Appendix A Summary Report Surface Area BET Surface Area: 1555.9551 m²/g Langmuir Surface Area: 1992.1415 m²/g Pore Volume Single point adsorption total pore volume of pores 0.619747 cm³/g t-plot micropore volume: 0.060144 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.193811 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.9323 Å BJH Adsorption average pore diameter (4V/A): 18.593 Å Nanoparticle Size Average Particle Size 38.562 Å Fig. 1 Nitrogen adsorption for Activated Carbon from Norit 1
Summary Report Surface Area Single point surface area at P/Po = 0.151133404: 1196.6062 m²/g BET Surface Area: 1200.2944 m²/g Langmuir Surface Area: 1504.1602 m²/g t-plot Micropore Area: 571.0213 m²/g t-plot External Surface Area: 629.2731 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 189.928 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.876 Å diameter at P/Po = 0.151133404: 0.500884 cm³/g t-plot micropore volume: 0.246338 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.088274 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.6920 Å BJH Adsorption average pore diameter (4V/A): 18.591 Å Nanoparticle Size Average Particle Size 49.988 Å Fig. 2 Nitrogen adsorption for activated Charcoal from Fluka 2
Summary Report Surface Area Single point surface area at P/Po = 0.151166798: 1062.3665 m²/g BET Surface Area: 1090.8798 m²/g Langmuir Surface Area: 1380.6524 m²/g t-plot Micropore Area: 332.6326 m²/g t-plot External Surface Area: 758.2472 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 229.336 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.878 Å diameter at P/Po = 0.151166798: 0.444711 cm³/g t-plot micropore volume: 0.138101 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.106503 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.3065 Å BJH Adsorption average pore diameter (4V/A): 18.576 Å Nanoparticle Size Average Particle Size 55.001 Å Fig. 3 Nitrogen adsorption for activated charcoal from BDH 3
Summary Report Surface Area Single point surface area at P/Po = 0.151113013: 770.1104 m²/g BET Surface Area: 785.2020 m²/g Langmuir Surface Area: 991.3003 m²/g t-plot Micropore Area: 214.0961 m²/g t-plot External Surface Area: 571.1059 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 172.295 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.875 Å diameter at P/Po = 0.151113013: 0.322351 cm³/g t-plot micropore volume: 0.091300 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.080104 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.4213 Å BJH Adsorption average pore diameter (4V/A): 18.597 Å Nanoparticle Size Average Particle Size 76.413 Å Fig. 4 Nitrogen adsorption for graphene Nano plates 4
Summary Report Surface Area Single point surface area at P/Po = 0.151392493: 229.6773 m²/g BET Surface Area: 236.2158 m²/g Langmuir Surface Area: 299.7008 m²/g t-plot Micropore Area: 34.1599 m²/g t-plot External Surface Area: 202.0559 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 60.729 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.888 Å diameter at P/Po = 0.151392493: 0.096169 cm³/g t-plot micropore volume: 0.014373 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.028266 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.2850 Å BJH Adsorption average pore diameter (4V/A): 18.618 Å Nanoparticle Size Average Particle Size 254.005 Å Fig. 5 Nitrogen adsorption for MWCNTs 5
Summary Report Surface Area Single point surface area at P/Po = 0.151216723: 727.8770 m²/g BET Surface Area: 732.9392 m²/g Langmuir Surface Area: 920.2689 m²/g t-plot Micropore Area: 310.3816 m²/g t-plot External Surface Area: 422.5576 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 127.570 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.880 Å diameter at P/Po = 0.151216723: 0.304710 cm³/g t-plot micropore volume: 0.133802 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.059273 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.6295 Å BJH Adsorption average pore diameter (4V/A): 18.585 Å Nanoparticle Size Average Particle Size 81.862 Å Fig. 6 Nitrogen adsorption for carbon black 6
Summary Report Surface Area Single point surface area at P/Po = 0.151355046: 13.3808 m²/g BET Surface Area: 15.3720 m²/g Langmuir Surface Area: 20.5837 m²/g t-plot External Surface Area: 24.7364 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 11.734 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.887 Å diameter at P/Po = 0.151355046: 0.005603 cm³/g t-plot micropore volume: -0.004408 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.005699 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 14.5785 Å BJH Adsorption average pore diameter (4V/A): 19.428 Å Nanoparticle Size Average Particle Size 3903.193 Å Fig.7 Nitrogen adsorption for graphite powder 7
