Synthesis_GB :38 Uhr Seite 1 C M Y CM MY CY CMY K Parallel Synthesis Probedruck

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1 Parallel Synthesis

2 Technical specifications Model Solid Phase Synthesis Liquid Phase Synthesis Multiple Evaporator P/N Solid 16: Liquid 12: Multiple Evaporator 12: Solid 20: Liquid 16: Multiple Evaporator 16: Solid 24: Liquid 24: Multiple Evaporator 24: Footprint (wxd) (mm) 310 x x x 500 Material of reaction vessels transparent PFA & PTFE glass, PTFE caps glass, PTFE caps Vibration frequency (rpm) Orbit (mm) Drive brushless, electronic brushless, electronic brushless, electronic D. C. motor D. C. motor D. C. motor Heating 4 different heating zones with 4 different heating zones with 4 different heating zones with individual heat control and individual heat control and individual heat control and temperature display temperature display temperature display Heating power (W) approx approx approx Temperature range / heating ( C) up to 160 up to 160 up to 160 Temperature range / cooling down to - 80 by external chiller down to - 80 by external chiller down to - 80 by external chiller Temperature accuracy ( C) ± 1 ± 1 ± 1 Temperature display digital digital digital Temperature ramping 4 heating zones with individual heat 4 heating zones with individual heat 4 heating zones with individual heat control allow for programming of auto- control allow for programming of auto- control allow for programming of auto- mated temp. ramping with up to 9 steps mated temp. ramping with up to 9 steps mated temp. ramping with up to 9 steps Number of reaction vessels (max.) 16 reaction vessels of 42 ml each 12 reaction vessels of 50 ml each 12 reaction vessels of 50 ml each 20 reaction vessels of 25 ml each 16 reaction vessels of 25 ml each 16 reaction vessels of 25 ml each 24 reaction vessels of 8 ml each 24 reaction vessels of 10 ml each 24 reaction vessels of 10 ml each Connection for inert gas atmosphere / vacuum via distributor block via distributor block via distributor block Adding of solvent via injection needles into septa via injection needles into septa via injection needles into septa Capacity of Waste Cube approx ml no Waste Cube no Waste Cube Interface RS 232 for monitoring and controlling for monitoring and controlling for monitoring and controlling temperature, vibration frequency temperature, vibration frequency temperature, vibration frequency and pressure* and pressure* and pressure* Operating conditions ( C) 0-40 at 80 % 0-40 at 80 % 0-40 at 80 % relative humidity relative humidity relative humidity Protection class (DIN EN 60529) IP 20 IP 20 IP 20 Weight (kg) 27,5 27,5 28,5 Timer (min) Over temperature protection electronic electronic electronic Supply power (W) Supply voltage (**) 230 V 50/60 Hz 230 V 50/60 Hz 230 V 50/60 Hz 115 V 50/60 Hz 115 V 50/60 Hz 115 V 50/60 Hz 100 V 50/60 Hz 100 V 50/60 Hz 100 V 50/60 Hz * Pressure via optional vacuum controller ** Standard 230 V/ 50/60 Hz: others upon request, please specify for order

3 While you concentrate on research, we ll look after your support needs The team at Heidolph is dedicated and committed about delivering the highest quality product and services to its customers, allowing you to concentrate on research. Take the walk with us and see for yourself. 24 hour service for all inquires Individual application support Short delivery time for standard equipment After sales service provided by your local dealer More than 80 distributors worldwide Priority technical service 3 year warranty allows for flexibility and highly efficient research in the field of parallel liquid and solid phase synthesis. The concept is superior especially for combinatorial synthesis, for drug research and new molecular additives and in the field of researching and optimizing chemical reactions and new catalysts. With additional accessories, allows for parallel solid or liquid phase synthesis and even simultaneous evaporation. Due to advanced technology, enables highly sophisticated reactions such as moisture and oxygen separation or precisely controlled low temperature applications to be performed. Your benefit: One base, 3 possible solutions Greater cost savings Space savings, no additional space required 4 independent heating zones Higher efficiency Time savings to end user Precise probe temperature control by temperature sensors Circular collocation of transparent reaction vessels Greater visbility and accessibility Accessories Page Solid Phase Synthesis Page 6-7 Liquid Phase Synthesis Page 8-9 Multiple Evaporator Page 10 Complete Systems Page 11 2

