Crude Assay Report. Crude Oil sample marked. "AL SHAHEEN CRUDE OIL" dated 10th April On Behalf Of. Maersk Oil Qatar AS

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1 Crude Assay Report on Crude Oil sample marked "AL SHAHEEN CRUDE OIL" dated 10th April 2006 On Behalf Of Maersk Oil Qatar AS With compliments Intertek Caleb Brett, Fujairah Caleb Brett Fujairah Fujairah Free Zone, Phase II, P.O. Box 1307, Fujairah, United Arab Emirates Tel: (971)(9) , Fax: Web:

2 "AL SHAHEEN CRUDE OIL" ASSAY INDEX Sl.No. Description Page No. 1 Description of sample 1 2 Summary and comments 2 3 Detailed Assay Base Cuts Overview 3 4 Whole Crude Characteristics 4 5 True Boiling Point Distillation data 5 6 True Boiling Point Distillation data - Graph 6 7 Summary of Product / Residue cut points & Yield 7 8 Properties of Cuts- C5-65 C C C C C C C C C Distilation data per fractions Fractions Mid B.P. Vs. Density - Chart Fractions Mid B.P. Vs. Sulphur Content - Chart Fractions Mid B.P. Vs. Nitrogen Content - Chart Fractions Mid B.P. Vs. Aniline Point - Chart 21

3 Date: June 5, 2006 Maersk Oil Qatar As P.O.Box Doha Qatar For the Attention of : Mr. Michael D. Pedersen Sample(s) received from : Maersk Oil Qatar As Sample(s) submitted as : Crude Oil - 3 x 20 Ltrs IATA Cans - 2 x 10 Ltrs IATA Cans Description(s) on Label(s) : Al Shaheen Crude Oil Ex Qatar sampled on 10th April Work Order No. : CWO Seals on Sample(s) : , , , , Sample(s) received on : May 2, 2006 The above sample(s) was/were examined as detailed below and the following results obtained: Please refer attached sheet for analytical results. Page 1

4 SUMMARY & COMMENTS General: The Al Shaheen Crude Oil samples were received from Intertek Caleb Brett Qatar Branch on May 02, The samples were in 3 x 20 Ltrs & 2 x 10 Ltrs IATA Cans. The labels indicated that the samples were drawn on 10th April Appearance & Initial Examination: The sample observed to be liquid at room temperature with good flow properties. After cooling (to Zero degree centigrade) and homogenization of the sample. H 2 S content on the vapour phase of the samples within the original containers were measured and noted to be in the range of ppm within the containers. A representative portion of the sample was drawn and tested for API and Water contents. API observed to be API and the Water content as 0.18% Vol. The Dry API of the sample was calculated and observed to be API. Distillation and Analysis: The distillation of the sample was carried out in two major steps as per (15 Theoretical plate column) & ASTM D 5236 (Vacuum potstill) methods. The yield pattern of each fraction collected are tabulated in percentage weight and percentage volume and in graphical form. Results of the analysis carried on the various fractions are shown in pages Some of the properties are also presented in chart form in pages Please do not hesitate to contact us for any additional information or clarifications that you may require on this analysis. Page 2