Summary Report Surface Area Single point surface area at P/Po = 0.150780111: 1724.1495 m²/g BET Surface Area: 1768.8221 m²/g Langmuir Surface Area: 2233.5608 m²/g t-plot Micropore Area: 696.9455 m²/g t-plot External Surface Area: 1071.8766 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 327.451 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.860 Å diameter at P/Po = 0.150780111: 0.721407 cm³/g t-plot micropore volume: 0.288768 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.151517 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.3138 Å BJH Adsorption average pore diameter (4V/A): 18.509 Å Nanoparticle Size Average Particle Size 33.921 Å Fig. 8 Nitrogen adsorption for extra activated carbon from Norit Extra 8
Summary Report Surface Area Single point surface area at P/Po = 0.150991905: 1496.9789 m²/g BET Surface Area: 1615.1025 m²/g Langmuir Surface Area: 2092.7808 m²/g t-plot External Surface Area: 1938.1714 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 584.131 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.870 Å diameter at P/Po = 0.150991905: 0.626512 cm³/g t-plot micropore volume: -0.157661 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.271661 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.5163 Å BJH Adsorption average pore diameter (4V/A): 18.603 Å Nanoparticle Size Average Particle Size 37.149 Å Fig. 9 Nitrogen adsorption for activated carbon from Norit after treatment 9
Summary Report Surface Area Single point surface area at P/Po = 0.151229555: 1913.5425 m²/g BET Surface Area: 1962.8472 m²/g Langmuir Surface Area: 2483.8031 m²/g t-plot Micropore Area: 581.3012 m²/g t-plot External Surface Area: 1381.5460 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 417.499 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.881 Å diameter at P/Po = 0.151229555: 0.801076 cm³/g t-plot micropore volume: 0.242380 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.193913 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.3248 Å BJH Adsorption average pore diameter (4V/A): 18.579 Å Nanoparticle Size Average Particle Size 30.568 Å Fig 10 Nitrogen adsorption for activated charcoal from Fluka after treatment 10
Summary Report Surface Area Single point surface area at P/Po = 0.150855688: 992.7042 m²/g BET Surface Area: 1006.0253 m²/g Langmuir Surface Area: 1265.0903 m²/g t-plot Micropore Area: 404.3515 m²/g t-plot External Surface Area: 601.6738 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 182.539 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.863 Å diameter at P/Po = 0.150855688: 0.415398 cm³/g t-plot micropore volume: 0.172242 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.084689 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.5164 Å BJH Adsorption average pore diameter (4V/A): 18.558 Å Nanoparticle Size Fig. 11 Nitrogen adsorption activated Charcoal BDH after treatment 11
Summary Report Surface Area Single point surface area at P/Po = 0.151343274: 873.0223 m²/g BET Surface Area: 889.1512 m²/g Langmuir Surface Area: 1122.5004 m²/g t-plot Micropore Area: 266.0594 m²/g t-plot External Surface Area: 623.0918 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 187.477 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.886 Å diameter at P/Po = 0.151343274: 0.365527 cm³/g t-plot micropore volume: 0.113356 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.087214 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.4438 Å BJH Adsorption average pore diameter (4V/A): 18.608 Å Nanoparticle Size Average Particle Size 67.480 Å Fig 12 Nitrogen adsorption for graphene nanoplates after treatment 12
Summary Report Surface Area Single point surface area at P/Po = 0.151266467: 306.5722 m²/g BET Surface Area: 315.0469 m²/g Langmuir Surface Area: 399.4910 m²/g t-plot Micropore Area: 46.7326 m²/g t-plot External Surface Area: 268.3143 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 80.614 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.883 Å diameter at P/Po = 0.151266467: 0.128347 cm³/g t-plot micropore volume: 0.019719 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.037533 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.2957 Å BJH Adsorption average pore diameter (4V/A): 18.624 Å Nanoparticle Size Average Particle Size 190.448 Å Fig. 13 Nitrogen adsorption for MWCNTs after treatment 13
Summary Report Surface Area Single point surface area at P/Po = 0.151121097: 1823.2883 m²/g BET Surface Area: 1886.0641 m²/g Langmuir Surface Area: 2395.6877 m²/g t-plot Micropore Area: 350.7967 m²/g t-plot External Surface Area: 1535.2674 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 463.561 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.876 Å diameter at P/Po = 0.151121097: 0.763195 cm³/g t-plot micropore volume: 0.142219 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.215415 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.1860 Å BJH Adsorption average pore diameter (4V/A): 18.588 Å Nanoparticle Size Average Particle Size 31.812 Å Fig. 14 Nitrogen adsorption for Carbon black after heat treatment 14