4 The Modular Concept One Base Unit for 3 Systems is a modular concept with a wide scope of applications. The base unit can be used for solid phase synthesis, for liquid phase synthesis as well as for multiple evaporation. The reaction blocks for solid & liquid phase synthesis are interchangeable and can be used with one single base unit. Accessories and glassware set for multiple evaporation can be configured individually. For superior results Individual configurations for your specific application Exceptional visual control of reaction due to circular design of reaction block Transparent reaction vessels allow clear visibility of samples Up to 24 samples to be synthesized simultaneously: volumes from 8 to 50 ml Quick and steady mixing of samples due to constant shaking Electronic speed control from 100 to 1000 rpm Refluxing of solvents due to additional condensation zone Central connection for vacuum and inert atmosphere Solid Phase Synthesis Liquid Phase Synthesis Multiple Evaporator Operational features Easy handling due to plug & play concept Quick and easy access to all samples due to revolving reaction block Easy operation due to interchangeable reaction blocks PTFE coating of septa gives acid resistance Vessel design ensures optimal septa fixing Built-in process timer allows for unattended operation Automated temperature ramping can be programmed with up to 9 steps No rattling of vessels due to elastic reaction block elements Solid Phase Synthesis 3 reaction blocks Liquid Phase Synthesis 3 reaction blocks Multiple Evaporator 3 reaction blocks Base Unit For your safety Optional guard hood with easily attachable hinge for added safety Exceptional stability and smooth shaking due to solid construction design Integrated collection tray for dripping condensate Interface RS 232 for monitoring and controlling of parameters Heating / Cooling 4 heating zones with individual heat control allow for different temperatures One temperature sensor per heating zone positioned in reaction vessel for precise temperature control Cooling down to - 80 C by connection to an external chiller. When working at temperatures below freezing and damp atmosphere, accumulation of ice on the reaction block may occur. Inert gas box When working at temperatures below 0 C it is recommended that the Inert gas box is applied. This will eliminate the forming of ice on the reaction block. P/N The Modular Concept Inert gas box 4 5

5 Solid For chemical reactions and processes by immobilization of the material with a resin. allows for adding samples, splitting off from the resin, filtration of by-products and purification of the product. Operational advantages Exceptional visual control of reaction due to circular design of reaction block Quick and easy access to all samples due to revolving reaction block Simple dismantling of reaction vessels Reaction vessels feature valves and eliminate the use of needles Reaction vessel screw fittings allow access for cleaning and filter replacement Washing and recovery of product by vacuum filtration All reaction vessels feature bottom valves for draining of washing solvent and for product collection Central connection and distributor for vacuum and inert atmosphere Reaction vessels for solid phase synthesis Transparent reaction vessels allow clear visibility of samples Exceptional chemical resistance due to PTFE & PFA material Resin will not stick to inner side of reaction vessel Bottom part of reaction vessel accommodates filter, valve and tubing connection to Waste Cube Upper part of reaction vessel accommodates septa and tubing connection for evacuation and inert atmosphere Vessel design ensures optimal septa fixing Reaction vessel screw fittings allow easy access for cleaning and filter replacement PTFE coating of septa gives acid resistance Vacuum Accessories Vacuum pump: Rotavac valve control Interchangeable reaction blocks Choose 3 different reaction blocks for different sample volumes and quantities: Solid 16 for 16 reaction vessels of 42 ml each Solid 20 for 20 reaction vessels of 25 ml each Solid 24 for 24 reaction vessels of 8 ml each Setting of 4 different reaction temperatures due to 4 heating zones with individual heat control Additional condensation zone allows for refluxing of solvents; optional chiller required Superior heat transfer from reaction block to sample Additional samples can be added via septa Product numbers Solid Base unit with reaction block for solid phase synthesis and 16 reaction vessels of 42 ml each Solid 20 P/N Waste Cube for 20 test tubes P/N P/N Two-stage diaphragm pump made from chemically resistant materials, achieves an ultimate vaccum of 9 mbar. High suction capacity of 1.7 m 3 /h Waste Cube Suction device to collect washing solvents in a vessel After synthesis process the product will be recovered by vacuum and collected in test tubes Clear visibility at all times due to transparent glass door Please note Samples and resins in required pore size can be bought from a local supplier specialized in chemicals Solid Phase Synthesis Solid Base unit with reaction block for solid phase synthesis and 20 reaction vessels of 25 ml each Solid Base unit with reaction block for solid phase synthesis and 24 reaction vessels of 8 ml each 6 7

