critical supplies Consumables and Accessories 2002 Catalog for your analytical instrument Atomic Absorption Inductively Coupled Plasma OES and MS

Transcription

1 Inorganic Analysis Chromatography Molecular Spectroscopy Thermal Analysis Informatics Consumables and Accessories 2002 Catalog critical supplies for your analytical instrument Atomic Absorption Inductively Coupled Plasma OES and MS Liquid Chromatography Gas Chromatography UV Visible, Fluorescence, and Polarimetry Thermal and Elemental Analysis Infrared Spectroscopy

2 Ordering Information How to Order US IN THE U.S. IN CANADA RETURN GOODS POLICY Order Online Place your order online at essentials. Online ordering currently is available in the U.S., Puerto Rico, and Canada. Call Toll Free Monday through Friday from 8:00 a.m. to 7:00 p.m. EST. Fax Us Your Order Fax your company Purchase Order to Us Your Order Visit our Web site at or us at Mail Us Your Order Mail your company Purchase Order to: PerkinElmer Instruments 710 Bridgeport Avenue M/S 270 Shelton, CT Visa, MasterCard, and American Express are accepted. Order Online Place your order online at essentials. Online ordering currently is available in the U.S., Puerto Rico, and Canada. Call Toll Free Monday through Friday from 8:30 a.m. to 5:00 p.m. EST. Fax Us Your Order Fax your company Purchase Order to Us Your Order Visit our Web site at or us at Mail Us Your Order Mail your company Purchase Order to: PerkinElmer Canada 501 Rowntree Dairy Road Unit 6 Woodbridge, ON Canada L4L 8H1 Before returning any item to PerkinElmer, please obtain a Return Authorization Number from a customer service representative. Call toll free in the U.S. or in Canada. Please have the following information ready: 1. Our Order Number or your Purchase Order Number. 2. The PerkinElmer part numbers of the items that you wish to return. 3. Reason for return. Our customer service representative will provide you with an RMA number and the return address.we cannot accept any returns without an RMA number. TECHNICAL SUPPORT Call toll free in the U.S. or in Canada. 8:30 a.m. to 5:00 p.m. EST. OUTSIDE THE U.S. & CANADA Contact your local sales office. A full list of Worldwide Support numbers follows the Table of Contents. Chiller for ICP/ICP-MS page ICP-5 Deuterium Lamp page LC-13 NewGuard Column pages LC-32 and LC-33 NCI 901/902 Interfaces page GC-46 THGA Graphite Tubes page 0

3 Canada Table of Contents SECTION PAGE AA Atomic Absorption ICP Inductively Coupled Plasma OES and MS LC Liquid Chromatography GC Gas Chromatography UV UV Visible, Fluorescence, and Polarimetry AA-1 to 1 ICP-1 to ICP-32 LC-1 to LC-49 GC-1 to GC-98 UV-1 to UV-19 FLR-20 to FLR-28 PLR-29 Lumina Hollow Cathode Lamps pages to AA-4 Headspace Septa page GC-3 TEA Deuterium Lamp page UV-19 Thermal and Elemental Analysis TEA-1 to TEA-44 IR Infrared Spectroscopy IR-1 to IR-20 Index IND-1 to IND-22 Aluminum Sample Pans and Covers page TEA-4 Terms and Conditions TC-1 to TC-4 IR Cells and Windows page

4 Worldwide Support US Austria Tel: Fax: Australia Melbourne Tel: Fax: Argentina Tel: Fax: Belgium Tel: Fax: Bolivia Tel: Fax: Brazil Tel: Fax: Canada Tel: Fax: CIS Tel: Fax: Chile Tel: Fax: China Beijing Tel: Fax: Columbia Tel: Fax: Costa Rica Tel: Fax: Czech Rep. Tel: Fax: Denmark Tel: Fax: Ecuador Tel: Fax: Egypt Tel: Fax: El Salvador Tel: Fax: Finland Tel: Fax: France Tel: Fax: Germany Tel: Fax: Guatemala Tel: Fax: Honduras Tel: Fax: Hong Kong Tel: Fax: Hungary Tel: Fax: India Tel: Fax: Indonesia Tel: Fax: Italy Tel: Fax: Japan Yokohama Tel: Fax: Japan Osaka Tel: Fax: Korea Tel: Fax: Luxembourg Tel: Fax: Malaysia Tel: Fax: Mexico Tel: Fax: The Netherlands Tel: Fax: Nicaragua Tel: Fax: Norway Tel: Fax: Panama Tel: Fax: Poland Tel: Fax: Philippines Tel: Fax: Singapore Tel: Fax: South Africa Tel: Fax: Spain Tel: Fax: Sweden Tel: Fax: Switzerland Tel: Fax: Taiwan Tel: Fax: Thailand Tel: Fax: United Kingdom Tel: Fax: United States Tel: Fax:

