Annex to the Accreditation Certificate D PL according to DIN EN ISO/IEC 17025:2005

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1 Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D PL according to DIN EN ISO/IEC 17025:2005 Period of validity: to Holder of certificate: Haltermann Carless Deutschland GmbH Qualitätssicherungs Labor Werk Hamburg Schlengendeich 17, Hamburg Tests in the fields: chemical and physical chemical testing of mineral oil and related products, selected properties of gasoline fuel, diesel fuels, diesel fuels from fatty acid methyl ester (FAME); printing ink distillates Abbreviations used: see last page Within the fields marked with * the testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, the following: usage of different versions of standard test s granted here. The testing laboratory maintains a current list of all testing s within the flexible scope of accreditation. This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/19

2 1. Fuels 1.1 Gasoline* Density DIN Testing of mineral oils and related materials Determination of density procedure 3 (withdrawn) DIN EN ISO ASTM D Crude petroleum and petroleum products Determination of density Oscillating U tube Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter Distillation Characteristics DIN EN ISO ASTM D 86 Petroleum products Determination of distillation characteristics at atmospheric pressure Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure Vapor Pressure ASTM D 5191 DIN EN Standard Test Method for Vapor Pressure of Petroleum Products (Mini Method) Vapor Pressure part 1: Determination of air saturated vapor pressure (ASVP) and calculation of equivalent to dry vapor pressure (DVPE) Period of validity: to Translation 2/19

3 Content of Lead DIN EN ASTM D 3237 Determination of low contents lead by atomic absorption spectroscopy Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy Content of sulphur DIN EN ISO ASTM D 5453 Determination of sulfur content of automotive fuels Ultraviolet fluorescence Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultra violet Fluorescence evaporation residue DIN EN ISO ASTM D 381 DIN Evaporation residue of volatile and middle distillate fuels jet evaporation Standard Test Method for Gum Content in Fuels by Jet Evaporation Solvents for coating materials determination of evaporation residue corrosiveness DIN EN ISO corrosiveness to copper copper strip test Period of validity: to Translation 3/19

4 ASTM D 130 Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test content of benzene DIN EN DIN EN ISO ASTM D 6839 Determination of the benezene content by infrared spectrometry Determination of hydrocarbon types and oxygenates in automotive motor gasoline and in ethanol (E85) automotive fuel Multidimensional gas chromatography Standard Test Method for Hydrocarbon Types, Oxygenated Compounds and Benzene in Spark Ignition Engine Fuels by Gas Chromatography Oxygenates ASTM D 4815 DIN EN ISO Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary Amyl Alcohol and C1 to C4 Alcohols in Gasoline by Gas Chromatography (withdrawn standard) Determination of hydrocarbon types and oxygenates in automotive motor gasoline and in ethanol (E85) automotive fuel Multidimensional gas chromatography Period of validity: to Translation 4/19

5 ASTM D 6839 ASTM D 5501 Standard Test Method for Hydrocarbon Types, Oxygenated Compounds and Benzene in Spark Ignition Engine Fuels by Gas Chromatography Standard Test Method for Determination of Ethanol and Methanol Content in Fuels containing greater 20 % Ethanol by Gas Chromatography Hydrocarbon types DIN EN ISO ASTM D 6839 Determination of hydrocarbon types and oxygenates in automotive motor gasoline and in ethanol (E85) automotive fuel Multidimensional gas chromatography Standard Test Method for Hydrocarbon Types, Oxygenated Compounds and Benzene in Spark Ignition Engine Fuels by Gas Chromatography ASTM D ISO Corrigendum Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption Liquid petroleum products Determination of hydro carbon types fluorescent indicator adsorption Neutralization number DIN ASTM D Testing of mineral oil Determination of neutralization number, colour indicator titration Standard Test Method for Acid and Base Number by Color Indicator Titration Period of validity: to Translation 5/19

6 n heptane, i octane und toluene ASTM D (reapproved ) Standard Test Method for Analysis of High Purity n Heptane and Isooctane by Capillary Gas Chromatography ASTM D Standard Test Method for Trace Impurities in Mono cyclic Aromatic Hydrocarbons by Gas Chromatography water content DIN EN ISO ASTM D ASTM E 1064 Determination of water Coulometric Karl Fischer titration Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration Calculation of net heat of combustion ASTM D 3338/D 3338M 2009 (reapproved: 2014) Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels Calculation of hydrogen content ASTM D (reapproved 2010) Standard Test Method for Estimation of Hydrogen Content of Aviation Fuels Period of validity: to Translation 6/19