6 Liquid Best for chemical reactions and processes without the use of resins. allows for set up and work up of a classical chemical synthesis. Operational advantages Exceptional visual control of reaction due to circular design of reaction block Quick and easy access to all samples due to revolving reaction block No counter contamination due to separate caps on all reaction vessels Easy handling of conventional glass reaction vessels with standard threads Allows for vacuum and inert atmosphere Base unit can be upgraded to a multiple evaporator by attaching the glassware set Central connection and distributor for vacuum and inert atmosphere Reaction vessels for liquid phase synthesis Transparent reaction vessels allow clear visibility of samples Exceptional chemical resistance due to materials used: reaction vessels made of glass; caps made of PTFE Glass reaction vessels come with standard threads Reaction vessels can be closed with conventional screw caps PTFE cap accommodates septa, valve and connection for vacuum or inert atmosphere Vessel design ensures optimal septa fixing PTFE coating of septa gives acid resistance Vacuum Accessories Vacuum pump: Rotavac valve control P/N Two-stage diaphragm pump made from chemically resistant materials, achieves an ultimate vaccum of 9 mbar. High suction capacity of 1.7 m 3 /h Interchangeable reaction blocks Choose 3 different reaction blocks for different sample volumes and quantities: Liquid 12 for 12 reaction vessels of 50 ml each Liquid 16 for 16 reaction vessels of 25 ml each Liquid 24 for 24 reaction vessels of 10 ml each Setting of 4 different reaction temperatures due to 4 heating zones with individual heat control Additional condensation zone allows for refluxing of solvents; optional chiller required Vacuum can be controlled individually due to valves in the upper part of reaction vessel Additional samples can be added via septa Product numbers Liquid Base unit with reaction block for liquid phase synthesis and 12 reaction vessels of 50 ml each Liquid 16 P/N Adapter Multiple Evaporator Adapter set for connecting a Liquid to the chiller of an already existing Laborota 40xx evaporator. The set includes: Woulff bottle, intermediate piece (between chiller & receiving flask), PTFE tubing, flask clamp, sealings and GL threads P/N Please note We will determine the results of your individual application. Please inform us about: - Partical size - Density - ratio solid / liquid - Viscosity - If there is use of solids which tend to clump Liquid Phase Synthesis Liquid Base unit with reaction block for liquid phase synthesis and 16 reaction vessels of 25 ml each Liquid Base unit with reaction block for liquid phase synthesis and 24 reaction vessels of 10 ml each 8 9

7 Multiple Evaporators Complete Packages at a special price Most appropriate for simultaneous evaporation or concentration of up to 24 samples. The multiple evaporator is an ideal addition to the liquid phase synthesis. Operational advantages Exceptional visual control of reaction due to circular design of reaction block Quick and easy access to all samples due to revolving reaction block Highest distillation rates possible due to quick heat up time Reproducible results due to temperature sensor positioned in reaction vessel for precise sample temperature reading and control Guard hood to ensure constant sample temperature and for added safety Interchangeable reaction blocks Simultaneous evaporation of solvents with different boiling points due to 4 heating zones with individual heat control Choose 3 different reaction blocks for different sample volumes and quantities: Multiple Evaporator 12 for 12 reaction vessels of 50 ml each Multiple Evaporator 16 for 16 reaction vessels of 25 ml each Multiple Evaporator 24 for 24 reaction vessels of 10 ml each Vacuum can be controlled individually due to valves in the upper part of reaction vessel Vacuum Accessories Vacuum pump: Rotavac valve control P/N Vacuum controller: Vac control automatic RS P/N Vacuum valve P/N Product numbers Multiple Evaporator Base unit with reaction block for liquid phase synthesis and 12 reaction vessels of 50 ml each, with glassware set and guard hood Multiple Evaporator 12 for Extraction Vessels Base unit with reaction block for 12 extraction vessels, with glassware set and guard hood. Please note: Delivery doesn t include vessels Multiple Evaporator Base unit with reaction block for liquid phase synthesis and 16 reaction vessels of 25 ml each, with glassware set and guard hood Solid System 20 P/N for Solid Phase Synthesis The systems include: Base unit Reaction block and reaction vessels Waste Cube with test tube rack, test tubes and Waste Cube Vessel Guard hood 4 sensors for sample temperature measuring Tube connection for vacuum and inert atmosphere PTFE connection tubes for Waste Cube Solid System Solid phase synthesis for 16 reaction vessels Solid System Solid phase synthesis for 20 reaction vessels Solid System Solid phase synthesis for 24 reaction vessels for Liquid Phase Synthesis The systems include: Base unit Reaction block and reaction vessels Guard hood 4 sensors for sample temperature measuring Tube connection for vacuum and inert atmosphere Liquid System Liquid phase synthesis for 12 reaction vessels Liquid System Liquid phase synthesis for 16 reaction vessels Liquid System Liquid phase synthesis for 24 reaction vessels for Multiple Evaporation This system is identical to Liquid System but includes in addition the glassware set. Multiple Evaporator System Liquid phase synthesis for 12 reaction vessels Multiple Evaporator System Liquid phase synthesis for 16 reaction vessels Multiple Evaporator System Liquid phase synthesis for 24 reaction vessels Multiple Evaporator - Complete Packages Multiple Evaporator Base unit with reaction block for liquid phase synthesis and 24 reaction vessels of 10 ml each, with glassware set and guard hood Multiple Evaporator 16 P/N