5 e-ssential supplies for Thermal and Elemental Analysis As innovators in developing thermal analysis systems, PerkinElmer gives the leading-edge R&D and routinely demanding QA/QC labs the speed and accuracy you seek, and the productivity and reliability you need. Built on PerkinElmer s 40 years of experience in the industry, PYRIS Thermal Analysis instrumentation provides answers researchers need to solve even their toughest problems. With over 30 years of experience as a leader in organic elemental analysis, PerkinElmer s 2400 Series Analyzers offer speed, precision, ease-of-use, and proven performance. PYRIS Diamond DSC

6 Top selling e-ssentials for Thermal and Elemental Analysis Aluminum Sample Pans and Covers Aluminum sample pans and covers are designed to have very small thermal resistance contributing to superior thermal conductivity and temperature control. Due to the high thermal conductivities of aluminum, heat transfer is maximized, so that sample size can be minimized. See page TEA-3 for our complete listing of sample pans and covers (400 of each) TEA-3 DSC Universal Crimper Press The Universal Crimper Press provides high-quality sample crimping for the autosampler sample pans and can crimp the standard aluminum pans, O-Ring sealed large-volume stainless steel pans, and the 20 µl volatile sample pans. Includes the standard sample pan manipulator and inserts to seal 10, 30, and 50 µl autosampler sample pans. B TEA-6 PYRIS Diamond DSC/PYRIS 1 DSC Intracooler 2P The Intracooler 2P is a subambient device that automatically controls the flow of coolant through a circulating chamber attached to the PYRIS 1 DSC or Diamond DSC analyzers. The Intracooler 2 permits operation of all analyzers from -65 C. See page TEA-9 for our full selection of Intracoolers for the PYRIS 1 DSC, PYRIS 6 DSC, DSC 7, TMA 7, or DMA 7 analyzers. 115 V, 50/60 Hz N TEA V, 50/60 Hz N Thermal Analysis Gas Station The Thermal Analysis Gas Station provides full control of all gases used in thermal analysis. In addition to performing gas switching, it also fully controls the gas flow rate, and detects rapid changes in pressure and empty cylinders. The Thermal Analysis Gas Station controls up to four purge gases, uses calibrated massflow controls, and is simple to program. N TEA-34 QUICK FIND INDEX DSC Sample Pans and Crimpers DSC Supplies and Accessories MP,Tg, and Structure of Common Polymers Ultramicrobalance Supplies TGA Supplies and Accessories Thermal Analysis Software DTA Supplies and Accessories DMA Measuring Systems, Replacement Parts, and Accessories TMA Measuring System Probes and Sample Tubes DMA/TMA Supplies and Accessories Gas Regulators Purge Flow Accessories Traps and Fittings Elemental Analysis Supplies and Accessories TEA-1 TEA-7 TEA-13 TEA-14 TEA-15 TEA-19 TEA-22 TEA-23 TEA-31 TEA-32 TEA-33 TEA-34 TEA-36 TEA-37 Large Volume Stainless Steel Pans, Covers, and O-Rings Capsules contain samples in a sealed environment throughout the experiment. The Viton O-Ring suppresses vaporization and eliminates the interfering effects of heat. Sealed capsules prevent any mass loss, high internal pressure capability allows water samples to be heated higher than 100 C and large sample capacity yields higher sensitivity TEA-4

7 Differential Scanning Calorimeter (DSC) Canada The most recent advances in microcomputer and microelectronic technologies have been incorporated into the newest DSC design from PerkinElmer, the PYRIS Diamond DSC Differential Scanning Calorimeter. Power Compensated DSC uses two independent furnaces, one for the sample and one for the reference. When an exothermic or endothermic change occurs in the sample material, energy is applied to or removed from one or both furnaces to compensate for the energy change occurring in the sample. This means that the system at all times directly measures energy flow to or from a sample. The PYRIS Diamond DSC features: Fastest heating and cooling rates Outstanding resolution Increased sensitivity True isothermal measurements High caloric accuracy The PYRIS 6 DSC is an ideal instrument for quality assurance/quality control and university laboratories. It performs routine experiments to characterize materials, predict product performance, optimize processing conditions, and improve quality. The PYRIS 6 DSC features: Exceptional value and performance Exceptional robustness and reliability Simple, inexpensive operation Space-saving footprint Easy-to-use Windows -based software With thousands of DSCs installed worldwide, PerkinElmer DSCs are recognized for their superior temperature control and H measurements. TEA-1 PYRIS 6 DSC PYRIS Diamond DSC

