IMPREGNANTS. DuPont TM Voltatex PUR Casting Resin CE 12-W/Z. Description. Properties. Applications. Processing

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1 Description Properties Applications Processing CE 12-W/Z is a grey polyurethane casting resin based on a hydroxyacrylate polyester. The hardener is based on an aromatic polyisocyanate. Once cured, the resin is an elastic material with low water absorption and is resistant to transformer oil, organic solvents and vapours, such as benzine and hydrocarbons. It provides excellent adhesion to most metals except the anodised, smooth surfaces of light metals. It is filled with chalk and is non-abrasive. PUR casting resin CE 12-W/Z is used for embedding and sealing transformers, components and assemblies which are to be UL listed, in particular heat-sensitive electronic components, such as transistors and photo cells. PUR casting resin CE 12-W/Z contains a non-abrasive filler and is, therefore, especially suitable for sensitive mixing and dosing plants. To achieve special technological properties of the end product, it is possible to add further non-abrasive fillers to the resin. Since the filler material contained in the PUR casting resin CE 12-W/Z settles if the resin is stored for a longer period, it is important to always stir the resin before removing it from the container. Try not to create bubbles when stirring. Subsequently allow the resin to de-aerate at room temperature for approx. two hours. By heating up the resin to approx. 60 C it is possible to drastically reduce the time required for good de-aerating, evacuating at approx. 20 mbar has the same effect. If the casting resin is to be used quickly, hardener W or Z can be stirred into the still warm resin. In other cases, the casting resin must be allowed to cool down to room temperature to ensure that the pot life is not reduced unnecessarily. Always protect the resin, hardener and prepared mixtures against moisture! The temperature in the working area should not fall below 18 C. Make sure that surfaces which are to be treated with the casting resin are dry. Completely eliminate any condensation by gently heating the parts (e.g. one hour at approx. 50 C), otherwise the resin will bubble during curing.

2 Processing If PUR casting resin CE 12 is to be used in its delivery format, the hardener W or Z is added to the de-aerated resin the specified mixing ratio. Gently stir (avoid bubbles) the mixture until it is completely homogenised. If the resin compound is to be blended with fillers, they can only be used in a completely dry state. In order to produce a filled resin compound, a suitable amount of filler for the application is at first slowly added to the resin and stirred until complete homogeneity occurs. It is recommended to heat up the resin to approx. 60 C to allow any air to escape more quickly. PUR casting resin CE 12 with hardener W or Z can be processed at all common mixing and dosing plants with or without vacuum. Curing Cleaning the tools Storage Curing, especially for thin-layer application, should occur in an environment with reduced relative humidity. Curing occurs at room temperature or is accelerated at a slightly higher ambient temperature (approx. 40 C). The resin can withstand maximum electrical and mechanical loads after 48 h curing at RT (min. 20 C). Since the cured resin is practically insoluble, plants and tools have to be cleaned as soon as possible with the E 5010 cleaner. The PUR resin CE 12 can be stored for 12 months and the hardener W or Z for 6 months at max. 25 C if sealed correctly in original containers. Due to their level of moisture sensitivity, the resin and hardener should not be stored outdoors. Protective measures Cured PUR casting resin CE 12-W/Z is biologically inactive and safe to health. Implement normal protective procedures when processing the liquid dip resin: See the DuPont TM EC safety data sheet and the M 044 data sheet of the German Chemical Industry Association (BG Chemie).

3 Standards Delivery format Thermal class B (130 C) RoHS compliant 2002/95 EC The dip resin is delivered in 30 kg disposable containers. Liquid phase CE 12 with hardener CE 12 with hardener W Z Values Values Mixing ratio 100 : : 30 Mixture viscosity (650 ± 100 mpa s) (1000 ± 250 mpa s) According to DIN at 25 C Pot life (45 ± 10) min (40 ± 10) min (100g sample) at C Curing time 48 h - RT 48 h - RT Impact on enamelled wires 3) Mixture density Compatible with all common enamelled wires. Compatible with all common enamelled wires. (1.25 ± 0.02) g/cm³ (1.25 ± 0.02) g/cm³ According to DIN53217 T.5, at 20 C Volume shrinkage Approx. 1.8% After 24 h / RT and 5 h / 80 C

4 Test on cured resin IEC Curing conditions for test specimen production 24 h at RT + 5 h at 80 C Mechanical Shore D hardness Conditions Values Harden er W Hardene r After 3 days After 4 weeks After 2 months 8 ± 3 38 ± 3 50 ± 3 Z 20 ± 3 53 ± 3 62 ± 3 According to DIN Water absorption After 96 h at 23 C 0.2% 1 ISO 62 Safety relevant details, transport regulations and labelling are continuously updated to comply with current statutory regulations. Please refer to the EC safety data sheet for these regulations. 1) The curing times start as soon as the parts have reached the specified temperature. It is recommended to increase the curing time for electrical equipment subject to high mechanical or chemical stress. 2) DuPont TM standard Herberts Electro 001 Measurement of the gel time and reaction time of 1K dip resins DIN ) The test is carried out IEC : 1996 Winding Wires - Test Methods, part 4: Chemical properties. The stated solvent is replaced by the dip resin. 4) DuPont TM standard Herberts Electro 002 Measurement of the VOC content of hot-curing UP dip resins.

5 Test on cured resin IEC Curing conditions for test specimen production 24 h at RT + 5 h at 80 C Electrical Dielectric strength Specific volume resistance Conditions Hardener W Hardener Z at 23 C 50 kv/mm 60 kv/mm and 50% r.h. at 23 C after 96 h storage at 92% r.h. 24 kv/mm 25 kv/mm test method IEC at 105 C 55 kv/mm 60 kv/mm after 168 h storage in oil at 23 C Ω*cm Ω*cm at 155 C Ω*cm Ω*cm Creep resistance CTI 450 M Relative permittivity ε r at 23 C from 50Hz - 1MHz Loss factor tan δ at 23 C from 50 Hz - 1MHz Intersection point 0.2 = According to IEC According to 6.2 IEC According to test method IEC C test method IEC between 50 Hz and 1 MHz

6 Thermal Values Temperature index TI / IEC IEC 216 Heat conductivity 0.3 W(m.K) -1 According to DIN Linear thermal expansion K K -1 Temperature range 0-10 C Temperature range C coefficient (Hardener Z) Dimensional stability under heat (hardener Z) (25 ± 2) C According to Martens (DIN 53462) Chemical Conditions Resistance Transformer oil, test method ISO 175

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