ANALYTICAL REPORT. Attn: Jean Neubeck
|
|
|
- Melvin Newton
- 7 years ago
- Views:
Transcription
1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. 0 Riverside Parkway West Sacramento, CA 0 Tel: ()-00 TestAmerica Job ID: 0-- Client Project/Site: HFCS For: Alpha Geosciences Plank Road Clifton Park, New York 0 Attn: Jean Neubeck Authorized for release by: //0 :: PM Jill Kellmann, Manager of Project Management ()-0 jill.kellmann@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.
2 Project/Site: HFCS Table of Contents TestAmerica Job ID: 0-- Cover Page Table of Contents Definitions/Glossary Case Narrative Detection Summary Client Sample Results Surrogate Summary QC Sample Results QC Association Summary Lab Chronicle Certification Summary Method Summary Sample Summary Chain of Custody Receipt Checklists Page of //0
3 Project/Site: HFCS Definitions/Glossary TestAmerica Job ID: 0-- Qualifiers LCMS Qualifier J Glossary Abbreviation Qualifier Description Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) Page of //0
4 Case Narrative Client: Alpha Geosciences TestAmerica Job ID: 0-- Project/Site: HFCS Job ID: 0-- Laboratory: Narrative Receipt The samples were received on //0 : AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 0.º C. LCMS - Method Results for sample BG Cold Tap (0--) were reported from the analysis of a diluted extract due to high concentration of the target analyte in the analysis of the undiluted extract. The dilution factor was applied to the labeled internal standard area counts and these area counts were within acceptance limits The internal standard (ISTD) response for the following samples was outside control limits compared to the most recent CCV: HS Kit Tap (0--) and BG Cold Tap (0--). The samples were re-analyzed with concurring results and the original set of data has been reported. The internal standards responses were in control as compared to the calibration curve. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Page of //0
5 Project/Site: HFCS Detection Summary TestAmerica Job ID: 0-- Client Sample ID: HS Kit Tap Lab Sample ID: 0-- No Detections. Client Sample ID: BG Cold Tap Lab Sample ID: 0-- Analyte Result Qualifier RL MDL Unit D Method Prep Type Perfluorooctanoic acid (PFOA) - DL ug/l Total/NA This Detection Summary does not include radiochemical test results. Page of //0
6 Project/Site: HFCS Client Sample ID: HS Kit Tap Date Collected: 0// : Date Received: 0// : Method: - Perfluorinated Alkyl Acids (LC/MS) Analyte Result Qualifier Client Sample Results RL MDL TestAmerica Job ID: 0-- Lab Sample ID: 0-- Matrix: Water Perfluorooctane Sulfonate (PFOS) ND ug/l 0/0/ : 0/0/ 0:00 Perfluorooctanoic acid (PFOA) Surrogate ND %Recovery Qualifier Limits Unit D ug/l 0/0/ : 0/0/ 0:00 C PFHxA 0-0 0/0/ : 0/0/ 0:00 C PFDA 0-0 0/0/ : 0/0/ 0:00 Client Sample ID: BG Cold Tap Date Collected: 0// : Date Received: 0// : Method: - Perfluorinated Alkyl Acids (LC/MS) Analyte Result Qualifier RL MDL Lab Sample ID: 0-- Matrix: Water Perfluorooctane Sulfonate (PFOS) ND ug/l 0/0/ : 0/0/ 0: Surrogate %Recovery Qualifier Limits C PFHxA 0-0 0/0/ : 0/0/ 0: Unit D C PFDA 0-0 0/0/ : 0/0/ 0: Method: - Perfluorinated Alkyl Acids (LC/MS) - DL Analyte Result Qualifier RL Perfluorooctanoic acid (PFOA) ug/l 0/0/ : 0/0/ : MDL Unit D Surrogate %Recovery Qualifier Limits C PFHxA 0-0 0/0/ : 0/0/ : C PFDA 0-0 0/0/ : 0/0/ : Page of //0
7 Project/Site: HFCS Method: - Perfluorinated Alkyl Acids (LC/MS) Matrix: Water Surrogate Summary C PFHxAC PFDA Lab Sample ID Client Sample ID (0-0) (0-0) 0-- HS Kit Tap 0-- BG Cold Tap DL BG Cold Tap LCS 0-/-A MB 0-/-A Surrogate Legend C PFHxA = C PFHxA C PFDA = C PFDA Lab Control Sample Method Blank 0 TestAmerica Job ID: 0-- Percent Surrogate Recovery (Acceptance Limits) Prep Type: Total/NA Page of //0