8 TEA-2 DSC Sample Pans and Crimpers DSC Sample Pan Chart US Operating Volume Crimper/Sealer Sample Pan Range (µl) Pressure Quantity Number Standard Aluminum* -170 C to 600 C Ambient TEA Standard Copper* -170 C to 730 C Ambient TEA Standard Gold* -170 C to 730 C Ambient TEA Alumina -170 C to 730 C Ambient N TEA-3 Not Required Platinum -170 C to 730 C Ambient TEA-3 Not Required Graphite -170 C to 730 C Ambient TEA-3 Not Required Stainless Steel/O-Ring* -40 C to 300 C Atm TEA Volatile Aluminum* -170 C to 600 C 20 2 Atm TEA Volatile Aluminum* (Pierced) -170 C to 600 C 20 Ambient N TEA-4, 18, Volatile Gold* -170 C to 730 C 20 2 Atm TEA Original High Pressure Stainless Steel -170 C to 400 C Atm TEA-5 Not Available Original High Pressure Gold-plated -170 C to 400 C Atm TEA-5 Not Available High Pressure Stainless Steel -170 C to 400 C Atm B TEA-5 B High Pressure Gold-plated -170 C to 400 C Atm B TEA-5 B High Pressure Titanium -170 C to 400 C Atm B TEA-5 B DPA C to 600 C 12.5 Ambient B TEA-13 Not Required Autosampler Aluminum -170 C to 600 C 10 1 Atm B TEA-6 B Autosampler Aluminum -170 C to 600 C 30 1 Atm B TEA-6 B Autosampler Aluminum -170 C to 600 C 50 1 Atm B TEA-6 B B Autosampler Aluminum (vented) -170 C to 600 C 30 1 Atm B TEA-6 B Autosampler Aluminum (vented) -170 C to 600 C 50 1 Atm B TEA-6 B Autosampler Gold -170 C to 730 C 50 1 Atm B TEA-6 B Autosampler Aluminum -170 C to 600 C 10 2 Atm B TEA-6 B Autosampler Aluminum -170 C to 600 C 30 2 Atm B TEA-6 B Autosampler Aluminum -170 C to 600 C 50 2 Atm B TEA-6 B *These pans may also be crimped using the Universal Crimper Press (B ), with the appropriate sealing insert. Please see page TEA-7. The 12.5 µl Aluminum Pan requires sealing insert (B ).

9 Canada DSC Sample Pans and Crimpers Standard and Specialty Sample Pans TEA-3 Standard Sample Pans and Crimper Press Standard sample pans are available in aluminum, copper, or gold. PerkinElmer offers sample pans to satisfy the needs of most thermal analysts. The sample is completely enclosed in a highly conductive capsule and distributed in a thin layer such that the internal resistance in the sample itself is very small. Sample pan material and sample holder design have very small thermal resistance. This contributes to a superior thermal conductivity and temperature control between the sample and sample pan. Due to the high thermal conductivities of aluminum, copper and gold, heat transfer is maximized. This means that sample size can be minimized. Because of their high-temperature capabilities, platinum and gold can be used to 730 C. Aluminum Sample Pans and Covers Used with nonvolatile solid samples, such as plastics and polymers. Routinely used for applications such as polymer melting, crystallization, glass transitions of polymers, thermoplastics, and thermosets. Pans are crimped but not hermetically sealed (400 of each) Copper Sample Pans and Covers Can be used for samples that have transitions that occur above the temperature range of the Al pans. Typical applications include antioxidant testing, thermoset and thermoplastic glass transition, and melting point determinations (200 of each) Gold Sample Pans and Covers Used for any non-metal, i.e., ceramics, coal, soils, or minerals. Can also be used for any material that reacts with aluminum or which must be heated over 600 C (10 of each) Standard Sample Pan Crimper Press Used to crimp covers on standard DSC pans of aluminum, gold, and copper. Design incorporates a replaceable crimper head Replacement Crimper Head Specialty Sample Pans Alumina Sample Pans and Covers Used for oxidation studies of metals, minerals, ceramics, clays, and soils. They can also be used for melting and eutectic diagrams in the metals industry. The covers are pierced. A crimper is not required. N (6 of each) Platinum Sample Pans and Covers Use these pans and covers when gold and graphite pans and covers are not suitable. Used to analyze mineral, soil, and ceramic samples. They are also used to allow a chemical reaction where platinum acts as a catalyst. They are easy to clean and reusable. A crimper is not required (4 of each) Graphite Sample Pans and Covers Use in an inert atmosphere. They are primarily used with metals, but not for oxidation studies. They have extremely good heat transfer properties which yield sharp transition curves. A crimper is not required (4 of each)

