IN SILICONICS APPLICATIONS INCI:SORBITAN OLIVATE

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1 OLIVEM 900 is a very versatile multifunctional ingredient, recommended not only as W/O emulsifier, but also as a functional lipid in the siliconic cosmetics, where interfacies interactions may easily cause formulation and manufacturing problems. Siliconic emulsions have a very shiny surface a fresh feel and leave on the skin a very pleasant feel of lightness even containing a high amount of siliconic phases at low volatility. CHARACTERISTICS INCI NAME: SORBITAN OLIVATE FORM: WAXY SOLID MELTING POINT: C emulsifier of natural origin low use level (1-2%) in siliconic emulsion, performing stabilizing properties viscosity stabilizer compatibility with a wide range of siliconic emulsifiers improvement of sensorial characteristics and after use feel effective dispersant for powders and pigments improvement of spreadability and texture MANUFACTURING METHOD OF SILICONIC EMULSIONS CONTAINING OLIVEM 900 OLIVEM 900 in siliconic emulsions excludes the possibility of cold manufacturing, in fact it is necessary to melt it, around 70 C. It is suggested to combine OLIVEM 900 and low volatile siliconic oils with high molecular weight (dimethicone preferably) with powders and pigments to be included in the formulation, to reach homogeneity of this blend by heating, and finally add the resting amount of silicons, mixing to homogeneity. Add watery phase (complete with moisturisers, and water soluble active ingredients) using a high speed stirrer (anchor shaped). When emulsion is complete, homogeneize the system in order to reduce the particle size and granting a longer stability. SILICONIC EMULSIONS The choice to employ formulations containing high quantities of silicons is due to the market request for OIL FREE products: greasy products but with a silky touch, easy and light to smear but still rich and nourishing. 1

2 The versatility of siliconic emulsions and the broad viscosity range, that may easily be modified, has determined their success and popularity on the market of protective and waterproof emulsions. The portions of the market where OIL FREE products are more present are: foundation (10.4%), make up removers (10.1%) and sun protecting factors (9.6%). The following chart shows the analysis of Personal Care products sold in the United States in While in 1990 only 19 products out of 443 where siliconic emulsions (4.2%), in 1991 the amount increases to 6.8%, with 33 siliconic emulsions out of 484 products. This trend of siliconic emulsions is still growing even is the request of more natural products is also becoming important. shampoo/cond. 17% body face moist. 4% mascara/eye liner 2% foundation 21% foundation face cleanser sun care face blusher Shampoo body face moist. mascara/eye liner face blusher 18% sun care 18% face cleanser 20% The presence of an OLIVE OIL DERIVED in an emulsion which is completely based on silicons makes W/Si emulsions more pleasant in the trend of a natural derived cosmetic required by the final user. OLIVEM 900 is an important viscosizing agent compared to AMS-C30 or paraffinic waxes, and it also performs stabilisation by increasing rigidity and plasticity features of the emulsion containing pigments and iron oxides commonly employed in color cosmetics. As reported in this chart, siliconic formulations are becoming more and more important in the cosmetic market: in fact, as we can see, several different formulations may be based on silicons.

3 VISCOSITY INCREASE Viscosity has been measured on samples of the emulsion ref. 1/ (W/S Foundation Sunscreen Base) three days after the preparation, in order to avoid the natural viscosity variations characteristics of W/S systems. The use of OLIVEM 900 sensitively increases the viscosity of the system without changing its organolectic characteristics and the skin feel, and allowing the evaluation of the emulsion also just after it has been VISCOSITY VARIATIONS Viscosity (Cps) Without Olivem 900 Olivem 900 1% Olivem 900 2% % Olivem 900 produced. In fact the siliconic emulsion without OLIVEM 900 needs some time for settlement (typical of this kind of systems), and it has been evaluated three days after the manufacture, while the addition of OLIVEM 900 allows the measure of viscosity at the end of the preparation, lowering the manufacturing times. The stability to centrifugation essay is also greatly increased by OLIVEM 900, and this trial may also be done right after the emulsion was prepared. The recommended concentration where OLIVEM 900 improves the characteristics of siliconic systems is around 2%, while between 1 and 2% it may be employed as viscosity enhancer and stabilizer. Viscosity was tested on a 100 g sample of emulsion at 25+1 C using a viscometer Brookfield model RV TDV II at 20 rpm (tirning device n. 5). One measure was taken just after the preparation, and following another measure was taken three days later. The maintenance of the same viscosity in a structure is a sign os stability during the time. STABILITY TEST 30 ml samples of the emulsions have been stored at different temperatures, in order to observe an acceleration of the termic degradation process. The stability and the organolectic characteristics of the samples has been observed at 40 C, 50 C, 4 C, room temperature with light exposure.