8 Project/Site: HFCS Method: - Perfluorinated Alkyl Acids (LC/MS) QC Sample Results TestAmerica Job ID: 0-- Lab Sample ID: MB 0-/-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: Prep Batch: MB MB Analyte Result Qualifier RL Perfluorooctane Sulfonate (PFOS) ND ug/l 0/0/ : 0/0/ : Perfluorooctanoic acid (PFOA) Surrogate %Recovery MDL Unit D ND ug/l 0/0/ : 0/0/ : MB MB Qualifier Limits C PFHxA 0-0 0/0/ : 0/0/ : C PFDA 0-0 0/0/ : 0/0/ : Lab Sample ID: LCS 0-/-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: Prep Batch: Spike LCS LCS %Rec. Analyte Added Result Qualifier Perfluorooctane Sulfonate J ug/l 0-0 (PFOS) Perfluorooctanoic acid (PFOA) J ug/l 0-0 Surrogate %Recovery LCS LCS Qualifier Limits C PFHxA C PFDA 0-0 Unit D %Rec Limits Page of //0
9 Project/Site: HFCS QC Association Summary TestAmerica Job ID: 0-- LCMS Prep Batch: Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 0-- HS Kit Tap Total/NA Water 0-- BG Cold Tap Total/NA DL BG Cold Tap Total/NA LCS 0-/-A Lab Control Sample Total/NA MB 0-/-A Method Blank Total/NA Analysis Batch: Water Water Water Water Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 0-- HS Kit Tap Total/NA Water 0-- BG Cold Tap Total/NA DL BG Cold Tap Total/NA LCS 0-/-A Lab Control Sample Total/NA MB 0-/-A Method Blank Total/NA Water Water Water Water Page of //0
10 Lab Chronicle Client: Alpha Geosciences TestAmerica Job ID: 0-- Project/Site: HFCS Client Sample ID: HS Kit Tap Lab Sample ID: 0-- Date Collected: 0// : Matrix: Water Date Received: 0// : Prep Type Batch Type Batch Method Run Dil Factor Initial Amount Amount or Analyst Total/NA Prep. ml.00 ml 0/0/ : JER TAL SAC Final Batch Number Total/NA Analysis. ml.00 ml 0/0/ 0:00 CBW TAL SAC Client Sample ID: BG Cold Tap Lab Sample ID: 0-- Date Collected: 0// : Matrix: Water Date Received: 0// : Prep Type Batch Type Batch Method Run Dil Factor Initial Amount Amount or Analyst Total/NA Prep 0. ml.00 ml 0/0/ : JER TAL SAC Final Batch Number Total/NA Analysis 0. ml.00 ml 0/0/ 0: CBW TAL SAC Total/NA Prep DL 0. ml.00 ml 0/0/ : JER TAL SAC Total/NA Analysis DL 0. ml.00 ml 0/0/ : CBW TAL SAC Laboratory References: TAL SAC =, 0 Riverside Parkway, West Sacramento, CA 0, TEL ()-00 Lab Lab Page of //0
11 Certification Summary Client: Alpha Geosciences TestAmerica Job ID: 0-- Project/Site: HFCS Laboratory: Unless otherwise noted, all analytes for this laboratory were covered under each certification below. Authority Program EPA Region Certification ID Expiration Date USEPA UCMR Federal CA Analysis Method Prep Method Matrix Analyte Page of //0
12 Project/Site: HFCS Method Summary TestAmerica Job ID: 0-- Method Method Description Protocol Laboratory Perfluorinated Alkyl Acids (LC/MS) EPA TAL SAC Protocol References: EPA = US Environmental Protection Agency Laboratory References: TAL SAC =, 0 Riverside Parkway, West Sacramento, CA 0, TEL ()-00 Page of //0
13 Project/Site: HFCS Sample Summary TestAmerica Job ID: 0-- Lab Sample ID Client Sample ID Matrix Collected Received 0-- HS Kit Tap Water 0// : 0// : 0-- BG Cold Tap Water 0// : 0// : Page of //0
14 Page of //0
15 Login Sample Receipt Checklist Client: Alpha Geosciences Job Number: 0-- Login Number: List Source: List Number: Creator: Nelson, Kym D Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact. Sample custody seals, if present, are intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the containers received and the COC. Samples are received within Holding Time (excluding tests with immediate HTs) Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs Containers requiring zero headspace have no headspace or bubble is <mm (/"). Multiphasic samples are not present. Samples do not require splitting or compositing. Residual Chlorine Checked. Seal N/A N/A N/A N/A Page of //0
Pace Analytical e-report
Date Issued: July 28, 2014 Pace Analytical e-report Report prepared for: ATLANTIC TESTING LABORATORIES, LTD 22 CORPORATE DR CLIFTON PARK, NY 12065 CONTACT: Derek Converse ----------------------------------------------
This report contains the analytical results for the samples received under chain of custody by TestAmerica on October 29, 2010.
