Centar za ekotoksikološka ispitivanja d.o.o Laboratorija za ekotoksikološka ispitivanja i zaštitu od zračenja Bulevar Šarla de Gola br.

Transcription

1 ` Dodatak Sertifikatu o akreditaciji sa akreditacionim brojem Li Annex to Accreditation Certificate - Accreditation Number Li Standard: MEST EN ISO IEC 17025: 2011 Datum dodjele/ obnavljanja akreditacije: Date of granting/ renewal of accreditation / Akreditacija važi do: Accreditation is valid to: Akreditovana laboratorija za ispitivanje Accredited laboratory of testing Centar za ekotoksikološka d.o.o Laboratorija za ekotoksikološka i zaštitu od zračenja Bulevar Šarla de Gola br. 2, Podgorica Centre for ecotoxicological research Laboratory for ecotoxicological research and radiation protection Street Šarla de Gola, Podgorica Područje akreditacije / Scope of accreditation: Fizičko-hemijska : voda za piće-led, ribe, rakovi i proizvodi od riba, meso, mlijeko, med, žita i mlinski proizvodi, proizvodi od voća i povrća, kakao proizvodi, proizvodi slični čokoladi, bombonski proizvodi, krem proizvodi, keks i proizvodi srodni keksu, meso i mesni proizvodi,hrana biljnog i životinjskog porijekla,hrana za životinje, vode za piće i površinske vode, povrće i voće, biološki materijal (urin,serum, plazma), alkoholna pića, pivo i vino,sokovi,sirupi i osvježavajuća bezalkoholna pića, vazduh,sediment, zemljište, vode i otpadne vode,otpad,transformatorska ulja Ispitivanje radioaktivnosti u uzorcima: voda, vazduh, zemljište, hrana, gradevinski materijal Ispitivanje nivoa spoljašnjeg zračenja, Ispitivanje izvora jonizujuceg zračenja Akusticko ispitivanje buke Uzorkovanje: površinskih voda i vode za piće, tečnosti i zapaljivih tečnosti,zemlje, sedimenata i mulja Ispitivanje emisije iz stacionarnih izvora - vazduh izdanje /izmjena 1/2 Datum: /94

2 Physical-chemical s: drinking water and ice,fish, crabs and fish products,meat,milk,honey,cereals and milled products,products of fruits and vegetables, cocoa products, like chocolate products, confectionery, cream products, cakes biscuits and similar products, meat and meat products, food plant and animal origin,food for animals, drinking water and surface water, vegetables and fruits,biological material (urine, serum, plasma),alcoholic beverages, beer and wine,juices, syrups and non-alcoholic beverages,air,sediment/soil,water and waste water,waste, transformer oil Radioactivity s in samples: water, air, soil, food, building material Analyses of external radiation levels, Analyses of ionizing radiation sources, Acoustic examination of noise, Sampling: surface and drinking water, liquids and inflammable liquids, soil, sediment and sludge Testing of emissions from stationary sources - air izdanje /izmjena 1/2 Datum: /94

3 1 Detaljan obim akreditacije/ Detailed scope of accreditation Mjesto : Laboratorija za ekotoksikološka i zaštitu od zracenja, Bulevar Šarla de Gola br.2, Podgorica i/ ili na terenu * se sprovodi na terenu ** se sprovodi u Laboratoriji i na terenu VODA ZA PIĆE-LED DRINKING WATER AND ICE s measurement uncertainty- 1 2 **Određivanje mutnoće turbidity L.D.: 0,1 NTU U: 5,52% ** Određivanje temperature temperature Opseg: C C U: C Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, strana 118 Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, page 118 (ASTM D B) Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, strana 111 Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, page 111 izdanje /izmjena 1/2 Datum: /94

4 measurement uncertainty- VODA ZA PIĆE-LED DRINKING WATER AND ICE s **Određivanje ph ph Opseg: 0 14 U: 3.66% **Određivanje elektroprovodljivosti electroconductivity L.D.: 0,1 μs/cm U: 0.56% Određivanje kalcijuma calcium L.D.: 0.8 mg/l U: 5.34% JUS HZ1.111 (1987) Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, strana 143 Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, page 143 (ASTM D ) Standard Methods for examination of water and wastewater 19 th edited by Andrew D. Eatonand Greenberg, 3500Ca D 6 7 Određivanje natrijuma sodium L.D.: 0,1 mg/l U: 6,65% Određivanje kalijuma potasium L.D.: 0,1 mg/l U: 10,15% Standard Methods for examination of water and wastewater 19 th edited by Andrew D. Eatonand Greenberg, 3500Na D Standard Methods for examination of water and wastewater 19 th edited by Andrew D. Eatonand Greenberg, 3500K D izdanje /izmjena 1/2 Datum: /94

5 measurement uncertainty- 8 Određivanje alkaliteta alkalinity L.D.: 5 mg CaCO 3 /l ili 1 ml 0,1 N HCl/l U: 14,76% JUS.HZ1.124 (1974 ) VODA ZA PIĆE-LED DRINKING WATER AND ICE s 9 Određivanje ukupne tvrdoće total hardness L.D.: 0,1 o dh U: 2,72% Standard Methods for examination of Water and Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg, 2340 izdanje /izmjena 1/2 Datum: /94

6 measurement uncertainty- VODA ZA PIĆE-LED DRINKING WATER AND ICE s Određivanje suvog ostatka dry residue L.D.: 5 mg/l U: 9,08% Određivanje nitrita nitrite L.D.: 0,005 mg/l U: 3,09% Određivanje nitrata nitrate L.D.: 0,04 mg/ U: 13,5% Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, strana 129 Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, page 129 (EPA ) Standard Methods for examination of water and wastewater 19 th edited by Andrew D. Eatonand Greenberg, 4500-NO 2 B, Colorimetric method Standard Methods for examination of water and wastewater 19 th edited by Andrew D. Eatonand Greenberg, 4500NO 3 -B. UV spectrophotometric screening method izdanje /izmjena 1/2 Datum: /94