7 Refractive Index Measurement DIN DIN measurement of relative refractive index by precision refractometer Testing of mineral oils part 2: measurement of relative refractive index by abberefractometer GC Composition DIN ASTM D 5580 ASTM D 5134 Testing of mineral oil hydrocarbons, similar liquids and solvents for paints and varnishes Analysis by gas chromatography General working principles Standard Test Method for Determination of Benzene, Toluene, Ethylbenzene, p/m Xylene, o Xylene, C9 and Heavier Aromatics, and Total Aromatics in Finished Gasoline by Gas Chromatography Standard Test Method for Detailed Analysis of Petroleum Naphthas through n Nonane by Capillary Gas Chromatography (Benzene and n Hexane Content) Miscellaneous ISO ASTM D 3703 ASTM D General for determination of chloride ions Potentiometric Standard Test Method for Hydroperoxide Number of Aviation Turbine Fuels, Gasoline and Diesel Fuels Standard Test Method for Oxidation Stability of Spark Ignition Fuel Rapid Small Scale Oxidation Test (RSSOT) (withdrawn) Period of validity: to Translation 7/19

8 DIN ISO Clear liquids Estimation of colour by the platinum cobalt colour scale 1.2 Diesel Fuel* Density DIN Testing of mineral oils and related materials Determination of density procedure 3 DIN EN ISO ASTM D Crude petroleum and petroleum products Determination of density Oscillating U tube Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter Distillation Characteristics DIN EN ISO ASTM D 86 Petroleum products Determination of distillation characteristics at atmospheric pressure Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure Period of validity: to Translation 8/19

9 Viscosity DIN EN ISO ASTM D Petroleum products Transparent and opaque liquids Determination of kinematic viscosity and calculation of dynamic viscosity Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) (withdrawn standard) Flash Point ASTM D 93 DIN EN ISO Standard Test Methods for Flash Point by Pensky Martens Closed Cup Tester (withdrawn standard) Determination of flash point Pensky Martens closed cup Sulphur Content DIN EN ISO ASTM D 5453 Determination of sulfur content of automotive fuels Ultraviolet fluorescence Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence Cold Filter Plugging Point (CFPP) ASTM D (reapproved 2010) DIN EN Standard Test Method for Cold Filter Plugging Point of Diesel and Heating Fuels Determination of cold filter plugging point Stepwise cooling bath Period of validity: to Translation 9/19

10 Cloud Point DIN EN ISO ASTM D Petroleum products determination of cloud point Petroleum products Determination of cloud point Standard Test Method for Cloud Point of Petroleum Products Pour Point DIN ISO ASTM D 97 ASTM D (reapproved: 2014) Petroleum products Determination of pour point Standard Test Method for Pour Point of Petroleum Products Standard Test Method for Pour Point of Petroleum Products (Robotic Tilt Method) Carbon Residue DIN EN ISO ASTM D Determination of carbon residue Micro (withdrawn) Standard Test Method for Determination of Carbon Residue (Micro Method) Water Content DIN EN ISO Determination of water Coulometric Karl Fischer titration Period of validity: to Translation 10/19

11 ASTM D ASTM E 1064 Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration Neutralization Number ASTM D Standard Test Method for Acid and Base Number by Color Indicator Titration Cetane Index DIN EN ISO ASTM D ASTM D (reapproved 2011) Calculation of cetane index of middledistillate fuels by the four variable equation Standard Test Method for Calculated Cetane Index by Four Variable Equation in Verbindung mit: und Standard Test Method for Calculated Cetane Index of Distillate Fuels Corrosiveness DIN EN ISO ASTM D 130 Petroleum products Corrosiveness to copper Copper strip test (ISO 2160:1998) Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test Period of validity: to Translation 11/19

12 Total Contamination DIN EN Determination of total contamination in middle distillates, diesel fuels and fatty acid methyl esters Lubricity DIN ISO ASTM D Assessment of lubricity using the highfrequency reciprocating rig (HFRR) Part 1: Test Standard Test Method for Evaluating Lubricity of Diesel Fuels by the High Frequency Reciprocating Rig (HFRR) Cetane and 1 Methylnaphthalene DIN Determination of purity by gaschromategraphy part 2: cetane and 1 methylnaphthalene Aromatic Hydrocarbons DIN EN Determination of aromatic hydrocarbon types in middle distillates High performance liquid chromatography with refractive index detection FAME DIN EN Determination of fatty acid methyl ester (FAME) content in middle distillates Infrared spectrometry Period of validity: to Translation 12/19