4 These test give quite a good prediction of the system s behaviour, and samples are considered compliant to stability tes ts (stability test passed) if there is no separation of phases, color or odor modification, unusual viscosity variations. These trials have been made on emulsions (at time 0) and after 3 months by centrifuge (centrifuge model ALC 4222) at 5000 rpm for 30 minutes. By increasing the rotations per minute the droplets of the emulsion may more easily cause coalescence induced by the destruction of the electrostatic barriers of emulsifiers and stabilizing agents. The test is passed is phases remain homogeneous. Requested characteristics in order to define acceptable quality are: pleasant aspect and perfume appreciable skin feel pleasant sensation while smearing the cream pleasant after feel hydrating and emollient properties as requested SENSORIAL EVALUTION OF EMULSIONS CONTAINING OLIVEM 900 The sensorial evaluation has been done on a panel of 10 people trained to compare the different sensorial characteristics of Personal Care and Skin Care products. They have been requested to evaluate two different formulations, one of the two having OLIVEM 900 in the formulation. The aim was to evaluate the different characteristics of the emulsion containing OLIVEM 900. The maximum score for each characteristic is 10. ABSORPTION SPEED: a light improvement of this characteristic with a lower sticky after feel. SPREADABILITY: increase remarked COLOR: OLIVEM 900 has whitening properties toward the emulsion SHINE: shine has remarkably increased CONSISTENCY: OLIVEM 900 improves the structure of the system without affecting its appearance.

5 SENSORIAL EVALUATION: The reported data underline the performances of OLIVEM 900 in siliconic emulsions, and the improvements that from this addition derive: presence of a natural derived ingredient, as a plus stability improvement and viscosity optimization consistency shine color with Olivem 900 without Olivem 900 spreadability absorption speed improvement of some sensorial characteristics low levels of use OLIVEM 900 offers to the formulator an interesting ingredient allowing to improve his product by satisfying the requests of using raw materials of natural origin, very important for the final user. The versatility of OLIVEM 900 (SORBITAN OLIVATE) and its characteristics of absorption make it recommended to be employed in sun care products, make up bases and all other topic products based on silicons. POWDER DISPERSION OLIVEM 900, thanks to its properties due to its structure, is very helpful in making powder dispersions homogeneous. In fact it is very effective in making the microgranules of the powders being wetted by the formulation, and this improves the homogeneity of the formulation. This characteristic is even more important since it is applicable to powders of any kind: talc, kaolin, zinc oxide, titanium dioxide, and even colored iron pigments and lakes. This characteristic in skin care is very important in particular for sun screens, because the homogeneous dispersion of the physical filter grants a safe protection for the skin towards the aggression of Uvs.

6 The gel created with the following formula: OLIVEM 900 (10%) and Mineral Oil (90%), has shown the property to enclose a very high amount of any kind of powders, as shown by the following chart: 80,0 70,0 % of powder enclosed 60,0 50,0 40,0 30,0 20,0 TiO2 ZnO K a o lin Talc Lake Iron O x id e 10,0 0,0 TiO2 ZnO Kaolin Talc Lake Iron Oxide It is also very interesting to remark that the powder dispersant properties which we have mentioned are still maintained also in siliconic emulsions: in fact the following formulation is based on the comparison with the product without OLIVEM 900. Protective Cream with Zinc Oxide A B A.1 Preserved Water up to 100 up to Sodium Chloride 1.0% 1.0% 3 Glycerin 10.0% 10.0% B.1 OLIVEM % 2 Cyclopentasiloxane and 10.0% 10.0% Dimethicone Copolyol 3 Cyclomethicone 6.0% 6.0% 4 Zinc Oxide 4.0% 4.0% 5 Dimethicone 2.0% 2.0% 6 Perfume as needed as needed The emulsion A has a very good viscosity, very shiny and zinc oxide is very well dispersed, compared to the emulsion B which is less viscous, less shiny and zinc oxide is not properly dispersed. The manufacturing method is the same. CONCLUSIONS OLIVEM 900 is compatible with all the siliconic ingredients testes, both silicon oils and siliconic emulsifiers. When included in siliconic emulsions, it improves the viscosity of the system without changing its organolectic characteristics. The skin feel improves as well, thanks to the high compliance of OLIVEM 900 with our skin (see sensorial evaluation results).

