2014 AAFCO Check Sample Mycotoxins Program. Samples Engineered to Contain Relevant Concentrations of Significant Mycotoxins.
|
|
|
- Peregrine Henry
- 8 years ago
- Views:
Transcription
1 2014 AAFCO Check Sample Mycotoxins Program Samples Engineered to Contain Relevant Concentrations of Significant Mycotoxins.
2 The Samples Source the base feed. Materials thoroughly processed with regard to particle size and blending. 70,000 lb Masters Collection Carefully sourced feeds naturally contaminated with Mycotoxins. Incubated to raise concentration. Homogenous Samples for distribution. Certificate of Analysis and homogeneity data.
3 In Sacramento Last Summer: I reported on Sample , Poultry Feed. Our First Sample! Two More Samples Completed Last Year: , Swine Feed (Issue Date: August 31 st ) , Cattle Feed (Issue Date: October 31 st ) All 3 Samples Reported: Using a Reference Lab Assigned Value for Measure of Location Horwitz %RSD Measure of Dispersion We will talk about the Learning Curve
4 3 Samples so Far in 2014 Number of Labs Participating Poultry Feed Swine Feed Cattle Feed Code Analyte (ppb) (23 Labs) (25 Labs) (26 Labs) 600 Total Aflatoxin AB AB AG AG Deoxynivalenol Total Fumonisin FB FB FB Ochratoxin A T Zearalenone
5 3 Samples so Far in 2014 Assigned Values (Reference Lab) Poultry Feed Swine Feed Cattle Feed Code Analyte (ppb) (23 Labs) (25 Labs) (26 Labs) 600 Total Aflatoxin AB AB AG1 ND (0.5) ND (0.5) AG2 ND (0.5) ND (0.5) ND (0.5) 610 Deoxynivalenol 1, , Total Fumonisin 1,900 2,100 1, FB1 1,300 1,500 1, FB FB Ochratoxin A T Zearalenone
6 Tracking Z Scores: Reference Lab vs Participant Consensus Measure of Location X A Z = X LAB X A σ ffp Horwitz Used as the Measure of Dispersion σ ffp in Both Cases Sample (218 Detects) Reference Consensus Compliant Z 68.8% 67.9% Warning Z 12.4% 12.8% Actionable Z 18.8% 19.3% Sample (237 Detects) Reference Consensus Compliant Z 69.6% 72.6% Warning Z 13.5% 13.1% Actionable Z 16.9% 14.3% Sample (252 Detects) Reference Consensus Compliant Z 55.2% 68.7% Warning Z 17.1% 10.3% Actionable Z 27.8% 21.0%
7 Sample Cattle Feed Detail Tracking Z Scores For The Mycotoxins: Reference Lab vs Participant Consensus, Measure of Location Participant Consensus Reference Lab Detects Value Compliant Warning Actionable Value Compliant Warning Actionable Total Aflatoxin % 4.3% 4.3% % 8.7% 2.2% AB % 0.0% 14.3% % 0.0% 14.3% AB % 16.7% 0.0% % 16.7% 8.3% AG % 0.0% 0.0% % 0.0% 0.0% AG2 0 ND (0.5) Deoxynivalenol 44 2, % 9.1% 34.1% 2, % 13.6% 34.1% Total Fumonisin 28 2, % 10.7% 28.6% 1, % 10.7% 57.1% FB1 12 1, % 16.7% 8.3% 1, % 0.0% 33.3% FB % 16.7% 0.0% % 33.3% 66.7% FB % 16.7% 0.0% % 0.0% 66.7% Ochratoxin A % 13.3% 33.3% % 23.3% 30.0% T % 14.3% 42.9% % 28.6% 42.9% Zearalenone % 12.5% 28.1% % 40.6% 12.5%
8 Let s Look at Some Data Distribution Charts For Sample , Cattle Feed Reference Lab vs Participant Consensus Compare Measure of Location Relative to Data Detects Reference Lab Normal Consensus Normal Consensus Ref. LAB
9 Total Aflatoxin (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb # Methods Used 10 Assigned Value (ppb) Kernel Bandwidth 5.92 (ppb) Unique LOD's at: Horwitz SD 7.90 (ppb) Number of Non-Detects 0 Reference Lab (ppb) Number of Detects 46 Horwitz SD 9.37 (ppb) Participating Labs 18 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
10 AB1 (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb # Methods Used 3 Assigned Value (ppb) Kernel Bandwidth 5.60 (ppb) Unique LOD's at: Horwitz SD 7.47 (ppb) Number of Non-Detects 0 Reference Lab (ppb) Number of Detects 14 Horwitz SD 8.84 (ppb) Participating Labs 7 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
11 1.2 1 AB2 (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb # Methods Used 3 Assigned Value (ppb) Kernel Bandwidth 0.32 (ppb) Unique LOD's at: 1 (ppb) Horwitz SD 0.42 (ppb) Number of Non-Detects 2 Reference Lab (ppb) Number of Detects 12 Horwitz SD 0.37 (ppb) Participating Labs 7 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
12 Deoxynivalenol (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb , , , , , , # Methods Used 7 Assigned Value 2114 (ppb) Kernel Bandwidth (ppb) Unique LOD's at: Horwitz SD (ppb) Number of Non-Detects 0 Reference Lab 2700 (ppb) Number of Detects 44 Horwitz SD (ppb) Participating Labs 22 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
13 Total Fumonisin (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb , , , , , , , # Methods Used 5 Assigned Value 2428 (ppb) Kernel Bandwidth (ppb) Unique LOD's at: Horwitz SD (ppb) Number of Non-Detects 0 Reference Lab 1800 (ppb) Number of Detects 28 Horwitz SD (ppb) Participating Labs 14 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
14 FB1 (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb , , , , , , # Methods Used 2 Assigned Value 1860 (ppb) Kernel Bandwidth (ppb) Unique LOD's at: Horwitz SD (ppb) Number of Non-Detects 0 Reference Lab 1400 (ppb) Number of Detects 12 Horwitz SD (ppb) Participating Labs 6 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
15 FB2 (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb , , # Methods Used 2 Assigned Value (ppb) Kernel Bandwidth (ppb) Unique LOD's at: Horwitz SD (ppb) Number of Non-Detects 0 Reference Lab (ppb) Number of Detects 12 Horwitz SD (ppb) Participating Labs 6 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
16 FB3 (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb # Methods Used 1 Assigned Value (ppb) Kernel Bandwidth (ppb) Unique LOD's at: Horwitz SD (ppb) Number of Non-Detects 0 Reference Lab (ppb) Number of Detects 6 Horwitz SD (ppb) Participating Labs 3 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
17 Ochratoxin A (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb # Methods Used 4 Assigned Value (ppb) Kernel Bandwidth (ppb) Unique LOD's at: Horwitz SD (ppb) Number of Non-Detects 0 Reference Lab (ppb) Number of Detects 30 Horwitz SD (ppb) Participating Labs 14 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
18 T-2 (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb # Methods Used 3 Assigned Value (ppb) Kernel Bandwidth (ppb) Unique LOD's at: 200 (ppb) Horwitz SD (ppb) Number of Non-Detects (ppb) Reference Lab (ppb) Number of Detects 14 Horwitz SD (ppb) Participating Labs 9 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
19 Zearalenone (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb # Methods Used 5 Assigned Value 216 (ppb) Kernel Bandwidth (ppb) Unique LOD's at: 0 (ppb) Horwitz SD (ppb) Number of Non-Detects (ppb) Reference Lab 251 (ppb) Number of Detects 32 Horwitz SD (ppb) Participating Labs 18 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
20 Now the Question is: What do we want our Z Score to tell us? Should we be assessed against a single Reference Lab Assigned Value? Reference Lab Normal Consensus Normal Should we be assessed against our best estimate of the center of all the data? Lab DATA Ref. LAB Consensus Z
21 2014 Mycotoxin CSP Ochratoxin Methods (Bias?)
