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1 Supplementary Information J. Braz. Chem. Soc., Vol. 25, No. 8, S1-S21, Printed in Brazil Sociedade Brasileira de Química $ SI Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonylγ-butyrolactone Derivatives Marcos F. Pinatto-Botelho, a Antonio E. M. Crotti, a Julia M. de Souza, b Lizandra G. Magalhães b and Paulo M. Donate*,a a Departamento de Química, Faculdade de Filosofia, Ciências e Letras de Ribeirão Preto, Universidade de São Paulo, Avenida Bandeirantes, 3900, Ribeirão Preto-SP, Brazil b Núcleo de Pesquisa em Ciências Exatas e Tecnológicas, Universidade de Franca, Avenida Dr. Armando Salles de Oliveira 201 Parque Universitário, Franca-SP, Brazil General Information * pmdonate@usp.br
2 S2 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S1. 1 H NMR spectrum of compound 1 (CDCl 3, 400 MHz). Figure S2. 13 C NMR spectrum of compound 1 (CDCl 3, 100 MHz).
3 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S3 Figure S3. IR (KBr) spectrum of compound 1. Figure S4. ESI-MS spectrum of compound 1.
4 S4 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S5. 1 H NMR spectrum of compound 2 (CDCl 3, 400 MHz). Figure S6. 13 C NMR spectrum of compound 2 (CDCl 3, 100 MHz).
5 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S5 Figure S7. ESI-MS spectrum of compound 2. Figure S8. 1 H NMR spectrum of compound 3 (CDCl 3, 400 MHz).
6 S6 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S9. 13 C NMR spectrum of compound 3 (CDCl 3, 100 MHz). Figure S10. IR (KBr) spectrum of compound 3.
7 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S7 Figure S11. ESI-MS spectrum of compound 3. Figure S12. 1 H NMR spectrum of compound 4 (CDCl 3, 400 MHz).
8 S8 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S C NMR spectrum of compound 4 (CDCl 3, 100 MHz). Figure S14. IR (KBr) spectrum of compound 4.
9 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S9 Figure S15. ESI-MS spectrum of compound 4. Figure S16. 1 H NMR spectrum of compound 5 (CDCl 3, 400 MHz).
10 S10 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S C NMR spectrum of compound 5 (CDCl 3, 100 MHz). Figure S18. ESI-MS spectrum of compound 5.
11 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S11 Figure S19. 1 H NMR spectrum of compound 6 (CDCl 3, 400 MHz). Figure S C NMR spectrum of compound 6 (CDCl 3, 100 MHz).
12 S12 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S21. IR (KBr) spectrum of compound 6. Figure S22. ESI-MS spectrum of compound 6.
13 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S13 Figure S23. 1 H NMR spectrum of compound 7 (CDCl 3, 400 MHz). Figure S C NMR spectrum of compound 7 (CDCl 3, 100 MHz).
14 S14 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S25. IR (KBr) spectrum of compound 7. Figure S26. ESI-MS spectrum of compound 7.
15 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S15 Figure S27. 1 H NMR spectrum of compound 8 (CDCl 3, 400 MHz). Figure S C NMR spectrum of compound 8 (CDCl 3, 100 MHz).
16 S16 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S29. IR (KBr) spectrum of compound 8. Figure S30. ESI-MS spectrum of compound 8.
17 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S17 Figure S31. 1 H NMR spectrum of compound 9 (CDCl 3, 400 MHz). Figure S C NMR spectrum of compound 9 (CDCl 3, 100 MHz).
18 S18 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S33. IR (KBr) spectrum of compound 9. Figure S34. ESI-MS spectrum of compound 9.
19 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S19 Figure S35. 1 H NMR spectrum of compound 10 (CDCl 3, 400 MHz). Figure S C NMR spectrum of compound 10 (CDCl 3, 100 MHz).
20 S20 Microwave-Assisted Synthesis and Antileishmanial Activity of 3-methoxycarbonyl-g-butyrolactone Derivatives J. Braz. Chem. Soc. Figure S37. ESI-MS spectrum of compound 10.
21 Vol. 25, No. 8, 2014 Pinatto-Botelho et al. S21 Figure S38. Curves used to calculate the IC 50 values of compounds 1-10.
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