CHAPTER 1: INTRODUCTION
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1 LIST OF CONTENTS Declaration Abstract Abstrak List of Publications Acknowledgement List of Contents Abbreviations List of Figures List of Tables Pages i iii v vii viii ix xv xvi xviii CHAPTER 1: INTRODUCTION 1 1.1: Research background 1.2: Problem statement 1.3: Scope and objective of the research 1.4: Objectives of the present work 1.5: Thesis organization CHAPTER 2: LITERATURE REVIEW 2.1 Introduction 2.2 Polymer electrolytes 2.3 Ionic Conductivity in Polymer 2.4 Classifications of polymer electrolytes 2.5 PVDF-HFP 2.6 Dye Sensitized Solar Cells (DSSCs) 2.7 DSSC structure 2.8 The working principle of a DSSC 2.9 Dye Materials 2.10 Summary ix
2 CHAPTER 3: EXPERIMENTAL METHODS 3.1 Introduction 3.2 Materials 3.3 Samples Preparation Preparation of NaI Based Polymer Preparation of KI Based Polymer Preparation of (PVDF-HFP)-(KI+TBAI)-(EC/PC) Double Salt System 3.4 Preparation of Dye Materials 3.5 Preparation of Electrodes 3.6 Preparation of DSSCs 3.7 Sample Characterization Techniques Fourier Transform Infrared Spectroscopy (FTIR) X-ray Diffraction (XRD) Electrochemical Impedance Spectroscopy (EIS) 3.8 Dye Characterizations 3.9 DSSCs Characterization 3.10 Summary CHAPTER 4: RESULTS ON FTIR STUDIES 4.1 Introduction 4.2 The Infrared Spectrum of PVDF-HFP 4.3 Infrared Spectrum of EC, PC and the EC/PC Mixture 4.4 Infrared Spectrum of NaI and KI 4.5 Intermolecular Interaction between PVDF-HFP and NaI 4.6 Interaction between PVDF-HFP, NaI and EC/PC x
3 4.7 Intermolecular Interaction between PVDF-HFP and KI 4.8 Intermolecular Interaction between PVDF-HFP, KI and (EC/PC) 4.9 Summary 76 CHAPTER 5: RESULTS ON XRD STUDIES 5.1 Introduction 5.2 XRD Studies on NaI Containing XRD Diffractogram for (PVDF-HFP) and (PVDF- HFP) NaI Deconvolution of (PVDF-HFP) and (PVDF-HFP) NaI X-ray Diffractograms X-ray Diffractograms for (PVDF-HFP) NaI (EC/PC) 5.3 XRD Studies for KI Containing XRD for (PVDF-HFP) KI system Deconvolution of X-ray Diffractograms for (PVDF-HFP) KI system XRD for (PVDF-HFP) KI (EC/PC) Deconvolution of X-ray Diffractograms for (PVDF-HFP KI (EC/PC) Electroytes 5.4 Summary CHAPTER 6: RESULTS ON EIS STUDIES 6.1 Introduction 6.2 Conductivity Studies on NaI Based Nyquist Plots of (PVDF-HFP) NaI xi
4 6.2.2 Ionic Conductivity of (PVDF-HFP) NaI Determination of n,, and D by the Equivalent Circuit Model Approach for (PVDF - HFP) - NaI Nyquist Plots of (PVDF-HFP) NaI- (EC/PC) Ionic Conductivity of Plasticized (PVDF-HFP) NaI (EC/PC) Determination of n,, and D by the Equivalent Circuit Model Approach for (PVDF- HFP) NaI (EC/PC) 6.3 Conductivity Studies on KI Based Nyquist Plots of (PVDF-HFP) KI Ionic Conductivity of (PVDF-HFP) KI system Determination of n,, and D by The Equivalent Circuit Model Approach for (PVDF-HFP)-KI electrolyte Nyquist Plots of (PVDF-HFP) - KI-(EC/PC) Ionic Conductivity of (EC/PC) Plasticized (PVDF-HFP) KI system Determination of n,, and D by the Equivalent Circuit Model Approach for (PVDF-HFP) KI (EC/PC) Summary 139 xii
