Navy and Marine Corps Public Health Center
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1 Navy and Marine Corps Public Health Center Appendix L Resolution Consultants Supplemental Environmental Investigation for the Sampling Results 6 May John Paul Jones Circle, Suite 1100 Portsmouth, VA
2 This page has been left blank to allow for double-sided printing i
3 Resolution Consultants A Joint Venture of AECOM & EnSafe 1500 Wells Fargo Building 440 Monticello Avenue Norfolk, Virginia May 2016 VIA ELECTRONIC MAIL Mr. Arne Olsen Remedial Project Manager Naval Facilities Engineering Command, Southeast IPT Gulf Coast OPUE3 Building 135 Naval Air Station Jacksonville Jacksonville, Florida RE: Supplemental Environmental Investigation Sampling Results Naval Station Guantanamo Bay, Cuba Contract No. N D-8013 Contract Task Order JMB5 Dear Mr. Olsen: Resolution Consultants performed a Supplemental Environmental Investigation of the Office of Military Commissions Camp Justice, also known as Area of Operation Patriot, at United States Naval Station Guantanamo Bay (NS GTMO), Cuba. The work was conducted at the request of Naval Facilities Engineering Command, Southeast, under Comprehensive Long-term Environmental Action Navy Contract No. N D-8013, Contract Task Order JMB5, Statement of Work Number SCSR1501 (Modification 2). This letter identifies sample dates and locations, presents analytical laboratory results, and discusses data validation and other activities associated with the collection of indoor air samples for formaldehyde analysis. Resolution Consultants mobilized to NS GTMO on 15 April 2016 and conducted sampling activities through 23 April Sample Locations As shown on Figures 1 through 6 in Attachment A, sorbent cartridges were used to collect 31 indoor air samples and 2 field blanks to determine the presence of formaldehyde in the following buildings, Cuzcos, and modular structures/trailers. Cuzcos on 21 April 2016 Various structures inside the Expeditionary Legal Complex used for meeting spaces or administrative purposes on 22 April 2016
4 Mr. Arne Olsen 6 May 2016 Page 2 Satellite and family trailers used for administrative purposes outside Building AV-29 on 22 and 23 April 2016 Multiple rooms used for administrative purposes in Hangar AV-32 on 22 and 23 April 2016 Sample Collection Prior to deploying sorbent cartridges, the heating, ventilating, and air conditioning systems at each location were operating at occupation levels. Prior to sample collection, each air sampling pump was calibrated to a flow rate of 1.2 liters per minute using a rotameter to measure the upstream airflow as it entered the cartridge. Once the calibration was complete, a new cartridge was connected to the air sampling pump and the starting time was recorded. Samples were collected for approximately 8 hours (480 minutes), except for samples collected in the satellite trailer outside of Building AV-29 and the Media Operations Room 1 in Hangar AV-32. Those two samples were collected for approximately 12 hours (720 minutes) following initial pump failure and to later facilitate coordination of sample collection. At the end of each sampling period, pumps were turned off, stop times were recorded, and the cartridge caps were replaced. Each cartridge was labeled with a sample identification number and air sampling pumps were recalibrated to verify the flow rate. Field blanks were collected in the same manner as the samples, except that no air was drawn through the cartridges. Analytical Results Sample media cartridges were chilled during storage, and were packed in a cooler with frozen ice packs for shipment and submittal to Eurofins Air Toxics, Inc., after sample collection. Each cartridge was analyzed for formaldehyde using United States Environmental Protection Agency (U.S. EPA) Method TO-11A. Table 1 summarizes sample identification numbers, sample locations, start and stop times, and sample results. The Eurofins Air Toxics laboratory report is included as Attachment B.