10 TEA-4 DSC Sample Pans and Crimpers Large Volume and Volatile Sample Pans US LARGE VOLUME O-RING SEALED STAINLESS STEEL PANS Capsules contain the sample in a sealed environment throughout an experiment. The Viton O-Ring allows formation of a seal which suppresses the vaporization of a solvent or contains a volatile reaction product, thereby eliminating the interfering effects of the heat of vaporization. Sealed capsules prevent any mass loss. Capsules can withstand an internal pressure of 24 atmospheres. High internal pressure capability allows water samples to be heated higher than 100 C. Capacity of 60 microliters. Large sample capacity yields higher sensitivity. Operating range of -40 C to 300 C unless otherwise limited by sample vapor pressure. Can be used on PYRIS Diamond DSC, PYRIS 1 DSC, DSC 6, DSC 7, DSC-4, and DSC-2 instruments. Major Applications The study of aqueous biological solutions (such as protein in water) where the dilution requires large sample sizes and water vaporization must be suppressed. Epoxy phenolic curing and vulcanization of rubber where the loss of volatiles can otherwise make interpretation difficult. Large Volume SS Pans, Covers, and O-Rings (20 of each) (1000 of each) Under no circumstances should the capsules be heated above 300 C. Any application requiring the heating beyond 200 C or where gaseous decomposition products may be generated should first be tested outside of the instrument. Always use guard ring inserts in conjunction with the sealed capsules. VOLATILE SAMPLE PANS Volatile sample pans are used with volatile solid or liquid samples which exert significant vapor pressure at the temperature of interest. Available in both aluminum and gold pans. Pans can withstand an internal pressure of two atmospheres (30 psi). Aqueous solutions can be scanned up to and through 100 C to observe solute behavior. Using the Vapor Pressure sample pan kit will allow a higher temperature to be reached. The heats of fusion of materials which sublime can be determined accurately. The effect of an enclosed atmosphere on thermal behavior of a sample can be observed. Capsules have an effective volume of 20 microliters. Gold pans are available for samples requiring temperatures above 600 C. Major Applications Purity analyses (i.e., pharmaceuticals, melting of lipids, or liquid crystals) Phase transitions, heat of vaporization, and boiling points Volatile Sample Pans and Covers, and Volatile Sealer Assembly Aluminum Pans and Covers (pkg. 400) Large Volume Stainless Steel Capsule Kit Includes: Description Quick Press Quick Press Spacer Die Guard Ring Inserts, 1 pair Gold Pans and Covers (pkg. 10) Volatile Sealer Assembly Pans, Covers, and O-Rings Replacement Lower Die for Sealer Replacement Upper Die for Sealer Vapor Pressure Sample Pan Kit This kit includes 100 volatile aluminum pans and 100 pierced covers. A 50-micron diameter hole is centered in the cover. Use this kit for more reproducible measurements of boiling points, heats of vaporization, and sublimation temperatures. Vapor pressure studies can be conducted when using these pans and covers with the High Pressure DSC or the TGA. N (100 of each) Large Volume Stainless Steel Capsule Kit

11 Canada For DSC runs where high pressure is expected in the capsule, we recommend you use high pressure capsules. DSC Sample Pans and Crimpers High Pressure Capsules and Sealer TEA-5 The capsules are safe to handle due to a bursting disk on the cover of the capsule which allows the sample to escape if the pressure should exceed 150 atmospheres. The use of high pressure capsules in DSC permits suppressing the endothermic signal resulting from the volatilization of sample material or from the volatilization or decomposition of reaction by-products. High pressure capsules permit the study of explosive materials and can be used in any situation where the advantage of a self-generating atmosphere is to be employed. Capsules available in steel, gold-plated steel, and titanium. Can withstand an internal pressure of 150 atmospheres maximum. Broad temperature range, subambient to 400 C. Capsules are reuseable after sealing. Used in hazard testing. High Pressure Capsule Sealing Tool High Pressure Capsules High Pressure Capsule Sealing Tool This reliable sealing tool is fast and precise. It employs a built-in torque clutch which guarantees that all capules are closed with the same torque. For sealing high pressure capsules B , B , B B Stainless Steel High Pressure Capsules Reuseable stainless steel capsules with internal volume of 30 microliters. Operating range subambient to 400 C unless otherwise limited by sample vapor pressure, not to exceed 150 bar. Includes five capsules and 20 goldplated copper seals. B Titanium High Pressure Capsules Reuseable titanium capsules with internal volume of 30 microliters. Operating range subambient to 400 C unless otherwise limited by sample vapor pressure, not to exceed 150 bar. Includes five capsules and 20 titanium seals. B Replacement Seals Gold-plated copper seals. B (10 of each) Titanium seals. B (10 of each) Original High Pressure Capsules Gold-Plated Stainless Steel High Pressure Capsules Reuseable gold-plated stainless steel capsules with internal volume of 30 microliters. Operating range subambient to 400 C unless otherwise limited by sample vapor pressure, not to exceed 150 bar. Includes five capsules and 20 gold-plated copper seals. B Gold-plated Capsule and Three Gold-plated Seals Gold-plated Copper Seals (10 of each) Stainless Steel Capsule and 10 Copper Seals Copper Seals (10 of each) Note 1: The sealer for the original high pressure capsules has been discontinued. Note 2: The specifications of the original high pressure capsules are identical to the new high pressure capsules.

