Overall Reaction Scheme: Step 1. Step 2. Step 3. R: HCl S: DMF. 4-hydroxybenzaldehyde. 4-hydroxybenzyl alcohol. C: NaOH S: H 2 O Me 2 CO R: AcOH

Size: px
Start display at page:

Download "Overall Reaction Scheme: Step 1. Step 2. Step 3. R: HCl S: DMF. 4-hydroxybenzaldehyde. 4-hydroxybenzyl alcohol. C: NaOH S: H 2 O Me 2 CO R: AcOH"

Transcription

1 Honors Cup Synthetic Proposal (250 II-W PM-W08) Section: 250 Group Members: Adrienne Cheng, Eric Chow, Hannah VanVels Title: Synthesis of Raspberry Ketone Introduction: We will be attempting to synthesize 4-(4-hydroxyphenyl)butan-2-one, also known as raspberry ketone. Raspberry ketone is the primary aroma of red raspberries. It is often industrially produced for perfumery, cosmetics, and food additives. Studies have also shown that when given to mice in large doses, it can assist in preventing obesity. verall Reaction Scheme: Step 1 CH 2 H R: MCPBA C 4-hydroxybenzyl alcohol R: HCl S: DMF Step 2 C C: NaH S: H 2 Me 2 C R: AcH Step 3 R: Zn, CH CH 2 CH 2 CMe 4-(4-hydroxyphenyl)butan-2-one

2 Procedure: Step 1 CH 2 H R: MCPBA C 4-hydroxybenzyl alcohol R: HCl S: DMF Synthetic transformation 1: Experimental 1 Add 250 mg MCPBA (1 mmol) in 5 ml of freshly distilled DMF. Add dropwise to 4- hydroxybenzyl alcohol. Mix the alcohol in a solution of HCl and DMF (0.1 ml of 1M solution of dry HCl in DMF) in 5 ml of DMF at room temperature. Stir reaction for 5 minutes and pour into cold aqueous 5% K 2 C 3. Extract with diethyl ether (2x15 ml). Wash extracts with aqueous 5% K 2 C 3 (2x15 ml) and dry with MgS 4. This creates. Expected yield: 100 % 122g Safety, disposal and green issues 1: 4-hydroxybenayl alcohol: This compound is photo-sensitive. It must be kept under nitrogen. It is also sensitive to air and an irritant to skin and eyes. Wear gloves and protective eye/face covering. MCPBA: This compound is an oxidizing agent. It is corrosive and may cause fire and burns. Keep in a cool place and keep bottle tightly closed. Do not heat over 40 degrees C. Keep hands and eyes covered. Step 2 C C: NaH S: H 2 Me 2 C R: AcH Synthetic Transformation of Experimental 2 Pour acetone and in equimolecular conditions with glacial acetic acid and heat up at the reflux condenser. Extract using NaH. In the original procedure, the aldehyde was extracted using rhodaninic acid.

3 Expected yield: 96 % g Safety, disposal and green issues 2: Sodium hydroxide: This substance is corrosive and causes severe burns. Keep under argon. It is also sensitive to carbon dioxide. Wear gloves and goggles when handling. Acetic Acid: This compound is corrosive and also flammable. It causes severe burns. Do not inhale. Step 3 R: Zn, H, H 2 CH 2 CH 2 CMe 4-(4-hydroxyphenyl)butan-2-one Synthetic Transformation of 4-(4-hydroxyphenyl)butan-2-one (raspberry ketone) Experimental 3 Use a three-necked flask, fitted with a reflux condenser and septa and purge with nitrogen gas 15 min. Make a zinc/thf slurry and transfer to the flask dropwise. Heat Zn suspension to reflux. Add methonal solution of (E)-4-(4-hydroxyphenyl)but-3-ene-2-one and add water in the ratio of THF:methanol:water used 7:5:1. Reflux 2.5 hours under nitrogen. Cool and flood with 150 ml of ether. Extract successively with 10% ammonium chloride (25 ml), 10% sodium bicarbonate (25 ml), and saturated sodium chloride (25 ml). Dry over anhydrous magnesium sulfate and strip solvents by rotary evaporation. In the original procedure, it was stated to use argon gas instead of nitrogen. Characterization of the final compound can be done with NMR analysis using CDCl3 for analysis. Expected yield: 100 % g Safety, disposal and green issues 3: Acetic Acid: This compound is corrosive and also flammable. It can cause severe burns. Do not inhale. Zinc: Zinc is dangerous for the environment especially the aquatic environment. It must be disposed of in a secure container labeled hazardous waste. Release into the environment should be avoided.

4 THF: This compound tends to form peroxides on storage in air. As a result, THF should not be distilled to dryness, which can leave a residue of highly-explosive peroxides. Take precautionary measures against static discharges. Do not empty into drains. Ammonium chloride: This compound is harmful if swallowed and toxic if it comes in contact with skin or inhaled. If it comes in contact with water, toxic gas is liberated. It can be highly flammable. It can cause severe burns and irritates eyes. Do not breathe dust. verall budget: Chemical Supplier Cost Amount Total Needed 4-hydroxybenzyl alcohol Aldrich $70.50/25 g 122 mg $0.34 MCPBA Aldrich $62.80/100 g 250 ml $157 HCl Sigma $43.40/100 ml ~20 ml $8.86 DMF Sigma $33.80/500 ml 5 ml $ M NaH in H 2 Fluka $55.80/100 ml ~20 ml $11.16 Ach Sigma $67.30/100 ml ~25 ml $16.83 Zinc Riedel-de Haeel $39.70/500 g ~130 g $10.32 K 2 C 3 Sigma $42.30/500 g ~30 ml $5.08 MgS 4 Fluka $41.30/250 g ~ 5 g $0.83 Diethyl Ether Fluka $96.40/2.5 L ~30 ml $1.16 Acetone Aldrich $46/1 L ~25 ml $1.15 THF Sigma $46.50/1 L 25 ml $0.02 Ammonium chloride Sigma $30.20/500 g 25 ml $1.21 Sodium chloride Fluka $21.10/100 ml 25 ml $5.28 References: Total costs per synthesis: $ Step 1: Kim H. R.; Jung J. H.; Kim J. N.; Ryu E. K. Synthetic Communications, 1990, 20(5), Step 2: Andreasch, Rudolph; Zipser, Arthur ver Substituted Rhodaninic Acid and Their Aldehyde Condensation Products (machine translation) Monatshefte fuer Chemie 1904, 25, Step 3:

5 Kroemera J. ;Kirkpatricka C.,Mariclea B.; Gawrycha R., Moshera M.D. Tetrahedron Letters, 2006, 47(36), pp

Honors Cup Synthetic Proposal

Honors Cup Synthetic Proposal onors Cup Synthetic Proposal Section: 230-IV Group Members: Alex yla, Lauren eath, Sahar Rahmani Title: Synthesis of Melatonin from 3-(3-phthalimidopropyl) ethyl acetacetate using Green Chemistry Introduction:

More information

4026 Synthesis of 2-chloro-2-methylpropane (tert-butyl chloride) from tert-butanol

4026 Synthesis of 2-chloro-2-methylpropane (tert-butyl chloride) from tert-butanol 4026 Synthesis of 2-chloro-2-methylpropane (tert-butyl chloride) from tert-butanol OH + HCl Cl + H 2 O C 4 H 10 O C 4 H 9 Cl (74.1) (36.5) (92.6) Classification Reaction types and substance classes nucleophilic

More information

Properties of Acids and Bases

Properties of Acids and Bases Properties of Acids and Bases (Adapted from Flinn Scientific Acid Base Test Kit I #AP4567) Introduction Battery acid, stomach acid, acid rain just a few acids in our everyday life! What does it mean when

More information

Synthesis of Isopentyl Acetate

Synthesis of Isopentyl Acetate Experiment 8 Synthesis of Isopentyl Acetate Objectives To prepare isopentyl acetate from isopentyl alcohol and acetic acid by the Fischer esterification reaction. Introduction Esters are derivatives of

More information

CH243: Lab 4 Synthesis of Artificial Flavorings by Fischer Esterification

CH243: Lab 4 Synthesis of Artificial Flavorings by Fischer Esterification H243: Lab 4 Synthesis of Artificial Flavorings by Fischer Esterification PURPSE: To prepare esters by reaction of carboxylic acids and alcohols. To modify a known procedure to prepare an unknown. DISUSSIN:

More information

Table 1. Common esters used for flavors and fragrances

Table 1. Common esters used for flavors and fragrances ESTERS An Introduction to rganic hemistry Reactions 2012, 2006, 1990, 1982 by David A. Katz. All rights reserved. Reproduction permitted for educationa use provided original copyright is included. In contrast

More information

DYES AND DYEING 2003 by David A. Katz. All rights reserved. Permission for classroom use provided original copyright is included.

DYES AND DYEING 2003 by David A. Katz. All rights reserved. Permission for classroom use provided original copyright is included. DYES AND DYEING 2003 by David A. Katz. All rights reserved. Permission for classroom use provided original copyright is included. Dyeing of textiles has been practiced for thousands of years with the first

More information

Experiment #7: Esterification

Experiment #7: Esterification Experiment #7: Esterification Pre-lab: 1. Choose an ester to synthesize. Determine which alcohol and which carboxylic acid you will need to synthesize your ester. Write out the reaction for your specific

More information

Saturated NaCl solution rubber tubing (2) Glass adaptor (2) thermometer adaptor heating mantle

Saturated NaCl solution rubber tubing (2) Glass adaptor (2) thermometer adaptor heating mantle EXPERIMENT 5 (Organic Chemistry II) Pahlavan/Cherif Dehydration of Alcohols - Dehydration of Cyclohexanol Purpose - The purpose of this lab is to produce cyclohexene through the acid catalyzed elimination

More information

Santa Monica College Chemistry 11

Santa Monica College Chemistry 11 Types of Reactions Objectives The objectives of this laboratory are as follows: To perform and observe the results of a variety of chemical reactions. To become familiar with the observable signs of chemical

More information

Experiment 3: Extraction: Separation of an Acidic, a Basic and a Neutral Substance

Experiment 3: Extraction: Separation of an Acidic, a Basic and a Neutral Substance 1 Experiment 3: Extraction: Separation of an Acidic, a Basic and a Neutral Substance Read pp 142-155, 161-162, Chapter 10 and pp 163-173, Chapter 11, in LTOC. View the videos: 4.2 Extraction (Macroscale);

More information

SAFETY DATA SHEET (according to EC directive 93/112/EC) Update : 14.07.2002 Version: 2.0 Date : 07.03.2003 TEGOAMIN BDE 100

SAFETY DATA SHEET (according to EC directive 93/112/EC) Update : 14.07.2002 Version: 2.0 Date : 07.03.2003 TEGOAMIN BDE 100 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND THE COMPANY/UNDERTAKING Trade name : Information on manufacturer/supplier : Goldschmidt AG Goldschmidtstr. 100 45127 Essen Telephone: +492011730 Telefax:

More information

DIAMOND POWDER - MICRON

DIAMOND POWDER - MICRON SAFETY DATA SHEET REVISION: 08/28/2015 DIAMOND POWDER - MICRON 1. PRODUCT & COMPANY INFORMATION 1.1 PRODUCT IDENTIFIER(S) PRODUCT NAME: DIAMOND POWDER - MICRON MICRON 5 CARAT PART # 100 CARAT PART# MICRON

More information

EXPERIMENT 3 (Organic Chemistry II) Nitration of Aromatic Compounds: Preparation of methyl-m-nitrobenzoate

EXPERIMENT 3 (Organic Chemistry II) Nitration of Aromatic Compounds: Preparation of methyl-m-nitrobenzoate EXPERIMENT 3 (Organic Chemistry II) Nitration of Aromatic Compounds: Preparation of methyl-m-nitrobenzoate Pahlavan/Cherif Purpose a) Study electrophilic aromatic substitution reaction (EAS) b) Study regioselectivity

More information

Safety Data Sheet. according to Regulation (EC) No 1907/2006 6% AFFF DC-6

Safety Data Sheet. according to Regulation (EC) No 1907/2006 6% AFFF DC-6 Page 1 of 5 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier 1.2. Relevant identified uses of the substance or mixture and uses advised against

More information

Swallowed Do not induce vomiting give 250 ml water to drink. Seek immediate medical attention.

