Schedule of Accreditation issued by United Kingdom Accreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK
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1 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK PO Box 11 Nepshaw Lane South Morley Leeds LS27 0UQ Contact: Mr M Bowden Tel: +44 (0) Fax: +44 (0) analyst@wyjs.org.uk Website: Testing performed at the above address only DETAIL OF ACCREDITATION ANIMAL FEEDING STUFFS Chemical Tests Ash Copper Crude Fibre Moisture Oil METH0227 using Ashing and Gravimetry METH017 using Flame Atomic Absorption Spectrometry METH0120 using Fibrecap METH0227 using oven drying and Gravimetry METH0014 using soxhlet extraction followed by Gravimetry Health and Hygiene Health and Safety Executive Asbestos: The analysts guide for sampling, analysis and clearance procedures (HSG 248) ASBESTOS IN BULK MATERIALS including materials and products suspected of containing asbestos Identification of: Amosite Chrysotile Crocidolite Fibrous Actinolite Fibrous Anthophyllite Fibrous Tremolite HSG 248:February 2005 by Documented In-House Procedure 1003 using stereo-microscopy polarised light microscopy and dispersion staining Assessment Manager: DF Page 1 of 8
2 BODY FLUIDS Chemical Tests Blood and urine (preserved/unpreserved) Detection and quantification of alcohol in relation to the Road Traffic Act (LOD 5 mg/100 ml) T0100 using Gas Chromatography/Flame Ionisation Detector (GC-FID) ENVIRONMENTAL SAMPLES Chemical Tests Ambient atmospheric pollutants Nitrogen Dioxide ( adsorbed onto Passive diffusion tubes ) METH0010 using Colorimetry FOOD CONTACT MATERIALS AND ARTICLES Melamine Kitchenware Chemical Tests Primary aromatic amines in 3% acetic acid simulant 4,4-diaminodiphenylmethane 4,4-oxydianiline 4-methyl-m-phenylenediamine 2-methyl-m-phenylene diamine aniline o-tolidine 1,3 phenylene diamine Migration of formaldehyde into 3% acetic acid food simulant METH0206 using Liquid Chromatography Tandem Mass Spectrometry METH0235 using spectrophotometry Chemical Tests General foods Additives, contaminants and food components Development and modification of methods/analysis using the flexible scope procedure No 0200 HPLC, GC, AAS and microscopy Assessment Manager: DF Page 2 of 8
3 General foods Artificial colours (qualitative): E102 Tartrazine E104 Quinoline Yellow E110 Sunset Yellow FCF E131 Patent Blue V E122 Carmoisine E123 Amaranth E124 Ponceau 4R E127 Erythrosine BS E128 Red 2G E129 Allura Red E132 Indigo Carmine E133 Brilliant Blue FCF E142 Green S E151 Black PN (Brilliant Black BN) E154 Brown FK E155 Chocolate Brown HT Ash for non-meat products Moisture for non-meat products Fat (total) ph Nitrogen (and protein by calculation) Sodium Sodium Chloride (Salt) Soluble solids Sugars METH0149 using Thin Layer Chromatography (TLC) METH0227 using ashing and gravimetry (prepash 229) METH0227 using oven drying and gravimetry (prepash 229) METH0056 by Werner Schmidt METH0060 using ph meter METH0238 using Rapid N Cube Analyser (Dumas Method) METH0135 using Flame Photometry METH0135 by Calculation based on sodium result METH0048 by Refractometry METH0050 using High Performance Liquid Chromatography/Refractive Index Detector (HPLC-RI) Assessment Manager: DF Page 3 of 8
4 General foods Sulphur dioxide METH0044 based on the modified Monier-Williams procedure Tin (Canned foods) METH0188 using Flame Atomic Absorption Spectrometry Beverages - alcoholic Beers, Lagers Alcohol by volume Original Gravity Acidity METH0031 based on method for the determination of original gravity. The Beer Regulations 1985 METH0031 by titration based on method for the determination of original gravity. The Beer Regulations 1985 Fermentation Products Alcohol by volume METH0074 using Gas Chromatography/Flame Ionisation Detector (GC-FID) Spirits Sulphur dioxide Total Acidity Alcohol by volume and original gravity Congeners: Ethyl acetate Methanol Propan-1-ol 2-methylpropan-1-ol Amyl alcohol (sum of 2-methylbutan-1-ol and 3-methylbutan-1-ol) Alcohol by volume METH0044 based on the modified Monier-Williams procedure METH0072 using Titrimetry METH0144 by Refractometry METH0030 using Gas Chromatography with Flame Ionisation Detector (GC-FID) METH0033 using gas chromatography/flame ionisation detector (GC-FID) (screening method) METH0032 specific gravity by pyknometry Assessment Manager: DF Page 4 of 8
