natural Sources Color 82 D3182-07(2012) Standard Practice for Rubber Materials, Equipment, and Procedures for Mixing Standard Compounds and Preparing Standard Vulcanized Sheets 83 D3183-10 Standard Practice for Rubber Preparation of Pieces for Test Purposes from Products 84 D3184-11 Standard Practice for Rubber - Evaluation of NR (Natural Rubber) 85 D3185-06(2010) Standard Test Methods for Rubber-Evaluation of SBR (Styrene-Butadiene Rubber) Including Mixtures With Oil 86 D3186-07(2011) Standard Test Methods for Rubber Evaluation of SBR (Styrene-Butadiene Rubber) Mixed With Carbon Black or Carbon Black and Oil 87 D3187-06(2011) Standard Test Methods for Rubber Evaluation of NBR (Acrylonitrile-Butadiene Rubber) 88 D3188-06(2010) Standard Test Methods for Rubber-Evaluation of IIR (Isobutene-Isoprene Rubber) 89 D3189-06(2011) Standard Test Methods for Rubber Evaluation of Solution BR (Polybutadiene Rubber) 90 D3190-06(2010) Standard Test Method for Rubber-Evaluation of Chloroprene Rubber (CR) 91 D3191-10(2014) Standard Test Methods for Carbon Black in SBR (Styrene-Butadiene Rubber) Recipe and Evaluation Procedures 92 D3192-09(2014) Standard Test Methods for Carbon Black Evaluation in NR (Natural Rubber) 2/5

93 D3194-04(2009) Standard Test Method for Rubber From Natural Sources-Plasticity Retention Index (PRI) 94 D3265-15 Standard Test Method for Carbon Black Tint Strength 95 D3313-12 Standard Test Method for Carbon Black Individual Pellet Hardness 96 D3314-02(2012) Standard Test Method for Rubber Chemical Analysis for Polystyrene Blocks In SBR (Styrene- Butadiene Rubber) and Styrene-Reinforced Latices 97 D3346-12 Standard Test Methods for Rubber Property Processability of Emulsion SBR (Styrene- Butadiene Rubber) With the Mooney Viscometer (Delta Mooney) 98 D3389-10 Standard Test Method for Coated Fabrics Abrasion Resistance (Rotary Platform Abrader) 99 D3403-07(2011) Standard Test Methods for Rubber Evaluation of IR (Isoprene Rubber) 100 D3452-06(2012) Standard Practice for Rubber Identification by Pyrolysis-Gas Chromatography 101 D3484-06(2010) Standard Test Methods for Rubber Evaluation of Oil-Extended Solution BR (Polybutadiene Rubber) 102 D3493-14 Standard Test Method for Carbon Black Oil Absorption Number of Compressed Sample (COAN) 103 D3566-03(2014) Standard Practice for Rubber Determination of Bromine in the Presence of Chlorine by Oxygen Combustion 104 D3568-03(2013) Standard Test Methods for Rubber Evaluation of EPDM (Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil 105 D3616-95(2014) Standard Test Method for Rubber Determination of Gel, Swelling Index, and Dilute Solution Viscosity 106 D3677-10e1 Standard Test Methods for Rubber - Identification by Infrared Spectrophotometry 107 D3767-03(2014) Standard Practice for Rubber Measurement of Dimensions 108 D3847-01(2012) Standard Practice for Rubber Directions for Achieving Subnormal Test Temperatures 109 D3848-03(2013) Standard Test Methods for Rubber Evaluation of NBR (Acrylonitrile-Butadiene Copolymers) Mixed With Carbon Black 110 D3849-14a Standard Test Method for Carbon Black Morphological Characterization of Carbon Black Using Electron Microscopy 111 D3853-12 Standard Terminology Relating to Rubber and Rubber Latices Abbreviations for Chemicals Used in Compounding 112 D3896-07(2011) Standard Practice for Rubber From Synthetic Sources Sampling Standard Test Methods for Rubber-Determination of Ethylene Units in Ethylene-Propylene 113 D3900-05a(2010) Copolymers (EPM) and in Ethylene-Propylene-Diene Terpolymers (EPDM) by Infrared Spectrometry 114 