22 Ochratoxin A (ppb) Code: In Sample # , Cattle Feed Kernel Density Envelope Detected Values Relative to Normal Horwitz Curve Robust Normal Kernel Envelope Data Reference Lab Normal Reference Lab Location Issue Date: 10/31/ Z ppb # Methods Used 4 Assigned Value (ppb) Kernel Bandwidth (ppb) Unique LOD's at: Horwitz SD (ppb) Number of Non-Detects 0 Reference Lab (ppb) Number of Detects 30 Horwitz SD (ppb) Participating Labs 14 Note: Area Under the Kernel Envelope is Identical to Area Under Horwitz Normal Curve within the chart.
23 Mycotoxin Proficiency Testing Issue Date: 10/31/2014 Analytes for Sample # Cattle Feed Detect? Probability Robust Lab # Code Analyte Method Result 1 Result 2 D1 D2 LOD of Detection Z Score Value Horwitz Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC Y Y 100% Ochratoxin A (ppb) LC post-col photochem der. Fl Y Y 100%
24 Mycotoxin Proficiency Testing Issue Date: 08/31/2014 Analytes for Sample # Swine Feed Detect? Probability Robust Lab # Code Analyte Method Result 1 Result 2 D1 D2 LOD of Detection Z Score Value Horwitz Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC Y Y 100% Ochratoxin A (ppb) LC post-col photochem der. Fl Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100%
25 Mycotoxin Proficiency Testing Issue Date: 05/31/2014 Analytes for Sample # Poultry Feed Detect? Probability Robust Lab # Code Analyte Method Result 1 Result 2 D1 D2 LOD of Detection Z Score Value Horwitz Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS N Y %
26 2014 Mycotoxin CSP Analyte Report Ordered by Z Score
27 Mycotoxin Proficiency Testing Issue Date: 10/31/2014 Analytes for Sample # Cattle Feed Detect? Probability Robust Lab # Code Analyte Method Result 1 Result 2 D1 D2 LOD of Detection Z Score Value Horwitz Total Aflatoxin (ppb) r-biopharm Ridascreen FAST Aflat Y Y 100% Total Aflatoxin (ppb) Vicam Aflatest Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) LC post-col photochem der. Fl Y Y 100% Total Aflatoxin (ppb) LC Y Y 100% Total Aflatoxin (ppb) LC post-col photochem der. Fl Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) LC-MS/MS Y Y 100% Total Aflatoxin (ppb) Neogen Veratox Aflatoxin Y Y 100% Total Aflatoxin (ppb) TLC Y Y 100% Total Aflatoxin (ppb) LC Y Y 100% Total Aflatoxin (ppb) Miscellaneous technique Y Y 100% Total Aflatoxin (ppb) r-biopharm Ridascreen FAST Aflat Y Y 100% Total Aflatoxin (ppb) LC Y Y 100% Total Aflatoxin (ppb) Other Rapid Test Kit Y Y 100% AB1 (ppb) LC-MS/MS Y Y 100% AB1 (ppb) LC-MS/MS Y Y 100% AB1 (ppb) LC post-col photochem der. -Fl Y Y 100% AB1 (ppb) LC-MS/MS Y Y 100% AB1 (ppb) Vicam Aflatest, LC-Fl Y Y 100% AB1 (ppb) LC-MS/MS Y Y 100% AB1 (ppb) LC-MS/MS Y Y 100% AB2 (ppb) LC-MS/MS Y Y 100% AB2 (ppb) Vicam Aflatest, LC-Fl Y Y 100% AB2 (ppb) LC post-col photochem der.-fl Y Y 100% AB2 (ppb) LC-MS/MS Y Y 100% AB2 (ppb) LC-MS/MS Y Y 100% Page 1 of 4
28 Detect? Probability Robust Lab # Code Analyte Method Result 1 Result 2 D1 D2 LOD of Detection Z Score Value Horwitz AB2 (ppb) LC-MS/MS Y Y 100% AB2 (ppb) LC-MS/MS N N % NoZ AG1 (ppb) LC-MS/MS Y Y 100% AG1 (ppb) LC post-col photochem der. -Fl N N % NoZ AG1 (ppb) LC-MS/MS N N % NoZ AG1 (ppb) LC-MS/MS N N % NoZ AG1 (ppb) LC-MS/MS N N % NoZ AG1 (ppb) LC-MS/MS N N % NoZ AG1 (ppb) Vicam Aflatest, LC-Fl N N % NoZ AG2 (ppb) LC post-col photochem der. -Fl N N 0.44 ND (0.5) AG2 (ppb) LC-MS/MS N N 0.5 ND (0.5) AG2 (ppb) LC-MS/MS N N 1 ND (0.5) AG2 (ppb) LC-MS/MS N N 0.3 ND (0.5) AG2 (ppb) LC-MS/MS N N 1 ND (0.5) AG2 (ppb) LC-MS/MS N N 1.6 ND (0.5) AG2 (ppb) Vicam Aflatest, LC-Fl N N 0.6 ND (0.5) Deoxynivalenol (ppb) Neogen Veratox for DON Y Y 100% , Deoxynivalenol (ppb) r-biopharm Ridascreen DON Y Y 100% , Deoxynivalenol (ppb) GC-MS Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON Y Y 100% , Deoxynivalenol (ppb) LC Y Y 100% , Deoxynivalenol (ppb) LC-MS/MS 1,271 1,199 Y Y 100% , Deoxynivalenol (ppb) LC-MS/MS 1,147 1,751 Y Y 100% , Deoxynivalenol (ppb) LC-MS/MS 1,688 1,661 Y Y 100% , Deoxynivalenol (ppb) LC-MS/MS 1,858 1,591 Y Y 100% , Deoxynivalenol (ppb) LC-MS/MS 2,100 2,030 Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON 2,300 2,000 Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON 2,300 2,100 Y Y 100% , Deoxynivalenol (ppb) LC-MS/MS 2,100 2,370 Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON 2,400 2,200 Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON 2,500 2,100 Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON 2,400 2,350 Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON 2,400 2,400 Y Y 100% , Deoxynivalenol (ppb) r-biopharm Ridascreen FAST DON 1,812 3,160 Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON 2,200 2,900 Y Y 100% , Deoxynivalenol (ppb) Neogen Veratox for DON 2,478 2,756 Y Y 100% , Deoxynivalenol (ppb) Miscellaneous technique 3,010 2,290 Y Y 100% , Total Fumonisin (ppb) Vicam FumoniTest Y Y 100% , Total Fumonisin (ppb) Neogen Veratox for Fumonisin 5/ Y Y 100% , Total Fumonisin (ppb) r-biopharm Ridascreen Fast Fumo 3 3 Y Y 100% , Total Fumonisin (ppb) Neogen Veratox for Fumonisin Y Y 100% , Total Fumonisin (ppb) Neogen Veratox for Fumonisin 1,600 1,900 Y Y 100% , Page 2 of 4
29 Detect? Probability Robust Lab # Code Analyte Method Result 1 Result 2 D1 D2 LOD of Detection Z Score Value Horwitz Total Fumonisin (ppb) Neogen Veratox for Fumonisin 1,900 1,600 Y Y 100% , Total Fumonisin (ppb) Neogen Veratox for Fumonisin 2,400 2,050 Y Y 100% , Total Fumonisin (ppb) LC-MS/MS 2,296 2,154 Y Y 100% , Total Fumonisin (ppb) Neogen Veratox for Fumonisin 2,200 2,450 Y Y 100% , Total Fumonisin (ppb) LC-MS/MS 2,630 2,440 Y Y 100% , Total Fumonisin (ppb) Neogen Veratox for Fumonisin 3,300 2,200 Y Y 100% , Total Fumonisin (ppb) Neogen Veratox for Fumonisin 2,925 2,690 Y Y 100% , Total Fumonisin (ppb) r-biopharm Ridascreen Fast Fumo 2,938 2,833 Y Y 100% , Total Fumonisin (ppb) Neogen Veratox for Fumonisin 3,000 3,000 Y Y 100% , FB1 (ppb) LC-MS/MS 1,679 1,605 Y Y 100% , FB1 (ppb) LC-MS/MS 1,720 1,650 Y Y 100% , FB1 (ppb) LC-MS/MS 1,758 1,692 Y Y 100% , FB1 (ppb) LC-MS/MS 1,770 1,768 Y Y 100% , FB1 (ppb) LC-Fl, OPA der. 2,494 2,466 Y Y 100% , FB1 (ppb) LC-MS/MS 2,139 3,307 Y Y 100% , FB2 (ppb) LC-MS/MS Y Y 100% FB2 (ppb) LC-MS/MS Y Y 100% FB2 (ppb) LC-MS/MS Y Y 100% FB2 (ppb) LC-MS/MS Y Y 100% FB2 (ppb) LC-Fl, OPA der Y Y 100% FB2 (ppb) LC-MS/MS Y Y 100% FB3 (ppb) LC-MS/MS Y Y 100% FB3 (ppb) LC-MS/MS Y Y 100% FB3 (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) Neogen Veratox for Ochratoxin Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC-MS/MS Y Y 100% Ochratoxin A (ppb) LC Y Y 100% Ochratoxin A (ppb) LC post-col photochem der. Fl Y Y 100% T-2 (ppb) LC-MS/MS Y Y 100% T-2 (ppb) LC-MS/MS Y Y 100% T-2 (ppb) LC-MS/MS Y Y 100% T-2 (ppb) LC-MS/MS Y Y 100% Page 3 of 4
30 Detect? Probability Robust Lab # Code Analyte Method Result 1 Result 2 D1 D2 LOD of Detection Z Score Value Horwitz T-2 (ppb) r-biopharm Ridascreen FAST T Y Y 100% T-2 (ppb) Neogen Veratox T-2 / HT-2 8,418 8,659 Y Y 100% T-2 (ppb) Neogen Veratox T-2 / HT-2 40,100 40,760 Y Y 100% T-2 (ppb) LC-MS/MS N N % NoZ T-2 (ppb) LC-MS/MS N N % NoZ Zearalenone (ppb) Neogen Veratox Zearalenone Y Y 100% Zearalenone (ppb) LC-MS/MS Y Y 100% Zearalenone (ppb) r-biopharm Ridascreen FAST Zear Y Y 100% Zearalenone (ppb) LC-MS/MS Y Y 100% Zearalenone (ppb) LC-MS/MS Y Y 100% Zearalenone (ppb) Neogen Veratox Zearalenone Y Y 100% Zearalenone (ppb) LC-MS/MS Y Y 100% Zearalenone (ppb) Neogen Veratox Zearalenone Y Y 100% Zearalenone (ppb) r-biopharm Ridascreen FAST Zear Y Y 100% Zearalenone (ppb) Neogen Veratox Zearalenone Y Y 100% Zearalenone (ppb) Neogen Veratox Zearalenone Y Y 100% Zearalenone (ppb) LC-MS/MS Y Y 100% Zearalenone (ppb) Neogen Veratox Zearalenone Y Y 100% Zearalenone (ppb) LC Y Y 100% Zearalenone (ppb) LC-MS/MS Y Y 100% Zearalenone (ppb) Neogen Veratox Zearalenone Y Y 100% Zearalenone (ppb) Neogen Veratox Zearalenone N N % NoZ Zearalenone (ppb) LC-MS/MS N N % NoZ Notes: Interpreting Z Scores: Red indicates a normally distributed Z value >3 or <-3 (requires action), Orange = Z between 2 and 3 or -2 and -3 (warning) and Green = Z < 2 and >-2 (OK at 95%). If only 1 of 2 results detected Z for that is Grey and Probability of Detection is for the Non-Detect (see documentation). A Red NoZ indicates both results Not Detected with a Probability Of Detecting a single value. Where the Assigned Value is ND then the LOD follows as (LOD) in the Analyte units. Page 4 of 4
31 Revised Mycotoxin Proposal Recommendations Use Robust Consensus to Calculate Z Scores. Where There is Minimal Data Use Reference Lab to Calculate Z Scores. Continue to Collect Reference Lab Homogeneity Data. Continue to Use Horwitz Relationship to Estimate σ p (fit for purpose). Continue to Calculate Probability of Detection for Non Detects. Include Analyte Report in the Data Reporting Website Comments?
