CERTIFICATE OF ANALYSIS
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1 Your C.O.C. #: Attention:Mike Squire Engineering and Operations Dpt PO Box 390 Parksville, BC Canada V9P 2H3 Report Date: 4//7 Report #: R68462 Version: - Final MAXXAM JOB #: B4A029 Received: 4//04, 09:00 Sample Matrix: Water # Samples Received: Analyses Alkalinity - Water Chloride by Automated Colourimetry Colour (True) Total Coliforms & E.coli Potable W- MF Conductance - water Fluoride Hardness Total (calculated as CaCO3) Hardness Total (calculated as CaCO3) Mercury (Total) by CVAF Na, K, Ca, Mg, S by CRC ICPMS (total) Na, K, Ca, Mg, S by CRC ICPMS (total) Elements by CRC ICPMS (total) Nitrate + Nitrite (N) Nitrite (N) by CFA Nitrogen - Nitrate (as N) Water () Water () Sulphate by Automated Colourimetry Total Dissolved Solids (Filt. Residue) Turbidity CERTIFICATE OF ANALYSIS Date Quantity Extracted Date Analyzed Laboratory Method 4//04 4//0 BBY6SOP N/A 4//04 BBY6SOP-000 N/A 4//04 BBY6SOP-0002 N/A 4//04 BBY4SOP-0000 N/A 4//0 BBY6SOP N/A 4//0 BBY6SOP N/A 4//2 BBY7SOP N/A 4//3 BBY7SOP //4 4// BBY7SOP-000 N/A 4//2 BBY7SOP N/A 4//3 BBY7SOP N/A 4//2 BBY7SOP N/A 4//0 BBY6SOP-0000 N/A 4//0 BBY6SOP-0000 N/A 4//06 BBY6SOP-0000 N/A 4//04 BBY6SOP N/A 4//0 BBY6SOP N/A 4//04 BBY6SOP //0 4//07 BBY6SOP N/A 4//04 BBY6SOP Analytical Method SM B m SM Cl- G m SM 22 2 B m SM m SM B m SM F C m EPA 60a R m EPA 60a R m BCMOE BCLM Oct3 m EPA 60A R m EPA 60A R m EPA 60A R m SM NO3- I m SM NO3- I m SM NO3 I m SM H+ B m SM H+ B m SM SO42- E m SM C m SM B m * RPDs calculated using raw data. The rounding of final results may result in the apparent difference. () The BC-MOE and APHA Standard Method require to be analysed within minutes of sampling and therefore field analysis is required for compliance. All Laboratory analyses in this report are reported past the BC-MOE/APHA Standard Method holding time. Page of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
2 Your C.O.C. #: Attention:Mike Squire Engineering and Operations Dpt PO Box 390 Parksville, BC Canada V9P 2H3 Report Date: 4//7 Report #: R68462 Version: - Final MAXXAM JOB #: B4A029 Received: 4//04, 09:00 CERTIFICATE OF ANALYSIS Encryption Key Please direct all questions regarding this Certificate of Analysis to your Project Manager. Shanaz Akbar, Project Manager SAkbar@maxxam.ca Phone# (604) ==================================================================== This report has been generated and distributed using a secure automated process. Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section.0.2 of ISO/IEC 702:0(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Total Cover Pages : 2 Page 2 of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
3 Report Date: 4//7 DRINKING WATER PACKAGE WITH CV HG (WATER) Maxxam ID Sampling Date COC Number Units LB07 4//03 :0 SPRINGWOOD WELL 8 LB08 4//03 : SPRINGWOOD WELL LB09 4//03 :40 RAILWAY WELL 4 RDL ANIONS Nitrite (N) Calculated Parameters < <0.000 < Total Hardness (CaCO3) Nitrate (N) Misc. Inorganics Fluoride (F) Alkalinity (Total as CaCO3) Alkalinity (PP as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Anions Dissolved Sulphate (SO4) Dissolved Chloride (Cl) MISCELLANEOUS True Colour Nutrients Col. Unit Nitrate plus Nitrite (N) Physical Properties Conductivity Physical Properties us/cm N/A Total Dissolved Solids Turbidity Elements NTU Total Mercury (Hg) Total Metals by ICPMS Total Aluminum (Al) Total Antimony (Sb) Total Arsenic (As) Total Barium (Ba) Total Boron (B) Total Cadmium (Cd) Total Chromium (Cr) < < < RDL = Reportable Detection Limit Page 3 of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
4 Report Date: 4//7 DRINKING WATER PACKAGE WITH CV HG (WATER) Maxxam ID Sampling Date COC Number Units LB07 4//03 :0 SPRINGWOOD WELL 8 LB08 4//03 : SPRINGWOOD WELL LB09 4//03 :40 RAILWAY WELL 4 RDL Total Cobalt (Co) Total Copper (Cu) Total Iron (Fe) Total Lead (Pb) Total Manganese (Mn) Total Molybdenum (Mo) Total Nickel (Ni) Total Selenium (Se) Total Silicon (Si) Total Silver (Ag) Total Uranium (U) Total Vanadium (V) Total Zinc (Zn) Total Calcium (Ca) Total Magnesium (Mg) Total Potassium (K) Total Sodium (Na) Total Sulphur (S) Microbiological Param < < < < < < E. coli Total Coliforms CFU/mL CFU/mL RDL = Reportable Detection Limit Page 4 of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