7 measurement uncertainty- VODA ZA PIĆE-LED DRINKING WATER AND ICE s Određivanje amonijaka ammonia L.D.: 0,02 mg/l U: 14,34% Određivanje azota po Kjeldalu nitrogen Kjeldahl L.D.: 3 mg/l U: 11,1% Određivanje trihalometana trichalometane L.D.: mg/l U: 10.25% 13.78% Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, strana 179 Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, page 179 (ASTM D ) Handbook for Kjeldahl digestion a recent review of the classical method with improvements, Developed by Tecator, 2 nd edition, May Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 6232B izdanje /izmjena 1/2 Datum: /94

8 measurement uncertainty- VODA ZA PIĆE-LED DRINKING WATER AND ICE s Određivanje mineralnih ulja petrol oil L.D.: 0,0025 mg/l U: 30,8% Određivanje ukupnih ulja i masti total oil and fat L.D.: 0,0025 mg/l U: 23,68% Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, strana 430 Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, page 430 (ASTM D ) Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, strana 563 Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, page 563 (ASTM D ) izdanje /izmjena 1/2 Datum: /94

9 measurement uncertainty Određivanje fenola phenols L.D.: 0,0005 mg/l U: 12,32% Određivanje gvožđa iron L.D.: 0,005 mg/l U: 24,56% Određivanje mangana manganese L.D.: 0,0025 mg/l U: 9,53% Određivanje bakra copper L.D.: 0,0025 mg/l U: 12,26% Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, strana 299, Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, page 299 (ASTM D 1783-B) Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500Fe B Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500Mn B Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500Cu B izdanje /izmjena 1/2 Datum: /94

10 measurement uncertainty- 22 Određivanje cinka Zinc L.D.: 0,0025 mg/l U: 9,22% Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500 Zn B VODA ZA PIĆE-LED DRINKING WATER AND ICE s 23 Određivanje fosfata phosphate L.D.: 0,01 mg/l P U: 17,03% Standard methods for the Examination of Water and Wastewater 19th edition, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg P D 24 Određivanje fluorida fluorides L.D.: 0,02 mg/l U: 12,26% Voda za piće-standardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, jon selektivna elektroda, str 326 Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, ion selective electrodes, page 326 (ASTM D ) izdanje /izmjena 1/2 Datum: /94

11 measurement uncertainty- VODA ZA PIĆE-LED DRINKING WATER AND ICE s Određivanje kobalta cobalt L.D.: 0,0025 mg/l U: 14,03% Određivanje barijuma barium L.D.: 0,001 mg/l U: 10,5% Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500 CoB Atomic absorption spectrophotometry Cookbook Section 5a Measuring conditions of relevant elements in drinking water (according to German drinking water Rulebook), page 21 VODA ZA PIĆE-LED DRINKING WATER AND ICE s 27 Određivanje kadmijuma cadmium 1. L.D.: 0,0005 mg/l U: 9,46% 2. L.D.: 0,0002 mg/l U: 21,62% 1. Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500 Cd B 2. Atomic absorption spectrophotometry Cookbook Section 5a Measuring conditions of relevant elements in drinking water (according to DIN E19-2), page 13 izdanje /izmjena 1/2 Datum: /94

12 measurement uncertainty- VODA ZA PIĆE-LED DRINKING WATER AND ICE s 28 Određivanje cijanida cianides 1.L.D.:. 0,005mg/l U: 12,42% 2..L.D.: 0,03 mg/l U: 10,78% 1.Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 4500 CN-C 2.Voda za pićestandardne metode za ispitivanje higijenske ispravnosti, Beograd 1990, Savezni zavod za zdrastvenu zaštitu, Jon selektivna elektroda str Drinking water Standard methods for hygienic testing, Belgrade 1990, the Federal Bureau for health protection, ion selective electrodes,page 277 (ASTM D ) 29 Određivanje hromaukupni total chromium L.D.: 0,005 mg/l U: 7,58% Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500Cr B izdanje /izmjena 1/2 Datum: /94

13 measurement uncertainty- 30 Određivanje arsena arsenic L.D.: 0,001 mg/l U: 20,5% Atomic absorption spectrophotometry Cookbook Section 4 Measuring conditions by element of furnace s method, Shimadzu corporation, page 10 VODA ZA PIĆE-LED DRINKING WATER AND ICE s Određivanje žive mercury L.D.: 0,0001 mg/l U: 9,62% Određivanje nikla nickel L.D.: 0,005 mg/l U: 7,56% Mercury in Hg Standard Solutions at the Lower Range Limit, Organic application note Leco AMA 254, Form no , Leco corporation, Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500Ni B izdanje /izmjena 1/2 Datum: /94

14 measurement uncertainty- VODA ZA PIĆE-LED DRINKING WATER AND ICE s Određivanje olova lead 1.L.D.: 0,005 mg/l U: 22,0% 2..L.D.: 0,005 mg/l U: 13,18% Određivanje antimona antimony L.D.: 0,005 mg/l U: 14,04% Određivanje selena selenium L.D.: 0,001 mg/l U: 14,86% 1. Standard Methods for examination of Water Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 3500 PbB 2. Atomic absorption spectrophotometry Cookbook Section 5a Measuring conditions of relevant elements in drinking water (according to DIN E6-3), page 17 Atomic absorption spectrophotometry Cookbook Section 5a Measuring conditions of relevant elements in drinking water (according to German drinking water Rulebook), page 23 Atomic absorption spectrophotometry Cookbook Section 5a Measuring conditions of relevant elements in drinking water (according to DIN D23-1), page 18, 19 izdanje /izmjena 1/2 Datum: /94

15 measurement uncertainty- 36 Određivanje volatilnih aromatičnih komponenti volatil aromatic compounds L.D.: mg/l U: 9.67% % Environmental protection agency (EPA) Method 5021 A VODA ZA PIĆE-LED DRINKING WATER AND ICE s Određivanje polihlorovanih bifenila PCB-s polichlorinated biphenils PCBs 1.L.D.: mg/l U: 13.11% 2.L.D.: 0, mg/l U: 9.25%-13.75% Određivanje policikličnih aromatskih ugljovodonika polycyclic aromatic hydrocarbons L.D.: mg/l U: 13.20% % 1. Standard Methods for examination of Water and Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 6431 B- 2. Standard Methods for examination of Water and Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 6431 C Standard Methods for examination of Water and Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 6440 C izdanje /izmjena 1/2 Datum: /94

