Newer Processing Methods for the Extraction and Refining of Rice Bran Oil
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1 Newer Processing Methods for the Extraction and Refining of Rice Bran Oil By S. M. Javed Husain MUEZ-HEST INDIA PVT. LTD. Global Rice Bran Oil Conference 2015 August 7-8 th 2015 Trident Hotel, Mumbai, India
2 RICE PADDY Rice is the seed of the monocot plants Oryza sativa (Asian rice) or Oryza Glaberrima (African rice). As a cereal grain, it is the most important staple food for a large part of the world's human population, especially in East Asia, Southeast Asia, South Asia, the Middle East, and the West Indies.
3 GLOBAL RICE PADDY PRODUCTION AND AREA Source- Food & Agriculture Organization of United Nations
4 ASIA RICE PADDY PRODUCTION Source- Food & Agriculture Organization of United Nations
5 EXTRACTION OF RICE BRAN OIL Conditioning Meal with Nutrients Raw Material Stabilization Pelletizing Hydraulic Press Separation Value Addition Hearty Biscuit Solvent Extraction Plant Meal Cooling Feed Industry Physical Refining Physical Refining
6 PHYSICAL REFINING OF CRUDE RICE BRAN OIL WITH VALUE ADDITION Refined RBO Crude RBO Degumming Agent (Enzyme) Water Degumming Enzymatic Assisted Conditioning Gums (Rice Lecithin ) Value Addition Bleaching Agents Bleaching Filtration Spent Bleaching Agents Dewaxing & Filtration Crude Wax Value Addition Fatty Acid Value Addition Stearic Acid Metallic Stearates Specific Distillation Winterization & Filtration Rice Oil Deodorizer Distillate (RODD) Crude Stearin Value Addition
7 COMPOSITION OF RICE BRAN CHARACTERISTICS FULL FAT RICE BRAN SEMIFAT RICE BRAN FROM HP DEFATTED RICE BRAN FROM SEP WHOLE WHEAT FLOUR Moisture (%) Fat Content (%) Total Carbohydrate (%) Protein (%) Crude Fiber (%) Ash Content (%) Silica Content (%) P Content (mg/g) γ- Oryzanol (%) Energy (kcal/100gm)
8 PHYSICAL & CHEMICAL PROPERTIES OF CRUDE & RBD RICE BRAN OIL CHARACTERISTICS UNIT VALUE Crude Oil Refined Oil IODINE VALUE (gl2/100g) PEROXIDE VALUE (Meq/kg) Max MOISTURE (%) Max COLOUR Tintometer 20Y+2.8R 10Y+1.0R ACID VALUE (mg KoH/gm) FREE FATTY ACID (AS OLEIC (%) Max ACID, WINTERIZED OIL ) SAPONIFICATION VALUE (mg KoH/gm) UNSAPONIFIABLE MATTER % γ-oryzanol ppm TOTAL TOCOPHEROL mg/kg (0.02%) SMOKE POINT (Degree C) FIRE POINT (Degree C) CLOUD POINT (WINTERIZED OIL ) (Degree C) 11 0 REFRACTIVE INDEX AT 25 ⁰ C (Degree C) SPECIFIC GRAVITY AT 25⁰C (Degree C) DENSITY
9 GLYCERIDE & FATTY ACID COMPOSITION OF RICE BRAN OIL GLYCERIDES CONTENT (%) FATTY ACID CONTENT (%) BOILING POINT (ºC/ 10 MMHG) MONOGLYCERIDES 5-6 Myristic Acid DIGLYCERIDE 2-3 Palmitic Acid TRIGLYCERIDES Steric Acid Oleic Acid Linoleic Acid Linolenic Acid Archidic Acid
10 PHOSPHOLIPID COMPOSITION OF SOME SELECTED VEGETABLE OILS Source % in Oil PC (%) PE (%) PI (%) *Soybean **Rice Bran Rapeseed Sunflower Groundnut Cottonseed Palm * Issue of GMO and Non GMO ** Free from issue of GMO Phospholipid Composition of both Soybean and Rice Bran Lecithin's are almost similar. Note :- PC : Phosphotidal Choline PE : Phosphotidal Ethanolamine PI : Phosphotidal Inositol
11 WATER DEGUMMING
12 LECITHIN PLANT NEW TECHNOLOGY
13 WHY RICE BRAN LECITHIN IS SUPERIOR TO SOYA LECITHIN? FATTY ACID SOYA LECITHIN RICE BRAN RICE BRAN LYSO LECITHIN LECITHIN 14: : : : : : Acid Value of Rice Bran and Soya Lecithin: Rice Bran Lecithin More Oxidative Stability due to less content of Linoleic and Linolenic acids Rice Bran Lecithin contains Oryzanol and Tocotrienols which enhances its Value, hence very useful as efficient emulsifier, growth promoter and so on