5 Report Date: 4//7 DRINKING WATER PACKAGE WITH CV HG (WATER) Maxxam ID Sampling Date COC Number Units LB0 4//03 :30 RAILWAY WELL 7 LB02 4//03 0: ENGLISHMAN RIVER RDL ANIONS Nitrite (N) Calculated Parameters <0.000 < Total Hardness (CaCO3) Nitrate (N) Misc. Inorganics Fluoride (F) Alkalinity (Total as CaCO3) Alkalinity (PP as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Anions Dissolved Sulphate (SO4) Dissolved Chloride (Cl) MISCELLANEOUS True Colour Nutrients Col. Unit Nitrate plus Nitrite (N) Physical Properties Conductivity Physical Properties us/cm N/A Total Dissolved Solids Turbidity Elements NTU Total Mercury (Hg) Total Metals by ICPMS 7778 Total Aluminum (Al) Total Antimony (Sb) Total Arsenic (As) Total Barium (Ba) Total Boron (B) Total Cadmium (Cd) Total Chromium (Cr) < < RDL = Reportable Detection Limit N/A = Not Applicable Page of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
6 Report Date: 4//7 DRINKING WATER PACKAGE WITH CV HG (WATER) Maxxam ID Sampling Date COC Number Units LB0 4//03 :30 RAILWAY WELL 7 LB02 4//03 0: ENGLISHMAN RIVER RDL Total Cobalt (Co) Total Copper (Cu) Total Iron (Fe) Total Lead (Pb) Total Manganese (Mn) Total Molybdenum (Mo) Total Nickel (Ni) Total Selenium (Se) Total Silicon (Si) Total Silver (Ag) Total Uranium (U) Total Vanadium (V) Total Zinc (Zn) Total Calcium (Ca) Total Magnesium (Mg) Total Potassium (K) Total Sodium (Na) Total Sulphur (S) Microbiological Param < < < < E. coli Total Coliforms CFU/mL CFU/mL 8 60 RDL = Reportable Detection Limit Page 6 of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
7 Report Date: 4//7 GENERAL COMMENTS Each temperature is the average of up to three cooler temperatures taken at receipt Package 7.7 C Results relate only to the items tested. Page 7 of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
8 Report Date: 4//7 QUALITY ASSURAE REPORT Parameter Date Matrix Spike % Recovery QC Limits Spiked Blank % Recovery QC Limits Method Blank Value Units RPD Value (%) QC Limits E. coli Total Coliforms Alkalinity (PP as CaCO3) Alkalinity (Total as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Alkalinity (PP as CaCO3) Alkalinity (Total as CaCO3) Bicarbonate (HCO3) Carbonate (CO3) Hydroxide (OH) Conductivity Turbidity Dissolved Chloride (Cl) Dissolved Sulphate (SO4) Total Dissolved Solids Total Dissolved Solids True Colour Fluoride (F) Nitrate plus Nitrite (N) Nitrite (N) Total Aluminum (Al) Total Antimony (Sb) Total Arsenic (As) Total Barium (Ba) Total Boron (B) Total Cadmium (Cd) Total Chromium (Cr) 4//04 4//04 4//04 4//04 4//04 4//04 4//04 4//04 4//04 4//0 4//0 4//0 4//0 4//0 4//0 4//0 4//04 4//04 4//04 4//07 4//07 4//04 4//0 4//0 4//0 4//2 4//2 4//2 4//2 4//2 4//2 4// <0.0 <0.000 <0 us/cm us/cm NTU Col. Unit N/A 4 N/A 2 Page 8 of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
9 Report Date: 4//7 QUALITY ASSURAE REPORT(CONT'D) 7778 Parameter N/A = Not Applicable Total Cobalt (Co) Total Copper (Cu) Total Iron (Fe) Total Lead (Pb) Total Manganese (Mn) Total Molybdenum (Mo) Total Nickel (Ni) Total Selenium (Se) Total Silicon (Si) Total Silver (Ag) Total Uranium (U) Total Vanadium (V) Total Zinc (Zn) Total Mercury (Hg) Date 4//2 4//2 4//2 4//2 4//2 4//2 4//2 4//2 4//2 4//2 4//2 4//2 4//2 4// % Recovery Matrix Spike QC Limits Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement. % Recovery Spiked Blank Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference QC Limits Method Blank Spiked Blank: A blank matrix sample to which a known amount of the analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination. 9 (Matrix Spike): The recovery in the matrix spike was not calculated. The relative difference between the concentration in the parent sample and the spiked amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than 2x that of the native sample concentration). Value <0. <0. 00 <0.0 Units Value (%) (Duplicate RPD): The duplicate RPD was not calculated. The concentration in the sample and/or duplicate was too low to permit a reliable RPD calculation (one or both samples < x RDL) RPD QC Limits Page 9 of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
10 Report Date: 4//7 VALIDATION SIGNATURE PAGE The analytical data and all QC contained in this report were reviewed and validated by the following individual(s). Andy Lu, Data Validation Coordinator Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section.0.2 of ISO/IEC 702:0(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Page 0 of Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 4606 Canada Way VG K Telephone(604) Fax(604)
11 Page of
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