Swallowed Do not induce vomiting give 250 ml water to drink. Seek immediate medical attention. Section 3- HAZARDS IDENTIFICATION R20/21 3.1 Hazardous substance dangerous goods 3.2 Risk Phrases R20/21 Harmful by inhalation in contact with skin. 3.3 Safety Phrases S16 Keep away from sources of ignition

More information

Designing An Experiment Using Baking Soda and Vinegar

Designing An Experiment Using Baking Soda and Vinegar Designing An Experiment Using Baking Soda and Vinegar Introduction: Kinetics is the study of chemical reaction rates. It is the study of how fast different chemicals react with one another to form new

More information

Separation by Solvent Extraction

Separation by Solvent Extraction Experiment 3 Separation by Solvent Extraction Objectives To separate a mixture consisting of a carboxylic acid and a neutral compound by using solvent extraction techniques. Introduction Frequently, organic

More information

CAS-No. EC-No. Index-No. Concentration Benzyl carbazate 5331-43-1 226-230-3 - -

CAS-No. EC-No. Index-No. Concentration Benzyl carbazate 5331-43-1 226-230-3 - - SIGMA-ALDRICH Material Safety Data Sheet Version 3.0 Revision Date 12/24/2008 Print Date 04/02/2009 1. PRODUCT AND COMPANY IDENTIFICATION Product name : Benzyl carbazate Product Number : 17307 Brand :

More information

Creation Date: 20.07.1999 Revision Date: 11.08.2009 Page: 1 of 7

Creation Date: 20.07.1999 Revision Date: 11.08.2009 Page: 1 of 7 Creation Date: 20.07.1999 Revision Date: 11.08.2009 Page: 1 of 7 1. Identification of Products Product Name: Guardex Chlor-Out Product Code: 20 35 568 010 Chemical Name: Sodium Sulphite Distributed by:

More information

Page 1 of 5. Purification of Cholesterol An Oxidative Addition-Reductive Elimination Sequence

Page 1 of 5. Purification of Cholesterol An Oxidative Addition-Reductive Elimination Sequence Page 1 of 5 Purification of Cholesterol An Oxidative Addition-Reductive Elimination Sequence From your lectures sessions in CEM 2010 you have learned that elimination reactions may occur when alkyl halides

More information

Preparation of frequently used solutions

Preparation of frequently used solutions Preparation of frequently used solutions Content 1. Diluting Concentrated Acids (Last Login: 08/08/2009) 2. Indicators (Last Login: 27/07/2009) 3. Standard Buffer Solutions (Last Login: 27/07/2009) 4.

More information

GRIGNARD REACTION: PREPARATION OF TRIPHENYLMETHANOL (12/22/2009)

GRIGNARD REACTION: PREPARATION OF TRIPHENYLMETHANOL (12/22/2009) GRIGNARD REACTIN: PREPARATIN F TRIPHENYLMETHANL (12/22/2009) Grignard reagents are among the most versatile organometallic reagents, and they are the easiest organometallic reagent to prepare. Grignard

More information

Properties of Acids and Bases

Properties of Acids and Bases Lab 22 Properties of Acids and Bases TN Standard 4.2: The student will investigate the characteristics of acids and bases. Have you ever brushed your teeth and then drank a glass of orange juice? What

More information

Material Safety Data Sheet 1. PRODUCT AND COMPANY INDENTIFICATION

Material Safety Data Sheet 1. PRODUCT AND COMPANY INDENTIFICATION Material Safety Data Sheet 1. PRODUCT AND COMPANY INDENTIFICATION POWDER 365 - RAL COLOURS Revision date: 09/20/2010 Supplier Powder 365 82 Green Acres Circle Lavonia GA 30553 For non-emergency information

More information

EXPERIMENT 12: Empirical Formula of a Compound

EXPERIMENT 12: Empirical Formula of a Compound EXPERIMENT 12: Empirical Formula of a Compound INTRODUCTION Chemical formulas indicate the composition of compounds. A formula that gives only the simplest ratio of the relative number of atoms in a compound

More information

Mechanical Systems Competency 1.20

Mechanical Systems Competency 1.20 Competency 1.20 Mechanical systems personnel shall demonstrate a working level knowledge of the safety and health fundamentals of mechanical systems and/or components. 1. Supporting Knowledge and Skills

More information

Date Printed: 08/29/2005 Date Updated: 03/07/2004 Version 1.4. CERIUM(III) NITRATE HEXAHYDRATE, 99.99% Product Number 392219

Date Printed: 08/29/2005 Date Updated: 03/07/2004 Version 1.4. CERIUM(III) NITRATE HEXAHYDRATE, 99.99% Product Number 392219 SIGMA-ALDRICH MATERIAL SAFETY DATA SHEET Date Printed: 08/29/2005 Date Updated: 03/07/2004 Version 1.4 Section 1 - Product and Company Information Product Name CERIUM(III) NITRATE HEXAHYDRATE, 99.99% Product

More information

experiment5 Understanding and applying the concept of limiting reagents. Learning how to perform a vacuum filtration.

