Chlorinated polyethylene ELASLEN TM. Application for Wire and Cable

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1 Chlorinated polyethylene ELASLEN TM Application for Wire and Cable 1

2 About the company Company Name : SHOWA DENKO K.K. Type of Industry : Diversified Chemical Company Formed : June 1, 1939 Employee : 10,577 (in December 31, 2014) Capital : 141 billion JPY (as of December 31, 2014) *1.0 billion Euro, 1.2 billion US$ Net Sales : 878 billion JPY (in 2014) *6.5 billion Euro, 7.6 billion US$ Business Sectors : Petrochemicals, Chemicals, Inorganic Materials, Aluminum, Electronics 2

3 Our CPE Business Product Name : ELASLEN TM Chemical Name : Chlorinated Polyethylene HS Code Number : Start of Sales : Oct Production Capacity : 5000MT/Y Quality Control Program : ISO 9001 Environmental Control Program : ISO

4 Global Locations Head Quarters: Tokyo (Japan) Plant Location: Kawasaki City (Japan) Sales Offices: Munich (Germany), New York (USA), Singapore (Singapore), Shanghai (China), Soul (Korea) 4

5 What is ELASLEN TM? ELASLEN is the product name of our Chlorinated Polyethylene. ELASLEN is a thermoplastic polymer, manufactured by chlorinating high density polyethylene. ELASLEN has excellent flexibility, weatherability, heat aging resistance, flame retardancy and chemical resistance. 5

6 Applications Modifier:Soft & Rigid PVC, FR-ABS, FR-PE (Wire & Cable) Rubber :Wire & Cable Jacket, Hose & Boots for Automotive, Rubber for Construction, Magnetic rubber TPE :FR-TPE 6

7 Comparison with Other Rubbers Item CPE CSM CR EPDM NBR Flame Retardancy Excellent Good Good Poor Poor Oil Resistance Excellent Good Good Poor Excellent Ozone Resistance Weather Resistance Excellent Excellent Fair Excellent Poor Excellent Excellent Fair Excellent Poor Heat Resistance Good Good Fair Excellent Fair Electrical Insulation Excellent Good Fair Excellent Fair Coloring Excellent Excellent Poor Fair Poor 7

8 A Wide Variety of Grades We can produce any custom-made grade by adjusting these 3 factors Chlorine Content From 23% to 45% From very low MW to extremely high MW Molecular Weight Crystallinity From non-crystallinity to high crystallinity 8

9 Three Factors of ELASLEN TM Flame retardancy Chemical resistance Mechanical strength Heat aging resistance Chlorine Content Molecular Weight Crystallinity 9

10 Molecular Weight Grade Map of ELASLEN TM Chlorine content vs Molecular Weight Heat Resistance Low Temp Property Flame Retardancy Oil Resistance Ultra High 301MA 301MB 451MB Mechanical Strength Heat Resistance Oil Resistance High 301AS 351AYS 401AY Medium 202KB 252B 302NAC 352GB 352NA 402NA 402B Low 303A 353A 303BS 303C 404B Chlorine Content (wt%) 45 Processability Compatibility 10

11 Crystallization Grade Map of ELASLEN TM Chlorine content vs Crystallization Heat Resistance Low Temp Property Flame Retardancy Oil Resistance 80J/g 70J/g 60J/g 50J/g 40J/g 30J/g 20J/g 10J/g Non-Crystallization < 2J/g 202KB 252B 303C 303BS 404B 301MB 352GB 402B 301AS 302NAC 351AYS 301MA 352NA 401AY 303A 353A 402NA Chlorine Content (wt%) 451MB 45 Mechanical Strength Heat Resistance Flexibility Filler acceptance 11

12 Grade List of ELASLEN TM Non Crystallinity Standard Items Unit Test Method 301MA 301AS 351AYS 401AY 302NAC 352NA 402NA 303A 353A Chlorine content % SDK method Crystallinty J/g SDK method <2 <2 <2 <2 <2 <2 <2 <2 <2 Specific Gravity - JIS K Melt Flow Rate(*) g/10min JIS K Mooney Viscosity ML1+4(121 ) JIS K Tensile Strength Mpa JIS K Elongation % JIS K % Modulas Mpa JIS K Brittle Temp JIS K6261 <-70 <-70 <-70 <-70 < <-70 <-70 Hardness JIS-A JIS K Volume Resistivity Ω-cm ASTM D (*)Measured at 180 under the load of 21.6kgf. Cable Jacket A M A M A Application Rigid PVC Modifier A M M A A A Flexible PVC Modifier A M A M: Most suitable A: Applicable TPE FR ABS Modifier Rubber Magnetic Rubber A A M A A M M A M M A M M A A A The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom. 12

