ANALYTICAL REPORT. Attn: Jean Neubeck

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1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. 0 Riverside Parkway West Sacramento, CA 0 Tel: ()-00 TestAmerica Job ID: 0-- Client Project/Site: HFCS For: Alpha Geosciences Plank Road Clifton Park, New York 0 Attn: Jean Neubeck Authorized for release by: //0 :: PM Jill Kellmann, Manager of Project Management ()-0 The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

2 Project/Site: HFCS Table of Contents TestAmerica Job ID: 0-- Cover Page Table of Contents Definitions/Glossary Case Narrative Detection Summary Client Sample Results Surrogate Summary QC Sample Results QC Association Summary Lab Chronicle Certification Summary Method Summary Sample Summary Chain of Custody Receipt Checklists Page of //0

3 Project/Site: HFCS Definitions/Glossary TestAmerica Job ID: 0-- Qualifiers LCMS Qualifier J Glossary Abbreviation Qualifier Description Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) Page of //0

4 Case Narrative Client: Alpha Geosciences TestAmerica Job ID: 0-- Project/Site: HFCS Job ID: 0-- Laboratory: Narrative Receipt The samples were received on //0 : AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 0.º C. LCMS - Method Results for sample BG Cold Tap (0--) were reported from the analysis of a diluted extract due to high concentration of the target analyte in the analysis of the undiluted extract. The dilution factor was applied to the labeled internal standard area counts and these area counts were within acceptance limits The internal standard (ISTD) response for the following samples was outside control limits compared to the most recent CCV: HS Kit Tap (0--) and BG Cold Tap (0--). The samples were re-analyzed with concurring results and the original set of data has been reported. The internal standards responses were in control as compared to the calibration curve. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Page of //0

5 Project/Site: HFCS Detection Summary TestAmerica Job ID: 0-- Client Sample ID: HS Kit Tap Lab Sample ID: 0-- No Detections. Client Sample ID: BG Cold Tap Lab Sample ID: 0-- Analyte Result Qualifier RL MDL Unit D Method Prep Type Perfluorooctanoic acid (PFOA) - DL ug/l Total/NA This Detection Summary does not include radiochemical test results. Page of //0

6 Project/Site: HFCS Client Sample ID: HS Kit Tap Date Collected: 0// : Date Received: 0// : Method: - Perfluorinated Alkyl Acids (LC/MS) Analyte Result Qualifier Client Sample Results RL MDL TestAmerica Job ID: 0-- Lab Sample ID: 0-- Matrix: Water Perfluorooctane Sulfonate (PFOS) ND ug/l 0/0/ : 0/0/ 0:00 Perfluorooctanoic acid (PFOA) Surrogate ND %Recovery Qualifier Limits Unit D ug/l 0/0/ : 0/0/ 0:00 C PFHxA 0-0 0/0/ : 0/0/ 0:00 C PFDA 0-0 0/0/ : 0/0/ 0:00 Client Sample ID: BG Cold Tap Date Collected: 0// : Date Received: 0// : Method: - Perfluorinated Alkyl Acids (LC/MS) Analyte Result Qualifier RL MDL Lab Sample ID: 0-- Matrix: Water Perfluorooctane Sulfonate (PFOS) ND ug/l 0/0/ : 0/0/ 0: Surrogate %Recovery Qualifier Limits C PFHxA 0-0 0/0/ : 0/0/ 0: Unit D C PFDA 0-0 0/0/ : 0/0/ 0: Method: - Perfluorinated Alkyl Acids (LC/MS) - DL Analyte Result Qualifier RL Perfluorooctanoic acid (PFOA) ug/l 0/0/ : 0/0/ : MDL Unit D Surrogate %Recovery Qualifier Limits C PFHxA 0-0 0/0/ : 0/0/ : C PFDA 0-0 0/0/ : 0/0/ : Page of //0

7 Project/Site: HFCS Method: - Perfluorinated Alkyl Acids (LC/MS) Matrix: Water Surrogate Summary C PFHxAC PFDA Lab Sample ID Client Sample ID (0-0) (0-0) 0-- HS Kit Tap 0-- BG Cold Tap DL BG Cold Tap LCS 0-/-A MB 0-/-A Surrogate Legend C PFHxA = C PFHxA C PFDA = C PFDA Lab Control Sample Method Blank 0 TestAmerica Job ID: 0-- Percent Surrogate Recovery (Acceptance Limits) Prep Type: Total/NA Page of //0