14 PHOSPHOLIPID COMPOSITION OF LYSO RICE LECITHIN PHOSPHOLIPID CRUDE RICE BRAN OIL DEWAXED RICE BRAN OIL Phosphatidyl Choline Phosphatidyl Etyhanolamine Phosphatidyl Inositol Other Phospholipids Triglycerides Wax Carbohydrates, sterols, FFA Moisture
15 PROPERTIES & USES OF LECITHIN Emulsifiers Wetting Agents Viscosity Modifiers Release Agents Separating Agents Extrusion Aids Anti-Dusting Agents Shelf- Life Aids Nutritional Supplements
16 ENZYMATIC DRY DEGUMMING
17 WET BLEACHING WITH PLF
18 PLC AUTOMATED DEWAXING (CRYSTALLIZATION) FOR CLOUD POINT 6ºC
19 RICE BRAN WAX Mixture of saturated mono esters (C46-C60)of long chain fatty acids (C22-C26) and long chain fatty alcohols (C26-C30). CH3-(CH2)mCOO(CH2)nCH3,m=C22-C26, n=c26-c30 Major Composition of Mono Esters Myricyl Cerotate % Ceryl Cerotate % Isoceryl Cerotate- 8-10%
20 POLYCOSANOL FROM RICE WAX Polycosanol a natural mixture of long chain fatty alcohols (C26- C36)extracted from Plant waxes. CH3-(CH2)n-CH2OH n=24-34 Major Polycosanol in Rice Bran Wax- Hexacosanol- C26 chain fatty alcohol Octacosanol- C28 chain fatty alcohol Triacontanol- C 30 chain fatty alcohol
21 RICE BRAN WAX/POLYCOSANOLS USES In Food and Feed Formulations Cosmetics Soaps Pharmaceuticals Nutritional Supplements To reduce LDL Cholesterol (Bad Cholesterol) Increase HDL Cholesterol (Good Cholesterol) Prevent Atherosclerosis
22 DATA GENERATED OF REFINING AT PILOT SCALE PROCESSING STEP COLOR ACID NUMBER PHOSPHOROUS (PPM) ORYZANOL WT % Crude Oil 44* Water Degumming Enzymatic Conditioning 44* * Bleaching 32** Dewaxing 27** *¼ cell ** 1 cell
23 DEODORIZATION WITH LT DISTILLER
24 BOILING TEMPERATURE VAPOR PRESSURE Effect of Vacuum: Boiling temperature decreases with lower operating vacuum. Heat sensitive liquids can be processed without product damage. Example: Stearic Acid Boiling point at 85 mbar (a) is 276 C At 0,0013 mbar (a) boiling point is at 96 C. 180 K temperature difference.
25 FEATURES OF DEODORIZER WITH SPECIAL LT DISTILLER Controlled Temperature and Pressure High Vacuum Low temperature difference in Heating fluid and Oil in LT Distillation No Polymerization of Oil Lowest Trans Fat Formation in Oil High Retention of Oryzanol, Tocopherol and Tocotrienol Content in Oil No Heat Damage to Oil Optimum Steam Utilization
26 DESCRIPTION DEODORIZER WITH DA COLUMN DEODORIZER WITH LT DISTILLER DESIGN DATA SUCTION PRESSURE 2.0 Torr Torr SUCTION TEMPERATURE 70 Deg C 70 Deg C SECTION LOAD :- WATER VAPOUR, KG / HR. 85 Kg / Hr 55 Kg / Hr FFA % 5 Kg 2 Kg / Hr AIR 10 Kg / Hr 10 Kg / Hr STEAM PRESSURE 8 Bar (g) 8 Bar (g) SYSTEM VOLUME 80 M 3 80 M 3 WATER TEMPERATURE, INLET ᴼ C 32 Deg C 32 Deg C STEAM CONSUMPTION VACUUM SYSTEM - BOOSTER EJECTORS TOTAL 790 kg 530 Kg STEAM CONSUMPTION PER TON OF FEED OIL
27 METALLIC STEARATES AND THEIR USES Calcium Stearate Magnesium Stearate Zinc Stearate Aluminum Stearate Uses Building Industry Lubricant Industry Rubber Industry Paper Industry Pharmaceutical and Cosmetics
28 WINTERIZATION (CRYSTALLIZATION) FOR CLOUD POINT 0ºC
29 FFA 0.07% COLOUR 1 -<8 UNITS CLOUD POINT- 0ºC RICE BRAN OIL SAMPLES Crude Rice bran Oil Rice Bran Bleached Oil Winterized Refined Rice Bran Oil COLOUR 1-20 UNITS
30 FACILITIES R&D Centre Drawing & Design Proto validation
31 MUEZ-HEST S STRATEGIC INITIATIVES Drawing & Design Laboratory Pilot Plant
32 R & D CENTRE
33 R & D LAB
34 PILOT PLANT
35 RECOGNITION AND APPROVALS
36 Thanks For Your Attention MUEZ-HEST INDIA PVT. LTD
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