5 TEST UNIT METHOD LABORATORY REPORT NO. - FUJ/FCA1025/06 Al Shaheen Crude Oil Ex Qatar sampled on 10th April CRUDE OIL - DETAILED ASSAY ALL CUTS OVERVIEW Whole Crude LIGHT ENDS - C4- Distillation of Crude Oil (15 plate) Yield % Wt. & Yield % Vol. ASTM D Cum. Yield % Wt. & Cum. Yield % Vol. ASTM D C kg/l ASTM D 5002 / IP 365 / IP Specific 60/60 F Conversion API 60 F Calculated C (dry) kg/l Calculated Specific 60/60 F (dry) Conversion API 60 F (dry) Calculated Water Content % Vol. ASTM D Light Ends methane ethane propane i-butane % mass GC n-butane Total C1-C i-pentane n-pentane Sulphur Content % mass ASTM D Mercaptan Sulphur mg/kg ASTM D Mercaptan Sulphur mg/kg UOP Total Nitrogen % mass ASTM D 5291 (Mod) 0.15 < 0.05 < Research Octane Number *** ASTM D Motor Octane Number *** ASTM D PIONA analysis Total paraffins Total olefins < 0.01 < 0.01 < 0.01 Total napthenes % Vol GC Total aromatics > 200 C & Unidentified < 0.01 < Poly-N < 0.01 < Aniline Point C ASTM D Smoke Point mm IP Naphthalene content %Vol. ASTM D Vanadium (V) 112 Nickel (Ni) mg/kg IP 470 ( AAS ) 38 Iron (Fe) 15 Nickel / Vanadium Ratio 0.34 Freeze Point C ASTM D 2386 Below Cloud Point C ASTM D 2500 Below ## Pour Point (upper) C ASTM D 5853 / D97 Below Pour Point (lower) C ASTM D 5853 / D97 Below -45 Kinematic 20 C Kinematic 40 C Kinematic 50 C mm 2 /S ASTM D 445 Kinematic 80 C Kinematic 100 C Kinematic 150 C Distillation C ASTM D 86 See page 17 See page 17 See page 17 * Cetane Index ASTM D * Refractive 20 C ASTM D Refractive 70 C ASTM D Micro Carbon Residue % mass ASTM D Asphaltene % mass IP Total Acid Number mgkoh/g ASTM D Benzene Content % mass GLC < 0.01 Salt Content PTB ASTM D Salt Content as NaCl mg/l IP Salt Content mg/kg IP Flash Point C ASTM D 93 (Mod.) Below -5 Sediment by Extraction % mass ASTM D Reid Vapour 100 F psi ASTM D Hydrogen Sulphide mg/kg UOP 163 < 1 Mercury mg/kg Cold Vapor < 1 Lead mg/kg ASTM D 5863 / AAS < 0.1 Wax Content prec. At -30 C % mass UOP C5-65 C C C C CUT RANGE C C C C 560 C + Note: * Unable to perform test due to the heavy nature of the fraction. *** Samples were blended with ASTM grade Iso Octane, and results were caluclated from the blend's result. ## Unable to test due to the dark colour of the fraction. Page 3

6 SUMMARY OF WHOLE CRUDE CHARACTERISTICS Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April TEST UNIT METHOD Whole Crude 15 C kg/l ASTM D Specific 60/60 F Calculated API 60 F Conversion C (dry) kg/l Calculated Specific 60/60 F (dry) Conversion API 60 F (dry) Calculated Water Content % Vol. ASTM D Light Ends methane ethane propane i-butane % mass GC n-butane Total C1-C i-pentane n-pentane Sulphur Content % mass ASTM D Mercaptan Sulphur mg/kg UOP Total Nitrogen % mass ASTM D 5291 (Mod) 0.15 Pour Point (upper) C ASTM D 5853 Below -45 Pour Point (lower) C ASTM D 5853 Below -45 Kinematic 20 C Kinematic 40 C mm 2 /S ASTM D Kinematic 50 C Refractive 70 C ASTM D Asphaltene % mass IP Total Acid Number mgkoh/g ASTM D Benzene Content % mass GLC < 0.01 Salt Content PTB ASTM D Salt Content as NaCl mg/l IP Salt Content mg/kg ASTM D Flash Point C ASTM D 93( Mod) Below -5 Sediment by Extraction % mass ASTM D Reid Vapour 100 F psi ASTM D Hydrogen Sulphide mg/kg UOP 163 < 1 Mercury mg/kg Cold Vapor < 1 Lead mg/kg ASTM D 5863 / AAS < 0.1 Wax Content prec. at -30 C % mass UOP Page 4