32 Dog Food # Ship Date ~ 12/20/2014 Data Due 01/10/2015 Reports Available 01/31/2015
33 THANK YOU!
LC-MS/MS, the new reference method for mycotoxin analysis
LC-MS/MS, the new reference method for mycotoxin analysis What is necessary for the implementation of the multi-residue mycotoxin method in an analytical laboratory? Azel Swemmer azel@fdalab.co.za AFMA
Improving mycotoxins measurements by combining rapid analysis with dust sampling
Improving mycotoxins measurements by combining rapid analysis with dust sampling Project presentation Dr. Scarlett Biselli, Mareike Reichel Mycotoxin Forum 5-6.09.13, Brussel www.eurofins.de Dust Sampling
ORDER FORM 2011 VETERINARY DRUG RESIDUES AND MYCOTOXINS
ORDER FORM 2011 VETERINARY DRUG RESIDUES AND MYCOTOXINS COMPANY NAME SHIPPING ADDRESS..... POST CODE:..CITY: COUNTRY.... CONTACT PERSON:... E-MAIL.. TEL.No:.FAX.No.. VAT N. (mandatory for EU companies):..
Magruder Statistics & Data Analysis
Magruder Statistics & Data Analysis Caution: There will be Equations! Based Closely On: Program Model The International Harmonized Protocol for the Proficiency Testing of Analytical Laboratories, 2006
AAFCO Check Sample Program New Data Reporting Website Manual Date of Issue: March 1 st 2014
Victoria S. Siegel, Ph.D., Chair Collaborative Check Sample Program Committee AAFCO Check Sample Program New Data Reporting Website Manual Date of Issue: March 1 st 2014 1. Registered participants in any
ONZENFUMOTADON UMOTADONZENFUM ENFUMOTAAflaDON ENDONFUMOTADON ENAflaOTAAflaDON ONFUMZEFUMOTAZ UMZENFUMOTADON TADONZENFUMDON
Mycotoxins fladonzenfumota ONZENFUMOTADON UMOTADONZENFUM ENFUMOTAAflaDON fladonzenotafum ENDONFUMOTADON UMOTADONZENFUM ENAflaOTAAflaDON ONFUMZEFUMOTAZ UMZENFUMOTADON TADONZENFUMDON ENFUMOTAAflaDON fladonzenfumota
PROFICIENCY TESTING PROGRAMS FOOD CONTAMINANTS
A28 A31a A31b A31c A31d A32a A32b A32c A32d A32e A44a A44b 74 76 77 PROFICIENCY TESTING PROGRAMS FOOD CONTAMINANTS Patulin determination Mycotoxins: dried fruits, spices and other products Mycotoxins:
Aflatoxin Handbook. United States Department of Agriculture. Grain Inspection, Packers and Stockyards Administration. Federal Grain Inspection Service
United States Department of Agriculture Aflatoxin Handbook Grain Inspection, Packers and Stockyards Administration Federal Grain Inspection Service Washington, DC March 2002 United States Department of
Monoclonal Antibodies Production for Quantification of Ochratoxin A in Feedstuffs by Enzyme-Linked Immunosorbent Assay
Kasetsart J. (Nat. Sci.) 37 : 137-144 (2003) Monoclonal Antibodies Production for Quantification of Ochratoxin A in Feedstuffs by Enzyme-Linked Immunosorbent Assay Montri Punyatong, Puntipa Pongpiachan
MYCO-GLOBE MEETING. Stanhope Hotel, Brussels, Belgium October 21 22, 2004
MYCO-GLOBE MEETING Stanhope Hotel, Brussels, Belgium October 21 22, 2004 MYCOTOXINS: A GLOBAL PROBLEM WFO MARASAS PROMEC UNIT, MEDICAL RESEARCH COUNCIL TYGERBERG, SOUTH AFRICA wally.marasas@mrc.ac.za MOST
MANAGING THE EFFECTS OF MOLDS AND MYCOTOXINS IN RUMINANTS
MANAGING THE EFFECTS OF MOLDS AND MYCOTOXINS IN RUMINANTS Brian Tarr, Ruminant Nutritionist Shur-Gain, Nutreco Canada Inc. November 2006 1 MANAGING THE EFFECTS OF MOLDS AND MYCOTOXINS IN RUMINANTS Brian
Mycotoxin Reference Materials
, Inc. www.trilogylab.com 1/4 A-C-215 A-C-276 A-C-277 A-C-279 AC-285 AC-287 AC-288 AC-289 AC-291 Concentration 1.7 ppb 50.8 ppb 98.7 ppb 5.9 ppb 5.4 ppb 21.7 ppb 9.6ppb 18.3ppb Expiry Date 11/1/2017 2/1/2018
COMMISSION REGULATION (EU)
L 52/32 Official Journal of the European Union 3.3.2010 COMMISSION REGULATION (EU) No 178/2010 of 2 March 2010 amending Regulation (EC) No 401/2006 as regards groundnuts (peanuts), other oilseeds, tree
The Use of Isolated Human Lymphocytes in Mycotoxin Cytotoxicity Testing
Int. J. Mol. Sci. 2008, 9, 1515-1526; DOI: 10.3390/ijms9081515 OPEN ACCESS International Journal of Molecular Sciences ISSN 1422-0067 http://www.mdpi.org/ijms Article The Use of Isolated Human Lymphocytes
Pesticide residue analysis: New Trends. Michal Godula, Ph.D. EU Marketing Manager Food Safety & Environmental Thermo Fisher Scientific
Pesticide residue analysis: New Trends Michal Godula, Ph.D. EU Marketing Manager Food Safety & Environmental Thermo Fisher Scientific Why pesticide analysis? Extensively used in agriculture to control
South East of Process Main Building / 1F. North East of Process Main Building / 1F. At 14:05 April 16, 2011. Sample not collected
At 14:05 April 16, 2011 At 13:55 April 16, 2011 At 14:20 April 16, 2011 ND ND 3.6E-01 ND ND 3.6E-01 1.3E-01 9.1E-02 5.0E-01 ND 3.7E-02 4.5E-01 ND ND 2.2E-02 ND 3.3E-02 4.5E-01 At 11:37 April 17, 2011 At
FAT, PROTEIN, CASEIN, LACTOSE, UREA COW MILK. FT 001 (series of 10 samples) FT 002 (series of 5 samples)
FAT, PROTEIN, CASEIN, LACTOSE, UREA COW MILK FT 001 (series of 10 samples) FT 002 (series of 5 samples) Sample description: 80 ml raw cow milk sample in a screw colored cap plastic vials. Scope: to be
Chapter 26: Tests of Significance
Chapter 26: Tests of Significance Procedure: 1. State the null and alternative in words and in terms of a box model. 2. Find the test statistic: z = observed EV. SE 3. Calculate the P-value: The area under
Bt corn in Italy: A missed opportunity for farmers and feeders
Emerging Market Leaders Workshop on Effective Messaging on Global Food Production Issues May 20 th 2015, Rome Bt corn in Italy: A missed opportunity for farmers and feeders Marco Aurelio Pasti AMI - Associazione