16 measurement uncertainty- 39 Određivanje organohlornih pesticida organochlorine pesticides L.D.: mg/l U: 10.43% % Standard Methods for examination of Water and Wastewater-19 th Edition 1995, edited by Andrew D.Eaton,Lenore S.Clasceri and Arnold E.Greenberg 6630 C 2 RIBE, RAKOVI I PROIZVODI OD RIBA FISH, CRABS AND FISH PRODUCTS s Određivanje organofosfornih pesticida organophosphorine pesticides L.D.: mg/l U: 13.65%-29.73% Određivanje ukupne suve materije total dry matters L.D.: 0,01% U: 0,46% Određivanje pepela ash L.D.: 0,001% U: 8,2% Određivanje ukupnog azota total nitrogen L.D.: 0,01% U: 3,42% Environmental protection agency (EPA) Method 8141 A Official Methods of Analysis of AOAC International 16 th Edition, 3 rd Revision,1997, AOAC Methods: Official Methods of Analysis of AOAC International 16 th Edition, 3 rd Revision,1997, AOAC Methods: Handbook for Kjeldahl digestion a recent review of the classical method with improvements, Developed by Tecator, 2 nd edition, May izdanje /izmjena 1/2 Datum: /94

17 measurement uncertainty- 44 soli soil content L.D.: 0,6% U: 3,54% Official Methods of Analysis of AOAC International 16 th Edition, 3 rd Revision,1997, AOAC Methods: RIBE, RAKOVI I PROIZVODI OD RIBA FISH, CRABS AND FISH PRODUCTS s 45 masti u morskoj hrani fat in seefood L.D.: 0,01% U: 8,98% Official Methods of Analysis of AOAC International 16 th Edition, 3 rd Revision,1997, AOAC Methods: Određivanje olova u ribama lead in fish L.D.: 0,25 mg/kg U: 30,36% Official Methods of Analysis of AOAC International 16 th Edition, 3 rd Revision,1997, AOAC Methods: Određivanje žive u ribama i hrani mercury in fish and food L.D.: 0,0001 mg/kg U: 11,28% mercury in animal tissue: Organic application note Leco AMA 254, Form N , Leco corporation,1999 izdanje /izmjena 1/2 Datum: /94

18 measurement uncertainty- 48 Određivanje metabolita nitrofurana u rakovima i školjkama metabolites of nitrofurans in fish and shells L.D.: 0.001mg/kg U: 11.33% % US Drug and Food Administartion- Department of health and human services RIBE, RAKOVI I PROIZVODI OD RIBA FISH, CRABS AND FISH PRODUCTS s Određivanje malahit zelenog i leukomalahit zelenog u rakovima malachite green and leukomalachitegreen in crabs L.D.: 0.001mg/kg U: 10.77% Određivanje histamina u morskim proizvodima histamines in see products L.D.: 25mg/kg U: 11.67% Wendy C. Andersen, Sherri B. Turnipseed, and José E. Roybal, Food and Drug Administration, Animal Drugs Research Center Official Methods of Analysis of AOAC International 16 th Edition, 3 rd Revision,1997, AOAC Methods: izdanje /izmjena 1/2 Datum: /94

19 measurement uncertainty- 51 Određivanje organohlornih pesticida i PCB-a u ribama GC metodom organochlorine pesticides ad PCBs in fish using GC method Official Methods of Analysis of AOAC International 16 th Edition, 3 rd Revision,1997, AOAC Methods: L.D.: mg/kg za OCl pesticide U: 10.14%-19.54% 3 MESO MEAT s L.D.: mg/kg za PCB kongenere U: 8.31%-10.98% 52. Određivanje nitroimidazola nitroimidazoles L.D.: Metroinidazole: mg/kg Ipronidazole: mg/kg Ronidazole: mg/kg Dimetridazole: mg/kg CLG-NIMZ Confirmation of Nitroimidazoles by ESI LC/MS/MS, United States Department of Agriculture Food Safety and Inspection Service, Office of Public Health Science U: 11.44% % 53 tetraciklina u mesu BAKER FF505 Extraction of tetracyclines from Animal Tissue and Eggs, JT Baker Aplication te FF505 modifikovana izdanje /izmjena 1/2 Datum: /94

20 measurement uncertainty- 4 MLIJEKO MILK s 54. Određivanje hloramfenikola chloramphenicol L.D.: mg/l U: 11.53% Validation of the gas chromatography-mass spectrometry method for the determination of chloramphenicol residues in milk, Tomasz Śniegocki, Andrzej Posyniak And Jan Żmudzki, Department of Pharmacology and Toxicology, National Veterinary Research Institute, Pulawy, Poland izdanje /izmjena 1/2 Datum: /94

21 measurement uncertainty- MLIJEKO MILK s 55. Određivanje kiselosti mlijeka acidity of milk L.D. 0,2 o SH U=1,30% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka I Mleko 2. Određivanje kiselosti mleka Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - milk I - 2 acidity of milk izdanje /izmjena 1/2 Datum: /94

22 measurement uncertainty- MLIJEKO MILK s 56. Određivanje masti u mlijeku fat in milk L.D. 0,1% U=3,16% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka I Mleko - 3. Određivanje masti u mleku Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - milk - 3 fat in milk izdanje /izmjena 1/2 Datum: /94

23 measurement uncertainty- MLIJEKO MILK s Određivanje suve materije u mlijeku dry matter in milk L.D. 0,01% U=0,77% makrolidau mlijeku MAC-1 Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka I Mleko - 4. Određivanje suve materije u mleku Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - milk I - 4 dry matter in milk Optimization and validation of Multiclass Multi residue LC-MS/MS Screening and Confirmation Method for Drug Residues in Milk, Food and Drug Administration LIB#4443 modifikovana izdanje /izmjena 1/2 Datum: /94

24 measurement uncertainty- MLIJEKO MILK s 59. Određivanje masti u kiselom mlijeku i jogurtu fat in yogurt L.D. 0,1% U=0,92% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka II Kiselo mleko i jogurt 1. Određivanje masti u kiselom mleku i jogurtu Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - II Sour milk and yogurt - 1 fat in yogurt izdanje /izmjena 1/2 Datum: /94