D3958-06(2011) Standard Test Methods for Rubber Evaluation of BIIR and CIIR (Halogenated Isobutene Isoprene Rubber) 115 D4004-06(2012) Standard Test Methods for Rubber Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis 116 D4026-06(2012) Standard Test Method for Rubber Latex Styrene-Butadiene Copolymer Determination of Residual Styrene 117 D4075-06(2012) Standard Test Methods for Rubber Compounding Materials Flame Atomic Absorption Analysis Determination of Metals 118 D4122-10a(2015) Standard Practice for Carbon Black Evaluation of an Industry Reference Black 119 D4295-89(2012) Standard Classification for Rubber Compounding Materials Zinc Oxide 120 D4315-94(2012) Standard Test Methods for Rubber Compounding Material Zinc Oxide 121 D4482-11 Test Method for Rubber Property - Extension Cycling Fatigue 122 D4483-14a Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries 123 D4527-99(2011) Standard Test Method for Carbon Black - Solvent Extractables 124 D4528-88(2012) Standard Classification for Rubber Compounding Materials Sulfur 125 D4569-06(2012) Standard Test Method for Rubber Compounding Materials Determination of Acidity in Sulfur 126 D4570-02(2012) Standard Test Method for Rubber Chemicals Determination of Particle Size of Sulfur by Sieving (Dry) 127 D4571-06(2012) Standard Test Methods for Rubber Compounding Materials Determination of Volatile Material 128 D4572-89(2012) Standard Test Method for Rubber Chemicals Wet Sieve Analysis of Sulfur 129 D4573-03(2014) Standard Test Method for Rubber Chemicals Determination of Oil Content in Oil-Treated Sulfur 130 D4574-06(2012) Standard Test Methods for Rubber Compounding Materials Determination of Ash Content 131 D4575-09 Standard Test Methods for Rubber Deterioration Reference and Alternative Method(s) for Determining Ozone Level in Laboratory Test Chambers 132 D4578-06(2012) Standard Test Methods for Rubber Chemicals Determination of Percent Sulfur by Extraction 3/5

133 D4583-95(2015) Standard Practice for Carbon Black Calculation of Process Indexes From an Analysis of Process Control Data 134 D4620-02(2012) Standard Test Method for Evaluating the Effective Surface Area of Zinc Oxide in Rubber 135 D4676-94(2012) Standard Classification for Rubber Compounding Materials Antidegradants 136 D4677-87(2013) Standard Classification for Rubber Compounding Materials Titanium Dioxide 137 D4678-11 Standard Practice for Rubber - Preparation, Testing, Acceptance, Documentation, and Use of Reference Materials 138 D4817-88(2012) Standard Classification for Rubber Compounding Materials Stearic Acid 139 D4818-89(2012) Standard Classification for Rubber Compounding Materials Vulcanization Accelerators 140 D4821-15 Standard Guide for Carbon Black Validation of Test Method Precision and Bias 141 D4924-89(2012) Standard Classification for Petroleum Waxes for Use in Rubber Compounding 142 D4934-02(2012) Standard Test Method for Rubber Compounding Materials: 2-Benzothiazyl Sulfenamide Accelerators Insolubles 143 D4936-10 Standard Test Method for Mercaptobenzothiazole Sulfenamide Assay by Reduction/Titration 144 D4937-96(2012) Standard Test Method for p-phenylenediamine Antidegradants Purity by Gas Chromatography 145 D5044-06(2012) Standard Test Method for Rubber Compounding Materials Free 2-Mercaptobenzothiazole (MBT) in Benzothiazyl Disulfide (MBTS) 146 D5051-06(2012) Standard Test Method for Rubber Compounding Materials Benzothiazyl Disulfide (MBTS) Assay 147 D5054-90(2014) Standard Test Method for Rubber Chemicals Diphenyl Guanidine (DPG) and Di-o-tolylguanidine (DOTG) Assay 148 