experiment5 Understanding and applying the concept of limiting reagents. Learning how to perform a vacuum filtration. 81 experiment5 LECTURE AND LAB SKILLS EMPHASIZED Synthesizing an organic substance. Understanding and applying the concept of limiting reagents. Determining percent yield. Learning how to perform a vacuum

More information

SAFETY DATA SHEET (according to EC directive 93/112/EC) Update : 14.07.2002 Version: 2.0 Date : 07.03.2003 TEGOAMIN DMCHA

SAFETY DATA SHEET (according to EC directive 93/112/EC) Update : 14.07.2002 Version: 2.0 Date : 07.03.2003 TEGOAMIN DMCHA 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND THE COMPANY/UNDERTAKING Trade name : Information on manufacturer/supplier : Goldschmidt AG Goldschmidtstr. 100 45127 Essen Telephone: +492011730 Telefax:

More information

SAFETY DATA SHEET. according to 1907/2006/EC, Article 31 CYTOFIXX (CYTOLOGICAL FIXATIVE)

SAFETY DATA SHEET. according to 1907/2006/EC, Article 31 CYTOFIXX (CYTOLOGICAL FIXATIVE) SAFETY DATA SHEET according to 197/26/EC, Article 31 Page 1/5 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier Product name 1.3. Details of the

More information

Dry Ice Color Show Dry Ice Demonstrations

Dry Ice Color Show Dry Ice Demonstrations elearning 2009 Introduction Dry Ice Color Show Dry Ice Demonstrations Publication No. 95016 Add a small piece of solid carbon dioxide to a colored indicator solution and watch as the solution immediately

More information

SAFETY DATA SHEET EVO-STIK GRIPFILL SOLVENT FREE (Irl)

SAFETY DATA SHEET EVO-STIK GRIPFILL SOLVENT FREE (Irl) Revision Date December 2014 SAFETY DATA SHEET According to Regulation (EC) No 1907/2006 1 / 6 SECTION 1: IDENTIFICATION OF THE SUBSTANCE/MIXTURE AND OF THE COMPANY/UNDERTAKING 1.1. Product identifier Product

More information

Health and Safety Guidance

Health and Safety Guidance Health and Safety Guidance Guidance on the Classification, Labelling and Packaging (CLP) Regulations GUIDANCE/29/CLP/11 This guidance is aimed at those handling hazardous chemicals; from single substances

More information

: Fairy Professional Original Washing Up Liquid 5L

: Fairy Professional Original Washing Up Liquid 5L PROFESSIONAL Fairy Professional Original Washing Up Liquid 5L Date of issue: 17/11/2011 Revision date: Version: 1.0 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1.

More information

Physical and Chemical Properties and Changes

Physical and Chemical Properties and Changes Physical and Chemical Properties and Changes An understanding of material things requires an understanding of the physical and chemical characteristics of matter. A few planned experiments can help you

More information

Lab #13: Qualitative Analysis of Cations and Anions

Lab #13: Qualitative Analysis of Cations and Anions Lab #13: Qualitative Analysis of Cations and Anions Objectives: 1. To understand the rationale and the procedure behind the separation for various cations and anions. 2. To perform qualitative analysis

More information

MATERIAL SAFETY DATA SHEET (MSDS) ZINC DUST

MATERIAL SAFETY DATA SHEET (MSDS) ZINC DUST Page 1 of 5 MATERIAL SAFETY DATA SHEET (MSDS) ZINC DUST SECTION 1 - PRODUCER & SUPPLIERS DETAILS Manufacturer & Supplier: NUMINOR CHEMICAL INDUSTRIES LTD. Address: P. O. BOX 92, MAALOT 24952, ISRAEL. Tel:

More information

ATMER 163 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING. Antistatic concentrate

ATMER 163 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING. Antistatic concentrate 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING Address/Telephone number UNIQEMA Wilton Centre, Wilton Redcar TS10 4RF England Tel. : +44 (0) 1642 456699 Emergency telephone

More information

Safety Data Sheet Euperlan PK 3000 AM Revision date : 2016/05/16 Page: 1/9

Safety Data Sheet Euperlan PK 3000 AM Revision date : 2016/05/16 Page: 1/9 Revision date : 2016/05/16 Page: 1/9 1. Identification Product identifier used on the label Euperlan PK 3000 AM Recommended use of the chemical and restriction on use Recommended use*: Chemical * The Recommended

More information

Teacher Demo: Turning Water into Wine into Milk into Beer

Teacher Demo: Turning Water into Wine into Milk into Beer SNC2D/2P Chemical Reactions/Chemical Reactions and their Practical Applications Teacher Demo: Turning Water into Wine into Milk into Beer Topics evidence of chemical change types of chemical reactions

More information

In this experiment, we will use three properties to identify a liquid substance: solubility, density and boiling point..

In this experiment, we will use three properties to identify a liquid substance: solubility, density and boiling point.. Identification of a Substance by Physical Properties 2009 by David A. Katz. All rights reserved. Permission for academic use provided the original copyright is included Every substance has a unique set

More information

Working with Hazardous Chemicals

Working with Hazardous Chemicals A Publication of Reliable Methods for the Preparation of Organic Compounds Working with Hazardous Chemicals The procedures in Organic Syntheses are intended for use only by persons with proper training

More information

Sodium Aluminum Tetrafluoride

Sodium Aluminum Tetrafluoride In an emergency, call CHEMTREC at 800-424-9300 or MEMC Pasadena at 713-740-1501 NaAlF 4 HEALTH FLAMMABILITY 2 0 2 0 0 PHYSICAL HAZARD 0 PERSONAL PROTECTION SECTION 1: CHEMICAL PRODUCT AND COMPANY IDENTIFICATION

More information

Austin Peay State University Department of Chemistry CHEM 1111. Empirical Formula of a Compound

Austin Peay State University Department of Chemistry CHEM 1111. Empirical Formula of a Compound Cautions Magnesium ribbon is flammable. Nitric acid (HNO 3 ) is toxic, corrosive and contact with eyes or skin may cause severe burns. Ammonia gas (NH 3 ) is toxic and harmful. Hot ceramic crucibles and

More information

PREPARATION AND PROPERTIES OF A SOAP

PREPARATION AND PROPERTIES OF A SOAP (adapted from Blackburn et al., Laboratory Manual to Accompany World of Chemistry, 2 nd ed., (1996) Saunders College Publishing: Fort Worth) Purpose: To prepare a sample of soap and to examine its properties.