November 17, 2010 TestAmerica Project Number: G0K120465 Cathy Knudsen Planteco Environmental Consult 337 S Milledge Avenue Suite 202 Athens, GA 30605 Dear Ms. Knudsen, This report contains the analytical
ANALYTICAL SUMMARY REPORT
ANALYTICAL SUMMARY REPORT OST-003 August 06, 2015 PO Box 2003 Rapid City, SD 57709 Work Order: Project Name: G15070702 Energy Laboratories Inc. Gillette WY received the following 2 samples for on 7/31/2015
1 Quality Assurance and Quality Control Project Plan
1 Quality Assurance and Quality Control Project Plan The purpose of this section is to describe the quality assurance/quality control program that will be used during the system specific field testing
MIDLAND AREA SOIL SAMPLING MIDLAND, MICHIGAN
QUALITY ASSURANCE PROJECT PLAN MIDLAND AREA SOIL SAMPLING MIDLAND, MICHIGAN Revised May 2013 URS Corporation 9400 Amberglen Boulevard Austin, Texas 78729 (512) 454-4797 TABLE OF CONTENTS Section 1 Objectives
Ecology Quality Assurance Glossary
Ecology Quality Assurance Glossary Edited by William Kammin, Ecology Quality Assurance Officer Accreditation - A certification process for laboratories, designed to evaluate and document a lab s ability
Evaluating Laboratory Data. Tom Frick Environmental Assessment Section Bureau of Laboratories
Evaluating Laboratory Data Tom Frick Environmental Assessment Section Bureau of Laboratories Overview of Presentation Lab operations review QA requirements MDLs/ PQLs Why do we sample? Protect physical,
CERTIFICATE OF ANALYSIS
Attention: Angela Mazza / Kathleen Wilson Catholic Education Centre 80 Sheppard Ave E North York, ON M2N 6E8 Your Project #: ANNUNCIATION Your C.O.C. #: na Report #: R3046860 Version: 1 MAXXAM JOB #: B488250
APPENDIX L DATA VALIDATION REPORT
APPENDIX L DATA VALIDATION REPORT FIELD AND DATA REPORT DOWNTOWN PORTLAND SEDIMENT CHARACTERIZATION PHASE II WILLAMETTE RIVER PORTLAND, OREGON JUNE 2010 Data Validation Report Downtown Portland Sediment
Third Party Data Validation: What you need to know and do!
Third Party Data Validation: What you need to know and do! Anand Mudambi & Pamela Wehrmann 2012 DoD EMDQ Workshop San Diego, CA Course Objectives/Outline The course will provide an overview of third party
ANALYTICAL SUMMARY REPORT July 06, 2011 303 Irene St Helena, MT 59601 Workorder No.: H11060340 Project Name: Beal Mtn Quote ID: H634 - Beal 2011 Site Wide Monitoring Energy Laboratories Inc Helena MT received
Sample Management SOP 2v8 Page 1 STANDARD OPERATING PROCEDURE NO. 2 SAMPLE MANAGEMENT REVISION LOG. Revision Number Description Date
Sample Management SOP 2v8 Page 1 STANDARD OPERATING PROCEDURE NO. 2 SAMPLE MANAGEMENT REVISION LOG Revision Number Description Date 2.0 Original SOP 2.1 Revisions by McLemore after field testing 1/3/04
Samples RMN070714. Analytical Report (0714-63) GC/FID Analysis (RM01) Nicotine Purity
For the benefit of VaporFi, Inc. Samples RMN070714 Analytical Report (0714-63) GC/FID Analysis (RM01) Nicotine Purity GC/MS Analysis (QG02) Anabasine, Anatabine, Myosmine, Nornicotine Enthalpy Analytical,
State Water Resources Control Board Environmental Laboratory Accreditation Program
State Water Resources Control Board Environmental Laboratory Accreditation Program P.O. Box 100, Floor 24 850 Marina Bay Parkway, Build. P 500 N Central Ave, Suite 500 Sacramento, CA 95812-0100 Richmond,
APPENDIX C. DATA VALIDATION REPORT
APPENDIX C. DATA VALIDATION REPORT T-117 Upland Investigation Upland Investigation Data Report Appendices PROJECT NARRATIVE Basis for the Data Validation This report summarizes the results of the validation
APPENDIX II TIER I CHECKLIST
APPENDIX II TIER I CHECKLIST Data Validation PRF - Tier I Page 1 Data Validation Plan Review Form Tier I This Plan Review Form is # 1 of 1 forms completed in the review of this closure plan. Facility Name
METHOD SUMMARY & DATA QUALITY OBJECTIVES
METHOD SUMMARY & DATA QUALITY OBJECTIVES TestAmerica West Sacramento Method 1613B: Polychlorinated Dibenzo-p-dioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High Resolution Gas Chromatography/High
QUALITY ASSURANCE PLAN
QUALITY ASSURANCE PLAN Revision 16.0 June 2013 (Initial Version Release: January 2001) Prepared By: J. Nathan Hawley and Josh Kirkpatrick Basic Laboratory, Inc. Basic Laboratory, Inc. 2218 Railroad Avenue
Approvals [Signature On File]
![Approvals [Signature On File]](/thumbs/24/4276680.jpg "Approvals [Signature On File]")
Page 1 of 7 Minimum Reporting Requirements for Analytical Data (Chemistry) for the Water Quality Planning Bureau Approvals SOP WQPBDMS-010 Prepared by: Chris Shirley, QA Officer, WQPB Michael Pipp, Environmental
Technical Guidance Manual for the Implementation of the Hawai`i State Contingency Plan. Interim Final SECTION 10
Technical Guidance Manual for the Implementation of the Hawai`i State Contingency Plan SECTION 10 DATA QUALITY ASSURANCE AND QUALITY CONTROL (QA/QC) Hawai`i HEER TGM 10-1 December 31, 2008 CONTENTS Acronyms
Medical Cannabis Laboratory Approval Program
Medical Cannabis Laboratory Approval Program Application Process and Required Documentation After the publication of the Medical Cannabis Laboratory Application, currently expected by February 16, 2015,
QUALITY ASSURANCE / QUALITY CONTROL POLICY BREG SOIL AND WATER QUALITY LABORATORY UNIVERSITY OF DELAWARE
QUALITY ASSURANCE / QUALITY CONTROL POLICY BREG SOIL AND WATER QUALITY LABORATORY UNIVERSITY OF DELAWARE Department of Bioresources Engineering Rm 111 Worrilow Hall 531 S. College Ave. Newark, DE 19716-2140
Central Valley Regional Data Center
Central Valley Regional Data Center CEDEN July 13, 2015 www.mlj-llc.com TABLE OF CONTENTS i. Introduction... 4 1. Water and Sediment Quality (Chemistry and Bacteria) Data... 6 1.1 Chemistry Results Worksheet...