5 Mr. Arne Olsen 6 May 2016 Page 3 Table 1 Analytical Results Naval Station Guantanamo Bay, Cuba Location (Building/Room No.) Sample Date Result (µg/m 3 ) Sample ID AV29IAFMFT AV-29/Family Trailer AV29IAFMST AV-29/Satellite Trailer AV32IAFMM01 AV-32/M AV32IAFMM02 AV-32/M AV32IAFMMP AV-32/MP CZIAFM10B CUZCOS/10B CZIAFM11B CUZCOS/11B CZIAFM16A CUZCOS/16A CZIAFM17A CUZCOS/17A CZIAFM22A CUZCOS/22A CZIAFM23A CUZCOS/23A CZIAFM27B CUZCOS/27B CZIAFM28B CUZCOS/28B CZIAFM35A CUZCOS/35A CZIAFM36A CUZCOS/36A CZIAFM43A CUZCOS/43A CZIAFM44A CUZCOS/44A CZIAFM47A CUZCOS/47A CZIAFM48A CUZCOS/48A CZIAFM4A CUZCOS/4A CZIAFM5A CUZCOS/5A ELCIAFMBL1 ELC/BL ELCIAFMBL1-COM ELC/BL-1 COM ELCIAFMBL11 ELC/BL ELCIAFMBL2 ELC/BL ELCIAFMBL29 ELC/BL ELCIAFMBL30 ELC/BL ELCIAFMBL3107 ELC/BL ELCIAFMBL4 ELC-BL ELCIAFMBL5 ELC/BL ELCIAFMBL8 ELC/BL CZIAFMBLK Cuzcos Field Blank AV32IAFMBLK AV-32 Field Blank Note: µg/m 3 = micrograms per cubic meter
6 Mr. Arne Olsen 6 May 2016 Page 4 Data Verification and Validation Data verification was performed to assess the completeness of laboratory data by reviewing chain-of-custody forms, laboratory sample logs, receipt condition reports, and laboratory deliverables. Data verification was performed on laboratory analytical data; 10 percent of the raw data (including instrument printouts) was manually validated. Laboratory data, provided in electronic format, was verified for accuracy prior to use and during the data validation process. After receipt of the full data package and electronic deliverables, results were validated independently from the laboratory to assess data quality against criteria established in the analytical methods, U.S. EPA data validation guidelines (U.S. EPA August 2014), and Department of Defense (DoD) Quality Systems Manual (QSM) for Environmental Laboratories Version 5.0 (DoD July 2013), where applicable. No results were qualified during data review; therefore, all results are considered usable by the project, according to U.S. EPA and DoD guidelines. An electronic version of this report has been electronically mailed to the NAVFAC SE Contracting Officers Technical Representative. Sincerely, Resolution Consultants By: Paul V. Stoddard, PG Robert Thomas, CHMM Task Order Manager Environmental Scientist Attachment A Attachment B Figures Laboratory Analytical Report
7 Attachment A Figures
8 AV29 FIRST FLOOR
9 AV32 FIRST FLOOR
10
11
12 NEW CUZCOS
13 OLD CUZCOS
14 Attachment B Laboratory Analytical Report
15 5/2/2016 Mr. Mike Dryden Earth Toxics, Inc. 206 Quail Way Logan UT Project Name: Site Investigation Project #: Workorder #: Dear Mr. Mike Dryden The following report includes the data for the above referenced project for sample(s) received on 4/27/2016 at Air Toxics Ltd. The data and associated QC analyzed by Modified TO-11A are compliant with the project requirements or laboratory criteria with the exception of the deviations noted in the attached case narrative. Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free the Project Manager: Kyle Vagadori at if you have any questions regarding the data in this report. Regards, Kyle Vagadori Project Manager Page 1 of 27
16 WORK ORDER #: Work Order Summary CLIENT: Mr. Mike Dryden Earth Toxics, Inc. 206 Quail Way Logan, UT BILL TO: Mr. Mike Dryden Earth Toxics, Inc. 206 Quail Way Logan, UT PHONE: FAX: DATE RECEIVED: 04/27/2016 DATE COMPLETED: 05/02/2016 P.O. # PROJECT # CONTACT: Site Investigation Kyle Vagadori FRACTION # NAME TEST 01A CZIAFM27B-1 Modified TO-11A 02A CZIAFM28B-1 Modified TO-11A 03A CZIAFM35A-1 Modified TO-11A 04A CZIAFM36A-1 Modified TO-11A 05A CZIAFM48A-1 Modified TO-11A 06A CZIAFM47A-1 Modified TO-11A 07A CZIAFM44A-1 Modified TO-11A 08A CZIAFM43A-1 Modified TO-11A 09A CZIAFM4A-1 Modified TO-11A 10A CZIAFM5A-1 Modified TO-11A 11A CZIAFM10B-1 Modified TO-11A 12A CZIAFM11B-1 Modified TO-11A 13A CZIAFM23A-1 Modified TO-11A 14A CZIAFM22A-1 Modified TO-11A 15A CZIAFM17A-1 Modified TO-11A 16A CZIAFM16A-1 Modified TO-11A 17A CZIAFMBLK Modified TO-11A 18A Lab Blank Modified TO-11A 19A LCS Modified TO-11A 19AA LCSD Modified TO-11A CERTIFIED BY: Technical Director DATE: 05/02/16 Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP , TX NELAP - T , UT NELAP CA , VA NELAP , WA NELAP - C935 Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program) Accreditation number: CA300005, Effective date: 10/18/2015, Expiration date: 10/17/2016. Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc. 180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA (916) (800) FAX (916) Page 2 of 27
