RecoPhos Bench Scale Reactor



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RecoPhos Bench Scale Reactor Design and Modelling Andreas Schönberg, Daniel Hariri RecoPhos Demonstration Event February 24th 2015

Content Basic of Development Setup and Design Modelling and Simulation Bench Scale Plant 2

Basic of Development Idea of Process Setup and Design Modelling and Simulation Experimental Work Bench/Pilot Scale Plant 3 Scale Experiments

Setup and Design required Reactor Atmosphere required Reactor and Packed Bed Dimensions required Power Distribution Design and construction of Induction Heating Systems required Power Supply required Periphery Design Process hand in hand with Modelling & Simulation and experimental work. 4

Lab Scale Induction Heating Measuring Equipment Power Supply 5 Resonance Circuit Switching Circuit

Modelling Slag Flow 6 Volume fraction slag

Modelling Slag Flow 7 Simplification of the computational mesh from 3D to 2D axsymmetric

Modelling Slag Flow Mass fraction of tracer at same time after pulse injection Viscosity low Viscosity high 8 µ 20 times higher

Modelling Slag Flow Effect of the dynamic viscosity of the molten ash on the RTD function during steady state variable 9

InduCarb Reactor Melting zone Ash feed P 2, CO Reaction zone Output area 10

InduCarb Reactor Unit 1 Unit 2 Unit 3 11

InduCarb Reactor Temperature 7 kg/h Ash -3,5 kw (melting) Heating power 70 % -1,75 kw (reactions) 40 % -1,75 kw (reactions) 40 % 12

Heating Test 13

Experimental Run 14

Process Flow Diagram (PFD) Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 15

Bench Scale Plant Combustion chamber Dosing system Scrubber IC- Reactor Heat exchanger Vessel 16

Bench Scale Plant Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 17

Construction & Commissioning of the Bench scale Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 18

Piping and Instrumentation Diagram (PID) & Process Automation Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 19

Bench Scale Plant 20

Bench Scale Plant Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 21

Gas supply Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 22

Process Automation, HMI Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 23

Process Automation, Control cabinet Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 24

Process Automation, HMI FRIP Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 25

Modelling of essential parts Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com Surface Temperature profile ensuring Temperature protection 26

Operation Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 27

Trend reporting Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 28

Data reporting Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 29

www.recophos.org Project RecoPhos H-CPE Hariri Chemical Process Engineering Hauptstrasse 16 4132 Muttenz, Switzerland Tel.: +41 (0)61 461 8075 daniel.hariri@h-cpe.com www.h-cpe.com 30