12 TEA-6 DSC Sample Pans and Crimpers Autosampler Sample Pans and Universal Crimper The Autosampler sample pans are used to prepare sample materials for the PYRIS 1 Autosampler, DSC 7 RS, and DSC-4 RS. Pans are available in sealed or vented versions. These pans may also be used for non-robotic systems US DSC Autosampler Sample Pans (Covers Not Included) Material Quantity Capacity Thickness Sealed Vented 1 bar maximum internal pressure Aluminum µl 0.1 mm x B µl 0.1 mm x B µl 0.1 mm x B µl 0.1 mm x B µl 0.1 mm x B µl 0.15 mm x B Gold µl 0.1 mm x B DSC Autosampler Sample Covers (Pans Not Included) Material Quantity To Fit Sample Pan Aluminum mm B mm B Gold mm B Bar Max Capsule Set (Includes Pans and Covers) Material Quantity Capacity Sealed Aluminum 400 each 10 µl x B each 30 µl x B each 50 µl x B Universal Crimper Press The Universal Crimper Press provides high quality sample crimping for the Autosampler sample pans and can crimp the standard aluminum pans, O-Ring sealed large volume stainless steel pans, and the 20 µl volatile sample pans. This is achieved simply by using the appropriate sealing insert. Includes standard Sample Pan Manipulator and inserts to seal 10 µl, 30 µl, and 50 µl Autosampler sample pans described on this page. B DSC Universal Crimper Press Autosampler Crimper Accessory Kit Includes standard Sample Pan Manipulator and inserts to seal 10 µl, 30 µl, and 50 µl Autosampler sample pans described on this page. B Sealing Inserts Sealing insert for volatile sample pans ( , , and N ). B Sealing insert for large volume stainless steel pans ( ). B Sealing insert for standard aluminum pans ( ). B Sealing insert for 10, 30, and 50 µl Autosampler sample pans. B Aluminum Pan Starter Kit 50 of each type of aluminum pan and 350 covers. B

13 Canada DSC High Pressure Cell DSC Supplies and Accessories DSC High Pressure Cell and Accessories TEA-7 The DSC High Pressure Cell is an accessory for performing DSC experiments at elevated pressure. The accessory operates with the PYRIS 1 DSC, DSC 7, DSC-4, and DSC-2 Differential Scanning Calorimeters that use the unique PerkinElmer power compensated principle. Pressure range is 42 Bar (600 psi) maximum; temperature range is 40 C to 600 C. Typical applications include: Oxidation testing of oils, fats, foods, and plastics Curing and crosslinking reactions Suppression of evaporation of volatiles Analysis of pressure-dependent chemical reactions There are built-in connections for a liquid cooling system (tap water or circulating system). PerkinElmer Service installation is recommended. DSC 7, DSC-4, and DSC-2 High Pressure Cell N PYRIS 1 DSC High Pressure Connection Kit Upgrade for existing DSC 7 or DSC 4 customers who need to use the High Pressure Cell (N ) on the PYRIS 1 DSC. N PYRIS 1 DSC High Pressure Cell Kit Includes: DSC High Pressure Cell (N ) and PYRIS 1 DSC High Pressure Connection Kit (N ). N DSC High Pressure Cell Accessories Pressure Regulator for Use With the DSC High Pressure Cell Allows operation to 15 Bar with nitrogen, helium, or argon purge gases. (CGA #580 tank fitting.) Replacement Sample Holder for DSC High Pressure Cell Replacement sample holder for use with the DSC High Pressure Cell tested to meet all temperature and pressure specifications. N O-Ring for DSC High Pressure Cell Enclosure Cover B Aluminum Sample Holder Cover for DSC High Pressure Cell B Glass Wool Pads for DSC High Pressure Cell B Sample Handling Tray DSC High Pressure Cell B Vapor Pressure Pan Kit This kit includes 100 volatile aluminum pans and 100 pierced covers. A 50-micron diameter hole is centered in the cover. Use this kit for more reproducible measurements of boiling points, heats of vaporization, and sublimation temperatures. Vapor pressure studies can be conducted when using these pans and covers with the High Pressure DSC or the TGA. Maximum temperature is 600 C. Use Sealer or Universal Press B with sealing insert B N (100 of each)