More information

Material Safety Data Sheet

Material Safety Data Sheet Material Safety Data Sheet Calcium acetate MSDS 0 1 0 He a lt h Fire Re a c t iv it y Pe rs o n a l Pro t e c t io n 1 1 0 E Section 1: Chemical Product and Company Identification Product Name: Calcium

More information

SAFETY DATA SHEET according to 1907/2006/EC, Article 31

SAFETY DATA SHEET according to 1907/2006/EC, Article 31 SAFETY DATA SHEET according to 1907/006/EC, Article 31 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier Product name Product code QAFS743 1.. Relevant

More information

Magnesium Carbonate, Lite, Powder USP

Magnesium Carbonate, Lite, Powder USP Safety Data Sheet Magnesium Carbonate, Lite, Powder USP 1. PRODUCT AND COMPANY IDENTIFICATION Product Name: Magnesium Carbonate, Lite, Powder USP Synonyms/Generic Names: None Product Number: 3170 Product

More information

: 3-Chloro-4-methoxybenzoic acid

: 3-Chloro-4-methoxybenzoic acid 1. IDENTIFICATION OF THE SUBSTANCE/MIXTURE AND OF THE COMPANY/UNDERTAKING Product name : 3-Chloro-4-methoxybenzoic acid Product Number : EX-002387 Brand : Exir Company : Exir GmbH Flotowgasse 18-22/2/1

More information

Experiment 8 Preparation of Cyclohexanone by Hypochlorite Oxidation

Experiment 8 Preparation of Cyclohexanone by Hypochlorite Oxidation Experiment 8 Preparation of Cyclohexanone by ypochlorite xidation In this experiment we will prepare cyclohexanone from cyclohexanol using hypochlorite oxidation. We will use common household bleach that

More information

: FAIRY ORIGINAL DISHWASHER TABLETS

: FAIRY ORIGINAL DISHWASHER TABLETS PROFESSIONAL FAIRY ORIGINAL DISHWASHER TABLETS Date of issue: 25/11/2011 Revision date: Version: 1.0 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier

More information

Safety Data Sheet. Product #: 300178. Aspira Scientific 521 Cottonwood Dr. Milpitas, CA 95035 408.571.1100 techsupport@aspirasci.com www.aspirasci.

Safety Data Sheet. Product #: 300178. Aspira Scientific 521 Cottonwood Dr. Milpitas, CA 95035 408.571.1100 techsupport@aspirasci.com www.aspirasci. Safety Data Sheet Aspira Scientific 521 Cottonwood Dr. Milpitas, CA 95035 408.571.1100 techsupport@aspirasci.com www.aspirasci.com Section 1: Product Identification Product Identifiers Product Name: L-

More information

MATERIAL SAFETY DATA SHEET Description: SAF DRAIN Revision Number: 00

MATERIAL SAFETY DATA SHEET Description: SAF DRAIN Revision Number: 00 GRANULAR, ALKALINE DRAIN CLEANER GENERAL SAF-DRAIN is a powerful alkaline drain cleaner designed so that the product reaches the problem area before the reaction takes place. It effectively cleans organic

More information

#9 Condensation Polymerization: Preparation of Nylon 6/10

#9 Condensation Polymerization: Preparation of Nylon 6/10 #9 Condensation Polymerization: Preparation of Nylon 6/10 Submitted by: Arturo Contreras, Visiting Scholar, Center for Chemical Education, Miami University, Middletown, OH; 1996 1997. I. INTRODUCTION Description

More information

CHEMISTRY 338 THE SYNTHESIS OF LIDOCAINE

CHEMISTRY 338 THE SYNTHESIS OF LIDOCAINE CHEMISTRY 338 THE SYTHESIS F LIDCAIE Lidocaine (1) is the common name of an important member of a category of drugs widely used as local anesthetics. Trade names for this substance include Xylocaine, Isocaine,

More information

Oxidizer(s) Management and Use Guidelines

Oxidizer(s) Management and Use Guidelines Facilities and Campus Services EHS/RMS 3101 Science Circle CPISB Room 102B Anchorage, AK 99508 Oxidizer(s) Management and Use Guidelines This document provides information concerning the handling, storage,

More information

Training Requirements for the Revised Hazard Communication Standard

Training Requirements for the Revised Hazard Communication Standard www.alterisus.com Training Requirements for the Revised Hazard Communication Standard As of December 1, 2013 OSHA revised its Hazard Communication Standard (HCS) to align with the United Nations Globally

More information

Recovery of Elemental Copper from Copper (II) Nitrate

Recovery of Elemental Copper from Copper (II) Nitrate Recovery of Elemental Copper from Copper (II) Nitrate Objectives: Challenge: Students should be able to - recognize evidence(s) of a chemical change - convert word equations into formula equations - perform

More information

MUCICARMINE STAIN - SOUTHGATE S - MUCIN PURPOSE:

MUCICARMINE STAIN - SOUTHGATE S - MUCIN PURPOSE: SURGICAL PATHOLOGY - HISTOLOGY Date: STAINING MANUAL - CARBOHYDRATES Page: 1 of 2 MUCICARMINE STAIN - SOUTHGATE S - MUCIN PURPOSE: To stain mucin which is a secretion produced by a variety of epithelial

More information

CAS-No. EC-No. Index-No. Concentration Controlled Pore Glass - - - - May be harmful if inhaled. May cause respiratory tract irritation.

