Dielectric Analysis Permittivity and dielectric loss 100. Dynamic Mechanical Analysis Mechanical strength and energy loss 200

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2 Relative Signal Technique Property Measured Change at Tg Differential Scanning Calorimetry Heat flow (heat capacity) 0.2 Thermomechanical Analysis Expansion coefficient or softening 3 Dielectric Analysis Permittivity and dielectric loss 100 Dynamic Mechanical Analysis Mechanical strength and energy loss 200

3 84.00 C 101.1C C C C C o Temperature ( C)

4

5

6 Specimen size: 18 mg Endset Midpoint Onset Tg ( C) Heating Rate ( C)

7 0.48 COOLING RATES Heat Flow (W/g) CURVES ARE FROM HEATING PORTION OF EXPERIMENT QUENCH COOLED 20 C 10 C 20 C 20 C Temperature ( C)

8

9

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12

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14 Method Thermal Conditions Onset Midpoint Endset DSC MDSC TMA N/A N/A DMA DEA N/A Polymer Type DSC MDSC TMA DMA DEA Amorphous best best best best better Semi-crystalline better best best best better Highly crystalline good good best best better Plasticized better best better best better Thermosetting resin best best better better best Cured thermoset good better better best better Elastomer better best better best better Glass Filled good good better best better Carbon Filled good good better best good Volume Relaxation Present (a) best (a) better better

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