DRAFT PRODUCT CERTIFICATION MANUAL FOR COMMENTS. Our Ref.: NRO/CHBO(FCT) 13 Jan 2014
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1 DRAFT PRODUCT CERTIFICATION MANUAL FOR COMMENTS Our Ref.: NRO/CHBO(FCT) 13 Jan 2014 Please find enclosed the following draft certification manual: Product manual on Skimmed Milk Powder, Extra Grade as per IS (Pt 2) : 1992 Kindly examine the draft product certification manual and forward your comments on the draft manuals. Last date for comments: 28 Jan Comments, if any, may please be made in the format as given below and mailed to CHBO(FCT) at the following id: mdch3@bis.org.in. Sl. No. Name of RO / BO Clause/ Sub-clause Paragraph / Figure / Table Type of comment (General / Technical / Editorial) Comments Proposed Change Note: Separate sheets may be attached in case comments are lengthy and cannot be incorporated in the table. 1 P a g e I S S U E N O 1
2 PRODUCT MANUAL ON SKIM MILK POWDER EXTRA GRADE IS 13334( Part 2):1992 Bureau of Indian Standards 2 P a g e I S S U E N O 1
3 AMENDMENT SHEET S NO AMENDMENT NO DATE PAGE NO CLAUSE NO 3 P a g e I S S U E N O 1
4 FOREWORD The milk production in our country is characterized by seasonal variations and drying of milk, an important method of preservation, facilitates later consumption during the lean season. The dried milk products, thus, have become an essential part of the chain between the producer and the consumer. A standard specification ( IS 1165 ) covering the provisions of skim milk powder and whole milk powder was formulated in 1957 and was subsequently revised in 1967, 1975 and 1986 to incorporate a number of modifications due to technological developments in the field from time to time. The Government of India, through the PFA Rules; 1955, had made the stipulation that milk powder shall be sold only under the BIS Certification Mark making a part of the standard obligatory in nature. There is a potential for export of skim milk powder and foreign buyers insist on extra grade specifications of milk powder of the American Dairy Products Institue ( ADPI ). Keeping this in view, the Technology Mission for Dairy Development, Government of India, had requested BIS to formulate a standard on Extra Grade Skim Milk Powder to incorporate, the requirements of skim milk powder which would meet the requirements of foreign buyers. Keeping above in view, it was decided to formulate a new standard covering the requirements for the skim milk powder both for standard grade and extra grade, in two parts. This part covers extra grade skim milk powder, while Part 1 covers standard grade skim milk powder. The earlier standard, namely IS 1165 will cover the requirements of milk powder only. While formulating this standard, due consideration has been given to the relevant Rules prescribed by the Government of India under the Prevention of Food Adulteration Act, 1954 and the Standards of Weights and Measures ( Packaged Commodities ) Rules, This standard is however, subject to the restrictions imposed under these Acts, wherever applicable. This Product Manual is intended to cover all elements needed for grant of a product certification licence and its continued operation providing reference material that can be used in all Regional / Branch Offices and by various applicants / licensees to ensure coherence of practice and transparency. 4 P a g e I S S U E N O 1