17 LABORATORY NARRATIVE Modified TO-11A Earth Toxics, Inc. Workorder# Seventeen TO-11 Cartridge samples were received on April 27, The laboratory performed analysis via modified Method TO-11A using reverse phase High Pressure Liquid Chromatography (HPLC) with an Ultraviolet (UV) Detector. The method involves eluting the sorbent tubes with acetonitrile using a gravity feed technique. Method modifications taken to run these samples include: Requirement ACN Purity Check Initial Calibration Curve (ICAL) Blank Subtraction TO-11A Contribution of analytes from ACN determined as described Sections and of Compendium TO-11A. Multi-point using linear regression performed every 6 months; r^2 > Average blank concentrations calculated. Blank value subtracted from sample result. ATL Modifications Total contribution of analytes from ACN and cartridge combined is determined. Multi-point using average Response Factor; % RSD </= 10 %. Re-calibration if daily cal. fails, major maintenance, or column change. Linear regression is performed when requested. One Lab Blank is analyzed per batch; no blank subtraction performed on samples. Receiving Notes There were no receiving discrepancies. Analytical Notes Sampling volume was supplied by the client. A sample volume of 586 L was used to report sample CZIAFMBLK and the Laboratory Blank. As per project specific client request the laboratory has reported estimated values for target compound hits that are below the Reporting Limit but greater than the Method Detection Limit. Media for this analysis was certified at the Reporting Limit. Concentrations that are below the level at which the media was certified may be false positives. Definition of Data Qualifying Flags Seven qualifiers may have been used on the data analysis sheets and indicate as follows: B - present in laboratory blank greater than reporting limit. J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits. U - analyzed for but not detected above the detection limit. M - Reported value may be biased due to apparent matrix interferences. Page 3 of 27
18 File extensions may have been used on the data analysis sheets and indicates as follows: a-file was requantified b-file was quantified by a second column and detector r1-file was requantified for the purpose of reissue Page 4 of 27
19 Summary of Detected s Client Sample ID: CZIAFM27B-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM28B-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM35A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM36A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM48A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM47A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Page 5 of 27
20 Summary of Detected s Client Sample ID: CZIAFM44A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM43A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM4A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM5A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM10B-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM11B-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Page 6 of 27
21 Summary of Detected s Client Sample ID: CZIAFM23A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM22A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM17A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFM16A-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: CZIAFMBLK Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount J J Page 7 of 27
22 File Name: f Air Sample Volume(L): 586 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM27B-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:50:00 PM Date of Analysis: 4/29/16 11:17 PM Rpt. Limit Amount Amount Page 8 of 27
23 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM28B-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:48:00 PM Date of Analysis: 4/29/16 11:43 PM Rpt. Limit Amount Amount Page 9 of 27
24 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM35A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:51:00 PM Date of Analysis: 4/30/16 12:09 AM Rpt. Limit Amount Amount Page 10 of 27
25 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM36A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:53:00 PM Date of Analysis: 4/30/16 12:35 AM Rpt. Limit Amount Amount Page 11 of 27