Health hazards associated with animal feed
SECTION 1 Health hazards associated with animal feed USDA Health hazards associated with animal feed SECTION 1 3 INTRODUCTION Food safety hazards associated with animal feed can be biological, chemical
PRICE LIST AND SUBSCRIPTION MODEL 2013 (to be sent by fax or email to Laboratorio Standard Latte) A) ANNUAL SUPPLY AGREEMENT
Laboratory Shipping address Billing address Tel Fax Vat No. Email Contact ASSOCIAZIONE ITALIANA ALLEVATORI PRICE LIST AND SUBSCRIPTION MODEL 2013 (to be sent by fax or email to Laboratorio Standard Latte)
Methodology Research San Ysidro Schools California 2005 2008
Methodology Research San Ysidro Schools California 20052008 Algebraic Thinking Results for San Ysidro Schools 2005 2008 Implementation: San Ysidro Schools began working with National Training Network to
FOOD FOR THOUGHT Topical Insights from our Subject Matter Experts UNDERSTANDING WHAT IS NEEDED TO PRODUCE QUALITY DATA
FOOD FOR THOUGHT Topical Insights from our Subject Matter Experts UNDERSTANDING WHAT IS NEEDED TO PRODUCE QUALITY DATA The NFL White Paper Series Volume 7, January 2013 Overview and a Scenario With so
Practical Aspects of Drug Testing in Human Hair
Practical Aspects of Drug Testing in Human Hair Laboratory Perspective James A. Bourland, Ph.D., DABFT FOR INTERNAL USE ONLY. NOT FOR PRINT OR DISTRIBUTION Overview of Collection Process FOR INTERNAL USE
I. RECOMMENDED PRACTICES BASED ON GOOD AGRICULTURAL PRACTICES (GAP) AND GOOD MANUFACTURING PRACTICES (GMP)
CAC/RCP 51-2003 Page 1 of 8 CODE OF PRACTICE FOR THE PREVENTION AND REDUCTION OF MYCOTOXIN CONTAMINATION IN CEREALS, INCLUDING ANNEXES ON OCHRATOXIN A, ZEARALENONE, FUMONISINS AND TRICOTHECENES CAC/RCP
Interlaboratory studies
Interlaboratory studies Department of Food Chemistry and Analysis, ICT Prague Vladimír Kocourek Prague, 2012 Interlaboratory studies Various titles: Interlaboratory proficiency test or studies Interlaboratory
Novel analytical methods for Fusarium toxins in the cereal food chain
Novel analytical methods for Fusarium toxins in the cereal food chain Nouvelles méthodes pour l analyse des mycotoxines de Fusarium dans la chaîne de transformation des céréales Visconti, Angelo ; De Girolamo,
Table 1: test materials. MA1140 maize 55 gr A x 2 55 gr B x 2. MA1141 maize 55 gr A x 2 55 gr B x 2. MI1142 lyophilized milk 110 ml A x 2 20 ml B x 2
1. REFERENCES Progetto Trieste 2011, Mycotoxins was managed in agreement with the principles of ISO GUIDE 17043:2010 and also in agreement with the procedure described in The International Harmonised Protocol
Consuming Real Time Analytics and KPI powered by leveraging SAP Lumira and SAP Smart Business in Fiori SESSION CODE: 0611 Draft!!!
Consuming Real Time Analytics and KPI powered by leveraging SAP Lumira and SAP Smart Business in Fiori SESSION CODE: 0611 Draft!!! Michael Sung SAP Consuming Real Time Analytics and KPI powered by leveraging
PRICE LIST AND SUBSCRIPTION MODEL 2015 (to be sent by fax or email to Laboratorio Standard Latte) A) ANNUAL SUPPLY AGREEMENT
Laboratory Shipping address Billing address Tel Fax Vat No. Email Contact ASSOCIAZIONE ITALIANA ALLEVATORI PRICE LIST AND SUBSCRIPTION MODEL 2015 (to be sent by fax or email to Laboratorio Standard Latte)
Seagate File Recovery for MAC. Seagate Recovery Services
Seagate File Recovery for MAC Seagate Recovery Services The Seagate File Recovery for Mac support includes:: - these specific error messages: broken file name; file already exists; bad sectors option;
Agri Livestock Asia. 5th International conference Karachi April 26-28 Alain Réocreux Olmix France Orient Animal Health
Agri Livestock Asia 5th International conference Karachi April 26-28 Alain Réocreux Olmix France Orient Animal Health Nanotechnology M T.X+ Toxin Binder in Livestock Industry and farm applications Eco
Estimating college enrollment rates for Virginia public high school graduates
ISSUES& ANSWERS REL 2011 No. 104 Estimating college enrollment rates for Virginia public high school graduates ISSUES& ANSWERS REL 2011 No. 104 Estimating college enrollment rates for Virginia public high
Implementing New USP Chapters for Analytical Method Validation
Implementing New USP Chapters for Analytical Method Validation March 2010 Ludwig Huber Fax.: +49 7243 602 501 E-mail: Ludwig_Huber@labcompliance.com Today s Agenda Handling Method Changes vs. Adjustments
Recent Developments in GMP s & HACCP
Recent Developments in GMP s & HACCP Good Manufacturing Practices Modern GMP s (mgmp s) Multiple updates, including: Strengthening ready-to-eat (RTE) controls Chemical Control Program Traceability Recall
ซ ต าเทคโนโลย แก ป ญหาสารพ ษเช อรา
ซ ต าเทคโนโลย แก ป ญหาสารพ ษเช อรา ซ ต าเทคโนโลย แก ป ญหาสารพ ษเช อรา Mycotoxin ความท าทาย Key Raw material : Mycotoxin contamination Aflatoxin Zearalenone Fumonisin T2 Toxin Soy Bean Meal ++ ++ ++ ++
PROFICIENCY TESTING PROGRAMS FEED
PROFICIENCY TESTING PROGRAMS FEED A13 Feed 14 Forages 22 A26a A42 A67 A67a Silages Amino acids Premix Pet food (10 rounds per year) Pet food (5 rounds per year) A = PTS accredited by COFRAC A = Circuit
A Guide to Using Excel in Physics Lab
A Guide to Using Excel in Physics Lab Excel has the potential to be a very useful program that will save you lots of time. Excel is especially useful for making repetitious calculations on large data sets.