14 TEA-8 DSC Supplies and Accessories DSC Subambient Accessories US PYRIS Diamond DSC/PYRIS 1 DSC Subambient Accessories PYRIS Diamond DSC/PYRIS 1 DSC CryoFill System Includes LN 2 Control Box and CryoFill Dewar Tank. N PYRIS Diamond DSC/PYRIS 1 DSC CryoFill Dewar Tank, 50 Liter N PYRIS Diamond DSC/PYRIS 1 DSC Long LN 2 Transfer Line, 2 m N PYRIS Diamond DSC/PYRIS 1 DSC Short LN 2 Transfer Line, 1 m N PYRIS Diamond DSC/PYRIS 1 DSC LN 2 Septum Assembly (LN 2 Receptical) N PYRIS 6 DSC/DSC 6 Subambient Accessories PRYIS 6 DSC/DSC 6 Subambient Kit with Dewar N PYRIS 6 DSC/DSC 6 Subambient Kit without Dewar N DSC 7 Subambient Accessories A B D E F Dry Box Assembly with Irises Includes all mounting hardware. N LN 2 Level Indicator Required for LN 2 operation. N Cold Water Turbulent Chamber Kit This kit can be used with a cold water faucet or water circulator if ice is not available for the reservoir. (Included with the Ambient DSC 7) Reservoir Kit For adding the reservoir assembly to any DSC 7 ambient version: Includes reservoir and cold finger. N Dry Box Assembly with Gloves Includes all mounting hardware. N Dry Box Glove Kit Allows existing dry box to be converted from Irises to gloves. Service installation recommended. N Subambient to Ambient Conversion Kit N Dry Box Sample Entry Port For DSC 7 Dry Box Assembly with gloves. N Dry Box Hold Down Screw Replacement Iris (Eight required) N Replacement Gloves with Arms Size Gloves Size 9, Butyl LN 2 Float and Shaft LN 2 Cold Finger Threaded Solid Aluminum Cylinder For use with ice water bath or LN Dry Box Gaskets Between deck lid and reservoir. N Between deck lid and dry box. N DSC 7 Gasket Red rubber vee gasket between sample holder and deck lid. N Intracooler Insulation For insulation of the intracooler expansion chamber. N DSC Configuration Lower Limit of Cooling DSC 7 Temperature Range Accessory Reservoir No Reservoir 25 C Ice Water D -30 C Intracooler 1 A / E A / E -65 C Intracooler 2 A / E A / E -140 C CCA7 A / E + F A / E -170 C Liquid Nitrogen A / E + B A / E + B + D

15 Canada DSC Supplies and Accessories DSC Subambient Accessories TEA-9 Intracoolers Intracoolers from PerkinElmer are subambient devices that automatically control the flow of coolant through a circulating chamber attached to the PYRIS 1 DSC, PYRIS 6 DSC, DSC 7, TMA 7, or DMA 7 analyzers. They are either single or dual-stage mechanical compression refrigeration units with cylindrical expansion chamber and special bolts and insulation for mounting directly on the sample holder block of the PYRIS 1 DSC, PYRIS 6 DSC, and DSC 7, or the furnace assembly of the DMA 7 or TMA 7. Intracooler 1 permits operation of all analyzers from -30 C; the Intracooler 2 from -65 C. PYRIS 6 DSC, Intracooler-ready (100/115/230 V) Includes: PYRIS 6 DSC Instrument with built-in gas switch, PYRIS Thermal Analysis Manager (single-user), and Accessory kit; Accessory kit includes tweezers, 5/16 in. Tygon (10 ft.), fuses, sample pans, sample holder platform, calibration weight, 9-25 pin RS232 cable, and power cord. N PYRIS 6 DSC Intracooler Allows for subambient operation to -65 C. N (115 V, 50/60 Hz) N (230 V, 50/60 Hz) DSC 7 Intracooler 1 Allows for subambient operation to -30 C (115 V, 50/60 Hz) (230 V, 50/60 Hz) DSC 7 Intracooler 2 Allows for subambient operation to -65 C (115 V, 50/60 Hz) (230 V, 50/60 Hz) PYRIS Diamond DSC/PYRIS 1 DSC Intracooler 1P N (115 V, 50/60 Hz) N (230 V, 50/60 Hz) PYRIS Diamond DSC/PYRIS 1 DSC Intracooler 2P N (115 V, 50/60 Hz) N (230 V, 50/60 Hz) Intracooler Spares Intracooler Bolt Kit for the PYRIS 1 DSC and DSC Includes: Description Intracooler Bolt Insulating Disk Split Bushing Bolt Mounting Bolt for the TMA 7/DMA 7 N Furnace Cover for the TMA 7/DMA 7, Top N Furnace Cover for the TMA 7/DMA 7, Bottom N Intracooler Insulation for the DSC 7 For insulation of the intracooler expansion chamber. N Silicone Grease Intracooler for PYRIS 6 DSC PYRIS 6 DSC with Intracooler Hose Attached PYRIS 6 DSC with Intracooler Hose

