14. INORGANICS IN AQUEOUS SOLUTION
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1 14. INRGANICS IN AQUEUS SLUTIN Acid-base chemistry 14.. Brønsted-Lowry or Lewis base? Ligand substitution reactions Inference from aqueous tests Inorganics aqueous solution answers Inorganics aqueous solution 14.
2 14.1. Acid-base chemistry For each of the test tube reactions described below; (a) Write a balanced symbol equation (cludg state symbols) for the reactions occurrg, (b) Describe what you would expect to observe. 1. Sodium hydroxide solution is added dropwise to an aqueous solution of copper(ii) sulfate until present. Equation... (1 mark) bservations.... Sodium hydroxide solution is added dropwise to an aqueous solution of iron(ii) sulfate until present. Equation... (1 mark) bservations Sodium carbonate solution is added dropwise to an aqueous solution of manganese(ii) sulfate until present. Equation... (1 mark) bservations Sodium carbonate solution is added dropwise to an aqueous solution of iron(iil) chloride until present. Equation... (1 mark) bservations Sodium hydroxide solution is added dropwise to an aqueous solution of chromium(iii) sulfate until present. Equation(s)... bservations... Inorganics aqueous solution 14.1.
3 14.. Brønsted-Lowry or Lewis base? A Brønsted-Lowry base is a proton acceptor. A Lewis base donates a pair of electrons. In each of the test tube reactions described below, ammonia acts either as a Brønsted-Lowry base or a Lewis base. Complete the descriptions by fillg the blanks labelled (10 marks) Aqueous alumium ions When an aqueous solution of ammonia is added dropwise to an aqueous solution of alumium sulfate, a is does not dissolve on addition of ammonia. Equation: [Al(H ) 6 ] 3+ (aq) + 3 NH 3 (aq) [Al(H ) 3 (H) 3 ](s) + 3 NHŸ(aq) In this reaction, ammonia is actg as a Aqueous cobalt ions When an aqueous solution of ammonia is added dropwise to a pk solution of aqueous cobalt(ii) chloride, a blue precipitate is formed itially. Equation: [Co(H ) 6 ] + (aq) + NH 3 (aq) In this reaction, ammonia is actg as a Brønsted-Lowry base. n addg ammonia solution, the blue precipitate re-dissolves to form a (which is oxidised by air to a dark brown mixture contag Co(III) compounds.) Equation: [Co(H ) 4 (H) ](s) + 6 NH 3 (aq) [Co(NH 3 ) 6 ] + (aq) + 4 H (l) + H (aq) In this second reaction, ammonia is actg as a Aqueous copper ions When an aqueous solution of ammonia is added dropwise to a blue solution of aqueous copper(ii) sulfate, a is itially Equation: [Cu(H ) 6 ] + (aq) + NH 3 (aq) [Cu(H ) 4 (H) ](s) + NHŸ(aq) In this reaction, ammonia is actg as a Brønsted-Lowry base. n the addition of ammonia solution, the re-dissolves to form Equation: [Cu(H ) 4 (H) ](s) + 4 NH 3 (aq) H (l) + H (aq) In this second reaction, ammonia is actg as a Inorganics aqueous solution 14..
4 14.3. Ligand substitution reactions For each of the criteria 1-5 below, identify a ligand substitution reaction startg from [Cu(H ) 6 ] + and selectg ligands from NH 3,, en (H NCH CH NH ), C Øʇ and EDTA 4 which meet the criteria required. Choose a different reaction for each set of criteria, and each case, draw a 3-dimensional representation of the fal product. 1. No either the coordation number or the overall charge on the complex....( marks). No the coordation number of the complex but a the overall charge on the complex....( marks) 3. A both the coordation number and overall charge on the complex....( marks) 4. The largest positive entropy....( marks) 5. Produces a chiral product....( marks) Inorganics aqueous solution 14.3.