Pacific Premier Bank s Business e- Banking Getting Started Guide with QuickBooks 2013-2015 for Windows
Pacific Premier Bank s Business e- Banking Getting Started Guide with QuickBooks 2013-2015 for Windows Table of Contents CONNECT AND UPDATE YOUR DATA... 2 SET UP AN ACCOUNT FOR ONLINE BANKING (DIRECT CONNECT)...
Delivering a. New Era. of Technical. Support Services
Delivering a New Era of Technical Support Services 1 Constantly setting new and unique standards for the quality of our products and support of our customers Jeff Layne, Ph.D. Technical Manager, Phenologix
How to Use Your Companion Service Two-Way Voice Unit.
How to Use Your Companion Service Two-Way Voice Unit. A personal response system from the #1 security company in America. Thank you for choosing Companion Service, a service offered by ADT Security Services,
Lab Service, Asset Management and Extending the Life of Your Lab Equipment. Scott Greenwood Director, Services
Lab Service, Asset Management and Extending the Life of Your Lab Equipment Scott Greenwood Director, Services PLEASE STOP ME AT ANY TIME TO ASK QUESTIONS OR MAKE A COMMENT Is this a business manager...
Save money and stay in. compliance. Know. what you have, keep. what you must, eliminate. what you should.
The solution Save money and stay in Know what you have, eliminate what you should. compliance. keep what you must, Manage and reduce paper as you bridge to digital. FileBRIDGE Paper actively manages your
ISSN 1810-1119 FAO ANIMAL PRODUCTION AND HEALTH. manual QUALITY ASSURANCE FOR ANIMAL FEED ANALYSIS LABORATORIES
14 ISSN 1810-1119 FAO ANIMAL PRODUCTION AND HEALTH manual QUALITY ASSURANCE FOR ANIMAL FEED ANALYSIS LABORATORIES Cover photographs: Left image: FAO/Giuseppe Bizzarri Centre: FAO/Ishara Kodikara Right
RIDA Tetracyclin Spiking Solution Art. No. R3599
Food & Feed Analysis Juni/2007 II/2014 RIDASCREEN Bacitracin Art. No. R2901 Bacitracin belongs to the group of polypeptide antibiotics. Through inhibition of cell wall synthesis, it has a broad spectrum
Feeding Flood-Damaged or Sprouted Crops to Livestock
Feeding Flood-Damaged or Sprouted Crops to Livestock High moisture conditions often lead to crop damage and losses. Some losses are from grain sprouting in the head before harvest. These sprouted grains
Validating Methods using Waters Empower TM 2 Method. Validation. Manager
Validating Methods using Waters Empower TM 2 Method Validation Manager (MVM) Anders Janesten Nordic Informatics Sales Specialist 2008 Waters Corporation Decision-centric centric method development information
Validation and Calibration. Definitions and Terminology
Validation and Calibration Definitions and Terminology ACCEPTANCE CRITERIA: The specifications and acceptance/rejection criteria, such as acceptable quality level and unacceptable quality level, with an
Qualitative and Quantitative Analysis of Mycotoxins A. Rahmani, S. Jinap, and F. Soleimany
Qualitative and Quantitative Analysis of Mycotoxins A. Rahmani, S. Jinap, and F. Soleimany ABSTRACT: Mycotoxin toxicity occurs at very low concentrations, therefore sensitive and reliable methods for their
L 70/12 Official Journal of the European Union 9.3.2006
L 70/12 Official Journal of the European Union 9.3.2006 COMMISSION REGULATION (EC) No 401/2006 of 23 February 2006 laying down the methods of sampling and analysis for the official control of the levels
AAFCO Board Conference Call Wednesday, 13 November 2013 11:00am-12:30pm EST
AAFCO Board Conference Call Wednesday, 13 November 11:00am-12:30pm EST BOD Present: Ali Kashani, Mark LeBlanc, Tim Darden, Ken Bowers, Sam Davis, Richard Ten Eyck, Dan Danielson, Bob Waltz, Linda Morrison
2. Filling Data Gaps, Data validation & Descriptive Statistics
2. Filling Data Gaps, Data validation & Descriptive Statistics Dr. Prasad Modak Background Data collected from field may suffer from these problems Data may contain gaps ( = no readings during this period)
Seagate File Recovery Software for Windows - User Guide August 2015
Seagate Recovery Services Seagate File Recovery Software for Windows - User Guide August 2015 The Seagate File Recovery for Windows PC support includes:: - - - - - - -) these specific error messages: broken
The Art of Workload Selection
The Art of Workload Selection 5-1 Overview Services Exercised Example: Timesharing Systems Example: Networks Example: Magnetic Tape Backup System Level of Detail Representativeness Timeliness Other Considerations
APPENDIX N. Data Validation Using Data Descriptors
APPENDIX N Data Validation Using Data Descriptors Data validation is often defined by six data descriptors: 1) reports to decision maker 2) documentation 3) data sources 4) analytical method and detection
Ecology Quality Assurance Glossary
Ecology Quality Assurance Glossary Edited by William Kammin, Ecology Quality Assurance Officer Accreditation - A certification process for laboratories, designed to evaluate and document a lab s ability
NANOCOMPOSIX'S GUIDE TO ICP-MS MEASUREMENT
NANOCOMPOSIX'S GUIDE TO ICP-MS MEASUREMENT AND ANALYSIS SEPTEMBER 2012, V 1.1 4878 RONSON CT STE K SAN DIEGO, CA 92111 858-565 - 4227 NANOCOMPOSIX.COM Note to the Reader: We at nanocomposix have published
HP's UNIX Patch Strategy: Moving from Tru64 to HP-UX
HP's UNIX Patch Strategy: Moving from Tru64 to HP-UX Bruce Henderson HP-UX Patch Program Manager Hewlett-Packard 2004 Hewlett-Packard Development Company, L.P. The information contained herein is subject
Otis Photo Lab Inkjet Printing Demo
Otis Photo Lab Inkjet Printing Demo Otis Photography Lab Adam Ferriss Lab Manager aferriss@otis.edu 310.665.6971 Soft Proofing and Pre press Before you begin printing, it is a good idea to set the proof
