ISO TC22/SC41 Specific aspects for gaseous fuels

ISO TC22/SC41 Specific aspects for gaseous fuels Paul Dijkhof Kiwa Nederland B.V., Apeldoorn, The Netherlands

Content of this presentation Update on ISOTC22/SC41 Introduction ISO standard in LNG Request for new topics in R67 and R110 2

Update on ISO TC22/SC41 Update on ISOTC22/SC41 (formally known as ISOTC22/SC25) ISO TC22/SC41 WG3 Fuel system components and refueling connector for vehicles propelled by gaseous fuel WG4 Fuel system components and refueling connector for vehicles propelled by Liquefied Natural Gas (LNG) WG5 Fuel system components and refueling connector for vehicles propelled by gaseous hydrogen or by blends of hydrogen and methane WG6 Fuel system components and refueling connector for vehicles propelled by Liquefied Petroleum Gas (LPG) WG7 General safety requirements for gas fuelled vehicles 3

WG3 Fuel system components and refueling connector for vehicles propelled by gaseous fuel Revision/Update on ISO15500 parts. Adding non-metallic material test from ECE R110 Editorial Revision of ISO14469 part 2 (new working item request part 1) 4

WG4 Fuel system components and refueling connector for vehicles propelled by Liquefied Natural Gas (LNG) Published ISO12617:2015 LNG receptacle Published ISO12614:2014 Road vehicles -- Liquefied natural gas (LNG) fuel system components Part 1: General requirements and definitions Part 2: Performance and general test methods Part 3: Check valve Part 4: Manual valve Part 5: Tank pressure gauge Part 6: Overpressure regulator Part 7: Pressure relief valve Part 8: Excess flow valve Part 9: Gas-tight housing and ventilation hose Part 10: Rigid fuel line in stainless steel Part 11: Fittings Part 12: Rigid fuel line in copper and its alloys Part 13: Pressure control regulator Part 14: Differential pressure fuel content gauge Part 15: Capacitance fuel content gauge Part 16: Heat exchanger vaporizer Part 17: Natural gas detector Part 18: Gas temperature sensor 5

WG5 Fuel system components and refueling connector for vehicles propelled by gaseous hydrogen or by blends of hydrogen and methane Working on ISO12619 Road vehicles Compressed Gaseous Hydrogen (CGH2) and Hydrogen/ Methane blends fuel system components Published in 2014 ISO12619 Part 1 General requirements and definitions ISO12619 Part 2 Performance and general test methods ISO12619 Part 3 Pressure regulator ISO16380 Road vehicles -- Blended fuels refueling connector Work in progress on the following: ISO12619 Part 4: Check valve ISO12619 Part 5: Manual cylinder valve 6

WG6 Fuel system components and refueling connector for vehicles propelled by Liquefied Petroleum Gas (LPG) ISO/WD 19825 Road vehicles - Liquefied Petroleum Gas (LPG) refueling connector ISO/NWIP 20766: Road vehicles Liquefied Petroleum Gas (LPG) fuel system components Part 1: General requirements and definitions active Part 2: Performance and general test methods active Part 3: Check valve not yet started Part 4: Manual valve not yet started Part 5: Manual tank valve not yet started Part 6: Automatic valve not yet started Part 7: Gas injector not yet started Part 8: Pressure indicator not yet started Part 9: Pressure regulator not yet started Part 10: Gas-flow adjuster not yet started Part 11: Gas/air mixer not yet started Part 12: Pressure relief valve (PRV) not yet started Part 13: Pressure relief device (PRD) not yet started Part 14: Excess flow valve not yet started Part 15: Gas-tight housing and ventilation hose not yet started Part 16: Rigid fuel line not yet started Part 17: Flexible fuel line not yet started Part 18: Filter not yet started Part 19: Fittings not yet started 7

WG7 General safety requirements for gas fuelled vehicles ISO15501-2 Road vehicles -- Compressed natural gas (CNG) fuel systems -- Part 2: Test methods under revision ISO/AWI 19723-1 Road vehicles -- Liquefied natural gas (LNG) fuel systems -- Part 1: Safety requirements ISO/AWI 19723-2 Road vehicles -- Liquefied natural gas (LNG) fuel systems -- Part 2: Test methods New working item proposal for ISOxxxxx covering Compressed Gaseous Hydrogen (CGH2) and Hydrogen/Natural Gas blends as use for vehicle fuel. Part 1: Safety requirements Part 2: Test methods 8

LNG Task Force Introduction ISO standard in LNG During the LNG Task force meetings was agreed to introduce the requirements from ISO12617:2015 LNG receptacle introduction using the example of the CNG nozzle (ISO14469) Reason for introduction: Uniform Profile of the receptacle Requirements in line with what is currently in ECE R110 for the CNG receptacle. 9

Request for new topics in R67 Request from OEM to update the R67 requirements on the fuel line and welding requirement. (see next sheets for explanation) 10

PROPOSAL: APPROVAL OF USING AUTOMOTIVE STEEL TUBING BRAKE SYSTEM LINES AS RIGID LIQUEFIED PETROLEUM GASES LINES DRAFT GME Engineering

Proposed amendment to ECE REGULATION No. 67 APPROVAL OF USING AUTOMOTIVE STEEL TUBING BRAKE SYSTEM LINES AS RIGID LIQUEFIED PETROLEUM GASES LINES Proposal: Part II, para 17.8.1 17.8. Gas connections between the components of the LPG-system 17.8.1. Soldered or welded joints and bite-type compression joints are not permitted. Soldering or welding can be permitted for connecting the individual parts of detachable couplings to the gas tube or component. DRAFT GME Engineering