5 TABLE OF CONTENTS SECTION CONTENT DETAIL PAGE NO I PRODUCT DESCRIPTION 5 II RAW MATERIAL/COMPONENTS 7 III MANUFACTURING PROCESS & IN-PROCESS 8 QUALITY CONTROLS IV CERTIFICATION CRITERIA 10 V INSPECTION AND TESTING 12 ANNEXURE 1 (CHECK LIST) 14 ANNEXURE 2 (SCHEME OF TESTING & INSPECTION) 20 5 P a g e I S S U E N O 1
6 PRODUCT DESCRIPTION SECTION 1.1 DESCRIPTION OF PRODUCT IS 13334( Part 2) : 1992 prescribes the requirements, methods of sampling and test for SKIM MILK POWDER, EXTRA GRADE. The SKIM MILK POWDER, EXTRA GRADE shall be white or white with greenish tinge or light cream in colour. It shall be free from lumps except those that break up readily under slight pressure and shall be reasonably free from scorched particles. It shall also be free from extraneous matter, whey, butter milk and additives. SECTION 1.2 LATEST INDIAN EXTRA WITH PRODUCT TITLE AND NUMBER OF AMENDMENTS IS 13334( Part 2) : 1992 SKIM MILK POWDER, EXTRA GRADE SPECIFICATION AMENDMENTS -3 SECTION 1.3 LIST OF REFERRED INDIAN EXTRAS FOR RAW MATERIALS/COMPONENTS AND TEST METHODS LIST OF REFERRED INDIAN EXTRAS 1S No. Title 1070 : 1977 Water for general laboratory use ( second revision) 1547 : 1985 Infant milk foods (secondrevision ) 2491:1992 Food hygienic General principal Code of practice (second revision ) 4905 : 1968 Methods for random sampling. 5401:1969 Methods for detection and estimation of coliform bacteria in foodstuffs 5402:1969 Methods for plate count of bacteria in foodstuffs 5887(Part 2): 1976 Methods for detection of bacteria responsible for food poisoning: Isolation, identification and enumeration of Staphylococcus Aureus and fecal streptococci (first revision ) ( Part 3):1976 Methods for detection of bacteria responsible for food poisoning: Part 3 Isolation and identification of Salmonella and Shigella (first revision ) 10030:1981 Method for sensory evaluation of MILK POWDER 11078:1984 Round open top sanitary cans for MILK POWDER 6 P a g e I S S U E N O 1
7 11202 : 1984 Method for determination of lactic acid and lactates content in milk powder and Similar products : 1985 Methods of sampling for milk and milk products 11623:1986 Method for determination of moisture content in MILK POWDER and similar products 11721:1986 Determination of fat content in MILK POWDER and similar products ( reference method) : 1986 Method for determination of titrable acidity in milk powder and similar products 11824: I986 Paper coated high density polyethylene woven sacks for packing skin milk powder 12759:1989 Dried milk and dried milk products - Determination of insolubility index SECTION 1.4 CHECK LIST FOR SUBMISSION OF AN APPLICATION FOR GRANT OF LICENCE KINDLY REFER ANNEX 1 7 P a g e I S S U E N O 1
8 SECTION 2.1 RAW MATERIALS It shall be the material prepared by spray drying of Standardized milk obtained from fresh cow milk or buffalo milk or a mixture thereof ( the Standardized milk shall be prepared by adjustment of suitably processed milk solids ). The Standardized milk shall be free from additives. 8 P a g e I S S U E N O 1
9 MANUFACTURING PROCESS AND IN-PROCESS QUALITY CONTROLS SECTION 3.1 DESCRIPTION OF MANUFACTURING PROCESSES (TYPICAL) Raw milk receipt Testing of Raw Milk Chilling and Unloading into Silos ( Raw Milk Storage Tanks) Cream Separators Pasteurization of Skim Milk Pasteurized Milk Storage Tank Evaporator section Spray Drying Sifting Packing 9 P a g e I S S U E N O 1