Application Note. Online SPE-LC analysis of aflatoxins advances in sample preparation. Summary. Introduction. Fig. 1. Category Food Matrix
Application Note Online SPE-LC analysis of aflatoxins advances in sample preparation Category Food Matrix Foodstuffs Method Online SPE, HPLC Keywords Aflatoxins, Coring cell Analytes Aflatoxin ID VFD4,
ASSURING THE QUALITY OF TEST RESULTS
Page 1 of 12 Sections Included in this Document and Change History 1. Purpose 2. Scope 3. Responsibilities 4. Background 5. References 6. Procedure/(6. B changed Division of Field Science and DFS to Office
High School A. Pool 2 #1. W. Fl. LC Orange 7 4. Empire Red CHAMPION 10 6. LB3 Jacksonville. AT9, 3pm Pasco Lions
High School A LCO Black AT1, 5pm Empire Red Pool 2 #1 Empire Red 10 6 FCA S. Florida AT8, 3pm W. Fl. LC Orange W. Fl. LC Orange 7 4 LB3 Jacksonville AT9, 3pm Pasco Lions LB3 Jacksonville 12 1 High School
Big Data Consumers and Firms The ebay Story
Big Data Consumers and Firms The ebay Story Neel Sundaresan ebay Data Labs nsundaresan@ebay.com The broken beginning When asked if he understood that the laser pointer was broken, the buyer said Of course,
The following rates are the maximum rates that should be illustrated. Be sure to update the IRIS illustration system
INTEREST RATES - June 16, 2016 to July 15, 2016 Notices 1. Before soliciting or taking any annuity applications, it is required that you have completed Lafayette Life's Annuity Training and any Continuing
Qualification Study CHO 360-HCP ELISA (Type A to D)
Short Report Qualification Study CHO 360-HCP ELISA (Type A to D) Presented by: http://www.biogenes.de Version 01 Issue date: 27.11.2013 Version 01 Page 1 of 8 Table of Content TABLE OF CONTENT... 2 1 INTRODUCTION...
Maximizing Shareholder Value with External Data Analytics
Maximizing Shareholder Value with External Data Analytics Increasing return on Equity and Assets using external drivers Maximizing Shareholder Value with External Data Analytics Today s global economy
PANTONE Solid to Process
PANTONE Solid to Process PANTONE C:0 M:0 Y:100 K:0 Proc. Yellow PC PANTONE C:0 M:0 Y:51 K:0 100 PC PANTONE C:0 M:2 Y:69 K:0 106 PC PANTONE C:0 M:100 Y:0 K:0 Proc. Magen. PC PANTONE C:0 M:0 Y:79 K:0 101
CONCEPTION AND MANAGEMENT OF CONTAMINANTS CONTROL PLAN FOR CEREALS
CONCEPTION AND MANAGEMENT OF CONTAMINANTS CONTROL PLAN FOR CEREALS SOMMAIRE INTRODUCTION I CONTROL PLAN CONCEPTION CLIENTS EXPECTATIONS RISK STUDIES MEANS II CONTROL PLAN MANAGEMENT SPECIES CONTROLED CONTAMINANTS
PRODUCTS CURRENTLY AVAILABLE FOR SALE. Marquis SP
INTEREST RATES - August 16, 2016 to September 15, 2016 Notices 1. Before soliciting or taking any annuity applications, it is required that you have completed Lafayette Life's Annuity Training and any
2015-2020 AG FINANCIAL PLANNING PREPARED BY PAUL C HAY, EXTENSION EDUCATOR
The points on these slides are my thoughts and explanations of ideas gleaned from presentations by Michael Boehlje, Purdue University Ag Economist: Tina Barrett, Nebraska Farm Business Association: Kansas
Applying Statistics Recommended by Regulatory Documents
Applying Statistics Recommended by Regulatory Documents Steven Walfish President, Statistical Outsourcing Services steven@statisticaloutsourcingservices.com 301-325 325-31293129 About the Speaker Mr. Steven
Innovative vs Traditional
And in the red corner, introducing the challenger NASDAQ April 4 2011 243.47 $ 1.38 $ 0.58 % 0.07 $ 0.02 $ 39.4 % Technology DVD Digital Streamline Instant Play Internet Access Unlimited Selection No Late
Determination of Mycotoxin Residues by LC MS/MS Featuring Two Alternate Sample Extraction Procedures
Determination of Mycotoxin Residues by LC MS/MS Featuring Two Alternate Sample Extraction Procedures UCT Part Numbers: ECHLD126 P EnviroClean HL DVB, 200 mg/6 ml cartridge ECMSSC MP Mylar pouch containing
PTAC: Applied Chemistry COURSE OUTLINE & OBJECTIVES ESC Approved November 19, 2004
INTRODUCTION PTAC: Applied Chemistry COURSE OUTLINE & OBJECTIVES ESC Approved November 19, 2004 A. Introduction to Chemistry Terms 1. Define basic terms associated with chemistry: Organic/inorganic/biochemistry/physical
ISO 17025 Accreditation/Quality Management Systems Panel Discussion
ISO 17025 Accreditation/Quality Management Systems Panel Discussion Management Review Presented by Teresa Grant North Carolina Department of Agriculture & Consumer Services Relevant section of the standard
ADVICE FOR OWNERS OF PET PIGS AND MICRO PIGS
ADVICE FOR OWNERS OF PET PIGS AND MICRO PIGS General guidance for keeping your pig ADVICE AND GUIDANCE Keeping pigs or micro pigs animals specially bred to be smaller in adulthood than most other pig species
Physician Relationship Management System
Physician Relationship Management System Guided Tour pg. What is Physician Relationship Management? Consumers vs. Physicians At a high level, most hospitals target their marketing efforts at primarily
Control Charts and Trend Analysis for ISO 17025. Speakers: New York State Food Laboratory s Quality Assurance Team
Control Charts and Trend Analysis for ISO 17025 Speakers: New York State Food Laboratory s Quality Assurance Team 1 ISO 17025 Requirements, 5.9.1: The laboratory shall have quality control procedures for
Feeding Value of Sprouted Grains
AS-647 (Revised) Feeding Value of Sprouted Grains Greg Lardy Department Head, Department of Animal Sciences Adverse weather conditions can cause problems in harvesting grain promptly. In North Dakota,
Macmillan Practice Online guide for teachers
Macmillan Practice Online guide for teachers Macmillan Practice Online is an online practice environment for learners of English. Students log in to complete resources from an online course that can match