26 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM48A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:31:00 PM Date of Analysis: 4/30/16 01:01 AM Rpt. Limit Amount Amount Page 12 of 27
27 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM47A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:33:00 PM Date of Analysis: 4/30/16 01:27 AM Rpt. Limit Amount Amount Page 13 of 27
28 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM44A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:36:00 PM Date of Analysis: 4/30/16 01:53 AM Rpt. Limit Amount Amount Page 14 of 27
29 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM43A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:38:00 PM Date of Analysis: 4/30/16 02:19 AM Rpt. Limit Amount Amount Page 15 of 27
30 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM4A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 4:10:00 PM Date of Analysis: 4/30/16 02:45 AM Rpt. Limit Amount Amount Page 16 of 27
31 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM5A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 4:13:00 PM Date of Analysis: 4/30/16 06:19 PM Rpt. Limit Amount Amount Page 17 of 27
32 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM10B-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 4:16:00 PM Date of Analysis: 4/30/16 04:29 AM Rpt. Limit Amount Amount Page 18 of 27
33 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM11B-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 4:20:00 PM Date of Analysis: 4/30/16 04:55 AM Rpt. Limit Amount Amount Page 19 of 27
34 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM23A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 4:01:00 PM Date of Analysis: 4/30/16 05:21 AM Rpt. Limit Amount Amount Page 20 of 27
35 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM22A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 3:59:00 PM Date of Analysis: 4/30/16 05:47 AM Rpt. Limit Amount Amount Page 21 of 27
36 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM17A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 4:04:00 PM Date of Analysis: 4/30/16 06:12 AM Rpt. Limit Amount Amount Page 22 of 27
37 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: CZIAFM16A-1 Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 4:07:00 PM Date of Analysis: 4/30/16 06:38 AM Rpt. Limit Amount Amount Page 23 of 27
38 File Name: f Air Sample Volume(L): 586 J = Estimated value. Container Type: TO-11 Cartridge Client Sample ID: CZIAFMBLK Lab ID#: A Rpt. Limit Date of Collection: 4/21/16 4:28:00 PM Date of Analysis: 4/29/16 10:51 PM Rpt. Limit Amount Amount J J Page 24 of 27
39 File Name: f Air Sample Volume(L): 586 J = Estimated value. Container Type: NA - Not Applicable Client Sample ID: Lab Blank Lab ID#: A Rpt. Limit Date of Collection: NA Date of Analysis: 4/30/16 04:03 AM Rpt. Limit Amount Amount J J Page 25 of 27
40 Client Sample ID: LCS Lab ID#: A File Name: f %Recovery Date of Collection: NA Date of Analysis: 4/29/16 09:34 PM Method Limits Air Sample Volume(L): 1.00 Container Type: NA - Not Applicable Page 26 of 27
41 Client Sample ID: LCSD Lab ID#: AA File Name: f %Recovery Date of Collection: NA Date of Analysis: 4/29/16 10:00 PM Method Limits Air Sample Volume(L): 1.00 Container Type: NA - Not Applicable Page 27 of 27
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44 5/2/2016 Mr. Mike Dryden Earth Toxics, Inc. 206 Quail Way Logan UT Project Name: Site Investigation Project #: Workorder #: Dear Mr. Mike Dryden The following report includes the data for the above referenced project for sample(s) received on 4/27/2016 at Air Toxics Ltd. The data and associated QC analyzed by Modified TO-11A are compliant with the project requirements or laboratory criteria with the exception of the deviations noted in the attached case narrative. Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free the Project Manager: Kyle Vagadori at if you have any questions regarding the data in this report. Regards, Kyle Vagadori Project Manager Page 1 of 26
