Vysoká škola báňská Technická univerzita Ostrava Energy Research Center 17. listopadu 15/2172, Ostrava - Poruba

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1 Letter E at the ordinal number identifies the tests performed by the Laboratory in accordance with the requirements for periodic emission measurement according to ČSN P CEN/TS 15675:2009. The Laboratory is qualified to update normative documents identifying the test procedures. The laboratory is qualified to provide expert opinions and to interpret test results in the field of emission measurement tests identified by superscript "E". The Laboratory is qualified to carry out independent sampling. Tests: concentration of carbon 1.* E dioxide (CO 2 ) by automated spectroscopy) 2.* E concentration of oxygen (O 2 ) by automatic analyzer (paramagnetic method) concentration of sulphur 3.* E dioxide (SO 2 ) by automated spectroscopy) concentration of nitrogen 4.* E oxide (NO x ) by automated spectroscopy, chemiluminescence) concentration of carbon 5.* E monoxide (CO) by automated spectroscopy) 6.* E Determination of total mass concentration of organic compounds expressed as total organic carbon (TOC) by automatic analyzers (FID) and infrared spectroscopy 7.* E concentration of solid pollutants by gravimetry VECS 001 (EPA Test Method 320) VECS 002 (ČSN EN 14,789) VECS 004 (ČSN ISO 7935, EPA Test Method 320) VECS 005 (ČSN ISO 10,849, EPA Test Method 320, ČSN ISO 14792) VECS 006 (ČSN ISO 15,058, EPA Test Method 320) VECS 007 (ČSN EN 12,619, ČSN EN 13,526, EPA Test Method 320) VECS 003 (ČSN EN 13,284-1, ČSN EN ISO 5167) filtration medium Page 1 of 8

2 8.* Overload test 9.* Heat resistance stability and burning time test 10.* Leakage test 11.a* E 11.b* E Determination of gas mixture moisture (condensation and absorption method - gravimetry) Determination of gas mixture moisture (capacitance detector) 12.* E Determination of pressure 13.* E Determination of temperature 14. Determination of ash content by gravimetry, calculation of combustible matter VECT 005 ( ČSN EN ) VECT 006 ( ČSN EN ) VECT 007 VECO part A, B, C (ČSN , ČSN , ČSN EN ) VECO 001 part D (ČSN , ČSN , ČSN EN ) VECO 002 (ČSN ISO 10,780 ČSN , ČSN , VECO 003 ČSN , VECO 004 (ČSN ISO 1171, ČSN 14775, ČSN EN 15403) Water, emission, environment, heat-power, water, environment, heat-power Page 2 of 8

3 * Determination of Water Content by Gravimetry Determination of gaseous fuel flow rate 17.* Determination of heat output 18.* 19.* 20.* Determination of efficiency Determination of water flow rate Test by temperature increase in the oven and oven baking capacity VECO 005 (ČSN , ČSN EN , ČSN EN , ČSN P CEN/TS , ČSN EN ) VECT 001 ČSN EN 297, ČSN EN 303-3, ČSN ) VECT 002 ČSN EN ) VECT 003 Commission Regulation (EU) 2015/1185, Annex III and 2015/1189, Annex III) VECT 004 ČSN EN 297, ČSN EN 303-3, ČSN , ČSN EN 304) VECT 008 (ČSN EN ), gaseous fuel, water Page 3 of 8

4 21.* Test of safe operation 22.a* Determination of the composition of combustion products - mass concentration CO, NO x, SO 2, CO 2 by automatic analyzers (infrared spectrometry) VECT 009 ( VECT 010 except chapter 6.4 ( ČSN EN 304, Commission Regulation (EU) 2015/1185, Annex III and 2015/1189, Annex III) from heat-power 22.b* 23. Determination of the composition of combustion products - determination of the mass concentration of oxygen (O2) by automatic analyzer (paramagnetic method) Determination of laboratory environment parameters (temperature, relative humidity, atmospheric pressure) 24.* E Determination of velocity and volume flow of gas concentration of persistent 25. E organic compounds (PCDD/PCDF, PCB, PAH) by calculation from measured values* concentration of As, Cd, Cr, 26. E Co, Cu, Mn, Ni, Pb, Sb, Tl, V, Hg by calculation from measured values * VECT 010 except chapter 6.3 ( ČSN EN 13,240, ČSN EN 12,815, ČSN EN 304, Commission Regulation (EU) 2015/1185, Annex III and 2015/1189, Annex III) VECO 006 VECS 008 (ČSN ISO 10780) VECS 009 (ČSN EN ) VECS 010 (ČSN EN 14385, ČSN EN 13211) from heat-power Laboratory environment Page 4 of 8