CAS-No. EC-No. Index-No. Concentration Controlled Pore Glass - - - - May be harmful if inhaled. May cause respiratory tract irritation. SIGMAALDRICH Material Safety Data Sheet Version 3.0 Revision Date 01/03/2009 Print Date 02/18/2009 1. PRODUCT AND COMPANY IDENTIFICATION Product name : Glass beads, acidwashed Product Number : G8772 Brand

More information

*** SAFETY DATA SHEET ***

*** SAFETY DATA SHEET *** *** SAFETY DATA SHEET *** 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING PRODUCT NAME ECCOBOND 50126 FC PART A RECOMMENDED USE SUPPLIER Adhesive ICI Belgium nv (Emerson &

More information

BOOSTER FLUID SOLUTION I. PRODUCT IDENTIFICATION

BOOSTER FLUID SOLUTION I. PRODUCT IDENTIFICATION Date: November 2014 PRODUCT CHEMICAL METHYL ALCOHOL / BORIC ACID MATERIAL SAFETY DATA SHEETS MATERIAL SAFETY DATA SHEET CHEMICAL NAME Methanol COMMON SYNONYMS BOOSTER FLUID SOLUTION I. PRODUCT IDENTIFICATION

More information

SAFETY DATA SHEET DOUBLE TT MAINTENANCE SPRAY

SAFETY DATA SHEET DOUBLE TT MAINTENANCE SPRAY Report Date : 11/05/2011 1 / 5 SAFETY DATA SHEET 1 IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING PRODUCT NAME PRODUCT NO. INTERNAL ID APPLICATION SUPPLIER DTT200, DTT400, DTT600,

More information

Supporting Information

Supporting Information Copyright WILEY VCH Verlag GmbH & Co. KGaA, 69469 Weinheim, Germany, 2012. Supporting Information for Adv. Funct. Mater., DOI: 10.1002/adfm.201102486 Colorimetric Detection of Warfare Gases by Polydiacetylenes

More information

Safety Data Sheet Aluminium profiles Apply for alloys Sapa EN AW 6060, 6063, 6005, 6005A, 6082, yellow chromated, with or without powder coating.

Safety Data Sheet Aluminium profiles Apply for alloys Sapa EN AW 6060, 6063, 6005, 6005A, 6082, yellow chromated, with or without powder coating. Apply for alloys Sapa EN AW 6060, 6063, 6005, 6005A, 6082, yellow chromated, with or without powder coating. 1. Identification of the Substance/Preparation and Company Product name: (Alloys, Sapa EN AW

More information

1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING

1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING SIGMA-ALDRICH SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 Version 3.3 Revision Date 11.12.2008 Print Date 16.01.2009 GENERIC EU MSDS - NO COUNTRY SPECIFIC DATA - NO OEL DATA 1. IDENTIFICATION

More information

MATERIAL SAFETY DATA SHEET. SODIUM HYDRIDE, 65% dispersion in mineral oil, toluene soluble bags

MATERIAL SAFETY DATA SHEET. SODIUM HYDRIDE, 65% dispersion in mineral oil, toluene soluble bags MATERIAL SAFETY DATA SHEET SODIUM HYDRIDE, 65% dispersion in mineral oil, toluene soluble bags SECTION 1 - CHEMICAL PRODUCT AND COMPANY IDENTIFICATION MSDS Name: SODIUM HYDRIDE, 65% dispersion in mineral

More information

CHEMICAL REACTIONS OF COPPER AND PERCENT YIELD KEY

CHEMICAL REACTIONS OF COPPER AND PERCENT YIELD KEY CHEMICAL REACTIONS OF COPPER AND PERCENT YIELD Objective To gain familiarity with basic laboratory procedures, some chemistry of a typical transition element, and the concept of percent yield. Apparatus

More information

Safety Data Sheet. MAPP Gas. Page 2 / 6. According to regulation (EC) 1907/2006. ROTHENBERGER Werkzeuge GmbH Industriestr.

Safety Data Sheet. MAPP Gas. Page 2 / 6. According to regulation (EC) 1907/2006. ROTHENBERGER Werkzeuge GmbH Industriestr. According to Page 2 / 6 ROTHENBERGER Werkzeuge GmbH Industriestr. 7 65779 Kelkheim Tel.: + 49 (0) 6195 800 1 Fax: + 49 (0) 6195 7 44 22 Mail: zentrale@rothenberger.com Web: www.rothenberger.com Seite 1

More information

PEROXIDE SAFETY DATA SHEET (60% H2O2) Safety Data Sheet

PEROXIDE SAFETY DATA SHEET (60% H2O2) Safety Data Sheet SAYFA : 1/6 1. Identification of the substance Identification of the product Product name : Hydrogen peroxide solution 60% Manufacturer / supplier identification Company : A.Ş. 600Evler Mahallesi Atatürk

More information

INCOMPATIBILITY OF COMMON LABORATORY CHEMICALS

INCOMPATIBILITY OF COMMON LABORATORY CHEMICALS INCOMPATIBILITY OF COMMON LABORATORY CHEMICALS When certain hazardous chemicals are stored or mixed together, violent reactions may occur because the chemicals are unsuitable for mixing, or are incompatible.