Justification for the proposal Double Wall steel tubing used for brake lines are feasible for much more than 67 bar. Overall, Parameters are set very high due to Safety and Quality issues that valued by GMW14658. From our point of view it makes sense to qualify more parts for the LPG usage regarding the Class 1. We all would gain more products on market which are feasible for us. Double Wall Tubes are already known in brake and fuel tubing applications and allows the whole variety of end forms and coupling techniques. Due to their usage they have to withstand high pressure and a high resistance for pressure pulses. From our experience the LPG pressure pulses are very much less strength than in brake lines. DRAFT Hence the amendment is proposed for more clarity and flexibility in the regulation for suppliers and customers and would help the commercialization process of LPG lines. GME Engineering

Brake lines Form & Size Minimum Requirements: Rm 0.2% Yield Strength Rp0.2 300 MPa 200 MPa Fracture Elongation A10 14% DRAFT ECE R67-01: max. 6,7 MPa GME Engineering

Brake Tube Coatings Over-View Name NyGal Metallic Protection Layer (C.) Galfan Layering Key (example) A. ALUMINUM FOIL (when used) B. NYLON C. Aluminum Rich Epoxy Paint (E), Electroplated Zinc (Z) or Zinc-aluminumalloy (G) D. STEEL SUBSTRATE Organic top coating (B.) NyAl Aluminum Extruded Nylon European Standard PA12, PA612 ( PA11 ) Remarks DRAFT Impl. in the USA since 1998 No introduction in europe planned NyZn Zinc European Standard GME Engineering

Process Mapping-Brake lines Outside Inside DRAFT =ZN finish =AN finish Source: TI automotive GME Engineering

Manufacturing Process (1) -DW Strip constructs Outside Strip (Copper plated steel preferred) is wound in longitudinal direction by rollingdrawing process to a double wall tubing, so that the appropriate processed longitudinal edges of the strip are overlapping. the tubing shall be copper brazed in a reducing atmosphere. Inside Outside Inside Outside DRAFT Inside Source: TI automotive GME Engineering

Manufacturing Process (2) NyAl NyZn DRAFT Source: TI automotive GME Engineering

Quality (GMW 14658) GM internal requirement Automotive steel tubing shall, and be commercially round, smooth and free from rust and defects. not exceed outside diameter tolerance not interfere with flare forming operation or with the accomplishment of leak-tight coupling joints when specific lengths are specified, reasonably straight, and ends shall be free from burrs DRAFT withstand internal cleanliness conforming to a maximum of 0.20 g per square meter of internal surface, determined by a test. GME Engineering

Detail of GMW 14658 - Summary of Requirements (1) DRAFT GME Engineering

Detail of GMW 14658 - Summary of Requirements (2) DRAFT GME Engineering

Request for new topics in R110 Request from OEM to update the ECE R110 with the following changes on couplings of hoses. 11

Submitted by the expert from Informal document GRSG-109- (109th GRSG, 29 September 2 October 2015, agenda item 11) Proposal for amendments to Regulation No. 110 (Specific components for CNG) The aim of this proposal is to allow Class 0 hoses with couplings using sealing technologies other than with 45 cone. I. Proposal Annex 4B, Paragraph 1.6.2.2., amend to read: "1.6.2.2 The sealing cone of swivel-nut type shall be of the type with a half vertical angle of 45.The interface type for the hose coupling shall be chosen as to comply with the tests described in Paragraph 1.7, as well as tests mentioned in Annexes 5A and 5B. In case of an interface type using a soft seal body (e.g. O ring), the type of material chosen shall be tested in accordance with Annexes 5D, 5F and 5G." II. Justification 1. Avoid design restrictive requirements, and have performance oriented regulation. 2. State of the art: other technologies than metal/metal with 45 cone can provide an adequate level of safety and durability. R110 should allow these technologies, as long as the hose assembly can withstand the impulse test of 1.7 and tests of Annexes 5A (overpressure test) and 5B (external leakage test). 3. When using soft seal body (e.g. O ring), the compatibility of the material with use conditions has to be demonstrated. This is done by testing according to Annexes 5D (CNG/LNG compatibility test), Annex 5F (resistance to dry heat) and Annex 5G (ozone ageing).

2 Sealing concepts for rigid and flexible fluid systems O-Ring Face Seal Vs. 45 degree conical face

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Errors in current regulation 110 Part 7.1.of paragraphs 8.12 to 8.21. of.. - Of paragraphs 8.12 to 8.22. of. Part 8.1.1. electromagnetic compatibility (EMC) requirements according to Regulation No. 10, 03 series of amendments, or equivalent. Current version of ECE R10 is revision 5 Annex 4A: double definition for class 1: 4.2.2. The pressure relief valve and pressure relief device of Class 1 shall be so designed as to be leak-proof at a pressure of 1.5 times the working pressure (MPa) with the outlet closed off (see Annex 5B). 4.2.3. The pressure relief valve of Class 1 and Class 2 shall be so designed as to be leak-proof at twice the working pressure with the outlets closed off. 12

Errors in current regulation 110 18.6.1.2. The automatic valve shall be operated such that the fuel supply is cut off when the engine is switched off, irrespective of the position of the ignition switch, and shall remain closed while the engine is not running. A delay of 2 seconds is permitted for diagnostic. Annex 4H 2.2. The switching off delay of the automatic valve after stalling of the engine may not be more than 5 seconds. 13

Thank you for your attention! Questions? 14

Kiwa, Team Automotive Paul Dijkhof Paul.Dijkhof@kiwa.com +31 6 55 5393 228 15