25 measurement uncertainty- MLIJEKO MILK s 60. Određivanje suve materije u kiselom mlijeku i jogurtu dry matter in yogurt L.D. 0,01% U=1,30% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka II Kiselo mleko i jogurt 3. Određivanje suve materije u kiselom mleku i jogurtu Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - II Sour milk and yogurt - 3 dry matter in yogurt izdanje /izmjena 1/2 Datum: /94

26 measurement uncertainty- MLIJEKO MILK s 61. Određivanje vode u mlijeku u prahu water in milk powder L.D. 0,01% U=7,42% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka IV Mleko u prahu 1. Određivanje vode u mleku u prahu Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - milk powder IV - 1 water in milk powder izdanje /izmjena 1/2 Datum: /94

27 measurement uncertainty- MLIJEKO MILK s 62. Određivanje masti u mlijeku u prahu fat content in milk powder L.D. 0,1% U=1,51% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka IV Mleko u prahu 2. Određivanje masti u mleku u prahu Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - milk powder IV - 2 fat content in milk powder izdanje /izmjena 1/2 Datum: /94

28 measurement uncertainty- MLIJEKO MILK s 63. Određivanje masti u pavlaci buritometrom za pavlaku fat in the cream by he cream butirometer L.D. 0,5% U=5,10% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka V Pavlaka 1. Određivanje masti u pavlaci butirometrom za pavlaku Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - V - Sour cream - 1 fat in the cream by he cream butirometer izdanje /izmjena 1/2 Datum: /94

29 measurement uncertainty- MLIJEKO MILK s 64. Određivanje vode u siru metodom sušenja water in the cheese using drying method L.D. 0,01% U=0,70% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka VI Sir 1. Određivanje vode u siru metodom sušenja Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - VI - Cheese - 1 Determination of water in the cheese using drying method izdanje /izmjena 1/2 Datum: /94

30 measurement uncertainty- MLIJEKO MILK s 65. Određivanje masti u siru butirometrom za sir fat in cheese by butirometer for cheese L.D. 0,5% U=3,08% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka VI Sir 2. Određivanje masti u siru butirometrom za sir Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - VI - Cheese - 2 Determination of fat in cheese by butirometer for cheese izdanje /izmjena 1/2 Datum: /94

31 measurement uncertainty- MLIJEKO MILK s 66. Određivanje vode u kajmaku water in cream L.D. 0,01% U=0,25% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka VII Kajmak 1. Određivanje vode u kajmaku Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - VII - Cream - 1 Determination of water in cream izdanje /izmjena 1/2 Datum: /94

32 measurement uncertainty- MLIJEKO MILK s 67. Određivanje masti u kajmaku fat in cream L.D. 0,5% U=1,09% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka VII Kajmak 1. Određivanje masti u kajmaku Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - VII - Cream - 1 Determination of fat in cream izdanje /izmjena 1/2 Datum: /94

33 measurement uncertainty- MLIJEKO MILK s 68. Određivanje masti u kefiru fat content in kefir L.D. 0,1% U=2,82% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka IX Kefir 1. Određivanje masti u kefiru Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - IX - Kefir - 1 Determination of fat content in kefir izdanje /izmjena 1/2 Datum: /94

34 measurement uncertainty- MLIJEKO MILK s 69. Određivanje suve materije u kefiru dry matter of Kefir L.D. 0,01% U=1,53% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka IX Kefir 3. Određivanje suve materije u kefiru Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - IX - Kefir - 3 Determination of dry matter of Kefir izdanje /izmjena 1/2 Datum: /94

35 measurement uncertainty- MLIJEKO MILK s 70. Određivanje masti u sladoledu fat in ice cream L.D. 0,5% U=3,76% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka X Sladoled 1. Određivanje masti u sladoledu Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - X - Ice cream -1. fat in ice cream izdanje /izmjena 1/2 Datum: /94

36 measurement uncertainty- MLIJEKO MILK s 71. Određivanje suve materije u sladoledu dry matter in ice cream L.D. 0,01% U=1,46% Pravilnik o metodama uzimanja uzoraka i metodama hemijskih i fizičkih analiza mleka i proizvoda od mleka (Sl. list SFRJ, br. 32/83) VII Metode hemijskih i fizičkih analiza mleka i proizvoda od mleka X Sladoled 2. Određivanje suve materije u sladoledu Rulebook on sampling methods and methods of chemical and physical analysis of milk and dairy products (Official Gazette. 32/83) - VII Methods of chemical and physical analysis of milk and dairy products - X - Ice cream - 2 dry matter in ice cream izdanje /izmjena 1/2 Datum: /94

37 measurement uncertainty- 72. Određivanje beta laktama u mlijeku ß- lactam in milk L.D. 2,5 μg/kg U=5,53-11,38% Prevalence of molecules of ß-lactam antibiotics in bovine milk in Lombardia and Emilia Romagna (Italy), Ghidini S., Zanardi E., Varisco G., Chizzolini R., Ann. Fac. Medic. Vet. di Parma (Vol. XXII, 2002) - pg pg. 252, modifikovana MLIJEKO MILK s 73. Određivanje antihelmintika u mlijeku antihelmintics in milk L.D. 4,0 μg/kg U=11,06-12,47% Validation and robustness testing of a HPLC method for the determination of avermectins and moxidectin in animal liver samples using an alumina column cleanup-the Analyst-full paper, Martin Danaher, Michael O Keeffe and Jeremy D.Glennon, modifikovana izdanje /izmjena 1/2 Datum: /94

38 measurement uncertainty- MLIJEKO MILK s 74. Određivanje hinolona u mlijeku hinolone in milk L.D. 20,0 μg/kg U=13,08-13,30% (Validation of a multiquinolone, multi-matrix, multi-species method for determination of quinolone residues by HPLC with fluorescence detection) poster 127 Euroresidues V, odwijkerhout, The Netherlands, May E.Verdon, P.Couedor, P.Sanders, AFSSA- LERMVD, French Agency for Food Safety, modifikovana Mod.AOAC Aflatoksina M1 u mlijeku izdanje /izmjena 1/2 Datum: /94

