CRUDE OIL ASSAY STATOIL. Draugen PRODUCT TECHNOLOGY AND CUSTOMER SERVICE. Crude Oil and Products Section DATE:
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1 CRUDE OIL ASSAY Draugen STATOIL PRODUCT TECHNOLOGY AND CUSTOMER SERVICE Crude Oil and Products Section DATE:
2 C O N T E N T S ******************* 1. SAMPLE DATA 2. DISTILLATION CONDITIONS 3. ANALYTICAL RESULTS 4. ANALYTICAL METHODS 5. TBP - CURVES
3 1. S A M P L E D A T A **************************** SAMPLE: Crude oil DESCRIPTION: Draugen DATE OF SAMPLING: SAMPLE VOLUME: 60 litres SAMPLE PACKAGE: Jerrycans LABORATORY: This assay was prepared by Statoil PTC
4 2. D I S T I L L A T I O N C O N D I T I O N S *********************************************************** The following conditions according to ASTM are used: TRUE BOILING POINT DISTILLATION EQUIPMENT: The distillation up to 375 C is performed according to D-2892/90, and from 375 C according to D-5236/92 (Vacuum Potstill Method) CONDITIONS: The cutpoints are as follows: Atmospheric distillation: C5-205 C AET 100 Torr: C AET 10 Torr: C AET 5 Torr: C AET From 1 to 0.1 Torr: C AET The atmospheric cutting points are corrected to 760 mmhg. VOLUME: Volume expansion or contraction are normalized among fractions boiling below 150 C in proportion to their yields. (Usually the "Loss" is negative due to volume expansion) HOLD UP: Hold up at 375 C AET is distributed as follows: 50% on the first fraction of the Pot Still (375 C- 420 C) and 50% in accordance with the mass-ratios of the fractions from 420 C AET. LOSS: Loss up to 375 C AET is distributed with 2/3 in the gas-fraction and 1/3 in the first liquidfraction.
5 3. ANALYTICAL RESULTS ******************************* PROJECT: CRUDE OIL ASSAY REF.NO: Table 1 SAMPLE: Draugen Crude oil Analysis of the whole crude: Light ends - see tables 8a-8e Density at 15 C kg/l Specific gravity at 60/60 F API gravity at 60/60 F API 39.9 Sulphur mass % Total Acid Number (TAN) mg KOH/g 0.09 Reid Vapor Pressure (RVP) kpa 62.3 Pour point C -15 Kin. viscosity at 20 C mm²/s (cst) 4.02 Kin. viscosity at 40 C mm²/s (cst) 2.49 Nitrogen mg/kg 540 Hydrogen sulphide mass % * ND Vanadium (V) mg/kg 1.1 Nickel (Ni) mg/kg 0.9 Sodium (Na) mg/kg 61 Salt as NaCl mg/l 201 Wax content mass % <5.0 Flash point C <10 Water content mass % 0.55 * ND: not detectable
6 Table 2 SAMPLE: Draugen Crude oil Fraction C C Yield on crude mass % Yield on crude vol % Density at 15 C kg/l Specific gravity at 60/60 F API gravity at 60/60 F API Sulphur mass % < Mercaptan sulphur mg/kg <3 <3 <3 n-paraffins mass % i-paraffins mass % Naphthenes mass % Aromatics (incl. benzene) mass % Benzene mass % n-paraffins vol % i-paraffins vol % Naphthenes vol % Aromatics (incl. benzene) vol % Benzene vol % Vapor Pressure (DVPE) kpa Flash point C <10 Research Octane Number (RON) Motor Octane Number (MON) Nitrogen mg/kg <1 <1
7 Table 3 SAMPLE: Draugen Crude oil Fraction C Yield on crude mass % Yield on crude vol % Density at 15 C kg/l Specific gravity at 60/60 F API gravity at 60/60 F API Sulphur mass % Mercaptan sulphur mg/kg Copper corrosion 1a 1a Total Acid Number (TAN) mg KOH/g < < n-paraffins mass % 5.5 i-paraffins mass % 30.0 Naphthenes mass % 45.6 Aromatics mass % 18.8 n-paraffins vol % 6.1 i-paraffins vol % 31.8 Naphthenes vol % 45.0 Aromatics vol % 17.1 Aromatics (HPLC) Total mass % Mono-Aromatics mass % Di-Aromatics mass % < Polycyclic Aromatics mass % <0.1 < Naphtalenes vol % Aniline point C Smoke point mm Watson K-factor 11.7 Flash point C 35.0 Freezing point C <-60 <-60 Cloud point C < Cold Filter Plugging Point (CFPP) C < Pour point C < Cetane number Cetane index (D-976) CCI (D-4737) Conradson Carbon Residue (CCR) mass % <0.10 Kin. viscosity at 20 C mm²/s (cst) Kin. viscosity at 50 C mm²/s (cst) Kin. viscosity at 100 C mm²/s (cst) 2.48 Nitrogen mg/kg <1 < Basic nitrogen mass % Refractive index at 67 C Distillation D-86 (50%) C
