1E5 Advanced design of glass structures. Martina Eliášová

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1E5 Advanced design of structures Martina Eliášová

List of lessons 1) History, chemical composition, production 2) Glass as a material for load bearing structures 3) Design of laminated plates 4) Design of beams 5) Design of compressed members 6) Hybrid load-bearing members 7) Curved members 8) Design of bolted connection 9) Design of glued connection 10) Glass facades 11) Glass roofs 12) Examples of structures 2

Toughened Heat- Laminated Objectives of the lecture Toughened, heat-, chemically Laminated Aesthetic 3

Toughened Heat- Laminated Toughened Annealed float - insufficient strength in tension Strength refined Treatment of : greater resistance to mechanical and thermal loads Three different basic types with regards to the strength and fracture patterns 4

Toughened Heat- Toughened Toughened (fully tempered ) Laminated Cleaning Heating > 600 C Cooling Manufacturing steps for tempered 5

Toughened Heat- Laminated Toughened quenching (fast cooling) with air cooling and stiffening first on the surface, delayed cooling and consolidation of the core internal stress (parabolic distribution) surface in compression, core in tension Compression Tension 0,2d d 0,6d 0,2d 6

Toughened Heat- Laminated Toughened Advantages high value of bending strength (compressive surface stress 90 150MPa + tensile strength of annealed 40MPa) compressive stress not influenced by surface defects withstand local temperature differences up to 150 C (float 40 C) overloading or damage breaks into numerous small pieces, not dangerous Typical fracture pattern of tempered : small fragments or dice 7

Toughened Heat- Laminated Toughened Disadvantages must be at least 4mm thick thermal treatment after mechanical work - cutting, drilling greater initial deformation sinusoidal waves from rollers spontaneous fracture: invisible nickel sulphide inclusions (NiS), which expand their volume; up to 2 years after production destructive Heat-soak test (DIN 18516): Nickel sulphide inclusions 8

Toughened Heat- Laminated Toughened Weakened areas of the edge stresses in comparison to the body stresses - toughened 1 ~2,1 + - - σ 1 = σ 2, σ 3 = 0 0,2D 0,6D 0,2D D weakening - σ 2 = 0 - + + ~D σ 1 σ 2, zone 2 σ 3 0 A B - + + - 0,2D 0,2D 0,6D zone 1,σ 1 = σ 2 σ 3 =0 D Zone 1: central area Zone 2: edge 9

Toughened Heat- Toughened Toughened upon loading Laminated Stress distribution in toughened Bending stress compression tension + = tension compression tension compression 10

Toughened Heat Laminated Heat Heat (partially tempered ) similar production from same initial temperature slower cooling reduction of the surface pre-stress level (35 55 MPa) withstand local temperature differences up to 100 C greater initial deformation in comparison with float compression tension 0,2d compression tension 0,2d d 0,6d d 0,6d 0,2d 0,2d internal stress: 90 150 MPa internal stress: 35 55 MPa 11

Toughened Heat galss Laminated Heat Advantages without spontaneous failures due to nickel sulphide inclusions fragmentation similar to annealed = keep panes in position after cracking when they are framed or laminated Comparison of fracture pattern: float x heat- Comparison of fracture pattern: heat- x tempered 12

Toughened Heat Laminated Heat Determination of the surface stress destructive tests: fragmentation test BS 6206, pr EN 12150 struck in a controlled manner number of fragments in a standard area surface compression can be deduced from the number of fragments (higher number of fragments = increasing surface stress in given area) non-destructive tests: optical instrument differential surface refractometr 13

Toughened Heat Laminated Heat Initial deformation float less than < L/2500 thermally strength refined the shape of sinusoidal waves ~ L/300 edge dip roller wave roller wave and edge dip caused by sagging in semi-molten state overall bow slow cooled face fast cooled face overall bow caused by differential cooling of the two sides of the plate 14

Toughened Heat- Laminated chemical pre-stressing is realized by ionic exchange pane is immersed in a hot molten salt (hot potassium chloride bath) smaller sodium ions in the surface are exchanged for the larger potassium ions fracture behaviour corresponds to float compression tension Stress cross-sectional diagram of chemically 15

Toughened Heat- Laminated Advantages without thermal deformation suitable for very thin panes chemically can be cut, edge has strength of normal Disadvantages small depth of penetration highly susceptibility to surface defects because zone is not very deep 16

Toughened Heat- Laminated Laminated with no interlayer / loose with flexible interlayer bond with stiff interlayer bond modification of the mechanical, optical properties through the selection of the component layers, their sequence and thickness overhead, wind screens, bullet proof, beams and columns, in automotive industry 17

Toughened Heat- Laminated Laminated Laminated with foil two or more panes bonded by a transparent interlayer of plastic (up to 25 layers, thickness over 100 mm); float, tempered, polycarbonate, bent panes are washed, foils are layered and the assembly is heated (70 C) and pressed (prelamination) by roller process to squeeze out the air, in autoclave is heated to 140 C under a pressure about 0,8 MPa; largest size of pane 6,0 x 3,21m positioning and layering prelamination by calender autoclave 18