10 SECTION 3.2 INFRASTRUCTURE FOR PRODUCTION Following infrastructure is generally required for production of SKIM MILK POWDER, EXTRA GRADE S.No. Typical List Of Machinery 1. DUMP TANK 2. MILK PUMPs 3. MILK CHILLER Machinery 4. RAW MILK STORAGE TANKS WITH AGITATORS 5. MILK PASTEURIZERS 6. MILK SEPARATORS 7. SKIM MILK STORAGE SILOS WITH AGITATORS 8. MILK EVAPORATOR 9. DRYING SECTION 10. SIFTER 11. DRY SKIM MILK POWDER FILLING M/C 12. WEIGHING SCALE, ELETRONIC, DIGITAL Note : Adequate Electric Power and Water supply is required 10 P a g e I S S U E N O 1
11 CERTIFICATION CRITERIA SECTION 4.1 CRITICAL REQUIREMENTS OF THE INDIAN EXTRA To be provided by CMD SECTION 4.2 SCHEME OF TESTING AND INSPECTION DOC: STI/13334( Part 2)/4 December Please see ANNEX 2. SECTION 4.3 MARKING FEE RATES Description Value Unit ONE TONNE Large Scale Units: Marking Fee (Minimum) Rs Small Scale Units: Marking Fee (Minimum) Rs Unit Rate Rs Qty Each Unit Enforcement Date SECTION 4.4 GROUPING GUIDELINES: NONE SECTION 4.5 GUIDELINES FOR WRITING SCOPE OF LICENCE "SKIM MILK POWDER, EXTRA GRADE SECTION 4.6 GUIDELINES FOR INCLUSION OF NEW VARIETIES Not Applicable 11 P a g e I S S U E N O 1
12 SECTION 4.7 SAMPLES SIZE Product-One sample comprising of 2 X 500 gm of SKIM MILK POWDER, EXTRA GRADE SECTION 4.8 MANNER OF SEALING THE SAMPLE Samples may be packed in suitable packing material (inert, preferably tin container), labeled and wax sealed or as an alternate code no and signatures of IO may be marked with a permanent marker pen on the foil/packing of the product. SECTION 4.9 REMNANTS ARE RETURNABLE/NON-RETURNABLE TO BE SCRAPPED/USED OR TO BE DESHAPED DISPOSAL IN CASE OF SAFETY ITEMS Sample is normally consumed in testing and Remnants are not returnable and may be suitably disposed off by the laboratory. SECTION 4.10 PROCEDURE TO BE FOLLOWED FOR DESTROYING/ DESHAPING/ RECYCLING THE PRODUCT THAT DOES NOT MEET THE QUALITY PARAMETERS DURING REGULAR PRODUCTION BIS Standard Mark to be marked only after ascertaining the quality of the material after testing as per Indian Standard and STI. The material may be reprocessed if it does not meet the quality requirements. 12 P a g e I S S U E N O 1
13 INSPECTION AND TESTING SECTION 5.1 PACKING MATERIAL REQUIRED FOR PKG/DESPATCH OF SAMPLE Any suitable material may be used for packing the sample to avoid any microbial contamination, moisture ingress and damage during transit. Samples may be packed in suitable packing material ( inert, preferably tin container). SECTION 5.2 LIST OF REQUIRED TEST EQUIPMENT/FACILITIES WITH REQUIREMENT & FREQUENCY OF CALIBRATION To be provided by CL SECTION 5.3 STATUS OF TEST FACILITIES IN BIS LAB AND OSL WITH TESTING CHARGES AND APPROXIMATE TIME REQUIRED FOR TESTING For latest information, please check the BIS web site or click the following link SECTION 5.4 WHETHER GRANT OF LICENCE WILL BE BASED ON FACTORY TESTING BASIS No INDEPENDENT TESTING BASIS Yes MIXED BASIS (FACTORY TESTING OF PRODUCT PLUS INDEPENDENT TESTING OF SOME RAW MATERIALS) No 13 P a g e I S S U E N O 1
14 SECTION 5.5 DETAILS OF TESTS TO BE CARRIED OUT IN FACTORY IN CASE OF APPLICANT/VERIFICATION SAMPLES Description as per clause 3.2 and Flavour & Taste as per clause 3.3 All Requirements as per Table 1 read with Clause 3.7 SURVEILLANCE SAMPLES Description as per clause 3.2 and Flavour & Taste as per clause 3.3 All Requirements as per Table 1 read with Clause 3.7 RAW MATERIAL SAMPLES TO BE GOT TESTED IF ANY --NIL 14 P a g e I S S U E N O 1
15 CHECKLIST 15 P a g e I S S U E N O 1
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