8 Project/Site: HFCS Method: - Perfluorinated Alkyl Acids (LC/MS) QC Sample Results TestAmerica Job ID: 0-- Lab Sample ID: MB 0-/-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: Prep Batch: MB MB Analyte Result Qualifier RL Perfluorooctane Sulfonate (PFOS) ND ug/l 0/0/ : 0/0/ : Perfluorooctanoic acid (PFOA) Surrogate %Recovery MDL Unit D ND ug/l 0/0/ : 0/0/ : MB MB Qualifier Limits C PFHxA 0-0 0/0/ : 0/0/ : C PFDA 0-0 0/0/ : 0/0/ : Lab Sample ID: LCS 0-/-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: Prep Batch: Spike LCS LCS %Rec. Analyte Added Result Qualifier Perfluorooctane Sulfonate J ug/l 0-0 (PFOS) Perfluorooctanoic acid (PFOA) J ug/l 0-0 Surrogate %Recovery LCS LCS Qualifier Limits C PFHxA C PFDA 0-0 Unit D %Rec Limits Page of //0

9 Project/Site: HFCS QC Association Summary TestAmerica Job ID: 0-- LCMS Prep Batch: Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 0-- HS Kit Tap Total/NA Water 0-- BG Cold Tap Total/NA DL BG Cold Tap Total/NA LCS 0-/-A Lab Control Sample Total/NA MB 0-/-A Method Blank Total/NA Analysis Batch: Water Water Water Water Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 0-- HS Kit Tap Total/NA Water 0-- BG Cold Tap Total/NA DL BG Cold Tap Total/NA LCS 0-/-A Lab Control Sample Total/NA MB 0-/-A Method Blank Total/NA Water Water Water Water Page of //0

10 Lab Chronicle Client: Alpha Geosciences TestAmerica Job ID: 0-- Project/Site: HFCS Client Sample ID: HS Kit Tap Lab Sample ID: 0-- Date Collected: 0// : Matrix: Water Date Received: 0// : Prep Type Batch Type Batch Method Run Dil Factor Initial Amount Amount or Analyst Total/NA Prep. ml.00 ml 0/0/ : JER TAL SAC Final Batch Number Total/NA Analysis. ml.00 ml 0/0/ 0:00 CBW TAL SAC Client Sample ID: BG Cold Tap Lab Sample ID: 0-- Date Collected: 0// : Matrix: Water Date Received: 0// : Prep Type Batch Type Batch Method Run Dil Factor Initial Amount Amount or Analyst Total/NA Prep 0. ml.00 ml 0/0/ : JER TAL SAC Final Batch Number Total/NA Analysis 0. ml.00 ml 0/0/ 0: CBW TAL SAC Total/NA Prep DL 0. ml.00 ml 0/0/ : JER TAL SAC Total/NA Analysis DL 0. ml.00 ml 0/0/ : CBW TAL SAC Laboratory References: TAL SAC =, 0 Riverside Parkway, West Sacramento, CA 0, TEL ()-00 Lab Lab Page of //0

11 Certification Summary Client: Alpha Geosciences TestAmerica Job ID: 0-- Project/Site: HFCS Laboratory: Unless otherwise noted, all analytes for this laboratory were covered under each certification below. Authority Program EPA Region Certification ID Expiration Date USEPA UCMR Federal CA Analysis Method Prep Method Matrix Analyte Page of //0

12 Project/Site: HFCS Method Summary TestAmerica Job ID: 0-- Method Method Description Protocol Laboratory Perfluorinated Alkyl Acids (LC/MS) EPA TAL SAC Protocol References: EPA = US Environmental Protection Agency Laboratory References: TAL SAC =, 0 Riverside Parkway, West Sacramento, CA 0, TEL ()-00 Page of //0

13 Project/Site: HFCS Sample Summary TestAmerica Job ID: 0-- Lab Sample ID Client Sample ID Matrix Collected Received 0-- HS Kit Tap Water 0// : 0// : 0-- BG Cold Tap Water 0// : 0// : Page of //0

14 Page of //0

15 Login Sample Receipt Checklist Client: Alpha Geosciences Job Number: 0-- Login Number: List Source: List Number: Creator: Nelson, Kym D Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact. Sample custody seals, if present, are intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the containers received and the COC. Samples are received within Holding Time (excluding tests with immediate HTs) Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs Containers requiring zero headspace have no headspace or bubble is <mm (/"). Multiphasic samples are not present. Samples do not require splitting or compositing. Residual Chlorine Checked. Seal N/A N/A N/A N/A Page of //0

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