Quality Assurance Manual
Clinical Laboratory of San Bernardino, Inc. Quality Assurance Manual Clinical Laboratory of San Bernardino, Inc. 21881 Barton Road, Grand Terrace, CA 92313 Telephone (909) 825-7693 Facsimile (909) 825-7696
Analytical Data Package Reports
Analytical Data Package Reports TriMatrix offers a variety of analytical data packages formatted to meet the reporting needs and varying data quality objectives of its clients. The data packages offered
Minnesota Pollution Control Agency. Quality Assurance Project Plan Guidance
www.pca.state.mn.us Minnesota Pollution Control Agency Quality Assurance Project Plan Guidance Overview The following guidance is for use in building Quality Assurance Project Plans (QAPPs) for the Minnesota
Draft. Quality Assurance Project Plan. Haul Road Fugitive Dust Study. Red Dog Mine, Alaska. Prepared for. Teck Cominco Alaska Inc.
Draft Quality Assurance Project Plan Haul Road Fugitive Dust Study Red Dog Mine, Alaska Prepared for Teck Cominco Alaska Inc. Anchorage, Alaska Draft Quality Assurance Project Plan Haul Road Fugitive Dust
QA/QC. Standard methods in field. QA/QC in the field. QA/QC in analysis
QA/QC To identify, measure and keep systematic and random errors under control in planning, sampling, analysis and reporting of data. Quality assurance = how samples and data are collected and managed.
Data Quality. Tips for getting it, keeping it, proving it! Central Coast Ambient Monitoring Program
Data Quality Tips for getting it, keeping it, proving it! Central Coast Ambient Monitoring Program Why do we care? Program goals are key what do you want to do with the data? Data utility increases directly
Laboratory Information Management System (LIMS) in EMRL
Laboratory Information Management System (LIMS) in EMRL History of LIMS at EMRL November of 2003, EMRL purchased a commercial LIMS system to replace an LLNL built system Use for multiple groups Keep current
ASSURING THE QUALITY OF TEST RESULTS
Page 1 of 12 Sections Included in this Document and Change History 1. Purpose 2. Scope 3. Responsibilities 4. Background 5. References 6. Procedure/(6. B changed Division of Field Science and DFS to Office
Appendix C Data Validation Report
Appendix C Data Validation Report INTRODUCTION Basis for the Data Validation This report summarizes the results of the summary (Level III) data validation performed on sediment, water, and quality control
Determination of Total Suspended Solids (TSS) and Total Volatile Solids (TVS) in Waters of Fresh/Estuarine/Coastal Waters
Determination of Total Suspended Solids (TSS) and Total Volatile Solids (TVS) in Waters of Fresh/Estuarine/Coastal Waters 1. SCOPE and APPLICATION 1.1 Gravimetric analysis is used to determine total suspended
Halogen Free: What, Why and How. Presented by : Jim Cronin Environmental Monitoring and Technologies, Inc.
Halogen Free: What, Why and How Presented by : Jim Cronin Environmental Monitoring and Technologies, Inc. We will discuss What are Halogens and how we interact with them. Why Halogens, within consumer
Commonwealth of Kentucky. Wastewater Laboratory Certification Manual
Commonwealth of Kentucky Wastewater Laboratory Certification Manual March 2013 This page intentionally left blank ii TABLE OF CONTENTS I. INTRODUCTION I-1 II. GENERAL LABORATORY REQUIREMENTS II-1 1.0 Personnel
APPENDIX N. Data Validation Using Data Descriptors
APPENDIX N Data Validation Using Data Descriptors Data validation is often defined by six data descriptors: 1) reports to decision maker 2) documentation 3) data sources 4) analytical method and detection
Drip Club 2540 Corporate Place, Suite B103 Monterey Park, CA 91754
Drip Club 2540 Corporate Place, Suite B103 Monterey Park, CA 91754 Carbonyl Assay Samples Received 11/25/2015 Analysis Report (1115-593B) GC/MS Analysis (ENT225) Diacetyl 2,3-Pentanedione (aka Acetyl propionyl)
CHAPTER ONE TABLE OF CONTENTS 1.0 INTRODUCTION... 1
CHAPTER ONE TABLE OF CONTENTS Section Page 1.0 INTRODUCTION... 1 2.0 QA PROJECT PLAN... 1 2.1 DATA QUALITY OBJECTIVES... 2 2.2 PROJECT OBJECTIVES... 2 2.3 SAMPLE COLLECTION... 3 2.4 ANALYSIS AND TESTING...