7 TRUE BOILING POINT DISTILLATION DATA ( & ASTM D 5236) Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April Vapour Temperature Cumulative % Sl. No. % Weight % Volume C Weight Cumulative % Volume 1 Gas Residue Page 5

8 LABORATORY REPORT NO. FUJ/FCA1025/ TRUE BOILING POINT DISTILLATION CURVE ( & ASTM D 5236) AL SHAHEEN CRUDE OIL Ex Qatar sampled on 10th April Temperature C Recovery % % Weight % Volume Page 6

9 SUMMARY OF PRODUCT / RESIDUE CUT POINTS AND YIELDS Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April Yield % Cut Points Al Shaheen Crude Oil Ex Qatar sampled on 10th April ( C) Weight % Volume % IBP Page 7

10 CUT RANGE - C5-65 C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD 2 C5-65 C Distillation of Crude Oil Yield % Wt Yield % Vol Cum. Yield % Wt Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated Sulphur Content % mass ASTM D Mercaptan Sulphur mg/kg ASTM D Research Octane Number *** ASTM D Motor Octane Number *** ASTM D PIONA analysis Total Paraffins Olefins < 0.01 Napthenes % Vol GC 4.65 Aromatics 0.03 > 200 C & Unidentified < 0.01 Poly-Naphthenes < 0.01 Note: *** Samples were blended with ASTM grade Iso Octane, and results were caluclated from the blend's result. Page 8

11 CUT RANGE C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD C Distillation of Crude Oil Yield % Wt Yield % Vol Cum. Yield % Wt Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated Sulphur Content % mass ASTM D Mercaptan Sulphur mg/kg ASTM D Research Octane Number *** ASTM D Motor Octane Number *** ASTM D PIONA analysis Total Paraffins Olefins < 0.01 Napthenes % Vol GC Aromatics 2.13 > 200 C & Unidentified < 0.01 Poly-Naphthenes < 0.01 Note: *** Samples were blended with ASTM grade Iso Octane, and results were caluclated from the blend's result. Page 9

12 CUT RANGE C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD C Distillation of Crude Oil Yield % Wt Yield % Vol Cum. Yield % Wt Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated Sulphur Content % mass ASTM D Mercaptan Sulphur mg/kg ASTM D PIONA analysis Total Paraffins Olefins < 0.01 Napthenes % Vol GC Aromatics > 200 C & Unidentified Poly-Naphthenes 5.97 Aniline Point C ASTM D Smoke Point mm IP Naphthalene content %Vol. ASTM D Freeze Point C ASTM D 2386 Below Page 10

13 CUT RANGE C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD C Distillation of Crude Oil Yield % Wt Yield % Vol Cum. Yield % Wt Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated Sulphur Content % mass ASTM D Mercaptan Sulphur mg/kg ASTM D Aniline Point C ASTM D Smoke Point mm IP Freeze Point C ASTM D Cloud Point C ASTM D 2500 Below -42 Kinematic 40 C mm 2 /S ASTM D 445 Kinematic 50 C Distillation ASTM D 86 See page 17 Cetane Index ASTM D Refractive 20 C ASTM D Page 11

14 CUT RANGE C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD C Distillation of Crude Oil Yield % Wt Yield % Vol Cum. Yield % Wt Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated Sulphur Content % mass ASTM D Mercaptan Sulphur mg/kg ASTM D Total Nitrogen % mass ASTM D 5291 (Mod) < 0.05 Aniline Point C ASTM D Cloud Point C ASTM D Pour Point (upper) C ASTM D Kinematic 40 C Kinematic 50 C mm 2 /S ASTM D Kinematic 80 C Distillation ASTM D 86 See page 17 Cetane Index ASTM D Refractive 20 C ASTM D Page 12

15 CUT RANGE C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD C Distillation of Crude Oil Yield % Wt Yield % Vol Cum. Yield % Wt Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated Sulphur Content % mass ASTM D Total Nitrogen % mass ASTM D 5291 (Mod) < 0.05 Aniline Point C ASTM D Cloud Point C ASTM D Pour Point (upper) C ASTM D 97-6 Kinematic 40 C Kinematic 50 C mm 2 /S ASTM D Kinematic 80 C Distillation ASTM D 86 See page 17 Cetane Index ASTM D Refractive 20 C ASTM D Page 13