8 Accessories for Solid Phase Synthesis Reaction Block Solid 16 Interchangeable reaction block with 16 reaction vessels of 42 ml each and vacuum distributor P/N Reaction Block Solid 20 Interchangeable reaction block with 20 reaction vessels of 25 ml each and vacuum distributor P/N Reaction Block Solid 24 Interchangeable reaction block with 24 reaction vessels of 8 ml each and vacuum distributor P/N Waste Cube 16 with test tube rack, 16 test tubes, Waste Cube vessel, insert and 16 m PTFE tube P/N Waste Cube 20 with test tube rack, 20 test tubes, Waste Cube vessel, insert and 20 m PTFE tube P/N Waste Cube 24 with test tube rack, 24 test tubes, Waste Cube vessel, insert and 24 m PTFE tube P/N Reaction Vessel Solid 16 for 42 ml with valve, connectors, filter & septa Recommended capacity: 20 ml P/N Reaction Vessel Solid 20 for 25 ml with valve, connectors, filter & septa Recommended capacity: 12 ml P/N Reaction Vessel Solid 24 for 8 ml with valve, connectors, filter & septa Recommended capacity: 5 ml P/N Insert for Waste Cube 16* P/N Insert for Waste Cube 20* P/N Insert for Waste Cube 24* P/N Filter 16, pore size 25 µ for reaction vessel Solid 16 P/N Filter 20, pore size 25 µ for reaction vessel Solid 20 P/N Filter 24, pore size 25 µ for reaction vessel Solid 24 P/N Test Tube Rack 16 for Waste Cube 16* with 16 test tubes of 42 ml each P/N Test Tube Rack 20 for Waste Cube 20* with 20 test tubes of 25 ml each P/N Test Tube Rack 24 for Waste Cube 24* with 24 test tubes of 8 ml each P/N Septa Solid P/N PTFE Tube (1/16 ) to connect vacuum distributor and Waste Cube to reaction vessel P/N Clamp Ring for PTFE Tubes (1/16 ) P/N Test Tube for Test Tube Rack 16 for Waste Cube 16 (ø 25 x 150 mm) P/N Test Tube for Test Tube Rack 20 for Waste Cube 20 (ø 20 x 150 mm) P/N Test Tube for Test Tube Rack 24 for Waste Cube 24 (ø 14 x 130 mm) P/N * to convert an existing Waste Cube to a different number of test tubes Accessories PTFE Vacuum Tube to connect vacuum source to vacuum distributor outer ø 8 mm; inner ø 6 mm P/N Temperature Sensor (135 mm) for sample temperature, PTFE coated. Temperature control on base unit ensures that set temperature is reached precisely P/N Guard Hood with attachable hinge for added safety prevents condensation in reaction vessel (comes as standard with multiple evaporator) P/N Waste Cube Vessel for collection of washing solvents in Waste Cube; ø 120 x 187 mm P/N Blanking Screw Cap for closing reaction vessels that will not be put under vacuum or inert atmosphere P/N

9 Accessories for Liquid Phase & Multiple Evaporator Heidolph Instruments, Schwabach, 11/2007 Reaction Block Liquid 12 Interchangeable reaction block with 12 reaction vessels of 50 ml each, with vacuum distributor P/N Reaction Block Liquid 16 Interchangeable reaction block with 16 reaction vessels of 25 ml each, with vacuum distributor P/N Reaction Block Liquid 24 Interchangeable reaction block with 24 reaction vessels of 10 ml each, with vacuum distributor P/N Reaction Vessel Liquid 12 reaction vessel 50 ml with screw cap, valve, connector & septa Recommended capacity: 25 ml P/N Reaction Vessel Liquid 16 reaction vessel 25 ml with screw cap, valve, connector & septa Recommended capacity: 12 ml P/N Reaction Vessel Liquid 24 reaction vessel 10 ml with screw cap, valve, connector & septa Recommended capacity: 5 ml P/N Glass Vessel Liquid 12 for 50 ml P/N Glass Vessel Liquid 16 for 25 ml P/N Glass Vessel Liquid 24 for 10 ml P/N Temperature Sensor (135 mm) for Liquid 24 for sample temperature, PTFE coated. Temperature control on base unit ensures that set temperature is reached precisely P/N Temperature Sensor (170 mm) for Liquid 12 and 16 P/N PTFE Vacuum Tube outer ø 8 mm; inner ø 6 mm P/N PTFE Connecting Tube 12 & 16 for reaction vessels Liquid 12 & 16 outer ø 8 mm; inner ø 6 mm P/N PTFE Connecting Tube 24 for reaction vessels Liquid 24 outer ø 6 mm; inner ø 4 mm P/N Glassware set with attachment. Upgrade to a multiple evaporator P/N Septa Liquid P/N Heidolph Instruments GmbH & Co. KG Walpersdorfer Str Schwabach / Germany Phone: (+49) Fax

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