Analytical Data Report for Sediment Samples Collected From 100-NR-2 Operable Unit
PNNL- 20826 Analytical Data Report for Sediment Samples Collected From 100-NR-2 Operable Unit Michael Lindberg October 2011 DISCLAIMER This report was prepared as an account of work sponsored by an agency
DRAFT Changes to 25 Pa. Code Chapter 252 For Discussion Purposes Only January 21, 2015 CHAPTER 252. ENVIRONMENTAL LABORATORY ACCREDITATION
CHAPTER 252. ENVIRONMENTAL LABORATORY ACCREDITATION Subchapter A. GENERAL PROVISIONS B. APPLICATION, FEES AND SUPPORTING DOCUMENTS C. GENERAL STANDARDS FOR ACCREDITATION D. QUALITY ASSURANCE AND QUALITY
Attachment 1 provides the analytical results provided by Eberline.
March 8, 2016 Brian Reams ECOTECH USA, LLC 1313 S Main Street London, KY 40741 Subject: Estill County Schools and Blue Ridge Landfill Water Sampling Summary Dear Mr. Reams, On February 28, 2016, a total
Methods of Data Collection and Field Planning
Quality Assurance and Quality Control Tools for Monitoring Projects Beverly H. van Buuren,, SWAMP QA Officer Amara Vandervort, SWAMP QA Coordinator Megan Kilner, SWAMP QA Specialist The Quality Assurance
Laboratory Data Management. August 2011
Laboratory Data Management and Reporting Mid-Atlantic ti EQuIS Users Group Meeting August 2011 Company Information Founded d 1986 Employee-owned since 1997 Laboratories Six Service Centers Two Total Staff
ITS REWORK DATA VERIFICATION REPORT for samples collected from CAMP STANLEY STORAGE ACTIVITY BOERNE, TEXAS
INTRODUCTION ITS REWORK DATA VERIFICATION REPORT for samples collected from CAMP STANLEY STORAGE ACTIVITY BOERNE, TEXAS Data Verifiers: Michelle Wolfe & Tammy Chang Parsons The following data validation
Division of Environmental Response and Revitalization
Division of Environmental Response and Revitalization Guidelines and Specifications for Preparing Quality Assurance Project Plans (QAPPs) September 1, 1998 - Final Purpose This document (1) presents guidelines
Proficiency Testing In A Global Analytical Environment Benefits & Challenges. AOAC September 2007
Proficiency Testing In A Global Analytical Environment Benefits & Challenges AOAC September 2007 1 The Coca-Cola Company The Coca-Cola Company is the largest manufacturer, distributor and marketer of nonalcoholic
US EPA - Region III BROWNFIELDS. Quality Assurance Project Plan. Template
U.S. Environmental Protection Agency (EPA) Region III 1650 Arch Street Philadelphia, PA 19107 US EPA - Region III BROWNFIELDS Quality Assurance Project Plan Template Interim Final March 2001 DISLAIMER
Quality Assurance Plan
Page 1 of 84 Quality Assurance Plan Analytical Laboratory Services, Inc. Prepared By: Environmental Program 34 Dogwood Lane Middletown, PA 17057 Tel: (717) 944-5541 Fax: (717) 944-1430 Helen MacMinn Quality
DEPARTMENT OF NATURAL RESOURCES and ENVIRONMENTAL CONTROL SITE INVESTIGATION & RESTORATION BRANCH
Page 1 DEPARTMENT OF NATURAL RESOURCES and ENVIRONMENTAL CONTROL SITE INVESTIGATION & RESTORATION BRANCH STANDARD OPERATING PROCEDURES FOR CHEMICAL ANALYTICAL PROGRAMS UNDER THE HAZARDOUS SUBSTANCE CLEANUP
Guidance for Industry
Guidance for Industry Q2B Validation of Analytical Procedures: Methodology November 1996 ICH Guidance for Industry Q2B Validation of Analytical Procedures: Methodology Additional copies are available from:
PERFORMANCE REPORT. Quality Assurance Program - January to June 2011
PERFORMANCE REPORT Quality Assurance Program - January to June 2011 The following discussion is prepared in accordance with the requirements for a Semiannual Performance Report on the Quality Assurance
How To Test For Contamination In Large Volume Water
Automated Solid Phase Extraction (SPE) of EPA Method 1694 for Pharmaceuticals and Personal Care Products in Large Volume Water Samples Keywords Application Note ENV0212 This collaboration study was performed
DATA QUALITY ASSESSMENT AND DATA USABILITY EVALUATION TECHNICAL GUIDANCE
New Jersey Department of Environmental Protection Site Remediation Program DATA QUALITY ASSESSMENT AND DATA USABILITY EVALUATION TECHNICAL GUIDANCE Version 1.0 April 2014 Preamble The results of analyses
LC-MS/MS, the new reference method for mycotoxin analysis
LC-MS/MS, the new reference method for mycotoxin analysis What is necessary for the implementation of the multi-residue mycotoxin method in an analytical laboratory? Azel Swemmer azel@fdalab.co.za AFMA
METHOD 9075 TEST METHOD FOR TOTAL CHLORINE IN NEW AND USED PETROLEUM PRODUCTS BY X-RAY FLUORESCENCE SPECTROMETRY (XRF)
METHOD 9075 TEST METHOD FOR TOTAL CHLORINE IN NEW AND USED PETROLEUM PRODUCTS BY X-RAY FLUORESCENCE SPECTROMETRY (XRF) 1.0 SCOPE AND APPLICATION 1.1 This test method covers the determination of total chlorine