More information

CRC Industries Europe bvba. 12, Bld des Martyrs de Chateaubriant F-95102 Argenteuil Cédex

CRC Industries Europe bvba. 12, Bld des Martyrs de Chateaubriant F-95102 Argenteuil Cédex 1. IDENTIFICATION OF PRODUCT AND COMPANY Productname : Application : Company : GASKET REMOVER Aerosol Cleaners - Heavy duty Touwslagerstraat 1 9240 ZELE Belgium Tel.: (+32)(0)52/456011 Fax: (+32)(0)52/450034

More information

Carbon. Extraction of Essential Oils from Spices using Steam Distillation. Carbon

Carbon. Extraction of Essential Oils from Spices using Steam Distillation. Carbon Extraction of Essential Oils from Spices using Steam Distillation Contents Objectives 1 Introduction 1 Extraction of trans-anethole from star anise 2 Extraction of trans-cinnamaldehyde from cinnamon 5

More information

MATERIAL SAFETY DATA SHEET (MSDS)/SAFETY DATA SHEET (SDS)

MATERIAL SAFETY DATA SHEET (MSDS)/SAFETY DATA SHEET (SDS) I. Product and Company Identification Product Name: VetScan FeLV-FIV Test A point of care blood diagnostic product Part Numbers: 250-0000-5, 250-0000-25 Manufactured For Abaxis By: SA Scientific, Inc.

More information

LITHIUM CARBONATE, 1% AQUEOUS

LITHIUM CARBONATE, 1% AQUEOUS Material Safety Data Sheet LITHIUM CARBONATE, 1% AQUEOUS Section 1 - Chemical Product and Company Identification MSDS Name: Lithium Carbonate, 1% Aqueous Catalog Numbers: SO-721 Company Identification:

More information

Date Printed: 04/29/2008 Date Updated: 11/08/2007 Version 1.8. BETA-CAROTENE, CA. 1600 U/MG Product Number 22040

Date Printed: 04/29/2008 Date Updated: 11/08/2007 Version 1.8. BETA-CAROTENE, CA. 1600 U/MG Product Number 22040 SIGMA-ALDRICH MATERIAL SAFETY DATA SHEET Date Printed: 04/29/2008 Date Updated: 11/08/2007 Version 1.8 Section 1 - Product and Company Information Product Name BETA-CAROTENE, CA. 1600 U/MG Product Number

More information

TBC (4-tert-butylpyrocatechol)

TBC (4-tert-butylpyrocatechol) GPS Safety Summary Contacts TBC (4-tert-butylpyrocatechol) Chemical Identity Brand names TBC CAS number 98-29-3 Chemical name (IUPAC) 4-tert-butylbenzene-1,2-diol Molecular formula C 10H 14O 2 Synonyms

More information

SAFETY DATA SHEET POTASSIUM NITRATE

SAFETY DATA SHEET POTASSIUM NITRATE SAFETY DATA SHEET 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND THE COM PANY: PRODUCT NAME: PART No.: SUPPLIER: RM214, RM215 J M Loveridge plc Southbrook Road, Southampton Hampshire SO15 1BH Tel:

More information

1-Bromo-2,5-dimethoxybenzene

1-Bromo-2,5-dimethoxybenzene 1. IDENTIFICATION OF THE SUBSTANCE/MIXTURE AND OF THE COMPANY/UNDERTAKING 1.1 Product identifiers Product name : 1-Bromo-2,5-dimethoxybenzene Product Number : EX-000823 Brand : Exir CAS-No. : 25245-34-5

More information

Stoichiometry. Can You Make 2.00 Grams of a Compound?

Stoichiometry. Can You Make 2.00 Grams of a Compound? Introduction Stoichiometry... Can You Make 2.00 Grams of a Compound? Catalog No. AP4554 Publication No. 4554 Use your skills of predicting chemical reactions, balancing equations, and calculating molar

More information

Safety Data Sheet Avesta Neutralization Agent 502

Safety Data Sheet Avesta Neutralization Agent 502 Safety Data Sheet Avesta Neutralization Agent 502 This Safety Data Sheet contains information to help users understand the potential hazards relating to this product and provides advice for risk management.

More information

Stalosan F 2014-01-15. Safety Data Sheet 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING

Stalosan F 2014-01-15. Safety Data Sheet 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING Safety Data Sheet 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING 1.1 Identification of the substance or preparation Stalosan F 1.2 Relevant identified uses of the substance

More information

hij GCSE Additional Science Chemistry 2 Foundation Tier Chemistry 2F SPECIMEN MARK SCHEME Version 1.0

hij GCSE Additional Science Chemistry 2 Foundation Tier Chemistry 2F SPECIMEN MARK SCHEME Version 1.0 hij GCSE Additional Science Chemistry 2 Foundation Tier Chemistry 2F SPECIMEN MARK SCHEME Version.0 Copyright 20 AQA and its licensors. All rights reserved. The Assessment and Qualifications Alliance (AQA)

More information

MATERIAL SAFETY DATA SHEET PRODUCT: SODIUM BISULFITE SOLUTION SECTION 1 - MANUFACTURER INFORMATION

MATERIAL SAFETY DATA SHEET PRODUCT: SODIUM BISULFITE SOLUTION SECTION 1 - MANUFACTURER INFORMATION MANUFACTURER/DISTRIBUTOR: MATERIAL SAFETY DATA SHEET PRODUCT: SODIUM BISULFITE SOLUTION SECTION 1 - MANUFACTURER INFORMATION PVS CHEMICAL SOLUTIONS, INC. 55 Lee Street Buffalo, New York 14210 (716) 825-5762

More information

SAFETY DATA SHEET. 955 Connecticut Ave, Suite 5202 Bridgeport, CT 06607 Tel: 800-242-1150 www.carbtrol.com Date Prepared: July 22, 2015

SAFETY DATA SHEET. 955 Connecticut Ave, Suite 5202 Bridgeport, CT 06607 Tel: 800-242-1150 www.carbtrol.com Date Prepared: July 22, 2015 CARBTROL C O R P O R A T I O N SAFETY DATA SHEET Section 1 Identity Identity (As Used on Label and List): Carbtrol Type: CSV, CV, CSL, CL, CAT2 Manufacturers Name: Carbtrol Corporation 955 Connecticut