13 Grade List of ELASLEN TM Semi Crystallinity Standard Specialty Items Unit Test Method 252B 303BS 303C 301MB 352GB 404B 451MB 202KB 402B Chlorine content % SDK method Crystallinty J/g SDK method Specific Gravity - JIS K Melt Flow Rate(*) g/10min JIS K Mooney Viscosity ML1+4(121 ) JIS K Tensile Strength Mpa JIS K Elongation % JIS K % Modulas Mpa JIS K Brittle Temp JIS K Hardness JIS-A JIS K Volume Resistivity Ω-cm ASTM D (*)Measured at 180 under the load of 21.6kgf. Cable Jacket M A M A M M M Rigid PVC Modifier A A Application M: Most suitable A: Applicable Flexible PVC Modifier TPE FR ABS Modifier Rubber A A M A A A A A A M M A M A A M M M Magnetic Rubber The information contained herein is believed to be reliable, but no representations, guarantees or warranties of 13 any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom.

14 Metallic Content Metallic Analysis (ppm) The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom. 14

15 Insulation Properties Formulation : CPE Tribasic lead sulphate 100phr 2phr Test Method : Immersion in 75 hot water 0~1000Hr (500V) Ω-cm) The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom. 15

16 Application for Wire Harness ELASLEN is used as a modifier for semi-rigid PVC wire harness Formulation To improve low temperature properties (Brittle Temp. etc.) To reduce the amount of plasticizer and prevent bleeding of it A B C PVC (p=1300) Stabilizer Plasticizer (TOTM) ELASLEN 401AY 10 Physical Properties Good! Brittle Temp. Celsius degree Hardness (Durometer D) Specific Gravity Yield Strength MPa Tensile Strength MPa Elongation %

17 Various Wire & Cable Applications ELASLEN has been used for these various wire & cable application (1) Rubber wire & cable jacketing requiring oil & heat resistance and flame retardancy (2) Insulated (Crosslinked) polyethylene wire & cable jacketing requiring flame retardancy and electrical properties Application Composition Elaslen Grade Transportation cable Insulation : EPDM /Jacket : CPE 401AY, 402B Polymer Blended EPDM Requirements for Elaslen FR, Oil resistance, Flexibility Vehicle cable Insulation : LDPE /Jacket : CPE 404B, 202KB, 402B LDPE FR, Chemical resistance, Flexibility Industrial power cable Single Layer with CPE 401AY, 402NA, 351AYS EPDM, EVA FR, Oil resistance, Flexibility Portable cord Single Layer with CPE 401AY, 402NA, 351AYS EPDM, EVA FR, Heat resistance, Flexibility Plug cord(for automobile) Single Layer with CPE 401AY, 402NA EPDM, EVA FR, Oil & heat resistance Telecommunication cable FR-PE Insulation(CPE Blended) 404B LDPE, HDPE FR, Flexibility Telecommunication cable PVC Insulation (CPE Blended) 401AY PVC Low temp Property, Plasticizer Power cable/semi-conductor PE/CPE/Carbon 401AY EVA Strippability Electronics wire FR-XLPE Insulation(CPE Blended) 202KB, 303BS, 404B EVA, LDPE FR, Electrical property PMMA optical fiber Core :PMMA /Jacket :CPE(FR-PE) 404B, 303BS LDPE FR, Zero plasticizer 17

18 Standard Formulation For crosslinked rubber wire & cable with ELASLEN Standard formulation Physical properties Ingredients Details Parts Test items Unit Elaslen(CPE) Polymer Blended Inorganic filler Flame Retardant aid Inorganic FR Organic FR Plasticizer Stabilizer Antioxidant Lubricant Crosslinking co-agent Chlorine Content 34~40wt% EPDM,EVA,etc Talc,Clay,etc Al(OH)3,Mg(OH)2 Sb203 (Antimony trioxide) Chlorinated paraffin Esters(DOP,DIDP,TOTM,etc) Magnesium oxide,hydrotalcite, Lead compounds, Thioethers, Hindered phenols Fatty acids,fatty acid amides TAIC,TAC 50~100 0~ 50 30~100 20~100 3~ 8 2~ 5 10~ 35 5~ ~ ~ ~3.0 Mooney viscosity(ml ) Scorch time Tensile strength Elongation Hardness(JIS-A) (ML ) Heat aging resistance Point min Mpa % Point Measurment s 30~ 55 10~ ~180 >300 65~ Hr~150 96Hr Tensile strength retention % > 80 Elongation retention Change in hardness Crosslinking agent Peroxide 1.5~3.0 Elongation retention *Zinc and red iron oxide should not be used in formulation. % Point > 80 <+10 Oil resistance tested with ASTM No Hr Tensile strength retention % > 80 Change in hardness Oxygen index Volume resistivity Specific gravity % Point Point Ω cm > 80 <+10 25~30 5 E13~8 E14 1.2~1.6 The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom. 18