Appendix B. Eugene/Springfield Environmental Services Laboratory Quality Assurance Plan
Appendix B Eugene/Springfield Environmental Services Laboratory Quality Assurance Plan City of Eugene NPDES Stormwater Monitoring Plan May 2011 Users of this document are responsible to ensure it is the
NUTC R304. Use of Absorption Mechanisms to Decrease Heavy Metal Mobility
Use of Absorption Mechanisms to Decrease Heavy Metal Mobility by Jianmin Wang Honglan Shi Joe G. Burken NUTC R304 A National University Transportation Center at Missouri University of Science and Technology
1.2 This TAP is applicable to concrete, charcoal, coral, debris, wipes and soil.
March 2012 8 1 of 17 1.0 SCOPE 1.1 This procedure describes the preparation and analysis of solid matrices and wipe samples. 1.2 This TAP is applicable to concrete, charcoal, coral, debris, wipes and soil.
PROCEDURES FOR HANDLING OOS RESULTS
SOP # A-195--0100 STANDARD OPERATING PROCEDURES Page: 1 of 6. PROCEDURES FOR HANDLING OOS RESULTS 1. PURPOSE The purpose of this Standard Operation Procedure is to establish a procedure for the routine
DATA QUALITY OBJECTIVES
The Wastewater Treatment Plant Operators Guide to Biosolids Sampling Plans CHAPTER 5 DATA QUALITY OBJECTIVES Goals of the Sampling Plan ESSENTIAL ELEMENTS OF A SAMPLING PLAN Description of the Facility
LC-MS/MS Method for the Determination of Docetaxel in Human Serum for Clinical Research
LC-MS/MS Method for the Determination of Docetaxel in Human Serum for Clinical Research J. Jones, J. Denbigh, Thermo Fisher Scientific, Runcorn, Cheshire, UK Application Note 20581 Key Words SPE, SOLA,
This study was performed by Patrick Sullivan and staff at TestAmerica Analytical Testing Corp., Westfield, MA, USA
An Automated Method for the Fractionation of Extractable Petroleum Hydrocarbons (EPH) from Water and Soil Extracts Using the Gilson GX-274 ASPEC System Keywords: Aliphatic Hydrocarbons, Aromatic Hydrocarbons,
Fast, Reproducible LC-MS/MS Analysis of Dextromethorphan and Dextrorphan
Fast, Reproducible LC-MS/MS Analysis of and Kimberly Phipps, Thermo Fisher Scientific, Runcorn, Cheshire, UK Application Note 685 Key Words Accucore C18, dextromethorphan, dextrorphan, SOLA CX Abstract
Radioanalytical Data Validation Issues and Solutions
Radioanalytical Data Validation Issues and Solutions Presented by: Terry McKibbin and Kevin Harmon Validata Chemical Services, Inc. Purpose of Data Validation The Presentation is Based on this Goal for
Step-by-Step Analytical Methods Validation and Protocol in the Quality System Compliance Industry
Step-by-Step Analytical Methods Validation and Protocol in the Quality System Compliance Industry BY GHULAM A. SHABIR Introduction Methods Validation: Establishing documented evidence that provides a high
ANALYTICAL METHODS INTERNATIONAL QUALITY SYSTEMS
VALIDATION OF ANALYTICAL METHODS 1 GERT BEUVING INTERNATIONAL PHARMACEUTICAL OPERATIONS TASKS: - Internal auditing - Auditing of suppliers and contract manufacturers - Preparing for and guiding of external
Work Assignment 5-03. Prepared for: Office of Air Quality Planning and Standards U.S. Environmental Protection Agency Research Triangle Park, NC
ERG No.: 0143.04.005 EPA Contract No.: 68-D-00-264 Standard Operating Procedure for the Determination of Metals In Ambient Particulate Matter Analyzed By Inductively Coupled Plasma/Mass Spectrometry (ICP/MS)
Investigation of outdoor textiles with respect to determine the content of ionic perfluorinated
OR 59/2014 Investigation of outdoor textiles with respect to determine the content of ionic perfluorinated substances (PFASs) Evaluation of results Linda Hanssen, Dorte Herzke Scientific report 2 3 Preface
CLIENT NAME: MISC AGAT CLIENT ON, ON (403) ATTENTION TO: Chantell Cambal
CLIENT NAME: MISC AGAT CLIENT ON, ON (403) WATER ANALYSIS REVIEWED BY: Anthony Dapaah, PhD (Chem), Inorganic Lab Manager DATE REPORTED: May 19, 2015 PAGES (INCLUDING COVER): 5 VERSION*: 1 Should you require
ATTACHMENT 2. BMP Monitoring Plan Template
ATTACHMENT 2 BMP Monitoring Plan Template Project SPR - 335 Water Quality Facility Investigation Response to Modified Task 4: Development of BMP Monitoring Plan Template December 2002 i Table of Contents
CEDEN. California Environmental Data Exchange Network
CEDEN California Environmental Data Exchange Network Chemistry Data Submission Guidance Document Updated August 10th, 2012 Table of Contents INTRODUCTION...1 CHEMISTRY DATA SUBMISSION STEPS...1 CEDEN CHEMISTRY
Introduction. The following definitions may help you better understand the components of the data report.