39 measurement uncertainty- 5 MED HONEY s 76. Određivanje redukovanih šećera reducing sugar L.D. 0,5% U=2,05% Pravilnik o kvalitetu meda i drugih pčelinjih proizvoda i metodama za kontrolu meda i drugih pčelinjih proizvoda (Sl.list SFRJ, br. 4/85) IV Metode za kontrolu meda i drugih pčelinjih proizvoda - 2. Metode fizičkih i hemijskih analiza 2. Određivanje redukovanih šećera Rulebook on the quality of honey and other bee products and methods to control the honey and other bee products (Official Gazette SFRY, no. 4/85) - IV - Methods for controlling honey and other bee products - 2 Methods of physical and chemical analysis - 2 reducing sugar izdanje /izmjena 1/2 Datum: /94

40 measurement uncertainty- MED HONEY s 77. Određivanje saharoze u medu sucrose in honey L.D. 0,5% U=8,20% Pravilnik o kvalitetu meda i drugih pčelinjih proizvoda i metodama za kontrolu meda i drugih pčelinjih proizvoda (Sl.list SFRJ, br. 4/85) IV Metode za kontrolu meda i drugih pčelinjih proizvoda - 2. Metode fizičkih i hemijskih analiza 3. Određivanje saharoze u medu Rulebook on the quality of honey and other bee products and methods to control the honey and other bee products (Official Gazette SFRY, no. 4/85) - IV - Methods for controlling honey and other bee products - 2 Methods of physical and chemical analysis - 3 sucrose in honey izdanje /izmjena 1/2 Datum: /94

41 measurement uncertainty- MED HONEY s 78. Određivanje kiselosti u medu acidity in honey L.D. 1,0 U=3,95% Pravilnik o kvalitetu meda i drugih pčelinjih proizvoda i metodama za kontrolu meda i drugih pčelinjih proizvoda (Sl.list SFRJ, br. 4/85) IV Metode za kontrolu meda i drugih pčelinjih proizvoda - 2. Metode fizičkih i hemijskih analiza 7. Određivanje kiselosti u medu Rulebook on the quality of honey and other bee products and methods to control the honey and other bee products (Official Gazette SFRY, no. 4/85) - IV - Methods for controlling honey and other bee products - 2 Methods of physical and chemical analysis - 7 acidity in honey izdanje /izmjena 1/2 Datum: /94

42 measurement uncertainty- 6 ŽITA I MLINSKI PROIZVODI CEREALS AND MILLED PRODUCTS s 79. Određivanje količine vode u žitu i mlinskim proizvodima water content in wheat and flour mill products L.D. 0,01% U=1,37% Pravilnik o metodama fizičkih i hemijskih analiza za kontrolu kvaliteta žita, mlinskih i pekarskih proizvoda, testenina i brzo smrznutih testa (Sl. list SFRJ, br. 74/88) 3. Metode fizičkih i hemijskih za kontrolu kvaliteta proizvoda I Žita i mlinski proizvodi 8. Određivanje količine vode u žitu i mlinskim proizvodima Rulebook on physical and chemical methods of analysis for quality control of grain, milling and bakery products, pasta and fast frozen dough (Official Gazette,. 74. / 88) - 3 Methods of physical and chemical tests for quality control of products - I - Grain and mill products - 8 water content in wheat and flour mill products izdanje /izmjena 1/2 Datum: /94

43 measurement uncertainty- ŽITA I MLINSKI PROIZVODI CEREALS AND MILLED PRODUCTS s 80. Određivanje količine pepela u žitu i mlinskim proizvodima ash in wheat and flour mill products L.D. 0,01% U=1,67% Pravilnik o metodama fizičkih i hemijskih analiza za kontrolu kvaliteta žita, mlinskih i pekarskih proizvoda, testenina i brzo smrznutih testa (Sl. list SFRJ, br. 74/88) 3. Metode fizičkih i hemijskih za kontrolu kvaliteta proizvoda I Žita i mlinski proizvodi 10. Određivanje količine pepela u žitu i mlinskim proizvodima Rulebook on physical and chemical methods of analysis for quality control of grain, milling and bakery products, pasta and fast frozen dough (Official Gazette,. 74. / 88) - 3 Methods of physical and chemical tests for quality control of products - I - Grain and mill products - 10 ash in wheat and flour mill products izdanje /izmjena 1/2 Datum: /94

44 measurement uncertainty- ŽITA I MLINSKI PROIZVODI CEREALS AND MILLED PRODUCTS s 81. Određivanje količine pepela nerastvorljivog u hlorovodoničnoj kiselina (pijeska) u žitu i mlinskim proizvodima ash insoluble in hydrochloric acid (sand) in wheat and flour mill products L.D. 0,001% U=4,03% Pravilnik o metodama fizičkih i hemijskih analiza za kontrolu kvaliteta žita, mlinskih i pekarskih proizvoda, testenina i brzo smrznutih testa (Sl. list SFRJ, br. 74/88) 3. Metode fizičkih i hemijskih za kontrolu kvaliteta proizvoda I Žita i mlinski proizvodi 11. Određivanje količine pepela nerastvorljivog u hlorovodoničnoj kiselina (pijeska) u žitu i mlinskim proizvodima Rulebook on physical and chemical methods of analysis for quality control of grain, milling and bakery products, pasta and fast frozen dough (Official Gazette,. 74. / 88) - 3 Methods of physical and chemical tests for quality control of products - I - Grain and mill products - 11 ash insoluble in hydrochloric acid (sand) in wheat and flour mill products izdanje /izmjena 1/2 Datum: /94