D5099-08(2013) Standard Test Methods for Rubber Measurement of Processing Properties Using Capillary Rheometry 149 D5230-14 Standard Test Method for Carbon Black Automated Individual Pellet Hardness 150 D5289-12 Standard Test Method for Rubber Property Vulcanization Using Rotorless Cure Meters 151 D5297-95(2014) Standard Test Methods for Rubber Chemical Accelerator Purity by High Performance Liquid Chromatography 152 D5376-06(2012) Standard Test Method for Rubber Compounding Materials Determination of the Basic Nitrogen Content in Rubber Antioxidant: Polymerized TMQ 153 D5377-93(2012) Standard Classification for Rubber Compounding Materials Ground Coal 154 D5406-93(2011) Standard Practice for Rubber - Calculation of Producer's Process Performance Indexes 155 D5460-02(2012) Standard Test Method for Rubber Compounding Materials Water in Rubber Additives 156 D5461-06(2012) Standard Test Method for Rubber Compounding Materials Wet Sieve Analysis of Powdered Rubber Compounding Materials 157 D5538-13 Standard Practice for Thermoplastic Elastomers Terminology and Abbreviations 158 D5603-01(2008) Standard Classification for Rubber Compounding Materials Recycled Vulcanizate Particulate Rubber 159 D5604-96(2012) Standard Test Methods for Precipitated Silica Surface Area by Single Point B.E.T. Nitrogen Adsorption 160 D5605-94(2011) Standard Practice for Styrene-Butadiene Rubber (SBR) Establishing Raw Mooney Viscosity Target Values 161 D5644-01(2013) Standard Test Methods for Rubber Compounding Materials Determination of Particle Size Distribution of Recycled Vulcanizate Particulate Rubber 162 D5666-95(2014) Standard Test Method for Rubber Chemical Antidegradants Purity of p -Phenylenediamine (PPD) Antidegradants by High Performance Liquid Chromatography 163 D5667-95(2010) Standard Test Method for Rubber From Synthetic Sources-Total and Water Soluble Ash 164 D5668-09(2014) Standard Test Methods for Rubber From Synthetic Sources Volatile Matter 165 D5670-95(2014) Standard Test Method for Rubber Determination of Residual Unsaturation in Hydrogenated Nitrile Rubber (HNBR) by Infrared Spectrophotometry 166 D5774-95(2014) Standard Test Methods for Rubber Chemical Analysis of Extractables 167 D5775-95(2014) Standard Test Method for Rubber Determination of Bound Styrene in Styrene Butadiene Rubber by Refractive Index 168 D5805-00(2014) Standard Test Methods for Rubber Determination of Carbon Black in Masterbatches 169 D5817-03a(2014) Standard Practice for Carbon Black, Pelleted Reduction, Blending, and Drying of Gross Samples for Testing 170 D5899-98(2013) Standard Classification System for Rubber Compounding Materials for Use in Computer Material Management Systems 171 D5900-14a Standard Specification for Physical and Chemical Properties of Industry Reference Materials (IRM) 4/5

172 D5902-05(2010) Standard Test Method for Rubber-Determination of Residual Unsaturation in Hydrogenated Nitrile Rubber (HNBR) by Iodine Value 173 D5963-04(2010)e1 Standard Test Method for Rubber Property Abrasion Resistance (Rotary Drum Abrader) 174 D5964-07(2014) Standard Practice for Rubber IRM 901, IRM 902, and IRM 903 Replacement Oils for ASTM No. 1, ASTM No. 2, and ASTM No. 3 Oils 175 D5992-96(2011) Standard Guide for Dynamic Testing of Vulcanized Rubber and Rubber-Like Materials Using Vibratory Methods 176 D6047-99(2014) Standard Test Methods for Rubber, Raw Determination of 5-Ethylidenenorbornene (ENB) or Dicyclopentadiene (DCPD) in Ethylene-Propylene-Diene (EPDM) Terpolymers 177 D6048-07(2012) Standard Practice for Stress Relaxation Testing of Raw Rubber, Unvulcanized