8 Table 4 SAMPLE: Draugen Crude oil Fraction C Yield on crude mass % Yield on crude vol % Density at 15 C kg/l Specific gravity at 60/60 F API gravity at 60/60 F API Sulphur mass % Total Acid Number (TAN) mg KOH/g Aniline point C Watson K-factor Pour point C >45 Conradson Carbon Residue (CCR) mass % < Kin. viscosity at 50 C mm²/s (cst) Kin. viscosity at 80 C mm²/s (cst) 70.7 Kin. viscosity at 100 C mm²/s (cst) Vanadium (V) mg/kg <0.1 <0.1 <0.1 Nickel (Ni) mg/kg <0.1 < Nitrogen mg/kg Basic nitrogen mass % Refractive index at 67 C
9 Table 5 SAMPLE: Draugen Crude oil Fraction C Yield on crude mass % Yield on crude vol % Density at 15 C kg/l (1) Specific gravity at 60/60 F API gravity at 60/60 F API Sulphur mass % Total Acid Number (TAN) mg KOH/g 0.18 Aniline point C Watson K-factor Pour point C 42 >45 45 Conradson Carbon Residue (CCR) mass % Asphaltenes mass % < n-pentane insolubles mass % Ash mass % Kin. viscosity at 50 C mm²/s (cst) 133 Kin. viscosity at 80 C mm²/s (cst) 694 Kin. viscosity at 100 C mm²/s (cst) Kin. viscosity at 135 C mm²/s (cst) 118 Vanadium (V) mg/kg Nickel (Ni) mg/kg Nitrogen mg/kg Basic nitrogen mass % Penetration at 25 C 0.1mm Refractive index at 67 C (1): Calculated density for 525+ and 565+ fractions.
10 Table 6 SAMPLE: Draugen Crude oil DISTILLATION YIELD MASS-% ******************** Date: Intake: g Density at 15 C: kg/l FRACTION Mass Yield Cumul. yield Temperature g mass % mass % C Loss Gases C
11 Table 7 SAMPLE: Draugen Crude oil DISTILLATION YIELD VOL-% AND DENSITY ************************************* Date: Intake: g Density at 15 C: kg/l FRACTION Density at Yield Cumul. yield Temperature 15 C (kg/l) vol % vol % C Loss Gases C
12 Table 8a SAMPLE: Draugen Crude oil COMPOSITIONAL ANALYSIS OF CRUDE OIL (MASS %) NORMAL PARAFFINS: Methane <0.01 Ethane 0.03 Propane 0.53 Butane 1.77 Pentane 2.10 Hexane 1.68 Heptane 1.33 Octane 0.95 Nonane 0.39 Sum n-paraffins 8.78 C4 HYDROCARBONS i-butane 0.47 C5 HYDROCARBONS ISO PARAFFINS: 2,2-Dimethylpropane <0.01 i-pentane 1.51 Sum C5 i-paraffins 1.51 NAPHTHENES: Cyclopentane 0.19
13 Table 8b SAMPLE: Draugen Crude oil C6 HYDROCARBONS ISO PARAFFINS: 2,2-Dimethylbutane ,3-Dimethylbutane Methylpentane Methylpentane 0.59 Sum C6 i-paraffins 1.74 NAPHTHENES: Methylcyclopentane 1.02 (Inc. 2,2-Dimethylpentane) Cyclohexane 1.38 Sum C6 naphthenes 2.40 AROMATICS: Benzene 0.02
14 Table 8c SAMPLE: Draugen Crude oil C7 HYDROCARBONS ISO PARAFFINS: 2,2,3-Trimethylbutane <0.01 3,3-Dimethylpentane ,4-Dimethylpentane Methylhexane ,3-Dimethylpentane Methylhexane 0.56 Sum C7 i-paraffins 1.31 NAPHTHENES: cis-1,3-dimethylcyclopentane 0.25 trans-1,3-dimethylcyclopentane 0.23 trans-1,2-dimethylcyclopentane 0.44 Methylcyclohexane 2.52 Ethylcyclopentane ,1-Dimethylcyclopentane 0.14 Sum C7 naphthenes 3.70 AROMATICS: Toluene 0.31