16 TEA-10 DSC Supplies and Accessories Sample Holder Supplies and DSC Calibration Reference Materials Vented Platinum Sample Holder Covers Each cover has two vent holes and is used for the PYRIS 1 DSC, DSC 7, DSC-4, and DSC-2 sample holders (2 of each) (6 of each) Sample Holder Cover Reforming Tool DSC performance is enhanced with sample holder covers that are formed properly and not degraded by extended usage. This tool allows the analyst to reform the platinum covers to their original dimensions Guard Ring Inserts A pair of removable, shaped aluminum inserts fitting in DSC 7, DSC-4, and DSC-2 sample holder cavities, preventing inadvertent dropping of pans, covers, etc., into the cavity. Also recommended for applications generating condensable gaseous products as the inserts are readily removed for cleaning (pair) Guard Ring Inserts for PYRIS 1 DSC A pair of removable, shaped aluminum inserts designed for the PYRIS 1 DSC. These inserts may stay in place and be used to temperatures as low as -170 C. N Hook Forceps O-Ring For standard swing-away cover on DSC 7, DSC-4, and DSC-2 instruments O-Ring for DSC 7 Flow-through Cover Large, two required. For flow-through cover DSC 7, DSC-4, DSC-2 Flow-through Cover Kits Flow-through Cover Kit The flow-through cover kit provides a short path for volatiles and/or decomposition products to exit from the DSC 7, DSC-4, and DSC-2 sample holder. The cover replaces the standard swing away cover and should be used with samples that undergo decomposition, dehydration, combustion, oxidation, etc O-Ring for Chimney Small, two required. For flow-through cover PYRIS 1 DSC Flow-through Cover 9 PYRIS 1 DSC Flow-through Cover Kit The flow-through cover provides a short path for volatiles or decomposition products to exit from the PYRIS 1 DSC sample holder. When the flow-through cover is installed, the sliding sample holder enclosure cover is displaced by the accessory. The flow-through cover should be used with samples that undergo decomposition, dehydration, or oxidation, especially if the thermal conductivity of the products of the reaction is different from that of the purge gas. N Miscellaneous Supplies Gasket for DSC 7 Draft Shield N DSC 7 Guard Ring Plastic Collar N DSC 7 Gasket Red rubber vee gasket between sample holder and deck lid. N Specific Heat Kit US Includes four sapphire disks manufactured to two separate diameters and thicknesses. Also includes a calibration chart giving the specific heat of aluminum oxide in the form of synthetic sapphire DSC Calibration Reference Materials PerkinElmer reference materials are % pure. DSC requires elements of this purity so that the instrument can be accurately calibrated. Depend on PerkinElmer for quality calibration reference materials. Reference Transition Material Point Indium C Tin C Lead C Zinc C Encapsulated Kit (includes a large and small indium, tin, and lead) Encapsulated Kit (includes indium and zinc) N