More information

MATERIAL SAFETY DATA SHEET (MSDS)/SAFETY DATA SHEET (SDS) General Chemistry 13

MATERIAL SAFETY DATA SHEET (MSDS)/SAFETY DATA SHEET (SDS) General Chemistry 13 I. Product and Company Identification Product Name: Piccolo Reagent Disc A point of care blood diagnostic product Part Numbers: 400-1029 (single); 400-0029 (10 pack); 400-0029-4 (4 pack) Company Information:

More information

MATERIAL SAFETY DATA SHEET

MATERIAL SAFETY DATA SHEET MATERIAL SAFETY DATA SHEET 1. PRODUCT AND COMPANY IDENTIFICATION Product name Chemical name Chemical family Manufacturer's code Use Manufacturer Address Telephone Contact person : Magnesium Stearate :

More information

Enantiomers: Synthesis, characterization, and resolution of tris(ethylenediamine)cobalt(iii) chloride Introduction:

Enantiomers: Synthesis, characterization, and resolution of tris(ethylenediamine)cobalt(iii) chloride Introduction: Enantiomers: Synthesis, characterization, and resolution of tris(ethylenediamine)cobalt(iii) chloride Introduction: The development of coordination chemistry prior to 1950 involved the synthesis and characterization

More information

LISLE CORPORATION. Safety Data Sheet Issued: May 25, 2015 Supersedes: March 15, 2014. Page 1. Section 1 - PRODUCT AND COMPANY IDENTIFICATION

LISLE CORPORATION. Safety Data Sheet Issued: May 25, 2015 Supersedes: March 15, 2014. Page 1. Section 1 - PRODUCT AND COMPANY IDENTIFICATION LISLE CORPORATION Section 1 - PRODUCT AND COMPANY IDENTIFICATION Safety Data Sheet Issued: May 25, 2015 Supersedes: March 15, 2014 1.1 Product Identifiers Product Name Combustion Leak Detector Fluid Product

More information

SIGMA-ALDRICH. SAFETY DATA SHEET Version 3.15 Revision Date 01/16/2014 Print Date 01/22/2014

SIGMA-ALDRICH. SAFETY DATA SHEET Version 3.15 Revision Date 01/16/2014 Print Date 01/22/2014 SIGMA-ALDRICH sigma-aldrich.com SAFETY DATA SHEET Version 3.15 Revision Date 01/16/2014 Print Date 01/22/2014 1. PRODUCT AND COMPANY IDENTIFICATION 1.1 Product identifiers Product name : Bovine Serum Albumin

More information

HAZARDOUS CHEMICAL WASTE DISPOSAL SECTION 7

HAZARDOUS CHEMICAL WASTE DISPOSAL SECTION 7 HAZARDOUS CHEMICAL WASTE DISPOSAL According to Ontario environmental legislation, generators of hazardous waste are responsible for properly packaging and labelling such wastes. The University of Toronto

More information

SAFETY DATA SHEET. according to 1907/2006/EC, Article 31. Zenith 2B Machine Rinse Aid (020000, 020100)

SAFETY DATA SHEET. according to 1907/2006/EC, Article 31. Zenith 2B Machine Rinse Aid (020000, 020100) SAFETY DATA SHEET according to 1907/2006/EC, Article 31 Page 1/5 date SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier Product name Product code

More information

SAFETY DATA SHEET according to Regulation (EC) No. 453/2010 Dental Use

SAFETY DATA SHEET according to Regulation (EC) No. 453/2010 Dental Use Page 1 of 7 SECTION 1 : Identification of the substance/preparation and of the company/undertaking 1.1. Product identifier Product code Product name Product description : BG/10329, CM/10332, WB/11436,

More information

SAFETY DATA SHEET LIQUITEX PROFESSIONAL SPRAY PAINT

SAFETY DATA SHEET LIQUITEX PROFESSIONAL SPRAY PAINT SAFETY DATA SHEET SECTION 1: IDENTIFICATION OF THE SUBSTANCE/MIXTURE AND OF THE COMPANY/UNDERTAKING 1.1. Product identifier Product Name 1.2. Relevant identified uses of the substance or mixture and uses

More information

MATERIAL SAFETY DATA SHEET PAGE 1

MATERIAL SAFETY DATA SHEET PAGE 1 1254 Chestnut Street Newton, MA 02464-1418 Tel: (617) 965-5511 Fax: (617) 965-5818 MATERIAL SAFETY DATA SHEET PAGE 1 SECTION 1. CHEMICAL IDENTIFICATION -- - CHEMICAL NAME: TRADE NAME: PRODUCT #: Organic

More information

Material Safety Data Sheet

Material Safety Data Sheet Material Safety Data Sheet 1. Product and Company Information Company: Ranger Industries, Inc. 15 Park Road Tinton Falls, N.J. 07724 Telephone: (732) 389-3535 Product Name: Adirondack Alcohol Ink (All

More information

SAFETY DATA SHEET. Zinc Acetate. Revision Date: 12.05.2016 Previous date: 05.03.2013 Print Date:12.05.2016

SAFETY DATA SHEET. Zinc Acetate. Revision Date: 12.05.2016 Previous date: 05.03.2013 Print Date:12.05.2016 1. IDENTIFICATION OF THE SUBSTANCE/MIXTURE AND OF THE COMPANY/UNDERTAKING 1.1 Product information Commercial Product Name 1.2 Relevant identified uses of the substance or mixture and uses advised against

More information

MATERIAL SAFETY DATA SHEET In accordance with CE Regulation n 1907/2006. Annex II.

MATERIAL SAFETY DATA SHEET In accordance with CE Regulation n 1907/2006. Annex II. Ref.: BA/909 ELSACYFRA Page: 1 of 5 RRR1. Identification of preparation and of the company/undertaking 1.1 Product name: ELSACYFRA 1.2 Use With the exception of products specifically labeled for In Vitro

More information