FM FILM ADHESIVE

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1 DESCRIPTION FM is a next generation film adhesive specially formulated for out-of-autoclave bonding of both metallic and composite structures. This new adhesive provides similar performance in vacuum-only versus autoclave cure and has a unique combination of toughness and shear strength up to 121 C (250 F). FM is designed for bonding metallic and composite substrates in monolithic and sandwich structures. It is compatible with most 121 C (250 F) and 177 C (350 F) curing epoxy-based prepreg systems for co-cure, co-bond and secondary bonding. FM adhesive film provides minimum shop life of 30 days at 24 C (75 F). FM adhesive has excellent resistance to both pre-bond and postbond humidity exposures. FM adhesive is supplied at various weights and thicknesses as an unsupported film or as a supported film with woven, knit or mat carrier. FM film adhesive can be cured within the temperature range of 71 C to 177 C (160 F to 350 F) under vacuum-only pressure. The standard cure cycle for FM is 121 C (250 F) for 90 minutes under full vacuum for out-of-autoclave (OOA) bonding applications or under 0.28 MPa (40 psi) pressure for autoclave cures. FEATURES & BENEFITS 121 C (250 F) curing high performance metal and composite bonding film Designed for out-of-autoclave bonding of metal and composite monolithic and sandwich structures Builds sufficient green strength at 71 C (160 F) when co-cured with CYCOM out-of-autoclave epoxy prepreg Excellent combination of high peel and shear properties from -55 C to 121 C (-67 F to 250 F) Excellent resistance to both pre-bond and post-bond humidity Service temperature of 121 C (250 F) Shop life of 30 days or more at 24 C (75 F) Dual curing capability; 121 C (250 F) and 177 C (350 F) Compatible with various solvent- and water-borne bond primers Storage life of 12 months from date of shipment when stored at or below -18 C (0 F) Capable of low temperature curing, x 121 C (250 F) SUGGESTED APPLICATIONS Out-of-autoclave bonding of metal and composite monolithic and sandwich structures Applications requiring low temperature cure Applications requiring good serviceability at low temperature AEAD

2 CHARACTERISTICS Table 1 Product Description Areal Weights Carriers Color 0.03, 0.05 and 0.06 psf (150, 245 and 300 gsm) Other weights available on request Mat, knit and unsupported Red Volatiles Less than 1% Density Tg Shop Life Shelf Life Recommended Storage Approx g/cc 132 C (269.6 F) 30 days at 24 C (75 F) 12 months from date of shipment at recommended storage temperature Store at or below -18 C (0 F) PROPERTIES Table 2 Mechanical Properties of FM M 0.05 psf Adhesive on Aluminum Substrate with BR Primer Test Condition Wide Area Lap Shear (Blister Shear), psi (MPa) Vacuum Only Cure Pressure Cure at 40 psi Tested at 75 F (24 C) 5180 (35.7) 5020 (34.6) ½ Lap Shear, psi (MPa) Tested at 75 F (24 C) (35.4) Tested at 220 F (104 C) (25.15) Tested at 250 F (121 C) (22.26) Metal to Metal Climbing Drum Peel, in-lb/in (N) Tested at -67 F (-55 C) (761.3) Tested at 75 F (24 C) 73.7 (328) (542.3) Tested at 250 F (121 C) (501.2) Flatwise Tensile, psi (MPa) Tested at 75 F (24 C) 953 (6.57)* 1160 (8.0)** Tested at 180 F (82 C) 627 (4.32)* 888 (6.12)** Tested at 250 F (121 C) 1.74 (1.20)* - Metal Primer: BR adhesive primer except where noted (*BR adhesive primer used) Adhesive Film: FM M 0.05 psf (250 gsm) adhesive cured 90 min at 250 F (121 C) under full vacuum or 40 psi (0.28 MPa) pressure except where noted [** FM M 0.06 psf (300 gsm) adhesive used] Core for FWT: Aluminum, 0.25 in (6.35 mm) cell, 7.9 pcf (0.126 g/cc) 2

3 Table 3 Out-of-Autoclave Composite Bonding Mechanical Properties of FM M 0.06 psf Adhesive Film Co-bonded with CYCOM OOA Composite (Uni-Tape) Test Condition 1/16 Slotted Lap Shear* psi (MPa) Flatwise Tensile psi (MPa) Tested at -67 F (-55 C) 2639 (18.2) - Tested at 75 F (24 C) 2479 (17.1) 1403 (9.67) Tested at 180 F (82 C) 2428 (16.7) - Tested at 220 F (107 C) Water Soak 1116 (7.69) - Tested at 250 F (121 C) 1708 (11.77) - Cure Cycle for OOA bonding with CYCOM composite tape or fabric: Vacuum only for the whole cycle. Ramp at 3 F (1.7 C)/min. to 200 F (93 C) then hold 12 hours at 200 F (93 C). Freestanding post-cure for 2 hours at 350 F (179 C) Core: HRP Honeycomb Core, 3/16" cell, 8.0 pcf, 0.5" thick *Substrate failure Table 4 Out-of-Autoclave Composite Bonding Mechanical Properties of FM M 0.06 psf Adhesive Film Co-cured with CYCOM OOA Composite (Uni-Tape) Test Condition Beam Shear* ksi (MPa) Flatwise Tensile psi (MPa) Tested at -67 F (24 C) 23.9 (164.8) - Tested at 75 F (24 C) 20.6 (142.03) 1411 (9.7) Tested at 180 F (82 C) 20.2 (139.3) - Tested at 220 F (107 C) (8.6) Tested at 250 F (121 C) 14.3 (98.6) 1233 (8.5) Cure Cycle for OOA bonding with CYCOM composite tape or fabric: Vacuum only for the whole cycle. Ramp at 3 F (1.7 C)/min. to 200 F (93 C) then hold 12 hours at 200 F (93 C). Freestanding post-cure for 2 hours at 350 F (179 C) Core: HRP Honeycomb Core, 3/16" cell, 8.0 pcf, 0.5" thick *Facing Stress 3