Introduction This document is designed to help our clients understand the quality control requirements and limitations of data reporting. There are three sections to this document. The first section will
ANALYTICAL RESULTS. Project: NLNA - Cistern Water Testing. Submittal Date: 04/26/2010 Group Number: 1191887 State of Sample Origin: PA
ANALYTICAL RESULTS Prepared by: Lancaster Laboratories 2425 New Holland Pike Lancaster, PA 7605-2425 Prepared for: Philadelphia PA 923 May 0, 200 Project: - Cistern Water Testing Submittal Date: 04/26/200
Multifunctional Autosampler AOC-6000 C146-E272A
Multifunctional Autosampler C146-E272A Multifunctional Autosampler Multifunctional Autosampler Dramatically Improves GC/MS Analysis Productivity Automatic Switching Between Three GC/MS Sample Injection
Data Quality Objectives and Quality Assurance Project
Data Quality Objectives and Quality Assurance Project Plans Quality assurance (QA) Integrated system of management procedures and activities to verify that the QC system is operating within acceptable
How To Get Blood Test Records From A Blood Alcohol Test
CAUSE NO. THE STATE OF TEXAS IN THE COUNTY CRIMINAL V. COURT AT LAW NO. HARRIS COUNTY, TEXAS STANDING DISCOVERY ORDER ON COPYING AND PRODUCTION OF BLOOD TESTING RECORDS THE COURT ORDERS the District Attorney
IN VITRO BINDING BIOEQUIVALENCE STUDY SUMMARY TABLES AND SAS TRANSPORT FORMATTED TABLES FOR DATASET SUBMISSION
IN VITRO BINDING BIOEQUIVALENCE STUDY SUMMARY TABLES AND SAS TRANSPORT FORMATTED TABLES FOR DATASET SUBMISSION I. For Calcium Acetate Drug Products Table I.1 Submission Summary * Drug Product Name Strength(s)
LOW LEVEL DETECTION OF PCE IN MONITORING WELL SAMPLES USING A TOTAL ORGANIC CHLORINE BASED FIELD METHOD
DTR-21-2 1 LOW LEVEL DETECTION OF PCE IN MONITORING WELL SAMPLES USING A TOTAL ORGANIC CHLORINE BASED FIELD METHOD Theodore B. Lynn, Ph.D., Director of Research, Dexsil Corporation, One Hamden Park Drive,
Data Management for the CRESP Amchitka Project
Appendix 8.I Data Management for the CRESP Amchitka Project Vikram M. Vyas, Yuri Mun and Lisa Bliss This Appendix describes the procedures followed by the project personnel for inventorying and tracking