13 Calorific Value ASTM D 3338/D 3338M 2009 (reapproved: 2014) Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels Hydrogen Content ASTM D (reapproved 2010) Standard Test Method for Estimation of Hydrogen Content of Aviation Fuels Oxidation Stability DIN EN DIN EN ISO DIN EN ASTM D ASTM D Fatty acid methyl ester (FAME) fuel and blends with diesel fuel Determination of oxidation stability by accelerated oxidation Determination of the oxidation stability of middle distillate fuels Middle distillates and fatty acid methyl ester (FAME) fuels and blends Determination of oxidation stability by rapid small scale oxidation Standard Test Method for Oxidation Stability of Middle Distillate Fuels Rapid Small Scale Oxidation Test (RSSOT) Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method) Conductivity ASTM D Standard Test Methods for Electrical Conductivity of Aviation and Distillate Fuels (withdrawn standard) Period of validity: to Translation 13/19

14 DIN Determination of electrical conductivity part 1: laboratory Refractive Index Measurement DIN DIN measurement of relative refractive index by precision refractometer Testing of mineral oils part 2: measurement of relative refractive index by abberefractometer GC Composition DIN Testing of mineral oil hydrocarbons, similar liquids and solvents for paints and varnishes Analysis by gas chromatography General working principles Aniline Point DIN ISO Determination of aniline point and mixed aniline point Period of validity: to Translation 14/19

15 Peroxid Number ASTM D 3703 DIN EN Anhang C Standard Test Method for Hydroperoxide Number of Aviation Turbine Fuels, Gasoline and Diesel Fuels Calculation of saturated monoglycerides content in diesel fuels by EN 590 in combination with: DIN EN Determination of monoglyceridecontent DIN EN Determination of cloudpoint FAME Period of validity: to Translation 15/19

16 1.3 Diesel Fuel from Fatty Acid Methylester (FAME) * Ester Content DIN EN Determination of ester and linolenic acid methyl ester contents (withdrawn standard) Density DIN EN ISO DIN Crude petroleum and petroleum products Determination of density Oscillating U tube Testing of mineral oils and related materials Determination of density procedure 3 Viscosity DIN EN ISO Petroleum products Transparent and opaque liquids Determination of kinematic viscosity and calculation of dynamic viscosity Sulphur Content DIN EN ISO ASTM D 5453 Determination of sulfur content of automotive fuels Ultraviolet fluorescence Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultra violet Fluorescence Period of validity: to Translation 16/19

17 Water Content DIN EN ISO Determination of water Coulometric Karl Fischer titration Total Contamination DIN EN Determination of total contamination in middle distillates, diesel fuels and fatty acid methyl esters Corrosiveness DIN EN ISO corrosiveness to copper copper strip test Oxidation Stability DIN EN Determination of oxidation stability (accelerated oxidation test) Acid DIN EN Determination of acid value Iodine Value DIN EN DIN EN Determination of iodine value Determination of iodine value in fatty acid methyl esters (FAME) Calculation from gas chromatographic data Period of validity: to Translation 17/19

18 Methanol DIN EN Determination of methanol content Content of free and total Glycerol and Mono, Di, Triglyceride / / DIN EN Determination of free and total glycerol and mono, di, triglyceride contents Cold Filter Plugging Point (CFPP) DIN EN Determination of cold filter plugging point Cloud Point DIN EN DIN EN Anhang C Petroleum products; determination of cloud point Calculation of saturated monoglycerides content in FAME in combination with: DIN EN Determination of monoglyceride content DIN EN Determination of cloudpoint FAME Period of validity: to Translation 18/19

19 2. Printing Ink Distillates * Density DIN EN ISO Crude petroleum and petroleum products Determination of density Oscillating U tube Aniline Point DIN ISO Determination of aniline point and mixed aniline point Abbreviations used: ASTM FAME ISO Process Matrix American Society for Testing and Materials fatty acid methyl ester (Fettsäuremethylester) International Organization for Standardization Number of the characteristics within the Process Matrix for Mineral Oel (72 FB Version 01, March ) Period of validity: to Translation 19/19

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