5 27. E 28. E 29.* E 30.* E 31.* 32.* 33. concentration of gases and vapours (HCl, HF, SO2, ammonia) by calculation from measured values * concentration of volatile organic compounds (VOC) by calculation from measured values * concentration of nitrogen monoxide (N 2 O), hydrogen chloride (HCl), hydrogen fluoride (HF) and ammonia (NH 3 ) by automated spectroscopy) Determination of gas mixture moisture by automated analyzer (infrared spectroscopy, Tunable Diode Laser Spectroscopy(TDLS)) Determination of dust emissions for small combustion installations dilution system Determination of sampling efficiency of aerosols monitors (gravimetry) Determination of hydraulic loss VECS 011 (ČSN EN 1911, ČSN , ČSN ) VECS 012 (ČSN EN 13649, ČSN EN ISO ) VECS 013 (EPA Test Metod 320, ČSN ISO (N2O)) VECS 014 (EPA Test Method 320, ČSN ISO 10155, ČSN ISO 10396)) VECT 011 ( DINplus EN , chap. 4 and Annex C, DINplus EN , chap.4 and Annex C, DINplus EN , chap.4 and Annex C, 1. BImSchV, 15a B-VG, Commission Regulation (EU) 2015/1185, Annex III and 2015/1189, Annex III) VECO 007 (ČSN EN , chap. 14.2) VECT 012 from heat-power Aerosol Page 5 of 8

6 * E Determination of the tightness of flue gas paths Determination of the content of volatile combustible matter by gravimetry Determination of gross calorific value and calculation of net calorific value Determination of carbon, hydrogen and nitrogen by CHN628 analyzer, determination of oxygen by calculation Determination of total sulphur by high-temperature combustion method by CHN 628 module Determination of ash fusibility temperature Determination of total mass concentration of mercury (Hg) in gas phase by automated analyzer (CVAAS) Determination of flash point by closed cup method Determination of maximum explosion pressure, maximum rate of explosion pressure rise, lower explosion limit and limit oxygen concentration of dust clouds VECT 013 VECL 001 (ČSN ISO 562, ČSN ISO , ČSN EN 15148, ČSN EN 15402) VECL 002 (ČSN ISO 1928, ČSN EN 14918, ČSN EN 15400) VECL 003 (ČSN ISO 29541, ČSN ISO 17247, ČSN EN 15104, ČSN EN 15407) VECL 004 (ČSN ISO 19579, ČSN ISO 17247) VECL 005 (ČSN ISO 540, ČSN ISO 1171, ČSN EN 14775, ČSN EN 15403, ČSN P CEN/TS , ČSN P CEN/TS 15404) VECS 015 (ČSN EN ISO 14884) VECB 001 (ČSN EN ISO 2719) VECB 002 (ČSN EN A1, ČSN EN A1, ČSN EN A1, ČSN EN A1) Solid alternative fuels solid alternative fuels s Liquids Dust clouds Page 6 of 8

7 Determination of maximum explosion pressure and maximum rate of explosion pressure rise of gases and vapours of liquids Determination of upper and lower explosion limit of gases and vapours of liquids Determination of the limiting oxygen concentration for flammable gases and vapours Determination of vapour ignition temperature VECB 003 (ČSN EN 15967) VECB 004 (ČSN EN 1839) VECB 005 (ČSN EN 14756) VECB 006 (Commission Directive 92/69/EEC, method A.15 ASTM E659:2005) Gases and vapours of liquids Gases and vapours of liquids Gases and vapours of liquids Vapours of liquids 1) Asterisk at the ordinal number identifies the tests performed outside/also outside the laboratory premises. 2) Asterisk at the test procedure name indicates that the laboratory determination of an analyte in the sample is subcontracted to an accredited testing laboratory. Sampling: number 1. E 2. E Sampling procedure name Sampling of persistent organic compounds (PCDD/PCDF, PCB, PAH) - isokinetic sampling with automatic or manual isokinetic control, filtration condensation method Sampling for the determination of heavy metals (As, Cd, Cr, Co, Cu, Mn, Ni, Pb, Sb, Tl, V, Hg) - isokinetic sampling with automatic or manual isokinetic control and absorption into liquid Sampling procedure VECV 001 (ČSN EN , ISO ) VECV 002 (ČSN EN 14,385, ČSN EN 13,211, ČSN EN 13,284-1) Sampled object Page 7 of 8

8 number Sampling procedure name Sampling of gases and 3. E vapours (HCl, HF, SO 2 a NH 3 ) by absorption into liquid 4. E Sampling of organic compounds by capture on a solid sorbent Sampling of solid pollutants 5. E (isokinetic sampling with automatic or manual isokinetic control) Sampling procedure VECV 003 (ČSN EN , ČSN , ČSN ) VECV 004 (ČSN EN 13649, ČSN EN ISO ) VECV 005 (ČSN EN , ČSN EN ISO 5167) Sampled object s waste gas containing pollutants, released in atmosphere in a controlled way Solid fuels black coal, brown coal, coke Explanation of abbreviations: VECS Internal test for combustion products VECO Other internal test VECT Internal test for heat-power VECV Internal sampling VECL Internal in the Fuel Laboratory VECP Internal procedure for comparative measurement VECB Internal test in the field of safety TOC Total Organic Carbon PCDD/PCDF - Polychlorinated Dibenzodioxins/Polychlorinated Dibenzofurans PCB Polychlorinated Biphenyls PAH Polycyclic Aromatic Hydrocarbons VOC Volatile Organic Compounds TZL Particulate Pollutants EPA Test Method Environmental Protection Agency (USA) method FID Flame Ionization Detection Page 8 of 8