45 measurement uncertainty- ŽITA I MLINSKI PROIZVODI CEREALS AND MILLED PRODUCTS s 82. Određivanje kiselinskog stepena u žitu i mlinskim proizvodima acid level in wheat and flour mill products L.D. 0,1 U=3,13% Pravilnik o metodama fizičkih i hemijskih analiza za kontrolu kvaliteta žita, mlinskih i pekarskih proizvoda, testenina i brzo smrznutih testa (Sl. list SFRJ, br. 74/88) 3. Metode fizičkih i hemijskih za kontrolu kvaliteta proizvoda I Žita i mlinski proizvodi 16. Određivanje kiselinskog stepena u žitu i mlinskim proizvodima Rulebook on physical and chemical methods of analysis for quality control of grain, milling and bakery products, pasta and fast frozen dough (Official Gazette,. 74. / 88) - 3 Methods of physical and chemical tests for quality control of products - I - Grain and mill products - 16 acid level in wheat and flour mill products izdanje /izmjena 1/2 Datum: /94

46 measurement uncertainty- 83. fuminozina fumonisins L.D. 1,0 μg/kg U=10,34% Foodstuffs - fumonisins B1 and B2 in maize - HPLC method with solid phase extraction clean-up, modifikovana ŽITA I MLINSKI PROIZVODI CEREALS AND MILLED PRODUCTS s zearalenona content of zearalenone L.D. 0,5 μg/kg U=9,57% trihotecena u žitaricama i njihovim proizvodima metodom GCMS trichothecenes in cereals and their products using GCMS L.D. 40,0 μg/kg U=9,55% 17 Mycotoxin screen by GCMS, Hovard H. Casper, rth Dakota State University, Department of Veterinary & Microbiological Science, Fargo, rth Dakota, modifikovana 17 Mycotoxin screen by GCMS, Hovard H. Casper, rth Dakota State University, Department of Veterinary & Microbiological Science, Fargo, rth Dakota, modifikovana izdanje /izmjena 1/2 Datum: /94

47 measurement uncertainty- 7 PROIZVODI OD VOĆA I POVRĆA PRODUCTS OF FRUITS AND VEGETABLES s 86. Određivanje ukupne suve materije total dry matter L.D. 0,01% U=0,42% Pravilnik o metodama uzimanja uzoraka i vršenja hemijskih i fizičkih analiza radi kontrole kvaliteta proizvoda od voća i povrća (Sl. list SFRJ, br. 29/83) 2. Određivanje ukupne suve materije Rulebook on sampling methods and performance of chemical and physical analysis for quality control of fruit and vegetables (Official Gazette. 29/83) - 2 total dry matter izdanje /izmjena 1/2 Datum: /94

48 measurement uncertainty- PROIZVODI OD VOĆA I POVRĆA PRODUCTS OF FRUITS AND VEGETABLES s 87. Određivanje ukupnih i direktno-redukujućih šećera Luffovim rastvorom total and direct-reduced sugar by Luff solution L.D. 0,5% ukupni šećeri: U=1,60% direktno-redukujući šećeri: 1,97% saharoza: 8,20% Pravilnik o metodama uzimanja uzoraka i vršenja hemijskih i fizičkih analiza radi kontrole kvaliteta proizvoda od voća i povrća ((Sl. list SFRJ, br. 29/83) 3. Određivanje ukupnih i direktnoredukujućih šećera Luffovim rastvorom Ruleboook on sampling methods and performance of chemical and physical analysis for quality control of fruit and vegetables (Official Gazette. 29/83) - 3 total and direct-reduced sugar by Luff solution izdanje /izmjena 1/2 Datum: /94

49 measurement uncertainty- PROIZVODI OD VOĆA I POVRĆA PRODUCTS OF FRUITS AND VEGETABLES s Određivanje L-askorbinske kiseline L- ascorbic acid L.D. 1,0 mg/100 g U=1,00% Određivanje ukupne kiselosti total acidity L.D. 0,1 g/kg U=2,97% Pravilnik o metodama uzimanja uzoraka i vršenja hemijskih i fizičkih analiza radi kontrole kvaliteta proizvoda od voća i povrća (Sl. list SFRJ, br. 29/83) 15. Određivanje L-askorbinske kiseline Rulebook on sampling methods and performance of chemical and physical analysis for quality control of fruit and vegetables (Official Gazette. 29/83)- 15 L- ascorbic acid Pravilnik o metodama uzimanja uzoraka i vršenja hemijskih i fizičkih analiza radi kontrole kvaliteta proizvoda od voća i povrća (Sl. list SFRJ, br. 29/83) 18. Određivanje ukupne kiselosti Rulebook on sampling methods and performance of chemical and physical analysis for quality control of fruit and vegetables (Official Gazette. 29/83)- 18 total acidity izdanje /izmjena 1/2 Datum: /94

50 measurement uncertainty- PROIZVODI OD VOĆA I POVRĆA PRODUCTS OF FRUITS AND VEGETABLES s 90. sorbinske kiseline u proizvodima od voća sorbic acid in fruit and vegetables and fruit products L.D. 5,0 mg/kg U=15,9% Pravilnik o metodama uzimanja uzoraka i vršenja hemijskih i fizičkih analiza radi kontrole kvaliteta proizvoda od voća i povrća (Sl. list SFRJ, br. 29/83) 8. Određivanje sadržaja sorbinske kiseline u voću i povrću i proizvodima od voća Rulebook on sampling methods and performance of chemical and physical analysis for quality control of fruit and vegetables (Official Gazette. 29/83)- 8 sorbic acid in fruit and vegetables and fruit products izdanje /izmjena 1/2 Datum: /94

51 measurement uncertainty- 8 KAKAO PROIZVODI, PROIZVODI SLIČNI ČOKOLADI, BONBONSKI PROIZVODI, KREM PROIZVODI, KEKS I PROIZVODI SRODNI KEKSU COCOA PRODUCTS, LIKE CHOCOLATE PRODUCTS, CONFECTIONERY, CREAM PRODUCTS, CAKES BISCUITS AND SIMILAR PRODUCTS Physical and chemical analysis 91. Određivanje vode sušenjem pod normalnim pritiskom water by drying under normal pressure L.D. 0,01% U=1,60% Pravilnik o metodama uzimanja uzoraka i metodama vršenja hemijskih i fizičkih analiza kakao-zrna, kakao-proizvoda, proizvoda sličnih čokoladi, bombonskih proizvoda, kremproizvoda, keksa i proizvoda srodnih keksu (Sl. list SFRJ, 41/87) II Metode fizičkih i hemijskih analiza proizvoda 1. Određivanje vode sušenjem pod normalnim pritiskom Rulebook on sampling methods and methods of performing chemical and physical analysis of cocoa beans, cocoa products, products like chocolate, confectionery, cream products, biscuits and biscuit related products (Official Gazette, 41/87) - II Methods of physical and chemical analysis products - 1 water by drying under normal pressure izdanje /izmjena 1/2 Datum: /94