Rubber Compounds, and Thermoplastic Elastomers 178 D6049-03(2013) Standard Test Method for Rubber Property Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates 179 D6085-97(2011) Standard Practice for Sampling in Rubber Testing - Terminology and Basic Concepts 180 D6147-97(2014) Standard Test Method for Vulcanized Rubber and Thermoplastic Elastomer Determination of Force Decay (Stress Relaxation) in Compression 181 D6204-12 Standard Test Method for Rubber Measurement of Unvulcanized Rheological Properties Using Rotorless Shear Rheometers 182 D6370-99(2014) Standard Test Method for Rubber Compositional Analysis by Thermogravimetry (TGA) 183 D6556-14 Standard Test Method for Carbon Black Total and External Surface Area by Nitrogen Adsorption 184 D6600-00(2013) Standard Practice for Evaluating Test Sensitivity for Rubber Test Methods 185 D6601-12 Standard Test Method for Rubber Properties Measurement of Cure and After-Cure Dynamic Properties Using a Rotorless Shear Rheometer 186 D6602-13 Standard Practice for Sampling and Testing of Possible Carbon Black Fugitive Emissions or Other Environmental Particulate, or Both 187 D6738-11 Standard Test Method for Precipitated Silica - Volatile Content 188 D6739-11 Standard Test Method for Silica - ph Value 189 D6740-10 (triethoxysilylpropyl)sulfanes): Residue on Ignition 190 D6741-10 Standard Test Methods for Silanes Used in Rubber Formulations (bis- (triethoxysilylpropyl)sulfanes): Sulfur Content 191 D6746-10 Standard Test Method for Determination of Green Strength and Stress Relaxation of Raw Rubber or Unvulcanized Compounds 192 D6814-02(2013) Standard Test Method for Determination of Percent Devulcanization of Crumb Rubber Based on Crosslink Density 193 D6843-10 (triethoxysilylpropyl)sulfanes): Characterization by Gas Chromatography (GC) 194 D6844-10 (triethoxysilylpropyl)sulfanes): Characterization by High Performance Liquid Chromatography (HPLC) 195 D6845-12 Standard Test Method for Silica, Precipitated, Hydrated CTAB (Cetyltrimethylammonium Bromide) Surface Area 196 D6854-12a Standard Test Method for Silica-Oil Absorption Number 197 D6915-12 Standard Practice for Carbon Black Evaluation of Standard Reference Blacks 198 D7050-04(2014) Standard Practice for Rubber from Natural Sources Sampling and Sorting Bales Based on Predicted Processing Properties 199 D7121-05(2012) Standard Test Method for Rubber Property Resilience Using Schob Type Rebound Pendulum 200 D7426-08(2013) Standard Test Method for Assignment of the DSC Procedure for Determining Tg of a Polymer or an Elastomeric Compound 201 D7605-11 Standard Test Method for Thermoplastic Elastomers - Measurement of Polymer Melt Rheological Properties and Congealed Dynamic Properties Using Rotorless Shear Rheometers 202 D7633-13 Standard Test Method for Carbon Black Carbon Content 203 D7662-13 Standard Test Method for Carbon Content in Carbon Black Feedstock Oils 204 D7679-13 Standard Test Method for Sulfur Content in Carbon Black Feedstock Oils 205 D7723-11 Standard Test Method for Rubber Property - Macro-Dispersion of Fillers in Compounds 206 D7724-11 Standard Test Method for Carbon Black - Non-Dispersible Matter by Mechanical Flushing (NDM) 207 D7771-15 Standard Test Method for Determination of Benzo-α-Pyrene (BaP) Content in Carbon Black 208 D7772-11 Standard Test Method for Carbon Black Extractables - Absorbance of Cyclohexane Extract 209 D7849-14 Standard Classification for Nomenclature of Reference Materials of Committee D24 210 D7854-13 Standard Test Method for Carbon Black-Void Volume at Mean Pressure 5/5