1. PURPOSE To provide a written procedure for laboratory proficiency testing requirements and reporting.
Document #: FDPD-QMS.024.003 Page 1 of 12 Table of Contents 1. Purpose 2. Scope 3. Responsibility 4. References 5. Related Documents 6. Definitions 7. Safety 8. Equipment/Materials Needed 9. Process Description
Uptake of perfluorinated alkyl substances (PFAS) by hydroponically grown lettuce (Lactuca sativa)
Uptake of perfluorinated alkyl substances (PFAS) by hydroponically grown lettuce (Lactuca sativa) Sebastian Felizeter Earth Surface Sciences University of Amsterdam Outline Introduction Materials and Method
Optimizing the Post-implementation Monitoring of a LC-MS/MS Method
Optimizing the Post-implementation Monitoring of a LC-MS/MS Method Julianne Cook Botelho, PhD Centers for Disease Control and Prevention Atlanta, GA AACC- Mass Spectrometry in the Clinical Lab: Best Practice
Standard Operating Procedure for Database Operations
PM 2.5 Diltabase Operations Date: May 8 2008 Page I of 18 Standard Operating Procedure for Database Operations Environmental Health and Safety Division RTl lnternational* Research Triangle Park, North
QUALITY ASSURANCE PROJECT PLAN FOR BROWNFIELDS/VOLUNTARY CLEANUP PROGRAM SITES
QUALITY ASSURANCE PROJECT PLAN FOR BROWNFIELDS/VOLUNTARY CLEANUP PROGRAM SITES Prepared by the Missouri Department of Natural Resources Division of Environmental Quality Hazardous Waste Program Brownfields/Voluntary
New Jersey Department of Environmental Protection Division of Remediation Management Response Site Remediation Program
New Jersey Department of Environmental Protection Division of Remediation Management Response Site Remediation Program NJDEP- SRP Low Level USEPA TO-15 Method (NJDEP-LLTO-15-3/2007) March 2007 March 2009
Laboratory Quality Assurance Manual
Laboratory Quality Assurance Manual (Revision 8) Effective Date: 03/22/2013 Approved By: Randall Warden President (260) 483-4759 03/22/2013 Date Greg Neyman Vice-President (260) 483-4759 03/22/2013 Date
Analytical Test Method Validation Report Template
Analytical Test Method Validation Report Template 1. Purpose The purpose of this Validation Summary Report is to summarize the finding of the validation of test method Determination of, following Validation
Laboratory Procedure Manual
Laboratory Procedure Manual Analyte: Matrix: Method: Method No.: Lead Dust Wipes Modification of the Automated AAII-25 Colorimetric method Nitric and Hydrochloric Acid Digestion followed by Atomic Absorption
Standard Operating Procedure for Document Storage, Archival, and Retrieval
SFWMDDVSSOP005003 Standard Operating Procedure for Version 3 Effective Date: Upon Final Approval Prepared by: Marina Gosis, Senior Scientist, Analytical Services Section Date: Approved by: Michael Wright,
Bryte Chemical Laboratory Quality Assurance Manual
Quality Assurance Technical Document 8 Bryte Chemical Laboratory Quality Assurance Manual May 2006 State of California The Resources Agency Department of Water Resources Bryte Chemical Laboratory Quality
Where does it come from?
What is Phosphorus? Phosphorus (P) is a nutrient that is vital to human, animal, and plant growth. It s one of the most common substances found in nature. It s found in our water, our food, and our bodies.
EPA NATIONAL LEAD LABORATORY ACCREDITATION PROGRAM. LABORATORY QUALITY SYSTEM REQUIREMENTS (LQSR) REVISION 3.0 (November 05, 2007)
EPA NATIONAL LEAD LABORATORY ACCREDITATION PROGRAM LABORATORY QUALITY SYSTEM REQUIREMENTS (LQSR) REVISION 3.0 (November 05, 2007) The requirements in this document apply to all lead testing laboratories
Quality Assurance Manual
Quality Assurance Manual Revision 9: Effective Date: 6/1/2015 Page: 1 of 25 Quality Assurance Manual For the Natural Resources Research Institute Central Analytical Laboratory University of Minnesota-Duluth
This example of a completed sampling plan worksheet has been included to illustrate the information
APPENDIX B EXAMPLE OF A COMPLETED SAMPLING PLAN WORKSHEET This example of a completed sampling plan worksheet has been included to illustrate the information necessary to document a sampling program for
Life & Times of a PM2.5 Filter: Quality Control in the Laboratory and Beyond
Life & Times of a PM2.5 Filter: Quality Control in the Laboratory and Beyond Brenda Saldana, Manager Inorganic Laboratory Section Monitoring and Laboratory Division Air Resources Board 1 Field Sampling
STANDARD OPERATING GUIDELINES: EVIDENTIAL BREATH ALCOHOL INSTRUMENT CALIBRATION
Directive from the Scientific Director Page 1 of 16 STANDARD OPERATING GUIDELINES: EVIDENTIAL BREATH ALCOHOL INSTRUMENT CALIBRATION 1 Scope To describe the procedure for breath alcohol instrument calibration
Building Credibility: Quality Assurance & Quality Control for Volunteer Monitoring Programs
Building Credibility: Quality Assurance & Quality Control for Volunteer Monitoring Programs Elizabeth Herron URI Watershed Watch/ National Facilitation of CSREES Volunteer Monitoring Ingrid Harrald Cook
QUALITY MANUAL Page 1 of 56 EMS LABORATORIES, INC. QUALITY MANUAL A. J. Kolk, Jr. Technical Director Revision #18 QM-001-18 Quality Manual Revision 2009.doc ANNUAL REVIEW OF QUALITY MANUAL QUALITY MANUAL
Working Copy - 1,- / t&,1 r. Responsibilities of the Laboratory Quality Assurance Officer. EffectiveDate: 7/ltl/ l'rritials: tuwt
QAM.Q-1 13 Approval: Responsibilities of the Laboratory Quality Assurance Officer Laboratory Manager/ Quality Assurance Officer Concurrefirco - -/^/ - 1,- Rev. 4 EffectiveDate: 7/ltl/ Date,i / t&,1 r Renewat
Thermo Scientific SOLAµ SPE Plates Technical Guide. Consistent excellence. for bioanalysis
Thermo Scientific SOLAµ SPE Plates Technical Guide Consistent excellence for bioanalysis SOLAµ - delivering reproducible low volume extractions. Everytime! Thermo Scientific SOLAµ plates are designed for