52 measurement uncertainty- KAKAO PROIZVODI, PROIZVODI SLIČNI ČOKOLADI, BONBONSKI PROIZVODI, KREM PROIZVODI, KEKS I PROIZVODI SRODNI KEKSU COCOA PRODUCTS, LIKE CHOCOLATE PRODUCTS, CONFECTIONERY, CREAM PRODUCTS, CAKES BISCUITS AND SIMILAR PRODUCTS Physical and chemical analysis 92. Određivanje vode u kolačima sušenjem pod normalnim pritiskom water in biscuits by drying under normal pressure L.D. 0,01% U=2,00% Pravilnik o metodama uzimanja uzoraka i metodama vršenja hemijskih i fizičkih analiza kakao-zrna, kakao-proizvoda, proizvoda sličnih čokoladi, bombonskih proizvoda, kremproizvoda, keksa i proizvoda srodnih keksu (Sl. list SFRJ, 41/87) II Metode fizičkih i hemijskih analiza proizvoda 2. Određivanje vode u kolačima pod normalnim pritiskom Rulebook on sampling methods and methods of performing chemical and physical analysis of cocoa beans, cocoa products, products like chocolate, confectionery, cream products, biscuits and biscuit related products (Official Gazette, 41/87) - II Methods of physical and chemical analysis products - 2 water in biscuits by drying under normal pressure izdanje /izmjena 1/2 Datum: /94

53 measurement uncertainty- KAKAO PROIZVODI, PROIZVODI SLIČNI ČOKOLADI, BONBONSKI PROIZVODI, KREM PROIZVODI, KEKS I PROIZVODI SRODNI KEKSU COCOA PRODUCTS, LIKE CHOCOLATE PRODUCTS, CONFECTIONERY, CREAM PRODUCTS, CAKES BISCUITS AND SIMILAR PRODUCTS Physical and chemical analysis 93. Određivanje pepela ash L.D. 0,01% U=4,03% Pravilnik o metodama uzimanja uzoraka i metodama vršenja hemijskih i fizičkih analiza kakao-zrna, kakao-proizvoda, proizvoda sličnih čokoladi, bombonskih proizvoda, kremproizvoda, keksa i proizvoda srodnih keksu (Sl. list SFRJ, 41/87) II Metode fizičkih i hemijskih analiza proizvoda 5. Određivanje pepela Rulebook on sampling methods and methods of performing chemical and physical analysis of cocoa beans, cocoa products, products like chocolate, confectionery, cream products, biscuits and biscuit related products (Official Gazette, 41/87) - II Methods of physical and chemical analysis products - 5, ash izdanje /izmjena 1/2 Datum: /94

54 measurement uncertainty- KAKAO PROIZVODI, PROIZVODI SLIČNI ČOKOLADI, BONBONSKI PROIZVODI, KREM PROIZVODI, KEKS I PROIZVODI SRODNI KEKSU COCOA PRODUCTS, LIKE CHOCOLATE PRODUCTS, CONFECTIONERY, CREAM PRODUCTS, CAKES BISCUITS AND SIMILAR PRODUCTS Physical and chemical analysis 94. Određivanje ukupne masti po Soksletu (Soxhlet) total fat by Soxhlet L.D. 0,01% U=1,60% Pravilnik o metodama uzimanja uzoraka i metodama vršenja hemijskih i fizičkih analiza kakao-zrna, kakao-proizvoda, proizvoda sličnih čokoladi, bombonskih proizvoda, kremproizvoda, keksa i proizvoda srodnih keksu (Sl. list SFRJ, 41/87) II Metode fizičkih i hemijskih analiza proizvoda 9. Određivanje ukupne masti po Soksletu (Soxhlet) Rulebook on sampling methods and methods of performing chemical and physical analysis of cocoa beans, cocoa products, products like chocolate, confectionery, cream products, biscuits and biscuit related products (Official Gazette, 41/87) - II Methods of physical and chemical analysis products -9 total fat by Soxhlet izdanje /izmjena 1/2 Datum: /94

55 measurement uncertainty- KAKAO PROIZVODI, PROIZVODI SLIČNI ČOKOLADI, BONBONSKI PROIZVODI, KREM PROIZVODI, KEKS I PROIZVODI SRODNI KEKSU COCOA PRODUCTS, LIKE CHOCOLATE PRODUCTS, CONFECTIONERY, CREAM PRODUCTS, CAKES BISCUITS AND SIMILAR PRODUCTS Physical and chemical analysis 95. Određivanje šećera po Luf-Šurlu (LUFF- SCHOORL) L.D. 0,1% sugar by Luff Schoorl U=2,24% Pravilnik o metodama uzimanja uzoraka i metodama vršenja hemijskih i fizičkih analiza kakao-zrna, kakao-proizvoda, proizvoda sličnih čokoladi, bombonskih proizvoda, kremproizvoda, keksa i proizvoda srodnih keksu (Sl. list SFRJ, 41/87) II Metode fizičkih i hemijskih analiza proizvoda 12. Određivanje šećera po Luf-Šurlu (LUFF- SCHOORL) Rulebook on sampling methods and methods of performing chemical and physical analysis of cocoa beans, cocoa products, products like chocolate, confectionery, cream products, biscuits and biscuit related products (Official Gazette, 41/87) - II Methods of physical and chemical analysis products -12 sugar by Luff Schoorl izdanje /izmjena 1/2 Datum: /94