WELCOME TO TROY UNIVERSITY INTERNATIONAL APPLICATION/ADMISSION GUIDE
WELCOME TO TROY UNIVERSITY INTERNATIONAL APPLICATION/ADMISSION GUIDE This document has been created to assist you in the step-by-step guide outline: - Getting started; - Learn about TROY; - How to create
Increasing Quality While Maintaining Efficiency in Drug Chemistry with DART-TOF MS Screening
Increasing Quality While Maintaining Efficiency in Drug Chemistry with DART-TOF MS Screening Application Note Forensics Author Erin Shonsey Director of Research Alabama Department of Forensic Science Abstract
Mycotoxins in aquaculture: Occurrence in feeds components and impact on animal performance
502 Mycotoxins in aquaculture: Occurrence in feeds components and impact on animal performance G. A. Santos 1*, I. Rodrigues 1, V. Starkl 1, K. Naehrer 1, U. Hofstetter 1, P. Encarnação 2 1 BIOMIN Holding
Szabolcs B. Tóth. Quantitative and qualitative analysis of mycotoxins in food samples. PhD thesis. Supervisor: Dr. László Pál
Szabolcs B. Tóth Quantitative and qualitative analysis of mycotoxins in food samples PhD thesis Supervisor: Dr. László Pál University of Pannonia Doctoral School of Animal- and Agricultural Environmental
Pantone Matching System Color Chart PMS Colors Used For Printing
Pantone Matching System Color Chart PMS Colors Used For Printing Use this guide to assist your color selection and specification process. This chart is a reference guide only. Pantone colors on computer
USER MANUAL FOR WEB INTERFACE. Contents
USER MANUAL FOR WEB INTERFACE Contents 1. Main user interface 1.1 Access main system functions 1.2 Control panel 1.3 Latest events panel 1.4 Multiple camera thumbnails 2. Event thumbnail screen 2.1 Event
API 3200 LC/MS/MS SYSTEM. Performance, productivity and value combined
API 3200 LC/MS/MS SYSTEM Performance, productivity and value combined API 3200 LC/MS/MS SYSTEM Reliability, reproducibility, and confidence in your data. With an unmatched heritage of technological innovation
ASMS Regulated Bioanalysis Interest Group (RBIG) Workshop. Antibody-Drug Conjugates (ADC) A Complex Problem in Regulated Bioanalysis.
ASMS Regulated Bioanalysis Interest Group (RBIG) Workshop Antibody-Drug Conjugates (ADC) A Complex Problem in Regulated Bioanalysis June 17, 2014 Presiding: Dr. Keyang Xu (Genentech) and Dr. Fabio Garofolo
Online Store order process within SAP 2 nd December 2013
Information Systems Services Online Store order process within SAP 2 nd December 2013 Contents Overview of functionality within SAP... 2 Store transaction / order reporting... 2 Printing invoices... 3
Useful Key Performance Indicators for Maintenance
PO BOX 2091, ROSSMOYNE, WA, 6148 AUSTRALIA Phone: Fax: Email: Website: +61 (0) 402 731 563 +61 (8) 9457 8642 info@lifetime-reliability.com www.lifetime-reliability.com Abstract Useful Key Performance Indicators
How To Color Print
Pantone Matching System Color Chart PMS Colors Used For Printing Use this guide to assist your color selection and specification process. This chart is a reference guide only. Pantone colors on computer
Instrumentation. (Figure 2)
X-Ray Fluorescence Lab Report Nydia Esparza Victoria Rangel Physics of XRF XRF is a non destructive analytical technique that is used for elemental and chemical analysis. X-Ray Fluorescence Spectroscopy
Transfection reagent for visualizing lipofection with DNA. For ordering information, MSDS, publications and application notes see www.biontex.
METAFECTENE FluoR Transfection reagent for visualizing lipofection with DNA For ordering information, MSDS, publications and application notes see www.biontex.com Description Cat. No. Size METAFECTENE
A COMPARISON OF POST-SECONDARY OUTCOMES FOR TECH PREP AND NON-TECH PREP STUDENTS AT SINCLAIR COMMUNITY COLLEGE. October, 2007
A COMPARISON OF POST-SECONDARY OUTCOMES FOR TECH PREP AND NON-TECH PREP STUDENTS AT SINCLAIR COMMUNITY COLLEGE October, 2007 Office of Research, Analytics and Reporting Sinclair Community College, 444
Fast, easy and effective transfection reagent for mammalian cells
METAFECTENE EASY + Fast, easy and effective transfection reagent for mammalian cells For ordering information, MSDS, publications and application notes see www.biontex.com Description Cat. No. Size METAFECTENE
Vitamin B 12 - A review of analytical methods for use in food. Government Chemist Programme Report
Vitamin B 12 - A review of analytical methods for use in food Government Chemist Programme Report March 2015 Vitamin B12 - A review of analytical methods for use in food Author: Paul Lawrance Contact point:
Document review management. Raising Sales Invoices user guide
Document review management Raising Sales Invoices user guide Conventions used in this document Note: something for you to take note of. For example: Every Customer must have at least one address. Important:
COMOS FEED Knowledge Base
COMOS FEED Knowledge Base White Paper Simple creation and checking of rules for process flow diagrams Summary Controlled planning processes are a fundamental factor in efficient plant engineering. During
DataDirector Getting Started
DataDirector Getting Started LOG-IN 1. Login to the DataDirector website: https://www.achievedata.com/yourdistrictname 2. Enter your User Name and Password. 3. You may need to select the site and level
Oregon State University Online Application A Guide for International Students 2014
Oregon State University Online Application A Guide for International Students 2014 Welcome! In this guide you will find: Step by step instruction for navigating the website Page by page explanation of