7 The addition of a natural derivative in siliconic emulsions is also a strong marketing claim of a more natural and safe cosmetic. Powder dispersions are also improved by the presence of this ingredient. FORMULATIONS The following formulations are here indicated in order to give general directions for the employment of OLIVEM 900. Although they have been realised according to the best information we owe, this does not exonerate the user from verifying their validity. B&T Technical Assistance is at the user s disposal in order to contribute to the development of new formulations, and to give the needful information for a correct use of our products. W/S Foundation Sunscreen Base (ref. 1/100600) A.1 Demineralized Water up to Sodium Chloride 1.0% B.1 OLIVEM % 2 Cyclomethicone and Dimethiconol 5.0% 3 Cyclopentasiloxane and Dimethicone Copolyol 10.0% 4 Cyclomethicone 8.0% 5 TiO2 10.0% 6 Octyl Metoxycinnamate as required 7 Perfume as needed Protective Cream with Zinc Oxide A.1 Demineralized Water up to Sodium Chloride 1.0% 3 Glycerin 10.0% B.1 OLIVEM % 2 Cyclopentasiloxane and Dimethicone Copolyol 10.0% 3 Cyclomethicone 6.0% 4 Zinc Oxide 4.0% 5 Dimethicone 2.0% 6 Perfume as neede

8 Tapioca Hydrating Lotion A.1 Cyclopentasiloxane and Dimethicone Copolyol 12.0% 2 Cycolpentasiloxane and Dimethiconol 10.0% 3 OLIVEM % 4 Tapioca 2.0% 5 Cyclomethicone 10.0% B.1 Glycerin 25.0% 2 Lactic Acid 1.0% 3 Preserved Water 40.0% C.1 Perfume and Color as needed Rice Starch Comparative Emulsions A.1 Demineralized Water up to 100 up to Sodium Chloride 2.0% 2.0% 3 Glycerin 3.0% 3.0% B.1 OLIVEM % - 2 Cyclopentasiloxane and 10.0% 10.0% Dimethicone Copolyol 3 Cyclomethicone 5.5% 5.5% 4 Rice Starch 3.5% 3.5% 5 Avocado Oil 1.0% 1.0% 6 Jojoba Oil 1.0% 1.0% 7 Shea Butter 1.0% 1.0% 8 Phytosqualane 1.0% 1.0% 9 Perfume as needed as needed Barrier Comparative Cream A.1 Preserved Water up to 100 up to Sodium Chloride 2.0% 2.0% B.1 OLIVEM % - 2 Laurylmethicone Copolyol 2.0% 2.0% 3 Cyclomethicone 10.0% 10.0% 4 Paraffinum Liquidum 7.0% 7.0% 5 Dimethicone 0.5% 0.5% 6 Perfume as needed as needed Mild Cleanser A.1 Demineralized Water up to Sodium Chloride 1.0% 3 EUROL BT 0.1% 4 Propylene Glycol 26.0% B.1 OLIVEM % 2 Cyclomethicone 25.0% 3 Cyclopentasiloxane and Dimethicone Copolyol 12.0% 4 Perfume as needed

9 0 PRODUCT AND COMPANY IDENTIFICATION OLIVEM 900 TECHNICAL DATA SHEET Trade Name... OLIVEM 900 Applications non ionic, not ethoxylated emulsifying system derive from olive oil for W/O creams and lotions INCI Name... SORBITAN OLIVATE CAS Number EINECS Number Legislative world-wide Approval Company... B & T Srl - Via O. da Tresseno, MILAN - Italy Tel Fax SPECIFICATIONS 20 C flakes, waxy solid Color.... ivory Odor... slight, characteristic Active Substance% 99.0 min Water Content %.. < 1.0 Acid Value SOLUBILITY Soluble... Dispersible.... in ethanol and xilol. in warm water 0 TYPICAL VALUES HLB Saponification Value Melting Point Additives and none preservatives 0 SHELF-LIFE 5 years stored unopened into original containers at a temperature between 5 and 3 following GMP guidelines Revision : The information contained in this bulletin to the best of our knowledge is currently true and accurate. Any recommendations or suggestions are made without any warranty or guarantee, since conditions of use and storage are beyond your control.

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