45 WORK ORDER #: Work Order Summary CLIENT: Mr. Mike Dryden Earth Toxics, Inc. 206 Quail Way Logan, UT BILL TO: Mr. Mike Dryden Earth Toxics, Inc. 206 Quail Way Logan, UT PHONE: FAX: DATE RECEIVED: 04/27/2016 DATE COMPLETED: 05/02/2016 P.O. # PROJECT # CONTACT: Site Investigation Kyle Vagadori FRACTION # NAME TEST 01A AV32IAFMMP-1 Modified TO-11A 02A AV32IAFMM01-1 Modified TO-11A 03A AV32IAFMM02-1 Modified TO-11A 04A AV32IAFMBLK Modified TO-11A 05A ELCIAFMBL29-1 Modified TO-11A 06A ELCIAFMBL30-1 Modified TO-11A 07A ELCIAFMBL11-1 Modified TO-11A 08A ELCIAFMBL5-1 Modified TO-11A 09A ELCIAFMBL2-1 Modified TO-11A 10A ELCIAFMBL4-1 Modified TO-11A 11A ELCIAFMBL8-1 Modified TO-11A 12A ELCIAFMBL Modified TO-11A 13A ELCIAFMBL1-1 Modified TO-11A 14A ELCIAFMBL1-COM Modified TO-11A 15A AV29IAFMST-1 Modified TO-11A 16A AV29IAFMFT-1 Modified TO-11A 17A Lab Blank Modified TO-11A 18A LCS Modified TO-11A 18AA LCSD Modified TO-11A CERTIFIED BY: Technical Director DATE: 05/02/16 Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP , TX NELAP - T , UT NELAP CA , VA NELAP , WA NELAP - C935 Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program) Accreditation number: CA300005, Effective date: 10/18/2015, Expiration date: 10/17/2016. Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc. 180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA (916) (800) FAX (916) Page 2 of 26
46 LABORATORY NARRATIVE Modified TO-11A Earth Toxics, Inc. Workorder# Sixteen TO-11 Cartridge samples were received on April 27, The laboratory performed analysis via modified Method TO-11A using reverse phase High Pressure Liquid Chromatography (HPLC) with an Ultraviolet (UV) Detector. The method involves eluting the sorbent tubes with acetonitrile using a gravity feed technique. Method modifications taken to run these samples include: Requirement ACN Purity Check Initial Calibration Curve (ICAL) Blank Subtraction TO-11A Contribution of analytes from ACN determined as described Sections and of Compendium TO-11A. Multi-point using linear regression performed every 6 months; r^2 > Average blank concentrations calculated. Blank value subtracted from sample result. ATL Modifications Total contribution of analytes from ACN and cartridge combined is determined. Multi-point using average Response Factor; % RSD </= 10 %. Re-calibration if daily cal. fails, major maintenance, or column change. Linear regression is performed when requested. One Lab Blank is analyzed per batch; no blank subtraction performed on samples. Receiving Notes The Chain of Custody (COC) information for sample ELCIAFMBL1-1 did not match the entry on the sample tag with regard to sample identification. The information on the COC was used to process and report the sample. Analytical Notes Sampling volume was supplied by the client. A sample volume of 723 L was used to report sample AV32IAFMBLK and the Laboratory Blank. As per project specific client request the laboratory has reported estimated values for target compound hits that are below the Reporting Limit but greater than the Method Detection Limit. Media for this analysis was certified at the Reporting Limit. Concentrations that are below the level at which the media was certified may be false positives. Definition of Data Qualifying Flags Seven qualifiers may have been used on the data analysis sheets and indicate as follows: B - present in laboratory blank greater than reporting limit. J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits. U - analyzed for but not detected above the detection limit. Page 3 of 26
47 M - Reported value may be biased due to apparent matrix interferences. File extensions may have been used on the data analysis sheets and indicates as follows: a-file was requantified b-file was quantified by a second column and detector r1-file was requantified for the purpose of reissue Page 4 of 26
48 Summary of Detected s Client Sample ID: AV32IAFMMP-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: AV32IAFMM01-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: AV32IAFMM02-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: AV32IAFMBLK Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount J J Client Sample ID: ELCIAFMBL29-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: ELCIAFMBL30-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Page 5 of 26
49 Summary of Detected s Client Sample ID: ELCIAFMBL11-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: ELCIAFMBL5-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: ELCIAFMBL2-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: ELCIAFMBL4-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: ELCIAFMBL8-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: ELCIAFMBL Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Page 6 of 26