5 14.4. Inference from aqueous tests Use the results of the simple test tube reactions shown below to identify the anion and the cation each of the unknown salts A-E. Each of the tests were carried out on a small sample of the salt dissolved water. Salt A Salt B Salt C Salt D Salt E Test 1 Add NaH(aq) dropwise until present re-dissolved to form a green solution A pale blue ppt A blue ppt A brown ppt Test Add NH 3 (aq) dropwise until present re-dissolved to form a purple solution A pale blue ppt re-dissolved to form a deep blue solution A pale blue ppt re-dissolved to form a pale yellow / brown solution slowed turned orange / brown on standg. No visible with A brown ppt Test 3 Add CÕʇ(aq) dropwise until present Effervescence. with A blue green ppt with A pk ppt with with A brown ppt Effervescence. with Test 4 Add HN 3 followed by AgN 3 (aq) was observed to dissolve dil. NH 3 (aq) A cream ppt was observed to dissolve conc. NH 3 (aq) was observed to dissolve dil. NH 3 (aq) Test 5 Add H followed by Ba (aq) formed formed Salt A is... Salt B is... Salt C is... Salt D is... Salt E is......( marks)...( marks)...( marks)...( marks)...( marks) Inorganics aqueous solution 14.4.
6 14. Inorganics aqueous solution answers Acid-base chemistry (1 mark for each correct equation with state symbols; 1 mark for each correct full observation) 1. Equation: [Cu(H ) 6 ] + (aq) + H (aq) [Cu(H ) 4 (H) ](s) + H (l) bservations: Blue solution to a blue precipitate which doesn t re-dissolve NaH.. Equation: [Fe(H ) 6 ] + (aq) + H (aq) [Fe(H ) 4 (H) ](s) + H (l) bservations: Pale green solution to a murky green precipitate which is oxidised the air to orange/brown [Fe(H ) 3 (H) 3 ](s). 3. Equation: [Mn(H ) 6 ] + (aq) + CÕʇ(aq) MnC 3 (s) + 6 H (l) bservations: Very pale pk solution to a very pale pk precipitate. 4. Equation: [Fe(H ) 6 ] 3+ (aq) + 3 CÕʇ(aq) [Fe(H ) 3 (H) 3 ](s) + 3 H (l) + 3 C (g) bservations: Yellow/brown solution to a orange/brown precipitate and effervescence. 5. Equations: [Cr(H ) 6 ] 3+ (aq) + 3 H (aq) [Cr(H ) 3 (H) 3 ](s) + 3 H (l) [Cr(H ) 3 (H) 3 ](s) + 3 H (aq) [Cr(H) 6 ] 3 (aq) + 3 H (l) bservations: Ruby or green solution to a green precipitate which dissolves NaH to form a green solution Brønsted-Lowry or Lewis base? 1. white precipitate. Brønsted-Lowry base 3. [Co(H ) 4 (H) ](s) 4. NHŸ(aq) 5. pale yellow/brown solution 6. Lewis base 7. blue precipitate 8. deep blue solution 9. [Cu(NH 3 ) 4 (H ) ] Lewis base Ligand substitution reactions 1. [Cu(H ) 6 ] + (aq) + 4 NH 3 (aq) [Cu(H ) (NH 3 ) 4 ] + (aq) + 4 H (l) H H N NH 3 A 3 Cu H N NH 3 H (10 marks) + 3 Inorganics aqueous solution answers
7 14. Inorganics aqueous solution answers 4. [Cu(H ) 6 ] + (aq) + 3 C Øʇ(aq) [Cu(C 4 ) 3 ] 4 (aq) + 6 H (l) Cu A 3. [Cu(H ) 6 ] + (aq) + 4 (aq) [Cu 4 ] (aq) + 6 H (l) Cu 4. [Cu(H ) 6 ] + (aq) + EDTA 4 (aq) [CuEDTA] (aq) + 6 H (l) N + N + Cu A 5. [Cu(H ) 6 ] + (aq) + 3 en (aq) [Cu en 3 ] + (aq) + 6 H (l) H N N H HN Cu A HN NH NH + (1 mark for each correct equation, 1 mark for each correct drawg) 14.4 Inference from aqueous tests Salt A is chromium(iii) sulfate Salt B is copper(ii) chloride Salt C is cobalt(ii) bromide Salt D is iron(ii) chloride Salt E is iron(iii) sulfate ( marks) ( marks) ( marks) ( marks) ( marks) Inorganics aqueous solution answers
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