4 RHEOLOGICAL BEHAVIOR APPLICATION NOTES FM is compatible with various solvent-based and water-based primers. The following 121 C (250 F) curing primers from Cytec Engineered Materials are recommended for metal bond applications using FM 209-1: BR (chromated) water-based corrosion inhibiting primer BR (non-chromated) water-based corrosion inhibiting primer Table 5 Process Information Cure Cycle: For Metal or Secondary Bonded Composite Substrates Prepreg Primer for Metal Substrates Ramp at 3 F (1.7 C)/min to 250 F (121 C) Hold 90 min at 250 F (121 C) with full vacuum or 40 psi (0.28 MPa) pressure CYCOM 977-2, CYCOM and others BR or BR 6700 cured at 250 F (121 C) Preparation of Aluminium A clean, dry, grease-free surface is required for optimum performance. A recommended procedure for cleaning aluminum skins prior to priming or bonding is the FPL cleaning method: 1. Vapor degrease, alkaline clean, rinse and check for water break 2. FPL etch per ASTM D G 3. Phosphoric acid anodize per ASTM D3933 4

5 Primer Application Although not mandatory, BR corrosion inhibiting primer is recommended for use with FM adhesive film in bonding of aluminum details. BR primer offers superior durability and resistance to hostile environments within the bond line and also may be used as a protective coating outside the bonded areas. Apply BR as follows: 1. Allow material to warm to room temperature prior to opening container 2. Thoroughly mix before application and agitate during application 3. Spary or brush coat to a dry primer thickness of in ( mm) nominal with a inch ( mm) maximum thickness. For protective coating applications, increase primer thickness to to inch ( to mm) 4. Air dry 30 minutes minimum prior to using 5. Oven dry 30 minutes at 250 ± 10 F (121 ± 6 C) Primer assemblies which have been cured and wrapped with a protective covering shuch as Kraft paper may be stored at 75 F (24 C) for 6 months or longer without fear of degradation of the final bond. Bonding Procedure Before bonding, detail parts and adhesive film must be properly assembled. Patterns of FM adhesive film should be cut as required before removal of the protective covering which is easily stripped from the film at room temperature. Apply the film adhesive smoothly to the parts. After assembly of the details, apply either vacuum or pressure and cure, using the standard cure cycle below. Heat at 3 5 F ( C)/minute to 250 F (121 C) Hold 90 minutes at 250 F ± 5 F (121 C ± 3 C) PRODUCT HANDLING AND SAFETY Cytec Engineered Materials recommends wearing clean, impervious gloves when working with film adhesives to reduce skin contact and to avoid contamination of the product. Materials Safety Data Sheets (MSDS) and product labels are available upon request and can be obtained from any Cytec Engineered Materials Office. DISPOSAL OF SCRAP MATERIAL Disposal of scrap material should be in accordance with local, state, and federal regulations. 5

6 CONTACT INFORMATION GLOBAL HEADQUARTERS Tempe, Arizona tel fax NORTH AMERICA Olean, New York tel fax Winona, Minnesota tel fax Greenville, Texas tel fax EUROPE AND ASIA Wrexham, United Kingdom tel fax Springfield, Massachusetts tel fax Anaheim, California tel fax Cytec Carbon Fibers LLC Piedmont, South Carolina tel fax Östringen, Germany tel fax Havre de Grace, Maryland tel fax Orange, California tel fax D Aircraft Products, Inc. Anaheim, California tel fax Shanghai, China tel fax DISCLAIMER: The data and information provided in this document have been obtained from carefully controlled samples and are considered to be representative of the product described. Cytec Engineered Materials (CEM) does not express or imply any guarantee or warranty of any kind including, but not limited to, the accuracy, the completeness or the relevance of the data and information set out herein. Because the properties of this product can be significantly affected by the fabrication and testing techniques employed, and since CEM does not control the conditions under which its products are tested and used, CEM cannot guarantee that the properties provided will be obtained with other processes and equipment. No guarantee or warranty is provided that the product is adapted for a specific use or purpose and CEM declines any liability with respect to the use made by any third party of the data and information contained herein. CEM has the right to change any data or information when deemed appropriate. All trademarks are the property of their respective owners. 6

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