5 Spirits Beverages - non alcoholic Sugar Markers Fructose Glucose Sucrose Artificial colours: E102 Tartrazine E104 Quinoline Yellow E110 Sunset Yellow FCF E122 Carmoisine E124 Ponceau 4R E129 Allura Red METH0078 using High Performance Liquid Chromatography with Pulsed Amperometric Detector (HPLC-PAD) METH0059 using High Performance Liquid Chromatography with Diode Array Detector (HPLC-DAD) Cereal and cereal products Crude Fibre METH0120 using Fibrecap Cereals, dried fruits, coffee and spices Confectionery products Dairy products Milk powder, condensed and evaporated milk, cream, ice-cream Ochratoxin A Artificial colours: E102 Tartrazine E104 Quinoline Yellow E110 Sunset Yellow FCF E122 Carmoisine E124 Ponceau 4R E129 Allura Red Fat METH0155 using HPLC METH0059 using High Performance Liquid Chromatography with Diode Array Detector (HPLC-DAD) METH0037 based on BS EN ISO 1736 and 1737 (Rose-Gottlieb) Liquid milk Acidity METH0174 using Titrimetry Antibiotic Residues Fat (total) Freezing Point Depression METH0036 using Delvotest METH0034 based on BS ISO 2446:2008. (Gerber Method) METH0035 based on BS EN ISO 5764:2009 Assessment Manager: DF Page 5 of 8
6 Fats and oils Total Solids Fatty Acid Profile of Fats and Extracted Fats Free fatty acids n-butyric acid and the methyl ester Peroxide value METH0175 using oven drying and Gravimetry METH0173 using Gas Chromatography with Flame Ionisation Detector (GC-FID) METH123 based on BS EN 660:2009 using Titrimetry METH0233 using Gas Chromatography with Flame Ionisation Detection (GC-FID) METH0122 based on BS EN ISO 3960:2010 using Titrimetry Fish and fish products Ash METH0001 based on BS :1998 METH0227 using ashing and Gravimetry (prepash 229 ) Fat Free fat Histamine Moisture METH0002 based on BS 4401:Part 4:1970 METH0099 using accelerated solvent extraction METH0222 using HPLC-DAD METH0003 based on BS :1997 METH0227 using oven drying and Gravimetry (prepash 229) Nitrogen and crude protein METH0004 based on BS 4401:Part 2:1980 (Kjeldahl) Assessment Manager: DF Page 6 of 8
7 Raw, Smoked and Lightly Cooked Fish Species identification (qualitative) METH0250 using PCR-RFLP and Agilent 2100 Bioanalyzer Raw fish Total volatile basic nitrogen METH0193 using steam distillation followed by titration meeting requirements of Commission Decision No 95/149/EC Meat and meat products Ash METH0001 based on BS :1998 METH0227 using ashing and Gravimetry (prepash 229 ) Fat Free fat Moisture METH0002 based on BS 4401:Part 4:1970 METH0099 using accelerated solvent extraction METH0003 based on BS :1997 METH0227 using oven drying and Gravimetry (prepash 229) Nitrogen and crude protein Hydroxyproline Nitrite Soya Speciation for cooked meat Speciation for raw meat Sulphur dioxide Total volatile nitrogen (Flesh foods) METH0004 based on BS 4401:Part 2:1980 (Kjeldahl) METH0142 based on BS :1995 METH0081 using Visible Spectroscopy METH0040 using ELISA METH0063 using ELISA Kit METH0064 using ELISA Kit METH0044 based on the modified Monier-Williams procedure METH0045 using distillation followed by Titrimetry Assessment Manager: DF Page 7 of 8
8 Meat and meat products Nitrogen (and protein by calculation) METH0238 using Rapid N Cube Analyser (Dumas Method) Spices Chrysoidine METH0209 using solvent extraction followed by High Performance Liquid Chromatography with Diode Array Detector (HPLC-DAD) Microscopy Herbs, spices and vegetable material Examination and identification METH0109 using Optical Microscopy CIGARETTES Electronic cigarette Nicotine content in charging materials METH0244 using organic solvent extraction and GC-MS determination END Assessment Manager: DF Page 8 of 8
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