17 Canada Designed to study the effects of UV light on a wide variety of materials, the DPA 7 extends the use of the DSC 7. The DPA 7 allows your DSC to be used to quantitatively measure enthalpy (heat flow) changes in a material during and after exposure to single wavelength or full spectrum UV light. Typical applications include: Monitoring the curing process for light-activated curing of printing inks and coatings Determining the effects of UV light on polymers in accelerated testing For information about the PerkinElmer DPA 7, please contact your local PerkinElmer Sales Representative. DSC Supplies and Accessories DPA 7 Double Beam Photocalorimetric Accessory Supplies DPA 7 Aluminum Capsules Aluminum Sample Pans and Covers for UV Curing Studies In response to requests from our DPA 7 customers, PerkinElmer developed these pans to allow reproducible isolation of small quantities of liquid samples (such as uncured resins) so that UV curing reactions may be more accurately monitored by DSC. Pans are available alone or with quartz covers. We recommend you use quartz covers when analyzing samples which will evaporate at the temperature of interest. DPA 7 Aluminum Sample Pans Volume of 12.5 microliters. B (pkg. 100) DPA 7 Aluminum Sample Pans and Quartz Covers Volume of 12.5 microliters. B (100 of each) Lamps and Lamp Adapters for DPA 7 DPA 7 Monochromator Option An optional accessory for the DPA 7 used in place of the standard transfer optics and water filter for the selection of monochromatic UV light. Wavelength range from 250 nm to 600 nm. B Replacement Quartz Windows for Sample Holder Cover Two windows are required for each sample holder. B Sample Holder Cover Without Quartz Windows B Graphite Disc B Choose the Xenon, Mercury, or Mercury/Xenon lamp that provides the wavelength range to match conditions used in your process. Item Range (nm) Power Mercury Lamp 285 to watt B Mercury/Xenon 250 to watt B Lamp Adapter (set of 2) required for installation B Xenon lamp 250 to watt B Lamp Adapter (set of 2) required for installation B Xenon Lamp 250 to watt B We recommend that an authorized PerkinElmer Service Engineer install your DPA 7 Lamps. Installation is not included. TEA-11 B

18 TEA-12 DSC Supplies and Accessories DSC Autosampler Supplies and Accessories PerkinElmer PYRIS Diamond DSC Autosampler provides the automation, convenience, and flexibility you need! Allows automated DSC testing of up to 48 samples for the PYRIS 1 and 44 samples for the PYRIS Diamond without operator attention Handles 10, 30, and 50 µl sealed pans and vented (open) pans as well as high pressure capsules Complete software control from a computer keyboard simplifies operation PYRIS Diamond DSC, PYRIS 1 DSC Autosampler, and DSC 7 Robotic System Supplies and Accessories Magazine Kit Set of 12 magazines. B Platinum Cover for Sample and Reference Cells Two required for each sample holder. B Note: Cover location is different for the PYRIS Diamond DSC. Slide Key One end is magnetized for easy removal of magazines from the sample carousel. Other end (not magnetic) is used to insert magazines in sample carousel. Used to insert and remove the sample magazine through the access port in the cover Inserting magazines with the slide key prevents humidity and dust from entering the working space when changing samples B Special Sample Pan Manipulator Specially designed to simplify the pickup and positioning of your sample pans and covers Stainless steel handle incorporates suction device B PYRIS 1 DSC Autosampler 5 1 Standard Sample Pan Manipulator Prevents contamination of your sample Simplifies the handling of your sample pans and covers B Replacement Rubber Tip Used on the Sample Pan Manipulators, the Autosampler Sample Arm, and the Robotic system. Replace the rubber tip regularly for reliable operation. B Large Flat Platinum Furnace LID Used when running sample specimens in large volume stainless steel pans with the Autosampler. Two required for each DSC. B US Sample Preparation Recommendations Never touch your sample, sample pan, sample cover, or platinum cover with your bare fingers. Body oils and greases may cause contamination and erroneous results. 5

19 MP, Tg, and Structure of Common Polymers Canada Melting Point (MP) and Glass Transition Temperature (Tg) are the most important thermodynamic parameters for the common polymers. These properties can be easily and quicky determined by DSC. Melting point temperature range ( C) Glass transition temperature range ( C) TEA-13

20 TEA-14 Ultramicrobalance Supplies Weights, Forceps, Stirrups, and Sample Pans for AD-4/AD US AD-6 Ultramicrobalance AD-6 Ultramicrobalance Provides highly accurate weighing of your samples Allows easy access to the weighing chamber for both right- and left-handed analysts Communicates your results to a printer or a computer via an optional RS-232C interface Designed for high-performance weighing procedures Features a maximum sensitivity of 0.1 µg and a capacity of 5.0 g Totally microcomputer controlled Autobalance Accessory Kit Includes non-magnetic stainless steel forceps, tare weight set, Class M calibrating weight, flat sample pans, and spare fuses Stirrup Kit Standard Stirrup Kit Includes two matched stirrups Aluminum Flat Pans Sample Pans Forceps Aluminum Flat Pans For Standard Stirrup Kit. C (pkg. 20) For Lightweight Stirrup Kit. C (pkg. 20) Weight and Weight Sets Class 1.1 Calibrating Weight Per ASTM E (100 mg) Tare Weight Set Includes 13 weights ranging from 1 mg to 1 g Non-Magnetic, Nonserrated Stainless Steel Straight Forceps Non-Magnetic, Hooked Forceps Repair Kit Hangdown Wire Repair Kit Use to repair one wire for the AD-2/AD-4/AD-6 Balance. C Manuals Autobalance Quick Reference Guide AD-6 Instruction Manual C