Toughened Heat- Laminated Laminated Intermediate layer: PVB foil (poly-vinyl-butyral) basic thickness 0,38 mm, maximal thickness of the interlayer = 6 mm EVA (ethylene vinyl-acetate) PU (polyurethane) Ionoplast SenryGlass influence of temperature influence of load duration Enter to the autoclave 19

Toughened Heat- Laminated Laminated Advantages laminated incorporates many thicknesses and combination of types many products with required mechanical and optical properties safety after failure broken pieces remain bonded to the foil = residual load-bearing capacity, interlayer can prevent penetration impact test Disadvantages thicker foils are used with heat treated to accommodate undulations = sinusoidal waves offset of adjacent edges due to the lamination process = misalignment up to 2 mm 20

Toughened Heat- Laminated Laminated Bending stress distribution of laminated depending on shear modulus G of PVB interlayer 21

Toughened Heat- Laminated Laminated Laminated with resin interlayer liquid cast resin (epoxy, acrylic, polyester) panels vertically positioned with defined gap (about 1 2mm), edges sealed with transparent double-sided adhesive tape, resin poured between two panels resin curing by chemical reaction or UV light Advantages no additional autoclave large panel size better acoustic insulation, suitable for thermally Disadvantages less residual load-bearing capacity post-fracture integrity 22

Toughened Heat- Laminated Glass appearance Influence of the surface type to transmission and reflection perfectly smooth surface textured surface rough surface 23

Toughened Heat- Laminated Rough surfaces of Sandblasting: abrasive is blasted under pressure onto the surface glazing surface is roughened and translucent pattern is created, reduction of the strength up to 50% Acid etching: liquid acid bath or acid pastes / screens, very durable patterns sand-blasted surface less optical quality etched surface 24

Toughened Heat- Laminated Texture rolled patterned is formed by reversal of pattern on the roller and cooled down, variety of architectural appearance the deeper the pattern, the greater the degree of obscuration and diffusion ornamented textured rolled surface with wire mesh 25

Toughened Heat- Laminated Enamelled ceramic pigments or frits are rolled, poured or screenprinted over one side of and are baked onto the during heat treatment = permanent bonded enamelling reduces the bending strength of tempered or heat- about 40% dosing roller coating trough pressure roller colour coating principle of roller-applied colour coating transport roller 26

Toughened Heat- Laminated laminated safety with coloured PVB films laminated safety with printed film interlayer laminated with decorative interlayer = metal sheet solar modules integrated into the skin 27

Toughened Heat- Laminated Electro-optic translucent glazing (B) unit becomes transparent (A) when an electric field is applied 1. 2. transparent electrode layer 3. polymer layer with aligned liquid crystals 4. polymer layer with randomly oriented liquid crystals A B 1 2 3 4 28

Toughened Heat- Laminated Coatings techniques impact on transmittance, absorption, reflection solar control hard fired into the surface under very high temperature 600 650 C, metallic oxides advantages: hardness can be glazed also to exterior sides, good economics in fabrication disadvantages: have to be integrated into the float process not flexible, maximum number of layers = 2 29

Toughened Heat- Laminated soft coating chemical or physical vapour deposition, most common technique = DC-magnetron sputtering process up to 15 different materials = big variety of the coating composition, typical coating material tin oxide, silver, total coating thickness about 0,01 0,1μm advantages: very precise, flexible with constant quality, possible to reproduce the same coating with the same technical properties after many years disadvantages: susceptibility to aggressive air pollution and mechanical damage, necessity of the protection by protective layer, placing onto the inner side of insulating units 30

Toughened Heat- Laminated Fire resistant glazing special transparent gels or intumescent (swelling) interlayer which are transparent at room temperature, but foaming above higher temperature glazing might break but stay in position without falling down special glazing products allow fire protection up to 120 minutes 31

Toughened Heat- Laminated Summary rising tensile bending strength annealed laminated safety - (45 N/mm 2 ) heat- laminated safety - (70 N/mm 2 ) toughened laminated safety - (120 N/mm 2 ) better residual safety after breakage 32

Toughened Heat- Laminated Tension strength of Glass type Use Tempered float Tempered rolled f k [MPa] 120 90 f d [MPa] 50 37 γ M 120/50 = 2,4 90/37 = 2,4 Enamelled tempered float 70 30 70/30 = 2,4 Annealed overhead 45 12 45/12 = 3,8 vertical 45 18 45/18 = 2,5 Rolled overhead 25 8 25/8 = 3,1 vertical 25 10 25/10 = 2,5 Laminated from annealed overhead vertical 45 45 15 22,5 45/15 = 3,0 45/22,5 = 2,0 Heat- float 70 29 70/29 = 2,4 Enamelled heat- float 48 18 45/18 = 2,5 33

Thank you for your kind attention 34