5 CHAPTER 7: FABRICATION AND CHARACTERIZATION OF DYE SENSITIZED SOLAR CELL 7.1 Introduction 7.2 Visible Absorption Spectra of Dye Materials 7.3 Characterizations of DSSCs Containing NaI based DSSCs with [47 wt.% (PVDF-HFP)-31 wt.% NaI- 19 wt.% (EC/PC)]-3 wt.% I 2 and anthocyanin, chlorophyll and the anthocyanin and chlorophyll mixed dyes DSSCs with anthocyanin-chlorophyll mixed dye and [47 wt.% (PVDF-HFP)-31 wt.% NaI- 19 wt.% (EC/PC)]- 3 wt.% I 2 electrolye at different light source intensities DSSC with [47 wt.% (PVDF-HFP)-31 wt.% NaI- 19 wt.% (EC/PC)]-3 wt.% I 2 and Rhutenizer 535 N3 dye DSSC with [47 wt.% (PVDF-HFP)-31 wt.% NaI- 19 wt.% (EC/PC)]-3 wt.% I 2 and Rhutenizer 535 N3 dye at different light intensities 7.4. Characterization of DSSCs Containing KI Based DSSCs with [40 wt.% (PVDF-HFP)-10 wt.% KI- 50 wt.% (EC/PC)]-1 wt.% I 2 and anthocyanin, chlorophyll and the anthocyanin and chlorophyll mixed dyes DSSCs with anthocyanin-chlorophyll mixed dye and [40 wt.% (PVDF-HFP)-10 wt.% KI- 50 wt.% (EC/PC)]-1 wt.% I 2 electrolye at different light source intensities DSSC with [40 wt.% (PVDF-HFP)-10 wt.% KI- 50 wt.% (EC/PC)]-1 wt.% I 2 and Rhutenizer 535 N3 dye DSSC with [40 wt.% (PVDF-HFP)-10 wt.% KI- 50 wt.% (EC/PC)]- 1 wt.% I 2 and Rhutenizer 535 N3 dye at different light intensities Performance of DSSC With Having Double Iodide Salts KI and TBAI Summary 157 xiii
6 CHAPTER 8: DISCUSSION CHAPTER 9: CONCLUSION AND SUGGESTIONS 9.1 Conclusion 9.2 Suggestions for further work REFERENCES APPENDIX A APPENDIX B 179 xxv xxxiii xiv
vii TABLE OF CONTENTS CHAPTER TITLE PAGE DECLARATION DEDICATION ACKNOWLEDGEMENT ABSTRACT ABSTRAK
vii TABLE OF CONTENTS CHAPTER TITLE PAGE DECLARATION DEDICATION ACKNOWLEDGEMENT ABSTRACT ABSTRAK TABLE OF CONTENTS LIST OF TABLES LIST OF FIGURES LIST OF SYMBOLS / ABBREVIATIONS LIST OF APPENDICES ii iii
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viii TABLE OF CONTENTS CHAPTER TITLE PAGE TITLE PAGE DECLARATION DEDICATION ACKNOWLEDGEMENT ABSTRACT ABSTRAK TABLE OF CONTENTS LIST OF TABLES LIST OF FIGURES LIST OF APPENDICES I II III IV VI VII VIII
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vii TABLE OF CONTENTS CHAPTER TITLE PAGE DECLARATION DEDICATION ACKNOWLEDGEMENT ABSTRACT ABSTRAK
vii TABLE OF CONTENTS CHAPTER TITLE PAGE DECLARATION DEDICATION ACKNOWLEDGEMENT ABSTRACT ABSTRAK TABLE OF CONTENTS LIST OF TABLES LIST OF FIGURES LIST OF ABBREVIATIONS LIST OF SYMBOLS LIST OF APPENDICES
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