56 measurement uncertainty- KAKAO PROIZVODI, PROIZVODI SLIČNI ČOKOLADI, BONBONSKI PROIZVODI, KREM PROIZVODI, KEKS I PROIZVODI SRODNI KEKSU COCOA PRODUCTS, LIKE CHOCOLATE PRODUCTS, CONFECTIONERY, CREAM PRODUCTS, CAKES BISCUITS AND SIMILAR PRODUCTS Physical and chemical analysis 96. Određivanje natrijumhlorida u trajnom slanom pecivu, po Moru (Mohr) sodium chloride in permanent saline baked goods by Mohr L.D. 0,05% U=2,51% Pravilnik o metodama uzimanja uzoraka i metodama vršenja hemijskih i fizičkih analiza kakao-zrna, kakao-proizvoda, proizvoda sličnih čokoladi, bombonskih proizvoda, kremproizvoda, keksa i proizvoda srodnih keksu (Sl. list SFRJ, 41/87) II Metode fizičkih i hemijskih analiza proizvoda 21. Određivanje natrijumhlorida u trajnom slanom pecivu, po Moru (Mohr) Rulebook on sampling methods and methods of performing chemical and physical analysis of cocoa beans, cocoa products, products like chocolate, confectionery, cream products, biscuits and biscuit related products (Official Gazette, 41/87) - II Methods of physical and chemical analysis products -21 sodium chloride in permanent saline baked goods by Mohr izdanje /izmjena 1/2 Datum: /94

57 measurement uncertainty- 97. ukupnog azota u mesu i mesnim proizvodima total nitrogen content in meat and meat products L.D. 0,01% U=1,35% ISO 937:1992 ukupnog azota u mesu i mesnim proizvodima total nitrogen content in meat and meat products 9 MESO I MESNI PROIZVODI MEAT AND MEAT PRODUCTS Physical and chemical analysis vlage moisture content L.D. 0,01% U=0,43% hlorida metodom po Volhardu chloride content by the Volhard method ISO 1442:1997 vlage moisture content ISO :1998 hlorida metodom po Volhardu chloride content by the Volhard method L.D. 0,6% U=1,92% izdanje /izmjena 1/2 Datum: /94

58 measurement uncertainty nitrita u prehrambenim proizvodima, mesu i proizvodima nitrite in food products, meat and meat products L.D. 1,0 mg/kg ISO 2918:1998 nitrita u prehrambenim proizvodima, mesu i proizvodima od mesa nitrite in food products, meat and meat products U=% MESO I MESNI PROIZVODI MEAT AND MEAT PRODUCTS Physical and chemical analysis 101. hidroksiprolina u mesu i proizvodima od mesa hydroxyproline content in meat and meat products JUS ISO 3496:2002 hidroksiprolina u mesu i proizvodima od mesa hydroxyproline content in meat and meat products L.D. 0,6% U=28,10% izdanje /izmjena 1/2 Datum: /94

59 measurement uncertainty ukupnog fosfora u mesu i proizvodima od mesa total phosphorus content in meat and meat products L.D. 0,1 g/kg JUS ISO 13730:1999 ukupnog fosfora u mesu i proizvodima od mesa total phosphorus content in meat and meat products U=15,34% MESO I MESNI PROIZVODI MEAT AND MEAT PRODUCTS Physical and chemical analysis hinolona quinolones content L.D. 20,0 μg/kg U=10,82-13,27% hloramfenikola L.D. 0,1 μg/kg U=9,96% Simultaneous Quatification of Ciprofloxacin, Enrofloxacin, and Balofloxacin in Broiler Chicken Muscle, H.Garcia Ovando, M.V.N. Gorla, M.Sc.L.Ugnia, A.Magnoli.M.V, Arch.Med.Vet.XXXVI, 1,2004, modifikovana Determination and Confirmation of Chloraphenicol Residues in swine muscle and liver, T.L. LI, Y.J. CHUNG-WANG, AND Y.C. SHIH, JFS: Food Chemistry and Toxicology,modifikovana izdanje /izmjena 1/2 Datum: /94

60 measurement uncertainty- 10 MESO I MESNI PROIZVODI MEAT AND MEAT PRODUCTS Hrana za životinje Food for animals Physical and chemical analysis Phisical and chemical analysis beta laktama β- Lactam content L.D. 2,5 μg/kg U=5,05-10,93% Aflatoksina B1,B2,G1 i G2 u stočnoj hrani metodom HPLC Screening and Confirmation of β- Lactam Antibiotics by HPLC-MS/MS, CLG- BLAC.02 United States Department of Agriculture Food Safety and Inspection Service, Office of Public Health Science, SOP HPLC 7 HRANA BILJNOG I ŽIVOTINJSKOG PORIJEKLA 107. olova lead content L.D. 0,10 mg/kg U=8,00% AOAC Official Method Lead, Cadmium, Copper, Iron and Zinc in Foods, J. AOAC Int. 83, 1204(2000), modifikovana 11 FOOD PLANT AND ANIMAL ORIGIN analysis 108. kadmijuma cadmium content L.D. 0,02 mg/kg U=6,40% AOAC Official Method Lead, Cadmium, Copper, Iron and Zinc in Foods, J. AOAC Int. 83, 1204(2000), modifikovana izdanje /izmjena 1/2 Datum: /94

61 measurement uncertainty cinka Zinc content L.D. 0,05 mg/kg U=8,93% AOAC Official Method Lead, Cadmium, Copper, Iron and Zinc in Foods, J. AOAC Int. 83, 1204(2000), modifikovana HRANA BILJNOG I ŽIVOTINJSKOG PORIJEKLA FOOD PLANT AND ANIMAL ORIGIN analysis 110. bakra copper content L.D. 0,05 mg/kg U=8,12% AOAC Official Method Lead, Cadmium, Copper, Iron and Zinc in Foods, J. AOAC Int. 83, 1204(2000), modifikovana 111. gvožđa iron content L.D. 0,05 mg/kg U=9,85% AOAC Official Method Lead, Cadmium, Copper, Iron and Zinc in Foods, J. AOAC Int. 83, 1204(2000), modifikovana 112. arsena arsenic content L.D. 0,06 mg/kg U=11,55% AOAC Official Method Arsenic, Cadmium, Lead, Selenium and Zinc in Human and Pet Foods, J. AOAC 63, 485(1980). izdanje /izmjena 1/2 Datum: /94