50 Summary of Detected s Client Sample ID: ELCIAFMBL1-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: ELCIAFMBL1-COM Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: AV29IAFMST-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Client Sample ID: AV29IAFMFT-1 Lab ID#: A Rpt. Limit Rpt. Limit Amount Amount Page 7 of 26
51 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: AV32IAFMMP-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 3:19:00 PM Date of Analysis: 4/30/16 10:58 AM Rpt. Limit Amount Amount Page 8 of 26
52 File Name: f Air Sample Volume(L): 723 Container Type: TO-11 Cartridge Client Sample ID: AV32IAFMM01-1 Lab ID#: A Rpt. Limit Date of Collection: 4/23/16 6:36:00 AM Date of Analysis: 4/30/16 11:24 AM Rpt. Limit Amount Amount Page 9 of 26
53 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: AV32IAFMM02-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 3:26:00 PM Date of Analysis: 4/30/16 11:50 AM Rpt. Limit Amount Amount Page 10 of 26
54 File Name: f Air Sample Volume(L): 723 J = Estimated value. Container Type: TO-11 Cartridge Client Sample ID: AV32IAFMBLK Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 3:30:00 PM Date of Analysis: 4/30/16 10:32 AM Rpt. Limit Amount Amount J J Page 11 of 26
55 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL29-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 4:20:00 PM Date of Analysis: 4/30/16 12:16 PM Rpt. Limit Amount Amount Page 12 of 26
56 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL30-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 4:23:00 PM Date of Analysis: 4/30/16 12:42 PM Rpt. Limit Amount Amount Page 13 of 26
57 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL11-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 4:29:00 PM Date of Analysis: 4/30/16 01:08 PM Rpt. Limit Amount Amount Page 14 of 26
58 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL5-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 4:34:00 PM Date of Analysis: 4/30/16 01:34 PM Rpt. Limit Amount Amount Page 15 of 26
59 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL2-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 4:39:00 PM Date of Analysis: 4/30/16 02:00 PM Rpt. Limit Amount Amount Page 16 of 26
60 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL4-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 4:44:00 PM Date of Analysis: 4/30/16 02:26 PM Rpt. Limit Amount Amount Page 17 of 26
61 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL8-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 4:50:00 PM Date of Analysis: 4/30/16 03:43 PM Rpt. Limit Amount Amount Page 18 of 26
62 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 4:55:00 PM Date of Analysis: 4/30/16 04:09 PM Rpt. Limit Amount Amount Page 19 of 26
63 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL1-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 5:02:00 PM Date of Analysis: 4/30/16 04:35 PM Rpt. Limit Amount Amount Page 20 of 26
64 File Name: f Air Sample Volume(L): 576 Container Type: TO-11 Cartridge Client Sample ID: ELCIAFMBL1-COM Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 5:07:00 PM Date of Analysis: 4/30/16 05:01 PM Rpt. Limit Amount Amount Page 21 of 26
65 File Name: f Air Sample Volume(L): 723 Container Type: TO-11 Cartridge Client Sample ID: AV29IAFMST-1 Lab ID#: A Rpt. Limit Date of Collection: 4/23/16 6:28:00 AM Date of Analysis: 4/30/16 05:27 PM Rpt. Limit Amount Amount Page 22 of 26
66 File Name: f Air Sample Volume(L): 577 Container Type: TO-11 Cartridge Client Sample ID: AV29IAFMFT-1 Lab ID#: A Rpt. Limit Date of Collection: 4/22/16 5:51:00 PM Date of Analysis: 4/30/16 05:53 PM Rpt. Limit Amount Amount Page 23 of 26
67 File Name: f a Air Sample Volume(L): 723 J = Estimated value. Container Type: NA - Not Applicable Client Sample ID: Lab Blank Lab ID#: A Rpt. Limit Date of Collection: NA Date of Analysis: 4/30/16 07:56 AM Rpt. Limit Amount Amount J J Page 24 of 26
68 Client Sample ID: LCS Lab ID#: A File Name: f %Recovery Date of Collection: NA Date of Analysis: 4/30/16 07:04 AM Method Limits Air Sample Volume(L): 1.00 Container Type: NA - Not Applicable Page 25 of 26
69 Client Sample ID: LCSD Lab ID#: AA File Name: f %Recovery Date of Collection: NA Date of Analysis: 4/30/16 07:30 AM Method Limits Air Sample Volume(L): 1.00 Container Type: NA - Not Applicable Page 26 of 26
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