15 Table 8d SAMPLE: Draugen Crude oil C8 HYDROCARBONS ISO PARAFFINS: 2,2,4-Trimethylpentane <0.01 2,5-Dimethylhexane ,4-Dimethylhexane ,4-Dimethylhexane ,3-Dimethylhexane ,3-Dimethylhexane 0.11 (Inc. naphthenic compound) 2-Methyl-3-ethylpentane Methylheptane Methylheptane Methylheptane ,3,4-Trimethylpentane 0.01 Sum C8 i-paraffins 1.91 NAPHTHENES: 1,1,3-Trimethylcyclopentane 0.15 (Inc. 2,2-Dimethylhexane) trans, cis-1,2,4-trimethylcyclopentane 0.14 trans,cis-1,2,3-trimethylcyclopentane 0.14 trans-1,4-dimethylcyclohexane ,1-Dimethylcyclohexane 0.08 trans-1-methyl-3-ethylcyclopentane 0.05 cis-1-methyl-3-ethylcyclopentane 0.04 trans-1-methyl-2-ethylcyclopentane 0.11 trans-1,2-dimethylcyclohexane Propylcyclopentane 0.02 cis-1,2-dimethylcyclohexane 0.13 Ethylcyclohexane Propylcyclopentane 0.19 cis,cis-1,2,4-trimethylcyclopentane Methyl-1-ethylcyclopentane 0.02 cis-1,3-dimethylcyclohexane <0.01 (Inc. naphthenic compound) Sum C8 naphthenes 2.25
16 Table 8e SAMPLE: Draugen Crude oil AROMATICS: Ethylbenzene 0.14 m- & p-dimethylbenzene (m- & p- xylene) 0.64 o-dimethylbenzene (o-xylene) 0.20 Sum C8 aromatics 0.98 C9 HYDROCARBONS ISO PARAFFINS: 3,5-Dimethylheptane Methyloctane Methyloctane Methyloctane ,3,4-Trimethylhexane <0.01 Unidentified paraffin 0.09 Sum C9 i-paraffins 0.82 NAPHTHENES: 1,1,3-Trimethylcyclohexane Methyl-2-propylcyclopentane Methyl-3-ethylcyclohexane Methyl-4-ethylcyclohexane ,1,4-Trimethylcyclohexane 0.10 Unidentified naphthenes 0.07 Sum C9 naphthenes 0.80 TOTAL IDENTIFIED TOTAL UNIDENTIFIED 0.27 TOTAL C
17 4. ANALYTICAL METHODS ********************************* Table 9a SAMPLE: Draugen Crude oil TEST UNITS METHOD Density at 15 C kg/l D-4052/D-5002 Specific gravity at 60/60 F - Total Sulphur mass % D-4294 Total Sulphur mass % D-5453 for sulphur content less than 0,01% Hydrogen sulphide mass % D-3227 Mercaptan sulphur mg/kg D-3227 n-paraffins mass % GC i-paraffins mass % GC Naphthenes mass % GC Aromatics mass % GC Benzene mass % GC Aromatics - HPLC mass % IP-391/95 Naphthalene vol % D-1840 Watson K UOP 375 Vapor Pressure (DVPE) kpa D-5191 Reid Vapor Pressure (RVP) kpa D-323 Flash point ( Pensky Martens) C D-93 Freezing point C D-2386 Cloud point C D-2500/D-5772 Pour point C D-5853/D-5950 Could Filter Plugging Point C IP 309 Kin. viscosity at 20 C mm²/s (cst) D-445 Kin. viscosity at 50 C mm²/s (cst) D-445 Kin. viscosity at 80 C mm²/s (cst) D-445 Kin. viscosity at 100 C mm²/s (cst) D-445 Kin. viscosity at 135 C mm²/s (cst) D-445
18 Table 9b SAMPLE: Draugen Crude oil TEST UNITS METHOD Aniline Point C D-611 Research Octane Number (RON) D-2699/95 Motor Octane Number (MON) D-2700/95 Cetane index D-976 Calculated Cetane Index (CCI) D-4737 Cetane number D-613 Smoke point mm D-1322 Distillation of the whole crude up to 375 C D-2892 Distillation of the indivudal fractions D-86 Distillation of 375+ C D-5236 Total Acid Number (TAN) mgkoh/g D-664 Copper corrosion D-130 Nitrogen: fractions up to 420 C mg/kg D-4629 Nitrogen: fractions above 420 C mg/kg D-4629 modified Basic nitrogen mass % UOP 269 Vanadium (V) mg/kg ICP-AES Nickel (Ni) mg/kg ICP-AES Sodium (Na) mg/kg ICP-AES Salt as NaCl mg/l IP 265 Conradson Carbon Residue or mass % D-189 Carbon Residue (Micro Method) mass % D-4530 Asphaltenes mass % IP 143 n-c5 Insolubles mass % D-4055 Ash mass % D-482 Penetration at 25 C 0.1mm D-1321 Refractive index at 67 C Abbe refractometer Wax content mass % UOP 46 (mod. acetone precip.) Water content mg/kg D-4928
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