16 CUT RANGE C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD C Distillation of Crude Oil Yield % Wt ASTM D 5236 Yield % Vol Cum. Yield % Wt. / ASTM D 5236 Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated Sulphur Content % mass ASTM D Total Nitrogen % mass ASTM D 5291 (Mod) 0.08 Aniline Point C ASTM D Cloud Point C ASTM D Pour Point (upper) C ASTM D Kinematic 40 C Kinematic 50 C mm 2 /S ASTM D Kinematic 80 C Distillation ASTM D 86 * Cetane Index ASTM D 976 * Note: * Unable to perform test due to the heavy nature of the fraction. Page 14

17 CUT RANGE C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD C Distillation of Crude Oil Yield % Wt ASTM D 5236 Yield % Vol Cum. Yield % Wt. / ASTM D 5236 Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated Sulphur Content % mass ASTM D Total Nitrogen % mass ASTM D 5291 (Mod) 0.15 Aniline Point C ASTM D Cloud Point C ASTM D 2500 ## Pour Point (upper) C ASTM D Kinematic 50 C Kinematic 80 C mm 2 /S ASTM D Kinematic 100 C Micro Carbon Residue % mass ASTM D Note: ## Unable to test due to the dark colour of the fraction. Page 15

18 CUT RANGE C Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April CUT RANGE TEST UNIT METHOD C + Distillation of Crude Oil Yield % Wt ASTM D 5236 Yield % Vol Cum. Yield % Wt. / ASTM D 5236 Cum. Yield % Vol C kg/l IP Specific 60/60 F Conversion API 60 F Calculated 6.45 Sulphur Content % mass ASTM D Total Nitrogen % mass ASTM D 5291 (Mod) 0.37 Vanadium (V) 112 Nickel (Ni) mg/kg IP 470 ( AAS ) 38 Iron (Fe) 15 Nickel / Vanadium Ratio Calculated 0.34 Pour Point (upper) C ASTM D Kinematic 100 C 3013 mm 2 /S ASTM D 445 Kinematic 150 C Micro Carbon Residue % mass ASTM D Asphaltene % mass IP Page 16

19 ASTM 86 - DISTILLATION DATA PER FRACTIONS Sample Descriptions / Label : Al Shaheen Crude Oil Ex Qatar sampled on 10th April Boiling range Yield on whole crude C Wt. % Vol.% Initial boiling point C ** 10% recovered C ** 20% recovered C ** 30% recovered C ** 40% recovered C ** 50% recovered C ** 60% recovered C ** 70% recovered C ** 80% recovered C ** 90% recovered C ** Final Boiling Point C ** Volume recovered % Vol ** Residue % Vol ** Loss % Vol ** Note: ** Unable to perform ASTM Distillation due to the heavy nature of the fraction. Page 17

20 LABORATORY REPORT NO. FCA/1025/06 Sample ID - Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006 Fraction's Mid B.P. Vs Density Density - (kg/l) C5-65 C C C C C C C C 15 C Fraction Page 18

21 LABORATORY REPORT NO. FCA/1025/06 Sample ID - Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006 Fraction's Mid B.P. Vs Sulphur Content Sulphur % mass C5-65 C C C C C C C C 560+ C Sulphur Fraction Page 19

22 LABORATORY REPORT NO. FCA/1025/06 Sample ID - Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006 Fraction's Mid B.P. Vs Nitrogen Content Nitrogen Content - % mass C C 560+ C Nitrogen Fraction Page 20

23 LABORATORY REPORT NO. FCA/1025/06 Sample ID - Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006 Fraction's Mid B.P. Vs Aniline Point Aniline Point - C C C C C C C Aniline Point Fraction Page 21

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