Summary Report Surface Area Single point surface area at P/Po = 0.151352234: 15.9715 m²/g BET Surface Area: 17.5314 m²/g Langmuir Surface Area: 22.9160 m²/g t-plot External Surface Area: 20.6877 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 6.174 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.887 Å diameter at P/Po = 0.151352234: 0.006687 cm³/g t-plot micropore volume: -0.001698 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.002882 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.2576 Å BJH Adsorption average pore diameter (4V/A): 18.670 Å Nanoparticle Size Average Particle Size 3422.435 Å Fig. 15 Nitrogen adsorption for graphite after treatment 15
Summary Report Surface Area Single point surface area at P/Po = 0.150554063: 1918.6543 m²/g BET Surface Area: 1969.5083 m²/g Langmuir Surface Area: 2485.9961 m²/g t-plot Micropore Area: 778.6096 m²/g t-plot External Surface Area: 1190.8987 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 364.902 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.849 Å diameter at P/Po = 0.150554063: 0.802577 cm³/g t-plot micropore volume: 0.322122 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.168705 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.3000 Å BJH Adsorption average pore diameter (4V/A): 18.493 Å Nanoparticle Size Average Particle Size 30.464 Å Fig. 16 Nitrogen adsorption for extra activated carbon Norit extra after treatment 16
Summary Report Surface Area Single point surface area at P/Po = 0.150735115: 2012.1380 m²/g BET Surface Area: 2088.3915 m²/g Langmuir Surface Area: 2650.7803 m²/g t-plot Micropore Area: 576.0703 m²/g t-plot External Surface Area: 1512.3212 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 461.669 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.858 Å diameter at P/Po = 0.150735115: 0.841861 cm³/g t-plot micropore volume: 0.231327 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.213716 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 16.1246 Å BJH Adsorption average pore diameter (4V/A): 18.517 Å Nanoparticle Size Average Particle Size 28.730 Å Fig. 17 Nitrogen adsorption for extra activated carbon from norit after treatment with optimizing the parameters. 17
Summary Report Surface Area Single point surface area at P/Po = 0.151116178: 2726.1651 m²/g BET Surface Area: 2926.9537 m²/g Langmuir Surface Area: 3785.1404 m²/g t-plot External Surface Area: 3421.0682 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 1030.251 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.876 Å diameter at P/Po = 0.151116178: 1.141115 cm³/g t-plot micropore volume: -0.243256 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.479249 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.5946 Å BJH Adsorption average pore diameter (4V/A): 18.607 Å Nanoparticle Size Average Particle Size 20.499 Å Fig. 18 Nitrogen adsorption for activated carbon Fluka after treatment more optimization 18
Fig. 19 FTIR for activated carbon from Norit 19
Fig.20 FTIR for activated carbon from Fluka 20
Fig.21 FTIR for activated carbon from BDH 21
Fig. 22 FTIR for graphene nano-plates 22
Fig. 23 FTIR for MWCNTs 23
Fig. 24 FTIR for carbon black 24
Fig. 25 FTIR for graphite 25
Fig. 26 FTIR for extra activated carbon from Norit 26
Fig. 27 TGA and DSC for activated carbon for Norit under flow of air 27
Fig. 28 TGA and DSC for activated charcoal from Fluka under flow of air 28
Fig 29 TGA and DSC for activated charcoal from BDH under flow of air 29
Fig 30 TGA and DSC for graphene under flow of air 30
Fig. 31 TGA and DSC for MWCNTs under flow of air 31
Fig. 32 TGA and DSC for carbon black under flow of air 32
Fig. 33 TGA and DSC for graphite under flow of air 33
Fig.34 TGA and DSC for extra activated carbon from Norit under flow of air 34
Fig. 35 XRD of activated carbon from Norit 35
Fig.36 XRD of activated carbon from Fluka 36
Fig 37 XRD of activated charcoal from BDH 37
Fig. 38 XRD of graphene 38
Fig. 39 XRD of MWCNTs 39
Fig. 40 XRD of Carbon black 40
Fig. 41 XRD of graphite 41
Fig 42 XRD of extra activated carbon from Norit extra 42
Fig. 43 Norit after heat treatment 43
Fig.44 Activated charcoal Fluka after heat treatment 44
Fig.45 Charcoal BDH after heat treatment 45
Fig.46 graphene after heat treatment 46
Fig.47 MWCNTs after heat treatment 47
Fig. 48 Carbon black after heat treatment 48
Fig.49 graphite after heat treatment 49
Fig. 50 Norit extra after heat-treatment 50