19 Starting Formulation For high mechanical strength and heat resistance Standard formulation Physical properties Ingredients Details Parts Test items Unit Measurements CPE: Elaslen 401AY Chlorine Content 40wt% 32 Tensile strength MPa 22.0 CPE: Elaslen 402NA Chlorine Content 40wt% 8 100% Modulas MPa 6.0 EVA 40 Elongation % 325 EPDM 20 Hardness(JIS-A) Point 85 Inorganic filler Talc 26 Heat aging resistance Hr Inorganic FR Antimony Trioxide 8 Tensile strength retention % 90 Stabilizer Hydrotalcite or Lead Stabilizers 4 Elongation retention % 90 Antioxidants 1.5 Change in hardness Point +2 Epoxy Plasticizers 2 Oxygen Index Point 27 Lubricant Fatty acid amides 1 Volume resistivity(500v,23 ) Ω cm 1.0 E14 Crosslinking agent Peroxide 1.5 Crosslinking co-agent Taic 1.2 Carbon Black HAF Carbon 3 *Zinc and red iron oxide should not be used in formulation. The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom. 19

20 Starting Formulation For flexibility & heat resistance (Portable Cord) Standard formulation Physical properties Ingredients Details Parts Test items Unit Measurements CPE: Elaslen 401AY Chlorine Content 40wt% 70 Tensile strength MPa 16.2 EPDM % Modulas MPa 3.0 Plasticizer 20 Elongation % 540 Inorganic filler Talc 65 Hardness(JIS-A) Point 70 Inorganic FR Antimony Trioxide 8 Heat aging resistance Hr Stabilizer Hydrotalcite or Lead Stabilizers 10 Tensile strength retention % 100 Metal Oxide 8 Elongation retention % 85 Antioxidants 3 Change in hardness Point +10 Lubricant Fatty acid amides 2 Oxygen Index Point 28 Crosslinking agent Peroxide 6 Volume resistivity(500v,23 ) Ω cm 1.0 E13 Crosslinking co-agent Taic 3 Carbon Black HAF Carbon 5 *Zinc and red iron oxide should not be used in formulation. The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom. 20

21 Starting Formulation For high heat resistance (Transit Cable) Standard formulation Physical properties Ingredients Details Parts Test items Unit Measurements CPE: Elaslen 202KB Chlorine Content 23wt% 50 Tensile strength MPa 15.0 EVA % Modulas MPa 7.4 Inorganic filler Talc 26 Elongation % 570 Inorganic FR Antimony Trioxide 10 Hardness(JIS-A) Point 91 Stabilizer Hydrotalcite/Metal Oxide 15 Heat aging resistance Hr Antioxidants 4 Tensile strength retention % 91 Lubricant Fatty acid amides 1 Elongation retention % 87 Crosslinking agent Peroxide 1.5 Change in hardness Point +1 Crosslinking co-agent Taic 2 Oxygen Index Point 24 Carbon Black HAF Carbon 3 Volume resistivity(500v,23 ) Ω cm 2.0 E14 *Zinc and red iron oxide should not be used in formulation. The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom. 21

22 Starting Formulation For high flame-retardant & oil resistance Standard formulation Physical properties Ingredients Details Parts Test items Unit Measureme nts CPE: Elaslen 402B Chlorine Content 40wt% 70 Tensile strength Mpa 19.0 EVA VA contents 25% % Modulas Mpa 7.0 Inorganic filler Clay 25 Elongation % 400 Inorganic FR Sb 20 3 (Antimony trioxide) 8 Hardness(JIS-A) Point 87 Stabilizer Tribasic lead sulphate 5 Heat aging resistance Hr Pb-st 0.3 Tensile strength retention % 90 Antioxidant Hindered phenols 0.5 Elongation retention % 90 Crosslinking co-agent TAIC 1.5 Change in hardness Point +3 Crosslinking agent Peroxide:1min half-valued period 3 0il resistance (ASTM No2oil 70 4Hr) 175 ~ 185 Tensile strength retention % 97 Carbon Black HAF Carbon 3 Elongation retention % 97 Change in hardness Point -7 *Zinc and red iron oxide should not be used in formulation. Oxygen Index - 30 Volume resistivity(500v,23 ) Ω cm 2.0 E14 The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained therefrom. 22

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