Summary Report Surface Area Single point surface area at P/Po = 0.151285970: 1073.5400 m²/g BET Surface Area: 1135.9289 m²/g Langmuir Surface Area: 1459.1441 m²/g t-plot External Surface Area: 1185.2167 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 356.835 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.883 Å diameter at P/Po = 0.151285970: 0.449451 cm³/g t-plot micropore volume: -0.030228 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.166010 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.8267 Å BJH Adsorption average pore diameter (4V/A): 18.609 Å Nanoparticle Size Average Particle Size 52.820 Å Fig. 51 Nitrogen adsorption for impregnated sucrose within the CBV 600 51
Fig 52 XRD of impregnated Sucrose Activated carbon within CBV 600 52
Summary Report Surface Area Single point surface area at P/Po = 0.151295466: 1306.9569 m²/g BET Surface Area: 1372.5600 m²/g Langmuir Surface Area: 1756.6389 m²/g t-plot Micropore Area: 57.7062 m²/g t-plot External Surface Area: 1314.8538 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 396.331 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.884 Å diameter at P/Po = 0.151295466: 0.547180 cm³/g t-plot micropore volume: 0.015168 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.184283 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.9463 Å BJH Adsorption average pore diameter (4V/A): 18.599 Å Nanoparticle Size Average Particle Size 43.714 Å Fig. 53 Nitrogen adsorption for impregnated F.A within the CBV 600 53
Fig 54 XRD of impregnated F.A Activated carbon within CBV 600 54
Fig. 55 SEM of the templated carbon within CBV 600 55
Summary Report Surface Area Single point surface area at P/Po = 0.151389328: 705.2684 m²/g BET Surface Area: 746.5925 m²/g Langmuir Surface Area: 959.3001 m²/g t-plot External Surface Area: 763.1117 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 229.735 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.888 Å diameter at P/Po = 0.151389328: 0.295306 cm³/g t-plot micropore volume: -0.013520 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.106856 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.8215 Å BJH Adsorption average pore diameter (4V/A): 18.605 Å Nanoparticle Size Average Particle Size 80.365 Å Fig. 56 Nitrogen adsorption for impregnated sucrose within the ZSM-5 56
Fig. 57 XRD of sucrose within the ZSM-5 57
Summary Report Surface Area Single point surface area at P/Po = 0.151384933: 826.2274 m²/g BET Surface Area: 865.0493 m²/g Langmuir Surface Area: 1105.7208 m²/g t-plot Micropore Area: 72.1642 m²/g t-plot External Surface Area: 792.8851 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 238.718 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.888 Å diameter at P/Po = 0.151384933: 0.345951 cm³/g t-plot micropore volume: 0.025083 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.111030 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.9968 Å BJH Adsorption average pore diameter (4V/A): 18.604 Å Nanoparticle Size Average Particle Size 69.360 Å Fig.58 Nitrogen adsorption for impregnated F.A within the ZSM-5 58
Fig. 59 XRD of F.A within the ZSM-5 59
Summary Report Surface Area Single point surface area at P/Po = 0.151230250: 1114.7809 m²/g BET Surface Area: 1175.8778 m²/g Langmuir Surface Area: 1506.2498 m²/g t-plot Micropore Area: 133.3230 m²/g t-plot External Surface Area: 1042.5548 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 315.513 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.881 Å diameter at P/Po = 0.151230250: 0.466687 cm³/g t-plot micropore volume: 0.045197 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.146454 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.8753 Å BJH Adsorption average pore diameter (4V/A): 18.567 Å Nanoparticle Size Average Particle Size 51.026 Å Fig. 60 Nitrogen adsorption of CVD deposited Triethylamine within CBV 780 60
Fig. 61 XRD of CVD deposited Triethylamine within CBV-780 61
Summary Report Surface Area Single point surface area at P/Po = 0.151297401: 672.1664 m²/g BET Surface Area: 713.9428 m²/g Langmuir Surface Area: 918.9476 m²/g t-plot External Surface Area: 763.5136 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å diameter: 229.352 m²/g Pore Volume Single point adsorption total pore volume of pores less than 19.884 Å diameter at P/Po = 0.151297401: 0.281415 cm³/g t-plot micropore volume: -0.027670 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å diameter: 0.106765 cm³/g Pore Size Adsorption average pore width (4V/A by BET): 15.7668 Å BJH Adsorption average pore diameter (4V/A): 18.620 Å Nanoparticle Size Average Particle Size 84.040 Å Fig. 62 Nitrogen adsorption of CVD deposited Triethylamine within silica gel 62
Fig. 63 XRD of CVD deposited Triethylamine within silica gel 63